#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:09:23 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180971 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/51/2205138.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205138_Fobs loop_ _publ_author_name 'Yang, De-Suo' _publ_section_title ; Bis[4-bromo-2-(cyclohexyliminomethyl)phenolato]copper(II) ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m249 _journal_page_last m250 _journal_volume 61 _journal_year 2005 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.9960 _cell_length_b 13.5970 _cell_length_c 25.1560 _exptl_crystal_F_000 2520.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file ob6467Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' yang2 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 475.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1820.21 2409.05 66.28 o 4 0 0 3393.23 3110.98 75.91 o 6 0 0 37727.70 38205.91 837.68 o 8 0 0 5687.93 6087.10 177.21 o 10 0 0 2721.94 2642.97 104.96 o 12 0 0 2172.70 2113.49 99.38 o 14 0 0 21.60 66.95 79.65 o 16 0 0 131.46 -13.46 115.66 o 18 0 0 98.93 15.91 111.96 o 2 1 0 17468.44 18851.51 291.97 o 4 1 0 121799.28 128732.12 2115.20 o 6 1 0 141.55 626.93 35.57 o 8 1 0 5439.14 4598.40 90.55 o 10 1 0 9839.86 9872.40 266.56 o 12 1 0 256.21 183.60 39.17 o 14 1 0 584.57 736.92 55.22 o 16 1 0 152.33 121.37 53.55 o 18 1 0 100.21 5.38 62.56 o 0 2 0 4114.79 4366.68 115.69 o 2 2 0 4606.09 4866.10 78.78 o 4 2 0 662.70 674.03 19.43 o 6 2 0 25866.53 25368.09 425.87 o 8 2 0 20357.36 20119.44 372.71 o 10 2 0 2978.34 3006.62 109.93 o 12 2 0 5073.00 4895.07 122.22 o 14 2 0 3145.38 3169.55 96.00 o 16 2 0 267.39 264.73 56.05 o 18 2 0 417.57 363.28 70.99 o 2 3 0 131212.92 134139.77 2059.55 o 4 3 0 4653.60 4172.92 72.06 o 6 3 0 5277.82 4944.99 93.78 o 8 3 0 4211.58 3856.51 92.09 o 10 3 0 6726.28 6249.43 147.34 o 12 3 0 18332.92 17170.71 363.38 o 14 3 0 80.80 72.04 45.75 o 16 3 0 6386.63 6366.80 154.86 o 18 3 0 132.18 116.39 91.42 o 0 4 0 32888.16 35681.47 901.37 o 2 4 0 5993.58 5483.44 90.35 o 4 4 0 10042.06 10531.08 169.54 o 6 4 0 3193.26 2782.00 55.37 o 8 4 0 28933.26 29680.71 501.02 o 10 4 0 448.83 487.21 38.77 o 12 4 0 6977.47 7130.35 195.36 o 14 4 0 2602.06 2656.10 87.29 o 16 4 0 408.20 385.07 66.48 o 18 4 0 145.02 157.41 95.18 o 2 5 0 57521.74 58199.79 897.45 o 4 5 0 14305.90 13755.75 219.69 o 6 5 0 2537.74 2414.82 52.02 o 8 5 0 7080.40 6977.72 132.00 o 10 5 0 130.77 327.21 32.86 o 12 5 0 218.14 156.08 40.66 o 14 5 0 649.70 721.13 55.49 o 16 5 0 367.21 242.60 65.06 o 18 5 0 8.75 -50.49 95.97 o 0 6 0 181647.42 188205.28 4716.67 o 2 6 0 29467.71 30206.61 544.81 o 4 6 0 80467.82 83737.64 1290.70 o 6 6 0 9472.62 8853.34 148.87 o 8 6 0 110.17 204.37 28.10 o 10 6 0 167.19 123.77 30.42 o 12 6 0 579.93 559.49 53.81 o 14 6 0 334.78 308.14 49.49 o 16 6 0 117.77 174.54 111.63 o 18 6 0 41.15 -8.80 100.06 o 2 7 0 554.27 641.08 24.72 o 4 7 0 21165.03 20438.31 347.31 o 6 7 0 2658.58 2211.28 58.03 o 8 7 0 5358.16 5283.92 109.11 o 10 7 0 1713.14 1641.34 82.48 o 12 7 0 173.44 211.65 57.02 o 14 7 0 266.25 389.58 57.88 o 16 7 0 82.89 -20.36 90.56 o 0 8 0 5833.41 5305.79 165.15 o 2 8 0 212.58 184.59 19.47 o 4 8 0 507.56 560.02 35.38 o 6 8 0 1726.69 1469.42 50.84 o 8 8 0 1125.70 1130.44 54.92 o 10 8 0 2480.53 2105.95 69.86 o 12 8 0 106.20 113.55 50.92 o 14 8 0 1444.55 1490.43 114.49 o 16 8 0 113.50 156.32 90.48 o 2 9 0 588.54 533.91 33.59 o 4 9 0 354.18 365.27 32.43 o 6 9 