#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:09:23 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180971 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/51/2205178.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205178_Fobs loop_ _publ_author_name 'Yu, Lin' 'Liu, Zhao' 'Fang, Hua' 'Zhao, Yu-Fen' _publ_section_title ; (3S,8S)-3,8-Dimethyl-1,6-dioxa-4,9-diaza-5\l^5^-phosphaspiro[4.4]nonane-2,7-dione ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o261 _journal_page_last o262 _journal_volume 61 _journal_year 2005 _space_group_IT_number 20 _symmetry_space_group_name_Hall 'C 2c 2' _symmetry_space_group_name_H-M 'C 2 2 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.1138 _cell_length_b 7.6933 _cell_length_c 19.8239 _exptl_crystal_F_000 432.00 _reflns_d_resolution_high 0.7557 _cod_data_source_file wn6313Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' A in C222(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 177.79 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-x, y, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5330.70 6811.93 48.95 o 4 0 0 4083.21 4830.99 59.26 o 6 0 0 85.93 90.35 14.39 o 8 0 0 62.17 65.14 16.88 o 1 1 0 561.30 218.90 18.33 o 3 1 0 3.65 1.32 6.21 o 5 1 0 117.84 103.17 13.00 o 7 1 0 1.26 12.60 11.86 o 0 2 0 31608.47 32484.12 610.31 o 2 2 0 145.10 68.46 13.93 o 4 2 0 2286.82 1529.93 59.14 o 6 2 0 0.75 4.03 9.13 o 1 3 0 55.45 76.86 9.01 o 3 3 0 15.38 10.54 7.59 o 5 3 0 233.57 170.87 22.20 o 7 3 0 3.54 6.61 13.68 o 0 4 0 164.81 151.76 12.64 o 2 4 0 138.41 164.31 14.60 o 4 4 0 726.56 614.40 36.66 o 6 4 0 128.71 103.69 19.71 o 1 5 0 76.75 98.84 11.19 o 3 5 0 27.96 38.27 11.22 o 5 5 0 62.73 24.19 17.80 o 7 5 0 13.49 -6.12 15.55 o 0 6 0 2.03 0.77 8.11 o 2 6 0 15.27 20.01 10.20 o 4 6 0 205.84 175.90 23.61 o 6 6 0 65.34 56.74 17.24 o 1 7 0 70.28 58.74 14.72 o 3 7 0 33.84 9.71 13.86 o 5 7 0 11.26 27.29 13.92 o 0 8 0 71.58 60.93 15.40 o 2 8 0 93.03 77.56 15.83 o 4 8 0 59.43 64.40 16.38 o 1 9 0 8.97 -9.07 13.74 o 3 9 0 12.91 0.00 11.10 o 0 10 0 17.47 16.26 15.71 o 2 0 1 580.16 748.93 16.21 o 4 0 1 8.31 1.26 8.98 o 6 0 1 21.51 28.74 11.22 o 8 0 1 12.79 0.00 15.09 o 1 1 1 5892.03 2536.08 56.90 o 3 1 1 1617.68 782.98 45.72 o 5 1 1 