#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:09:23 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180971 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/51/2205180.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205180_Fobs loop_ _publ_author_name 'Xu, Liang-Zhong' 'Li, Kai' 'Yu, Guan-Ping' 'Si, Guo-Dong' 'Yu, Cheng-Long' _publ_section_title ; 2-Oxo-2-phenylethyl morpholine-4-carbodithioate ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o215 _journal_page_last o216 _journal_volume 61 _journal_year 2005 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.5294 _cell_length_b 8.4805 _cell_length_c 33.3618 _exptl_crystal_F_000 1184.00 _reflns_d_resolution_high 0.8408 _cod_data_source_file wn6317Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 41128D in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 242.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 31169.27 29849.28 192.74 o 4 0 0 0.78 30.00 19.70 o 6 0 0 1564.12 1676.20 82.60 o 8 0 0 304.95 332.22 43.32 o 10 0 0 53.41 52.83 46.79 o 2 1 0 58772.82 50673.86 1180.49 o 4 1 0 2167.04 2154.99 41.53 o 6 1 0 1530.04 1501.99 76.99 o 8 1 0 170.29 169.53 31.28 o 10 1 0 808.51 828.40 60.07 o 0 2 0 2157.81 2176.98 34.83 o 2 2 0 4108.10 4105.19 144.34 o 4 2 0 6891.44 6719.80 136.39 o 6 2 0 1157.55 1156.07 41.82 o 8 2 0 277.92 202.22 46.79 o 10 2 0 225.85 275.17 56.50 o 2 3 0 52.58 51.32 8.32 o 4 3 0 740.35 915.73 26.35 o 6 3 0 256.19 259.96 37.01 o 8 3 0 190.36 201.38 44.16 o 10 3 0 65.15 74.02 50.27 o 0 4 0 324.35 323.50 20.81 o 2 4 0 4947.36 5404.89 134.73 o 4 4 0 227.85 193.17 24.41 o 6 4 0 258.94 237.95 55.07 o 8 4 0 332.55 358.65 51.44 o 10 4 0 104.93 150.06 57.76 o 2 5 0 1276.75 1301.90 29.30 o 4 5 0 939.96 973.28 38.30 o 6 5 0 146.89 132.55 31.01 o 8 5 0 490.29 535.14 66.37 o 0 6 0 210.75 220.16 25.31 o 2 6 0 648.79 685.44 30.09 o 4 6 0 74.53 72.48 22.94 o 6 6 0 51.00 78.45 32.12 o 8 6 0 217.23 219.31 57.93 o 2 7 0 2514.14 2530.40 85.68 o 4 7 0 24.05 11.02 28.27 o 6 7 0 1.12 -0.14 32.98 o 8 7 0 54.34 20.33 51.12 o 0 8 0 975.73 936.82 95.36 o 2 8 0 103.83 96.21 42.73 o 4 8 0 9.36 6.29 33.07 o 6 8 0 0.91 1.83 38.97 o 2 9 0 215.00 231.06 53.58 o 4 9 0 107.83 90.21 52.20 o 0 10 0 3.31 -11.64 65.81 o 1 1 1 2593.22 2700.77 46.02 o 2 1 1 273.97 280.62 8.17 o 3 1 1 2623.27 2596.96 42.79 o 4 1 1 4687.90 4640.02 41.90 o 5 1 1 1127.73 1141.72 25.83 o 6 1 1 293.26 301.03 19.15 o 7 1 1 566.27 514.76 25.59 o 8 1 1 934.58 932.58 34.97 o 9 1 1 59.00 62.69 21.02 o 10 1 1 97.64 118.70 28.12 o 11 1 1 61.65 40.86 30.40 o 0 2 1 20681.77 21357.20 297.70 o 1 2 1 8458.73 8394.27 66.27 o 2 2 1 7900.52 7979.06 163.08 o 3 2 1 3305.98 3254.94 31.75 o 4 2 1 90.99 95.32 10.97 o 5 2 1 1124.70 1132.78 26.09 