0 8540.37 8080.67 165.18 o 8 9 0 894.62 891.66 47.09 o 10 9 0 2512.37 2358.17 84.71 o 12 9 0 5209.41 5479.87 204.86 o 14 9 0 176.55 266.69 99.51 o 16 9 0 990.64 1030.73 211.72 o 0 10 0 2705.63 3089.14 256.80 o 2 10 0 4511.07 4085.29 96.12 o 4 10 0 913.54 941.39 56.93 o 6 10 0 2591.67 2625.46 123.38 o 8 10 0 4723.46 4713.89 127.00 o 10 10 0 301.42 342.48 49.65 o 12 10 0 760.46 1033.89 124.36 o 14 10 0 88.55 -94.97 109.34 o 2 11 0 16847.73 16370.74 311.56 o 4 11 0 5726.53 5499.05 124.52 o 6 11 0 1862.07 1745.32 62.16 o 8 11 0 1416.34 1309.53 105.56 o 10 11 0 435.76 355.91 53.17 o 12 11 0 232.58 323.64 111.01 o 14 11 0 160.26 46.43 119.58 o 0 12 0 12980.70 12736.22 380.84 o 2 12 0 3120.34 3040.37 85.84 o 4 12 0 2895.95 2953.42 86.80 o 6 12 0 2297.87 2508.15 79.84 o 8 12 0 427.65 473.25 56.64 o 10 12 0 1574.22 1713.81 245.85 o 12 12 0 4.95 -5.22 80.28 o 2 13 0 414.42 485.26 46.48 o 4 13 0 3022.03 2847.53 86.97 o 6 13 0 3.27 -55.73 40.74 o 8 13 0 285.70 380.64 56.99 o 10 13 0 325.97 550.86 97.26 o 12 13 0 172.33 101.47 104.70 o 0 14 0 187.90 186.76 90.68 o 2 14 0 43.00 47.37 60.03 o 4 14 0 91.12 178.02 47.68 o 6 14 0 15.18 19.17 52.10 o 8 14 0 412.92 312.49 86.88 o 10 14 0 144.66 42.87 108.85 o 2 15 0 1105.73 1059.54 95.70 o 4 15 0 92.52 62.33 49.00 o 6 15 0 578.48 769.65 80.58 o 8 15 0 231.76 212.63 103.95 o 0 16 0 40.36 25.49 67.63 o 2 16 0 2.18 17.84 49.79 o 4 16 0 1.90 -28.47 52.41 o 6 16 0 202.76 233.83 115.56 o 2 17 0 804.72 939.87 69.91 o 4 17 0 120.79 62.85 74.21 o 1 1 1 454.61 581.13 12.22 o 2 1 1 48358.95 55803.37 606.50 o 3 1 1 19546.32 21533.46 262.19 o 4 1 1 41286.42 44631.78 521.19 o 5 1 1 35787.02 36982.26 450.15 o 6 1 1 19443.83 19727.25 235.28 o 7 1 1 881.31 1149.35 23.85 o 8 1 1 2665.52 2347.27 39.10 o 9 1 1 2310.57 2246.71 39.89 o 10 1 1 1632.77 1675.77 56.88 o 11 1 1 295.32 268.41 26.00 o 12 1 1 6511.73 6335.86 100.39 o 13 1 1 1423.60 1421.08 43.88 o 14 1 1 14.57 -0.51 31.14 o 15 1 1 103.67 54.52 34.73 o 16 1 1 541.05 570.91 49.84 o 17 1 1 321.54 461.06 45.40 o 18 1 1 0.58 -1.07 45.05 o 19 1 1 7.40 25.11 50.45 o 0 2 1 18486.16 23878.98 393.99 o 1 2 1 20665.78 24492.96 276.17 o 2 2 1 41755.96 43987.47 478.98 o 3 2 1 27896.25 30597.06 345.92 o 4 2 1 6768.71 6906.19 79.53 o 5 2 1 27771.73 30302.03 344.04 o 6 2 1 17846.53 18782.03 233.86 o 7 2 1 12869.41 12560.40 154.33 o 8 2 1 15201.79 15851.60 193.23 o 9 2 1 4969.12 5229.76 73.12 o 10 2 1 2639.08 2465.73 50.39 o 11 2 1 1521.19 1482.79 55.06 o 12 2 1 176.46 286.87 30.74 o 13 2 1 44.86 81.85 30.10 o 14 2 1 1589.77 1665.84 49.29 o 15 2 1 3.76 -17.60 32.65 o 16 2 1 103.37 56.90 37.69 o 17 2 1 53.80 124.78 41.62 o 18 2 1 617.50 581.62 52.06 o 19 2 1 4.17 -41.86 63.99 o 1 3 1 1312.03 1603.47 20.95 o 2 3 1 3136.85 3323.39 39.94 o 3 3 1 5.78 168.88 8.68 o 4 3 1 768.41 767.98 19.47 o 5 3 1 7533.39 7606.64 88.64 o 6 3 1 118.13 249.24 11.54 o 7 3 1 166.61 345.06 14.13 o 8 3 1 483.50 504.76 19.62 o 9 3 1 1317.52 1143.66 28.00 o 10 3 1 0.50 96.55 18.62 o 11 3 1 588.18 632.62 35.50 o 12 3 1 88.03 74.00 27.41 o 13 3 1 348.46 292.63 31.47 o 14 3 1 20.32 38.46 31.77 o 15 3 1 102.85 120.49 37.14 o 16 3 1 204.04 238.23 40.79 o 17 3 1 57.08 -14.51 41.58 o 18 3 1 40.51 30.75 49.33 o 19 3 1 0.55 -49.39 68.32 o 0 4 1 1236.03 1196.92 27.88 o 1 4 1 3583.31 3653.74 45.39 o 2 4 1 13765.50 16273.05 186.60 o 3 4 1 6167.88 5812.24 70.57 o 4 4 1 8150.83 7751.28 89.86 o 5 4 1 3380.03 3593.00 46.70 o 6 4 1 227.33 154.58 11.88 o 7 4 1 4473.19 