118.49 115.04 16.76 o 7 1 1 284.59 360.29 27.31 o 0 2 1 10029.42 11324.66 65.82 o 2 2 1 863.04 291.52 32.75 o 4 2 1 21.04 8.30 11.37 o 6 2 1 163.17 117.11 22.20 o 1 3 1 835.33 903.13 22.48 o 3 3 1 822.24 379.71 33.82 o 5 3 1 294.91 220.59 25.00 o 7 3 1 267.44 235.44 26.97 o 0 4 1 946.43 1101.13 29.87 o 2 4 1 4.67 11.13 6.12 o 4 4 1 48.63 36.95 13.22 o 6 4 1 64.60 66.95 16.63 o 1 5 1 275.02 302.64 16.95 o 3 5 1 422.86 434.64 24.49 o 5 5 1 213.01 123.63 25.09 o 7 5 1 74.95 57.14 20.07 o 0 6 1 237.01 194.69 18.51 o 2 6 1 212.39 153.47 15.65 o 4 6 1 100.26 79.16 16.02 o 6 6 1 7.70 7.16 13.49 o 1 7 1 147.14 150.46 15.89 o 3 7 1 126.61 131.64 17.31 o 5 7 1 71.81 66.09 19.67 o 0 8 1 167.69 158.92 22.47 o 2 8 1 31.30 31.48 13.25 o 4 8 1 44.45 41.40 15.86 o 1 9 1 31.33 40.24 13.56 o 3 9 1 37.03 35.99 17.70 o 0 10 1 48.66 41.31 17.95 o 0 0 2 14735.80 15049.73 216.84 o 2 0 2 421.11 534.80 13.46 o 4 0 2 1165.82 1371.25 31.04 o 6 0 2 12.32 19.98 9.47 o 8 0 2 124.02 138.61 20.47 o 1 1 2 2837.71 3033.57 34.14 o 3 1 2 97.61 59.00 12.05 o 5 1 2 821.59 777.47 38.61 o 7 1 2 37.60 38.70 16.94 o 0 2 2 6566.99 7619.04 55.63 o 2 2 2 922.39 471.06 32.60 o 4 2 2 982.45 578.09 42.79 o 6 2 2 19.73 14.51 11.34 o 1 3 2 177.20 197.18 11.66 o 3 3 2 602.41 414.19 32.63 o 5 3 2 211.18 162.41 23.80 o 7 3 2 30.49 33.87 15.46 o 0 4 2 1537.20 1650.52 35.54 o 2 4 2 566.61 656.32 26.59 o 4 4 2 729.57 590.27 37.74 o 6 4 2 67.66 75.90 17.28 o 1 5 2 132.78 140.20 13.62 o 3 5 2 149.36 167.56 17.13 o 5 5 2 145.70 103.21 23.27 o 7 5 2 41.93 34.55 17.49 o 0 6 2 319.56 291.08 22.30 o 2 6 2 93.49 137.23 15.68 o 4 6 2 287.13 276.08 26.54 o 6 6 2 44.56 39.19 19.30 o 1 7 2 104.95 113.41 16.14 o 3 7 2 100.25 118.94 16.17 o 5 7 2 24.74 25.05 14.45 o 0 8 2 81.06 37.44 16.78 o 2 8 2 53.52 51.76 13.92 o 4 8 2 74.37 82.20 17.68 o 1 9 2 37.60 36.46 14.48 o 3 9 2 23.93 26.00 15.43 o 0 10 2 21.83 17.74 14.48 o 2 0 3 2199.36 2618.50 30.57 o 4 0 3 15.83 29.26 7.38 o 6 0 3 37.47 56.96 12.14 o 8 0 3 72.75 117.27 17.92 o 1 1 3 965.49 1160.78 18.40 o 3 1 3 497.83 496.49 19.33 o 5 1 3 166.06 186.14 14.97 o 7 1 3 97.77 89.82 16.38 o 0 2 3 4725.63 5519.86 47.55 o 2 2 3 1901.43 1645.98 42.33 o 4 2 3 301.59 238.43 23.96 o 6 2 3 22.05 30.34 13.62 o 1 3 3 657.55 