4762.08 61.09 o 8 4 1 5851.78 5757.07 78.95 o 9 4 1 2039.34 2073.27 39.79 o 10 4 1 5421.10 5222.56 75.75 o 11 4 1 672.85 767.55 40.28 o 12 4 1 1761.85 1791.05 46.47 o 13 4 1 530.80 560.82 34.92 o 14 4 1 1279.22 1402.13 46.69 o 15 4 1 0.50 -34.36 33.90 o 16 4 1 0.87 36.28 41.07 o 17 4 1 141.12 200.48 48.87 o 18 4 1 548.28 582.15 59.43 o 1 5 1 152.96 177.77 12.20 o 2 5 1 38614.80 40983.23 448.32 o 3 5 1 9410.78 9709.92 110.92 o 4 5 1 11626.43 11953.05 140.32 o 5 5 1 9011.02 8788.40 102.71 o 6 5 1 380.49 375.70 14.91 o 7 5 1 624.80 668.06 19.10 o 8 5 1 2824.57 2760.43 52.43 o 9 5 1 5654.82 5405.44 77.23 o 10 5 1 3699.20 3749.33 60.65 o 11 5 1 1839.90 1623.55 43.23 o 12 5 1 2394.75 2307.68 53.14 o 13 5 1 327.69 317.70 33.90 o 14 5 1 30.62 68.86 32.26 o 15 5 1 272.40 269.00 38.60 o 16 5 1 921.61 829.24 52.42 o 17 5 1 223.52 276.22 53.50 o 18 5 1 1.20 -27.41 66.60 o 0 6 1 1373.96 1722.13 81.25 o 1 6 1 1595.63 1515.46 26.36 o 2 6 1 2985.02 3108.53 42.14 o 3 6 1 2850.98 2861.34 38.89 o 4 6 1 101.81 139.03 14.06 o 5 6 1 124.51 164.68 12.90 o 6 6 1 963.70 1082.97 23.35 o 7 6 1 7302.07 7024.70 89.99 o 8 6 1 2040.67 1918.30 38.37 o 9 6 1 414.45 458.16 24.05 o 10 6 1 2.94 8.87 21.21 o 11 6 1 450.60 447.48 33.90 o 12 6 1 92.99 98.93 28.45 o 13 6 1 128.48 182.88 31.72 o 14 6 1 109.05 125.58 34.00 o 15 6 1 36.89 15.80 40.11 o 16 6 1 13.05 -59.41 45.21 o 17 6 1 0.52 17.42 50.04 o 18 6 1 33.59 70.88 53.93 o 1 7 1 4615.34 4973.94 65.96 o 2 7 1 20341.70 22082.81 263.21 o 3 7 1 5099.19 4829.55 60.35 o 4 7 1 947.14 1104.54 22.30 o 5 7 1 293.45 369.81 16.04 o 6 7 1 2456.94 2202.84 39.84 o 7 7 1 1927.61 1845.61 34.08 o 8 7 1 579.49 591.55 26.88 o 9 7 1 37.18 88.36 21.50 o 10 7 1 2701.88 2586.32 52.94 o 11 7 1 1.71 16.62 22.91 o 12 7 1 2877.76 2828.62 65.06 o 13 7 1 81.71 77.12 32.61 o 14 7 1 18.04 98.22 46.88 o 15 7 1 63.47 -27.40 45.88 o 16 7 1 422.32 339.52 86.81 o 17 7 1 9.49 -5.36 61.23 o 0 8 1 3523.95 3716.15 84.11 o 1 8 1 5212.88 4689.70 70.94 o 2 8 1 0.47 32.92 12.18 o 3 8 1 5917.02 5889.52 78.90 o 4 8 1 2446.90 2481.23 41.96 o 5 8 1 2763.69 2564.43 44.01 o 6 8 1 272.05 350.31 21.52 o 7 8 1 2073.69 2107.09 40.86 o 8 8 1 1636.51 1663.18 45.58 o 9 8 1 300.32 288.53 26.95 o 10 8 1 182.51 267.05 28.92 o 11 8 1 79.25 114.82 28.10 o 12 8 1 773.17 800.86 54.21 o 13 8 1 24.93 14.16 41.57 o 14 8 1 1153.75 1163.52 60.39 o 15 8 1 21.82 -75.42 62.97 o 16 8 1 51.23 -17.46 61.81 o 17 8 1 22.11 3.05 64.73 o 1 9 1 957.64 849.92 26.88 o 2 9 1 547.83 461.32 22.69 o 3 9 1 2131.04 1894.69 42.28 o 4 9 1 641.62 678.99 33.18 o 5 9 1 4425.31 4339.27 70.72 o 6 9 1 684.80 752.12 27.22 o 7 9 1 34.51 32.65 19.63 o 8 9 1 1912.24 1758.72 53.25 o 9 9 1 1180.19 1198.34 52.21 o 10 9 1 375.52 478.55 33.58 o 11 9 1 678.49 719.94 40.18 o 12 9 1 56.78 -9.19 47.87 o 13 9 1 81.96 -0.48 40.90 o 14 9 1 7.36 46.84 54.36 o 15 9 1 0.45 4.24 56.95 o 16 9 1 6.31 -91.81 61.20 o 0 10 1 8381.27 7659.93 177.07 o 1 10 1 598.48 594.11 29.04 o 2 10 1 599.74 604.69 29.52 o 3 10 1 135.21 186.69 22.67 o 4 10 1 8447.58 7846.88 114.10 o 5 10 1 92.73 122.13 23.30 o 6 10 1 3734.02 3535.02 66.82 o 7 10 1 273.12 300.32 30.84 o 8 10 1 80.85 -4.05 28.37 o 9 10 1 696.66 696.71 38.05 o 10 10 1 965.06 912.84 55.97 o 11 10 1 129.91 111.10 43.95 o 12 10 1 724.95 771.36 61.65 o 13 10 1 85.68 98.37 76.32 o 14 10 1 898.22 1155.44 98.69 o 15 10 1 100.65 -16.68 82.38 o 1 11 1 240.93 284.61 28.12 o 2 11 1 6192.04 6183.90 95.64 o 3 11 1 24.94 12.68 23.43 o 4 11 1 3872.87 3884.55 68.83 o 5 11 1 329.18 306.91 34.85 o 6 11 1 815.79 748.47 32.83 o 7 11 1 149.41 134.03 31.51 o 8 11 1 10.93 -21.86 31.25 o 9 11 1 341.26 392.43 36.93 o 10 11 1 38.18 76.92 55.65 o 11 11 1 440.78 394.63 47.41 o 12 11 1 1810.47 1938.35 96.62 o 13 11 1 70.91 150.30 77.49 o 14 11 1 16.01 87.68 81.77 o 0 12 1 231.43 226.95 41.19 o 1 12 1 99.28 75.20 25.36 o 2 12 1 687.33 664.59 31.95 o 3 12 1 511.90 529.51 30.65 o 4 12 1 418.92 456.39 32.14 o 5 12 1 20.21 9.67 26.35 o 6 12 1 23.79 -0.74 27.37 o 7 12 1 1297.27 1430.35 53.93 o 8 12 1 377.07 401.54 38.27 o 9 12 1 10.56 -56.13 40.61 o 10 12 1 0.74 31.62 48.45 o 11 12 1 274.89 266.82 59.01 o 12 12 1 13.44 34.81 60.43 o 13 12 1 10.99 -79.43 83.40 o 1 13 1 1254.63 1183.54 39.65 o 2 13 1 2047.11 2024.79 66.09 o 3 13 1 1511.70 1633.31 46.73 o 4 13 1 5.51 28.79 28.31 o 5 13 1 78.15 54.30 29.39 o 6 13 1 821.92 777.49 37.69 o 7 13 1 425.14 423.75 39.49 o 8 13 1 291.73 221.33 45.96 o 9 13 1 34.02 43.28 46.60 o 10 13 1 292.66 350.21 72.69 o 11 13 1 34.57 -44.07 60.80 o 12 13 1 914.46 1054.04 113.02 o 0 14 1 941.62 865.00 101.56 o 1 14 1 562.12 578.03 36.24 o 2 14 1 245.89 178.04 33.17 o 3 14 1 40.44 14.73 30.60 o 4 14 1 354.62 331.59 40.79 o 5 14 1 195.71 216.66 33.48 o 6 14 1 214.20 213.92 39.58 o 7 14 1 123.77 88.08 45.77 o 8 14 1 149.63 180.77 50.69 o 9 14 1 24.74 53.04 73.88 o 10 14 1 140.40 192.65 65.46 o 11 14 1 48.54 17.04 65.13 o 1 15 1 59.22 64.31 33.34 o 2 15 1 263.34 281.70 36.50 o 3 15 1 31.84 73.71 33.72 o 4 15 1 16.47 -21.72 33.98 o 5 15 1 388.71 429.76 42.83 o 6 15 1 0.64 -7.57 47.70 o 7 15 1 1.31 27.65 55.21 o 8 15 1 28.55 -57.87 66.98 o 9 15 1 183.15 159.48 85.78 o 10 15 1 15.35 -10.50 105.51 o 0 16 1 1507.18 1627.88 80.65 o 1 16 1 13.28 78.85 36.60 o 2 16 1 337.74 330.05 39.19 o 3 16 1 0.22 -11.78 35.76 o 4 16 1 778.31 856.14 57.28 o 5 16 1 16.49 -16.35 46.89 o 6 16 1 85.69 193.75 57.63 o 7 16 1 15.80 -18.99 70.04 o 8 16 1 104.83 55.48 110.08 o 1 17 1 8.12 4.53 41.30 o 2 17 1 259.05 244.89 46.99 o 3 17 1 0.05 -60.94 41.30 o 4 17 1 21.20 -8.16 46.95 o 5 17 1 93.04 97.88 72.11 o 0 0 2 6456.85 8973.75 196.94 o 1 0 2 231.03 203.83 11.95 o 2 0 2 15261.57 17177.17 266.13 o 3 0 2 114792.24 125922.46 1932.50 o 4 0 2 116816.91 129332.32 1985.74 o 5 0 2 2045.22 2576.30 47.71 o 6 0 2 10580.54 10966.16 176.19 o 7 0 2 1508.77 1520.39 35.84 o 8 0 2 6171.03 7039.88 119.66 o 9 0 2 19530.42 18890.02 352.87 o 10 0 2 14345.33 13103.60 253.67 o 11 0 2 312.00 332.11 37.49 o 12 0 2 374.34 376.16 42.76 o 13 0 2 3955.72 3850.95 119.35 o 14 0 2 5583.67 5310.32 131.12 o 15 0 2 2525.87 2567.55 88.70 o 16 0 2 368.86 334.95 56.90 o 17 0 2 15.58 31.69 58.23 o 18 0 2 811.33 901.71 83.31 o 19 0 2 224.28 311.95 97.09 o 1 1 2 2085.70 3010.17 36.94 o 2 1 2 26254.57 30227.21 352.15 o 3 1 2 43996.94 46346.00 504.87 o 4 1 2 1337.91 1173.34 18.30 o 5 1 2 54361.25 56988.76 641.98 o 6 1 2 13444.85 13401.58 156.30 o 7 1 2 8437.48 9069.25 113.69 o 8 1 2 200.62 200.13 20.27 o 9 1 2 6201.71 6276.21 84.76 o 10 1 2 7904.29 7336.50 140.21 o 11 1 2 4800.98 4730.47 79.08 o 12 1 2 917.78 1043.79 52.11 o 13 1 2 709.85 760.99 38.07 o 14 1 2 59.76 76.79 33.58 o 15 1 2 403.85 474.20 39.89 o 16 1 2 297.07 300.14 40.59 o 17 1 2 321.89 407.38 43.99 o 18 1 2 2.18 93.06 48.55 o 19 1 2 2.71 -66.47 49.21 o 0 2 2 90887.95 98436.48 1514.14 o 1 2 2 61359.38 65192.90 731.50 o 2 2 2 1517.16 1367.84 18.59 o 3 2 2 3853.44 4366.74 51.37 o 4 2 2 141.89 254.14 11.54 o 5 2 2 9404.57 8698.95 