856.30 22.03 o 3 3 3 450.88 387.93 28.56 o 5 3 3 178.16 85.54 23.40 o 7 3 3 118.78 169.54 21.03 o 0 4 3 876.58 1055.96 29.40 o 2 4 3 165.66 183.91 15.28 o 4 4 3 272.69 277.39 24.60 o 6 4 3 14.08 36.67 12.33 o 1 5 3 193.83 238.62 15.47 o 3 5 3 421.46 503.29 26.58 o 5 5 3 89.28 91.36 15.55 o 0 6 3 80.95 70.61 14.51 o 2 6 3 130.00 133.98 15.56 o 4 6 3 124.92 147.32 20.51 o 6 6 3 18.32 13.28 12.79 o 1 7 3 34.29 51.12 11.53 o 3 7 3 101.63 122.96 16.05 o 5 7 3 48.28 32.49 16.91 o 0 8 3 62.62 75.43 15.92 o 2 8 3 43.49 29.60 14.54 o 4 8 3 29.47 39.28 15.25 o 1 9 3 24.67 20.93 13.46 o 3 9 3 50.11 62.40 17.12 o 0 10 3 33.31 10.39 15.49 o 0 0 4 1455.21 1589.05 18.31 o 2 0 4 487.18 651.99 15.74 o 4 0 4 526.13 594.72 21.33 o 6 0 4 367.60 367.83 24.82 o 1 1 4 1213.76 1401.63 20.95 o 3 1 4 2141.88 2740.77 38.66 o 5 1 4 189.14 184.36 14.24 o 7 1 4 0.94 -3.38 11.83 o 0 2 4 1554.83 1485.30 25.36 o 2 2 4 674.60 782.84 22.80 o 4 2 4 697.53 603.64 31.46 o 6 2 4 117.59 107.97 19.55 o 1 3 4 753.18 959.91 22.99 o 3 3 4 369.88 317.67 23.78 o 5 3 4 97.91 84.63 17.43 o 7 3 4 36.17 17.27 18.69 o 0 4 4 4531.38 4801.66 61.02 o 2 4 4 977.65 1057.81 32.26 o 4 4 4 727.06 603.30 36.60 o 6 4 4 10.21 20.53 13.22 o 1 5 4 154.30 182.30 14.24 o 3 5 4 37.78 39.28 9.28 o 5 5 4 55.55 62.15 13.43 o 0 6 4 1050.22 1137.54 38.72 o 2 6 4 82.24 82.42 15.59 o 4 6 4 293.11 292.16 26.29 o 6 6 4 7.60 10.51 14.81 o 1 7 4 65.46 75.25 13.28 o 3 7 4 43.50 42.97 12.79 o 5 7 4 25.85 37.13 12.79 o 0 8 4 81.74 78.51 15.92 o 2 8 4 5.54 -7.16 10.57 o 4 8 4 55.99 59.45 14.69 o 1 9 4 69.29 32.95 16.51 o 3 9 4 18.62 42.36 13.31 o 0 10 4 21.95 11.93 14.29 o 2 0 5 576.10 630.16 16.48 o 4 0 5 8.55 3.50 7.04 o 6 0 5 4.79 1.87 10.88 o 1 1 5 5466.57 5810.29 45.67 o 3 1 5 2142.28 2560.15 37.57 o 5 1 5 1076.58 1202.16 33.48 o 7 1 5 111.15 88.23 16.23 o 0 2 5 5623.91 5845.25 51.41 o 2 2 5 246.53 264.70 13.13 o 4 2 5 135.77 115.94 15.16 o 6 2 5 85.28 62.10 17.64 o 1 3 5 2286.80 2819.47 39.79 o 3 3 5 1310.03 1475.09 40.27 o 5 3 5 340.39 328.98 26.63 o 7 3 5 48.28 60.00 17.15 o 0 4 5 957.05 1200.32 31.25 o 2 4 5 25.67 29.82 7.10 o 4 4 5 100.37 123.74 15.28 o 6 4 5 23.13 -5.13 15.49 o 1 5 5 352.79 435.94 20.98 o 3 5 5 308.56 307.33 20.91 o 5 5 5 29.53 24.81 13.09 