99.68 o 6 2 2 4735.98 4631.69 59.58 o 7 2 2 39493.30 40443.70 476.79 o 8 2 2 273.92 462.86 20.80 o 9 2 2 8.19 75.02 24.36 o 10 2 2 4531.26 4233.20 90.44 o 11 2 2 1240.97 1072.44 46.81 o 12 2 2 7.49 112.90 27.70 o 13 2 2 75.93 110.23 29.54 o 14 2 2 42.80 34.96 31.60 o 15 2 2 156.08 182.62 36.17 o 16 2 2 14.85 41.97 38.34 o 17 2 2 65.68 65.68 42.69 o 18 2 2 116.11 17.41 55.18 o 19 2 2 1.08 -48.03 49.83 o 1 3 2 1723.66 2133.84 36.68 o 2 3 2 226362.31 244720.91 2739.53 o 3 3 2 76841.60 80936.96 908.76 o 4 3 2 1809.15 1968.96 28.04 o 5 3 2 227.04 198.56 10.13 o 6 3 2 30153.14 30040.57 331.82 o 7 3 2 17051.74 17173.64 193.54 o 8 3 2 16.77 33.83 14.75 o 9 3 2 3710.00 3219.43 51.95 o 10 3 2 5568.91 5230.73 75.48 o 11 3 2 61.58 62.77 24.10 o 12 3 2 53.73 67.85 26.46 o 13 3 2 212.73 138.92 29.97 o 14 3 2 503.58 706.45 47.96 o 15 3 2 89.35 87.27 34.48 o 16 3 2 589.13 607.35 46.79 o 17 3 2 0.16 -35.04 45.18 o 18 3 2 0.31 -70.08 46.72 o 19 3 2 457.01 514.91 67.20 o 0 4 2 1039.96 1227.09 29.94 o 1 4 2 65382.68 69353.79 754.30 o 2 4 2 6179.46 6306.31 72.75 o 3 4 2 603.98 567.60 12.62 o 4 4 2 9451.29 9526.67 112.75 o 5 4 2 15445.78 15426.78 173.51 o 6 4 2 8834.42 8501.02 99.88 o 7 4 2 25310.10 24872.30 286.46 o 8 4 2 2940.20 2758.78 48.14 o 9 4 2 14.22 38.89 17.31 o 10 4 2 481.27 327.55 22.01 o 11 4 2 2541.27 2504.21 53.06 o 12 4 2 254.04 304.98 29.21 o 13 4 2 114.50 165.34 39.97 o 14 4 2 877.09 826.11 55.21 o 15 4 2 62.04 94.99 37.64 o 16 4 2 61.35 92.42 43.11 o 17 4 2 2.55 -69.96 46.64 o 18 4 2 18.40 -0.59 45.35 o 1 5 2 18.02 45.62 7.96 o 2 5 2 33.89 45.74 8.19 o 3 5 2 20752.11 20890.06 231.61 o 4 5 2 1889.49 1948.48 29.51 o 5 5 2 21239.17 20735.24 239.19 o 6 5 2 1129.26 1110.76 24.30 o 7 5 2 153.86 185.90 15.80 o 8 5 2 29.39 28.19 18.72 o 9 5 2 7896.11 7615.63 106.18 o 10 5 2 424.75 540.44 28.86 o 11 5 2 6246.90 6115.22 107.22 o 12 5 2 1744.80 1521.19 69.64 o 13 5 2 502.04 492.53 34.33 o 14 5 2 77.66 67.45 31.85 o 15 5 2 917.78 1010.33 62.79 o 16 5 2 665.15 654.18 53.09 o 17 5 2 136.82 125.62 47.68 o 18 5 2 127.73 69.53 48.74 o 0 6 2 4143.62 3720.87 71.33 o 1 6 2 103.66 92.85 9.80 o 2 6 2 1360.96 1446.73 23.42 o 3 6 2 1439.00 1475.70 24.83 o 4 6 2 29.79 112.33 26.20 o 5 6 2 713.34 705.60 19.04 o 6 6 2 2889.54 2863.32 42.31 o 7 6 2 8151.21 7933.00 99.69 o 8 6 2 162.26 190.04 21.53 o 9 6 2 8631.49 8278.84 114.97 o 10 6 2 7684.70 7455.01 106.77 o 11 6 2 86.61 60.11 22.60 o 12 6 2 509.40 461.37 31.81 o 13 6 2 3057.14 3030.47 64.60 o 14 6 2 2735.45 2858.34 76.14 o 15 6 2 916.26 970.14 50.71 o 16 6 2 134.48 201.36 46.43 o 17 6 2 111.86 88.58 47.71 o 18 6 2 279.80 335.18 58.56 o 1 7 2 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5.30 15.04 o 4 4 13 1934.41 1791.88 37.65 o 5 4 13 5764.05 6095.95 83.42 o 6 4 13 2076.44 2011.55 39.49 o 7 4 13 1.23 14.19 19.16 o 8 4 13 803.72 936.01 29.92 o 9 4 13 2351.48 2371.50 67.78 o 10 4 13 160.96 144.65 31.57 o 11 4 13 4.88 13.07 36.06 o 12 4 13 8.62 71.91 39.50 o 13 4 13 2138.80 2050.29 73.13 o 14 4 13 259.12 220.18 48.65 o 15 4 13 525.54 557.28 55.87 o 16 4 13 0.56 12.50 52.78 o 17 4 13 170.82 90.56 74.06 o 1 5 13 15263.59 15781.27 185.85 o 2 5 13 10841.71 10608.19 133.69 o 3 5 13 10245.11 10038.48 127.79 o 4 5 13 908.01 839.66 25.37 o 5 5 13 2696.76 2528.25 45.32 o 6 5 13 706.36 694.77 25.75 o 7 5 13 3219.89 3062.20 60.41 o 8 5 13 402.22 444.15 25.53 o 9 5 13 12.77 50.74 25.11 o 10 5 13 143.67 164.32 29.53 o 11 5 13 2876.99 2802.53 64.35 o 12 5 13 16.47 71.39 36.27 o 13 5 13 10.30 -34.92 41.33 o 14 5 13 1.71 -13.96 49.86 o 15 5 13 255.17 298.11 55.17 o 16 5 13 140.58 221.23 55.30 o 17 5 13 65.06 102.88 112.29 o 0 6 13 1125.08 1004.42 33.10 o 1 6 13 7012.22 6719.68 89.77 o 2 6 13 228.30 258.57 19.01 o 3 6 13 1400.18 1626.22 34.06 o 4 6 13 568.90 569.40 23.68 o 5 6 13 396.06 473.65 29.70 o 6 6 13 512.79 671.59 26.27 o 7 6 13 863.60 872.89 29.72 o 8 6 13 2107.83 2001.48 46.51 o 9 6 13 485.97 546.83 31.81 o 10 6 13 383.64 424.07 32.14 o 11 6 13 565.46 542.69 37.28 o 12 6 13 70.56 34.97 36.93 o 13 6 13 3.34 25.59 60.11 o 14 6 13 2.77 -12.68 45.35 o 15 6 13 0.91 -7.10 51.15 o 16 6 13 1.35 -3.57 52.88 o 1 7 13 2602.93 2430.25 45.00 o 2 7 13 1229.22 1230.04 30.14 o 3 7 13 5967.94 5745.78 81.10 o 4 7 13 229.40 217.44 22.64 o 5 7 13 0.52 0.34 20.68 o 6 7 13 8.92 -9.07 21.54 o 7 7 13 2476.10 2331.78 50.38 o 8 7 13 1185.78 1102.60 37.01 o 9 7 13 12.83 73.01 28.11 o 10 7 13 128.54 93.15 30.34 o 11 7 13 520.96 486.20 36.12 o 12 7 13 0.58 -41.22 38.74 o 13 7 13 482.54 441.61 51.11 o 14 7 13 22.57 3.98 51.50 o 15 7 13 308.48 211.88 64.08 o 16 7 13 7.53 14.39 101.29 o 0 8 13 3224.17 3002.43 95.62 o 1 8 13 152.38 178.11 21.61 o 2 8 13 151.93 153.19 27.21 o 3 8 13 504.48 384.21 24.77 o 4 8 13 876.66 846.71 30.87 o 5 8 13 4382.94 4551.98 86.65 o 6 8 13 5.35 14.24 24.97 o 7 8 13 246.81 322.85 29.55 o 8 8 13 33.42 17.58 30.98 o 9 8 13 407.63 511.50 38.48 o 10 8 13 249.03 305.16 37.49 o 11 8 13 71.11 80.76 37.54 o 12 8 13 7.56 73.38 44.58 o 13 8 13 512.02 555.35 75.98 o 14 8 13 49.07 78.30 57.61 o 15 8 13 298.62 195.25 66.17 o 1 9 13 3983.59 4079.43 88.88 o 2 9 13 158.68 139.67 31.14 o 3 9 13 56.15 50.54 27.91 o 4 9 13 1674.14 1676.04 51.39 o 5 9 13 37.29 112.62 27.89 o 6 9 13 1580.10 1549.46 50.34 o 7 9 13 86.01 77.25 28.65 o 8 9 13 21.70 -4.37 32.63 o 9 9 13 247.71 256.90 37.05 o 10 9 13 140.30 87.44 38.01 o 11 9 13 75.47 77.74 39.55 o 12 9 13 51.33 33.58 46.99 o 13 9 13 20.99 -11.36 48.30 o 14 9 13 77.89 137.64 57.03 o 0 10 13 496.05 589.53 57.08 o 1 10 13 2436.35 2489.96 68.58 o 2 10 13 528.10 455.07 39.16 o 3 10 13 1557.07 1672.74 66.30 o 4 10 13 550.97 476.21 36.14 o 5 10 13 3011.64 2898.25 68.11 o 6 10 13 481.88 419.16 38.09 o 7 10 13 299.16 363.16 39.08 o 8 10 13 1.58 -5.35 39.24 o 9 10 13 1116.54 1039.25 58.10 o 10 10 13 45.83 57.79 48.95 o 11 10 13 19.54 -44.83 51.00 o 12 10 13 4.21 102.01 58.46 o 13 10 13 882.47 919.33 122.44 o 14 10 13 22.17 -52.62 91.59 o 1 11 13 755.53 766.59 68.31 o 2 11 13 547.49 665.06 52.24 o 3 11 13 1417.64 1337.76 54.30 o 4 11 13 326.35 269.16 39.92 o 5 11 13 24.87 12.38 34.09 o 6 11 13 185.49 87.51 36.47 o 7 11 13 105.94 77.18 43.11 o 8 11 13 241.10 309.89 47.46 o 9 11 13 21.70 111.82 46.61 o 10 11 13 2.70 -69.55 46.37 o 11 11 13 568.23 507.99 56.41 o 12 11 13 22.52 61.21 57.49 o 13 11 13 66.57 -7.40 83.63 o 0 12 13 669.10 681.40 73.67 o 1 12 13 531.70 632.38 47.29 o 2 12 13 32.00 -3.72 38.86 o 3 12 13 430.74 496.54 47.41 o 4 12 13 224.21 184.55 44.06 o 5 12 13 394.68 593.38 53.82 o 6 12 13 755.85 748.42 48.62 o 7 12 13 86.97 108.16 46.58 o 8 12 13 319.98 291.16 50.72 o 9 12 13 42.79 27.27 47.98 o 10 12 13 13.75 19.67 50.36 o 11 12 13 0.16 29.82 52.60 o 12 12 13 17.14 -61.91 71.65 o 1 13 13 427.22 396.73 47.36 o 2 13 13 5.37 41.36 42.46 o 3 13 13 557.15 652.29 52.23 o 4 13 13 435.62 412.87 48.44 o 5 13 13 10.28 40.56 44.88 o 6 13 13 321.79 184.86 48.52 o 7 13 13 374.12 378.23 64.02 o 8 13 13 69.37 