o 0 6 5 14.76 -0.83 11.80 o 2 6 5 24.67 27.85 10.11 o 4 6 5 30.98 17.00 14.57 o 6 6 5 13.97 18.13 13.34 o 1 7 5 23.41 42.66 11.96 o 3 7 5 92.30 105.50 17.15 o 5 7 5 8.31 -8.67 13.71 o 0 8 5 8.32 7.96 9.71 o 2 8 5 18.51 25.45 10.91 o 4 8 5 13.17 5.72 14.29 o 1 9 5 15.17 11.96 13.25 o 3 9 5 19.85 -2.95 16.41 o 0 0 6 33.01 35.26 5.04 o 2 0 6 2508.27 2762.14 34.70 o 4 0 6 1011.94 1117.56 29.97 o 6 0 6 564.41 674.42 30.73 o 1 1 6 196.03 199.83 9.60 o 3 1 6 2571.82 3125.77 42.71 o 5 1 6 42.42 49.77 11.07 o 7 1 6 41.57 56.71 14.26 o 0 2 6 631.66 586.13 16.98 o 2 2 6 1467.06 1761.05 31.00 o 4 2 6 706.03 661.39 27.95 o 6 2 6 295.97 347.30 25.31 o 1 3 6 988.55 1245.94 27.13 o 3 3 6 50.32 64.58 11.25 o 5 3 6 326.10 341.12 24.30 o 7 3 6 2.55 -5.62 12.57 o 0 4 6 1707.20 1644.86 37.17 o 2 4 6 465.35 475.70 21.35 o 4 4 6 360.97 312.74 23.78 o 6 4 6 68.80 60.16 17.40 o 1 5 6 547.28 587.89 25.42 o 3 5 6 22.39 26.25 10.05 o 5 5 6 205.27 193.70 21.61 o 0 6 6 735.17 776.69 31.86 o 2 6 6 57.85 89.45 13.09 o 4 6 6 133.41 125.03 17.58 o 6 6 6 6.99 -4.55 14.20 o 1 7 6 89.46 103.57 14.60 o 3 7 6 40.89 46.38 13.22 o 5 7 6 24.68 39.37 13.59 o 0 8 6 146.08 124.33 19.12 o 2 8 6 6.67 20.87 11.19 o 4 8 6 34.48 14.48 14.91 o 1 9 6 23.43 6.73 12.23 o 3 9 6 17.84 16.35 14.94 o 2 0 7 3.27 31.47 5.72 o 4 0 7 3.79 6.88 6.64 o 6 0 7 19.46 20.41 11.28 o 1 1 7 554.38 683.77 17.37 o 3 1 7 443.47 556.81 19.23 o 5 1 7 779.11 916.48 31.37 o 7 1 7 91.79 98.22 16.29 o 0 2 7 330.96 344.41 13.39 o 2 2 7 116.11 131.35 10.18 o 4 2 7 49.56 42.70 9.74 o 6 2 7 8.63 0.00 10.42 o 1 3 7 1065.59 1173.56 27.84 o 3 3 7 345.54 322.18 18.21 o 5 3 7 442.99 509.56 27.53 o 7 3 7 50.07 68.09 16.72 o 0 4 7 610.85 597.89 22.97 o 2 4 7 4.55 9.28 7.84 o 4 4 7 51.38 69.65 12.11 o 6 4 7 3.61 -13.12 13.12 o 1 5 7 814.75 888.54 30.36 o 3 5 7 304.79 308.67 21.71 o 5 5 7 33.83 11.93 13.62 o 0 6 7 291.63 256.39 21.19 o 2 6 7 117.26 104.74 15.19 o 4 6 7 47.57 47.46 14.42 o 6 6 7 29.69 45.89 15.46 o 1 7 7 253.31 282.80 21.83 o 3 7 7 97.02 137.26 17.58 o 5 7 7 1.53 16.17 12.88 o 0 8 7 15.75 21.02 12.14 o 2 8 7 40.05 85.85 13.80 o 4 8 7 26.00 32.21 15.49 o 1 9 7 29.81 32.67 12.91 o 3 9 7 17.13 42.14 12.60 o 0 0 8 815.56 716.87 17.45 o 2 0 8 2232.80 2330.93 34.72 o 4 