116.06 52.46 o 9 13 13 178.00 164.47 54.49 o 10 13 13 96.78 139.25 56.27 o 0 14 13 349.15 383.94 73.56 o 1 14 13 496.23 649.93 69.41 o 2 14 13 11.99 -38.29 45.90 o 3 14 13 135.59 124.87 49.16 o 4 14 13 56.82 36.79 47.95 o 5 14 13 499.22 571.66 56.34 o 6 14 13 10.98 -8.58 58.26 o 7 14 13 0.00 19.22 57.90 o 8 14 13 27.93 -36.11 57.31 o 9 14 13 366.18 559.12 98.21 o 1 15 13 2.21 -71.18 47.45 o 2 15 13 20.94 77.95 51.42 o 3 15 13 8.94 124.02 53.26 o 4 15 13 121.39 61.97 52.93 o 5 15 13 8.99 -3.80 51.20 o 6 15 13 43.05 93.76 79.40 o 0 16 13 3.95 -164.82 113.44 o 1 16 13 315.00 264.04 87.12 o 2 16 13 10.61 -131.25 144.98 o 0 0 14 12720.88 13217.25 302.10 o 1 0 14 60463.26 61023.61 943.67 o 2 0 14 1070.58 909.94 33.43 o 3 0 14 12845.63 12599.16 204.76 o 4 0 14 613.37 804.82 27.27 o 5 0 14 28286.10 26788.89 451.66 o 6 0 14 9558.54 8929.59 177.94 o 7 0 14 131.64 171.01 31.69 o 8 0 14 12318.33 11568.59 248.48 o 9 0 14 5498.71 5415.15 139.44 o 10 0 14 2594.65 2128.93 113.83 o 11 0 14 27.53 60.87 50.31 o 12 0 14 1133.69 1201.48 78.46 o 13 0 14 659.37 681.46 70.29 o 14 0 14 121.57 97.38 64.57 o 15 0 14 1.32 -77.56 68.17 o 16 0 14 6.66 -61.23 78.62 o 17 0 14 186.00 146.26 84.53 o 1 1 14 583.88 649.40 22.57 o 2 1 14 21741.71 21166.35 236.89 o 3 1 14 8585.55 8455.27 100.26 o 4 1 14 6072.72 5678.39 77.21 o 5 1 14 5053.06 4959.69 69.83 o 6 1 14 1335.33 1281.73 43.52 o 7 1 14 953.63 1018.03 31.84 o 8 1 14 20.47 43.66 21.96 o 9 1 14 635.27 773.01 33.51 o 10 1 14 1066.09 1115.97 47.55 o 11 1 14 697.10 748.24 46.23 o 12 1 14 147.42 211.92 41.46 o 13 1 14 12.80 7.44 41.26 o 14 1 14 1.91 4.06 43.12 o 15 1 14 261.75 255.94 53.15 o 16 1 14 79.85 134.92 54.05 o 17 1 14 89.86 63.95 56.08 o 0 2 14 12123.29 11932.84 207.97 o 1 2 14 48.14 99.42 11.59 o 2 2 14 957.16 860.91 19.37 o 3 2 14 1685.26 1579.33 31.55 o 4 2 14 28.39 49.16 15.62 o 5 2 14 178.16 246.57 18.38 o 6 2 14 2040.73 1702.99 38.03 o 7 2 14 5290.36 4882.47 78.43 o 8 2 14 1793.39 1838.82 40.41 o 9 2 14 5954.42 5852.06 96.85 o 10 2 14 251.67 254.03 34.14 o 11 2 14 658.11 736.06 49.10 o 12 2 14 635.84 706.61 48.41 o 13 2 14 672.95 874.02 56.96 o 14 2 14 1015.75 1096.31 65.48 o 15 2 14 207.68 248.26 52.56 o 16 2 14 0.74 -28.79 51.43 o 17 2 14 5.14 22.42 56.50 o 1 3 14 922.52 847.76 19.59 o 2 3 14 0.35 29.63 14.59 o 3 3 14 84.89 70.81 17.90 o 4 3 14 8240.01 7897.56 103.14 o 5 3 14 446.41 429.14 20.77 o 6 3 14 7285.70 7080.64 95.68 o 7 3 14 1816.34 1799.69 37.93 o 8 3 14 2697.20 2581.81 48.27 o 9 3 14 1139.75 1238.99 37.05 o 10 3 14 8021.47 7464.48 125.41 o 11 3 14 3235.80 3022.46 81.72 o 12 3 14 891.86 893.01 51.30 o 13 3 14 1224.23 1427.37 61.82 o 14 3 14 268.29 236.55 51.92 o 15 3 14 735.97 809.81 61.33 o 16 3 14 414.87 565.27 65.73 o 17 3 14 783.52 875.36 116.37 o 0 4 14 27221.10 26530.83 418.02 o 1 4 14 1056.45 1024.63 29.45 o 2 4 14 486.51 433.00 23.50 o 3 4 14 5942.34 5673.33 77.91 o 4 4 14 5590.90 5287.68 74.61 o 5 4 14 3138.07 2884.81 49.46 o 6 4 14 2514.04 2337.61 43.98 o 7 4 14 2272.42 2233.87 44.17 o 8 4 14 924.71 963.49 31.01 o 9 4 14 4536.04 4241.80 77.77 o 10 4 14 983.99 927.03 37.77 o 11 4 14 21.17 51.13 37.07 o 12 4 14 310.07 363.28 47.94 o 13 4 14 616.95 632.72 51.89 o 14 4 14 297.49 428.20 53.76 o 15 4 14 555.28 434.42 55.90 o 16 4 14 3.50 -43.37 53.34 o 17 4 14 0.69 67.17 114.11 o 1 5 14 3567.75 3543.55 54.39 o 2 5 14 3617.49 3495.32 61.49 o 3 5 14 7127.25 6883.55 92.51 o 4 5 14 4872.32 4438.32 65.97 o 5 5 14 204.86 217.37 20.70 o 6 5 14 724.58 733.73 27.15 o 7 5 14 1711.63 1552.69 36.83 o 8 5 14 1153.84 1159.89 33.92 o 9 5 14 7.19 -9.34 25.05 o 10 5 14 963.48 1085.89 40.57 o 11 5 14 0.58 -1.28 31.53 o 12 5 14 78.11 128.21 42.03 o 13 5 14 4.33 9.32 42.28 o 14 5 14 256.79 232.58 50.17 o 15 5 14 146.76 101.95 53.70 o 16 5 14 3.03 60.61 55.34 o 0 6 14 19573.65 18780.56 349.59 o 1 6 14 20932.02 20319.52 265.15 o 2 6 14 7324.62 6972.36 97.05 o 3 6 14 5149.91 4531.39 75.13 o 4 6 14 149.45 173.45 20.69 o 5 6 14 5846.63 5619.15 80.72 o 6 6 14 5499.22 5380.42 90.42 o 7 6 14 120.77 108.58 22.98 o 8 6 14 1557.63 1402.84 40.76 o 9 6 14 2606.54 2649.22 64.78 o 10 6 14 1138.21 1120.84 40.40 o 11 6 14 5.06 60.60 33.20 o 12 6 14 369.68 370.14 42.64 o 13 6 14 282.13 396.49 49.88 o 14 6 14 4.78 -11.07 47.68 o 15 6 14 4.23 -27.33 50.32 o 16 6 14 5.92 -49.61 55.53 o 1 7 14 22.35 45.41 19.79 o 2 7 14 11616.97 11572.15 152.37 o 3 7 14 62.75 86.66 20.41 o 4 7 14 7086.07 6691.10 92.78 o 5 7 14 5161.36 5141.39 76.70 o 6 7 14 242.88 217.48 23.80 o 7 7 14 26.60 42.50 22.99 o 8 7 14 76.47 91.17 25.73 o 9 7 14 74.25 185.47 30.09 o 10 7 14 12.28 53.97 30.72 o 11 7 14 151.74 212.01 34.25 o 12 7 14 148.37 276.36 45.75 o 13 7 14 0.45 51.48 46.69 o 14 7 14 78.92 -1.59 59.38 o 15 7 14 67.69 167.06 65.86 o 0 8 14 3168.46 3236.98 83.81 o 1 8 14 806.64 852.71 30.71 o 2 8 14 2050.43 2089.54 49.38 o 3 8 14 308.13 308.96 24.97 o 4 8 14 15.41 57.68 23.19 o 5 8 14 504.39 563.30 29.45 o 6 8 14 1299.73 1353.77 39.95 o 7 8 14 295.28 338.40 30.31 o 8 8 14 2242.64 2249.43 58.84 o 9 8 14 1195.92 1234.19 48.59 o 10 8 14 5.55 -2.12 34.71 o 11 8 14 438.47 453.02 42.79 o 12 8 14 666.40 715.04 54.94 o 13 8 14 175.28 170.15 52.12 o 14 8 14 71.02 35.55 57.97 o 15 8 14 203.05 211.94 71.04 o 1 9 14 334.74 361.36 35.93 o 2 9 14 474.29 442.08 39.49 o 3 9 14 45.56 25.52 28.21 o 4 9 14 227.67 298.36 30.42 o 5 9 14 13.98 -4.56 28.18 o 6 9 14 692.16 741.59 37.55 o 7 9 14 2007.12 1990.00 63.54 o 8 9 14 1215.15 1172.04 49.43 o 9 9 14 26.64 59.09 35.93 o 10 9 14 1008.78 939.31 67.57 o 11 9 14 1492.78 1558.10 57.91 o 12 9 14 329.83 243.20 49.98 o 13 9 14 310.18 393.05 70.96 o 14 9 14 0.10 96.54 57.22 o 0 10 14 407.81 486.55 56.36 o 1 10 14 656.85 552.05 41.88 o 2 10 14 430.85 418.35 40.41 o 3 10 14 298.89 296.90 37.73 o 4 10 14 477.10 432.62 38.46 o 5 10 14 388.27 320.20 39.68 o 6 10 14 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41.29 66.79 o 7 0 28 379.59 334.43 73.49 o 8 0 28 1198.11 1452.17 97.78 o 9 0 28 140.91 25.10 77.08 o 1 1 28 370.16 426.08 50.93 o 2 1 28 77.11 150.38 47.07 o 3 1 28 1693.11 1864.56 71.44 o 4 1 28 30.67 7.93 45.75 o 5 1 28 80.85 109.30 46.88 o 6 1 28 10.69 -11.54 46.83 o 7 1 28 73.24 -24.16 47.13 o 8 1 28 18.52 68.90 49.47 o 9 1 28 0.99 -52.31 63.75 o 0 2 28 687.38 759.38 111.37 o 1 2 28 172.09 250.01 48.93 o 2 2 28 157.70 181.50 48.73 o 3 2 28 24.43 -2.59 46.50 o 4 2 28 690.04 696.82 91.98 o 5 2 28 11.77 22.08 49.10 o 6 2 28 191.70 181.72 49.60 o 7 2 28 381.20 515.96 54.52 o 8 2 28 11.89 42.87 49.77 o 9 2 28 222.78 230.02 60.39 o 1 3 28 490.48 581.35 55.82 o 2 3 28 633.55 668.07 55.19 o 3 3 28 9.42 48.76 47.18 o 4 3 28 262.13 276.13 50.82 o 5 3 28 1262.34 1413.55 66.58 o 6 3 28 37.14 66.38 47.98 o 7 3 28 256.89 259.01 52.04 o 8 3 28 652.49 706.48 63.62 o 9 3 28 173.54 208.19 52.31 o 0 4 28 248.60 144.12 68.86 o 1 4 28 1146.04 1333.40 73.10 o 2 4 28 181.54 234.08 50.41 o 3 4 28 8.08 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