0 8 515.69 503.61 21.57 o 6 0 8 123.43 128.16 14.91 o 1 1 8 608.04 645.60 17.96 o 3 1 8 94.42 89.25 9.68 o 5 1 8 34.01 19.21 8.33 o 7 1 8 16.74 1.17 12.29 o 0 2 8 1.14 -5.10 5.10 o 2 2 8 443.77 521.00 18.03 o 4 2 8 227.19 265.74 16.54 o 6 2 8 141.08 172.59 17.40 o 1 3 8 1830.63 2245.82 37.90 o 3 3 8 183.37 227.66 15.93 o 5 3 8 67.58 52.29 13.83 o 7 3 8 4.62 17.98 11.80 o 0 4 8 1.40 -6.73 6.73 o 2 4 8 100.22 91.28 12.48 o 4 4 8 42.38 41.47 10.94 o 6 4 8 84.98 107.01 17.55 o 1 5 8 745.73 854.97 30.48 o 3 5 8 203.63 214.83 18.73 o 5 5 8 47.13 51.70 15.89 o 0 6 8 173.99 162.43 16.30 o 2 6 8 148.01 183.88 17.22 o 4 6 8 14.84 22.22 11.53 o 6 6 8 11.36 -3.07 13.89 o 1 7 8 125.55 103.91 17.19 o 3 7 8 104.46 114.23 16.48 o 5 7 8 38.88 29.63 15.12 o 0 8 8 130.80 91.27 18.57 o 2 8 8 96.79 123.58 18.87 o 4 8 8 14.40 39.93 12.82 o 1 9 8 14.96 13.80 12.51 o 2 0 9 124.93 154.66 10.09 o 4 0 9 3.30 6.12 6.12 o 6 0 9 1.90 -1.01 8.94 o 1 1 9 26.66 20.69 5.81 o 3 1 9 676.46 635.04 22.26 o 5 1 9 341.88 330.55 20.24 o 7 1 9 95.47 89.18 16.54 o 0 2 9 384.20 410.66 15.82 o 2 2 9 12.74 18.17 5.93 o 4 2 9 57.25 50.75 9.68 o 6 2 9 13.27 21.09 9.77 o 1 3 9 168.54 170.94 12.64 o 3 3 9 735.59 809.68 28.35 o 5 3 9 213.43 225.28 19.83 o 7 3 9 49.86 30.43 17.49 o 0 4 9 7.64 6.27 6.45 o 2 4 9 154.97 162.31 14.94 o 4 4 9 15.83 11.25 9.74 o 6 4 9 9.37 16.84 11.96 o 1 5 9 527.81 541.57 25.29 o 3 5 9 147.25 161.01 16.36 o 5 5 9 92.05 75.65 16.45 o 0 6 9 152.95 139.43 16.02 o 2 6 9 214.09 195.89 21.12 o 4 6 9 26.12 40.36 12.88 o 1 7 9 261.44 265.61 23.68 o 3 7 9 35.75 22.99 15.15 o 5 7 9 36.49 37.47 15.22 o 0 8 9 20.10 10.88 12.73 o 2 8 9 21.48 15.37 14.72 o 4 8 9 30.86 34.40 15.03 o 1 9 9 27.06 52.07 13.43 o 0 0 10 1575.28 1576.15 29.13 o 2 0 10 1518.58 1552.17 30.83 o 4 0 10 700.84 688.09 26.44 o 6 0 10 277.04 297.07 23.09 o 1 1 10 1244.94 1413.00 28.41 o 3 1 10 354.78 369.13 18.15 o 5 1 10 350.62 339.35 21.56 o 7 1 10 1.31 0.00 10.02 o 0 2 10 464.80 511.57 17.67 o 2 2 10 1032.32 1148.26 28.63 o 4 2 10 338.54 384.94 20.67 o 6 2 10 207.10 208.70 20.81 o 1 3 10 116.44 139.92 11.99 o 3 3 10 185.89 187.72 14.85 o 5 3 10 1.59 -9.96 10.14 o 7 3 10 20.77 43.09 11.86 o 0 4 10 57.52 49.21 9.84 o 2 4 10 575.14 614.80 25.76 o 4 4 10 47.19 52.62 13.09 o 6 4 10 104.86 140.02 20.72 o 1 5 10 69.55 74.36 11.68 o 3 5 10 269.49 270.21 20.88 o 5 5 10 13.40 18.63 12.36 o 0 6 10 19.32 32.95 10.02 o 2 6 10 326.14 338.99 23.80 o 4 6 10 12.33 10.88 12.05 o 1 7 10 32.41 27.20 12.54 o 3 7 10 37.80 46.88 14.29 o 5 7 10 22.58 27.33 16.20 o 0 8 10 4.80 2.46 11.83 o 2 8 10 91.03 100.74 17.21 o 1 9 10 9.13 8.61 11.10 o 2 0 11 162.71 185.85 12.51 o 4 0 11 109.65 95.18 12.54 o 6 0 11 13.15 21.52 10.33 o 1 1 11 1746.49 1718.76 33.32 o 3 1 11 1183.18 1179.66 31.86 o 5 1 11 329.08 340.16 21.37 o 7 1 11 70.19 86.22 16.81 o 0 2 11 27.90 30.83 6.49 o 2 2 11 381.67 415.37 18.27 o 4 2 11 25.83 21.18 9.71 o 6 2 11 11.96 13.31 10.85 o 1 3 11 798.31 839.30 26.67 o 3 3 11 582.06 672.48 25.91 o 5 3 11 217.08 214.52 19.46 o 0 4 11 18.49 21.33 7.75 o 2 4 11 201.29 191.07 16.82 o 4 4 11 28.48 16.69 10.70 o 6 4 11 13.10 22.56 12.08 o 1 5 11 190.28 187.31 16.23 o 3 5 11 55.65 73.56 12.36 o 5 5 11 121.56 117.89 18.75 o 0 6 11 11.14 17.03 7.68 o 2 6 11 34.77 61.20 12.97 o 4 6 11 0.85 -7.41 11.74 o 1 7 11 44.25 40.17 14.48 o 3 7 11 11.36 -1.26 13.40 o 0 8 11 8.37 -8.85 10.20 o 2 8 11 9.26 17.40 12.76 o 1 9 11 13.65 38.02 11.50 o 0 0 12 179.20 204.52 12.02 o 2 0 12 93.51 104.50 10.98 o 4 0 12 29.50 47.55 10.14 o 6 0 12 197.18 205.47 21.03 o 1 1 12 620.70 590.19 20.75 o 3 1 12 2.60 5.96 7.19 o 5 1 12 92.99 105.93 12.88 o 7 1 12 12.01 -12.91 12.91 o 0 2 12 50.21 45.46 7.38 o 2 2 12 611.20 689.48 24.07 o 4 2 12 109.66 107.78 12.39 o 6 2 12 128.37 152.39 17.55 o 1 3 12 63.53 62.68 9.87 o 3 3 12 26.04 29.45 8.76 o 5 3 12 42.95 53.15 13.86 o 0 4 12 268.51 243.16 15.96 o 2 4 12 936.56 951.26 32.98 o 4 4 12 72.67 85.76 11.90 o 6 4 12 97.06 106.55 16.91 o 1 5 12 6.19 6.09 9.07 o 3 5 12 23.39 28.37 10.45 o 5 5 12 39.80 45.37 13.77 o 0 6 12 15.15 21.58 10.63 o 2 6 12 294.07 265.53 23.09 o 4 6 12 15.88 -1.26 13.83 o 1 7 12 29.59 58.56 12.42 o 3 7 12 16.23 20.66 10.79 o 0 8 12 2.89 6.49 10.48 o 2 8 12 39.37 28.77 14.82 o 2 0 13 70.45 72.39 10.21 o 4 0 13 106.25 107.26 13.43 o 6 0 13 5.96 8.02 9.80 o 1 1 13 476.44 423.56 18.25 o 3 1 13 82.29 80.54 11.47 o 5 1 13 41.88 31.01 11.47 o 0 2 13 229.10 261.03 15.44 o 2 2 13 402.98 418.46 19.96 o 4 2 13 103.06 89.00 13.40 o 6 2 13 20.14 23.70 11.74 o 1 3 13 356.98 344.59 18.95 o 3 3 13 112.82 119.03 13.37 o 5 3 13 61.74 74.05 15.43 o 0 4 13 10.67 10.67 8.21 o 2 4 13 139.77 159.04 14.82 o 4 4 13 39.83 46.81 13.13 o 6 4 13 48.76 76.91 16.60 o 1 5 13 99.73 71.38 14.39 o 3 5 13 64.55 63.81 13.37 o 5 5 13 95.02 132.43 17.95 o 0 6 13 0.10 -3.04 9.50 o 2 6 13 32.65 33.78 13.40 o 4 6 13 17.34 22.13 13.46 o 1 7 13 5.41 7.10 11.25 o 3 7 13 16.27 9.28 13.46 o 0 8 13 14.95 17.34 11.40 o 2 8 13 28.14 16.84 13.74 o 0 0 14 3.22 0.00 4.92 o 2 0 14 701.82 668.23 24.96 o 4 0 14 37.19 44.72 9.59 o 6 0 14 53.34 36.76 13.68 o 1 1 14 26.01 26.96 7.41 o 3 1 14 155.41 155.60 14.20 o 5 1 14 22.38 24.28 11.10 o 0 2 14 7.61 9.53 6.89 o 2 2 14 587.21 603.72 24.49 o 4 2 14 15.21 9.07 9.07 o 6 2 14 70.00 95.75 16.48 o 1 3 14 25.56 43.06 8.42 o 3 3 14 84.49 85.43 12.33 o 5 3 14 55.63 64.77 13.03 o 0 4 14 13.68 23.24 9.19 o 2 4 14 311.33 324.05 21.43 o 4 4 14 55.87 54.81 12.48 o 6 4 14 88.15 84.13 17.86 o 1 5 14 3.87 17.89 8.70 o 3 5 14 76.48 82.26 13.96 o 5 5 14 33.07 33.90 14.17 o 0 6 14 1.85 -3.17 9.53 o 2 6 14 63.73 37.29 16.26 o 4 6 14 36.86 41.53 14.35 o 1 7 14 46.44 22.01 14.97 o 3 7 14 17.27 15.00 12.85 o 0 8 14 2.68 10.97 11.80 o 2 8 14 16.81 12.97 13.89 o 2 0 15 0.46 1.41 8.48 o 4 0 15 0.21 9.96 6.95 o 6 0 15 0.38 -10.63 10.63 o 1 1 15 646.49 564.34 24.25 o 3 1 15 131.31 145.51 14.30 o 5 1 15 108.76 100.52 16.97 o 0 2 15 141.44 153.08 11.44 o 2 2 15 106.94 112.49 12.79 o 4 2 15 35.33 46.75 10.24 o 6 2 15 29.62 30.55 12.85 o 1 3 15 202.27 210.25 16.57 o 3 3 15 167.54 216.51 16.08 o 5 3 15 109.91 119.77 17.83 o 0 4 15 14.46 17.74 8.15 o 2 4 15 27.11 30.09 9.87 o 4 4 15 36.07 48.93 12.30 o 1 5 15 51.60 37.38 12.60 o 3 5 15 71.06 83.03 15.12 o 5 5 15 58.63 75.16 15.25 o 0 6 15 26.69 30.86 10.70 o 2 6 15 22.76 36.36 11.19 o 4 6 15 15.25 13.80 12.02 o 1 7 15 14.75 13.92 11.10 o 3 7 15 27.80 33.69 12.88 o 0 8 15 11.10 -15.52 15.52 o 0 0 16 978.72 776.40 28.43 o 2 0 16 2267.29 2082.05 48.52 o 4 0 16 7.45 22.84 8.39 o 6 0 16 54.72 43.25 15.80 o 1 1 16 69.15 91.64 11.80 o 3 1 16 5.11 -1.69 8.48 o 5 1 16 8.56 -6.64 12.72 o 0 2 16 150.66 122.70 14.57 o 2 2 16 884.30 932.69 33.37 o 4 2 16 21.08 32.12 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