o 6 2 1 151.52 149.00 16.29 o 7 2 1 7.23 2.08 15.12 o 8 2 1 25.01 13.24 22.94 o 9 2 1 66.64 79.23 29.56 o 10 2 1 2.51 1.21 32.37 o 11 2 1 4.76 -1.52 29.94 o 1 3 1 2466.54 2513.48 32.41 o 2 3 1 4537.12 4632.31 68.13 o 3 3 1 5069.73 5081.28 62.58 o 4 3 1 10.80 12.55 8.01 o 5 3 1 34.40 47.50 12.01 o 6 3 1 34.57 27.22 16.11 o 7 3 1 617.44 573.59 36.01 o 8 3 1 114.08 119.50 28.31 o 9 3 1 108.60 119.55 32.32 o 10 3 1 1.15 -0.67 33.97 o 0 4 1 56.26 35.22 9.20 o 1 4 1 50.31 48.95 7.32 o 2 4 1 0.09 4.43 6.76 o 3 4 1 28.17 39.91 8.95 o 4 4 1 310.97 291.05 15.45 o 5 4 1 951.67 925.58 30.39 o 6 4 1 55.92 56.96 21.61 o 7 4 1 57.49 62.09 25.90 o 8 4 1 46.92 36.41 26.82 o 9 4 1 205.79 240.94 37.51 o 10 4 1 33.27 19.79 35.28 o 1 5 1 1335.26 1374.96 19.66 o 2 5 1 258.08 239.35 13.57 o 3 5 1 2239.13 2198.41 40.03 o 4 5 1 201.08 222.12 18.23 o 5 5 1 3.39 4.14 16.08 o 6 5 1 103.07 106.17 21.17 o 7 5 1 167.62 178.10 31.14 o 8 5 1 1.91 8.42 27.23 o 9 5 1 1.87 0.52 33.02 o 0 6 1 111.25 97.28 15.75 o 1 6 1 339.57 362.07 16.27 o 2 6 1 370.99 377.25 18.26 o 3 6 1 912.82 918.21 29.99 o 4 6 1 173.21 148.07 19.06 o 5 6 1 218.05 216.05 24.45 o 6 6 1 275.85 266.89 27.00 o 7 6 1 0.01 2.86 24.23 o 8 6 1 32.37 43.16 33.24 o 9 6 1 9.42 5.73 35.21 o 1 7 1 481.10 498.84 25.13 o 2 7 1 16.44 10.56 16.63 o 3 7 1 231.16 214.75 24.50 o 4 7 1 67.33 47.01 21.76 o 5 7 1 89.16 59.19 23.52 o 6 7 1 49.70 53.44 24.88 o 7 7 1 119.47 122.91 29.66 o 8 7 1 12.63 2.95 35.34 o 0 8 1 0.12 -9.87 35.93 o 1 8 1 591.86 602.43 41.20 o 2 8 1 31.38 37.22 26.70 o 3 8 1 131.60 150.21 26.18 o 4 8 1 62.64 35.16 24.27 o 5 8 1 58.95 48.73 27.51 o 6 8 1 16.57 36.98 28.39 o 1 9 1 11.77 14.58 30.47 o 2 9 1 30.49 33.78 30.78 o 3 9 1 1.05 -3.97 31.48 o 4 9 1 1.80 11.17 29.67 o 5 9 1 70.41 56.89 32.73 o 0 10 1 62.98 67.31 56.27 o 1 10 1 45.14 55.67 37.70 o 0 0 2 6608.22 4.03 3.13 o 1 0 2 3331.92 3396.16 33.82 o 2 0 2 2776.66 2692.83 38.82 o 3 0 2 384.97 404.39 22.89 o 4 0 2 53.27 67.08 16.45 o 5 0 2 9127.95 8861.42 108.94 o 6 0 2 672.91 594.10 33.62 o 7 0 2 20.06 7.31 18.12 o 8 0 2 186.03 191.32 27.78 o 9 0 2 116.62 147.75 29.83 o 10 0 2 62.88 36.23 31.57 o 11 0 2 21.16 9.15 46.68 o 1 1 2 751.45 781.34 17.93 o 2 1 2 430.46 435.02 10.21 o 3 1 2 163.60 160.89 9.54 o 4 1 2 142.84 160.71 11.66 o 5 1 2 150.42 106.10 12.69 o 6 1 2 8.51 14.45 12.68 o 7 1 2 2.35 -1.33 14.58 o 8 1 2 1.24 1.64 17.64 o 9 1 2 91.73 92.86 23.67 o 10 1 2 0.82 -2.75 24.07 o 11 1 2 70.86 49.14 31.35 o 0 2 2 14693.30 14013.24 167.14 o 1 2 2 1580.64 1660.73 18.11 o 2 2 2 19464.37 19165.45 339.67 o 3 2 2 1085.20 1130.71 20.56 o 4 2 2 3685.40 3781.22 51.22 o 5 2 2 3474.23 3356.71 47.82 o 6 2 2 322.58 327.21 19.75 o 7 2 2 183.01 220.02 20.24 o 8 2 2 0.02 -0.48 22.74 o 9 2 2 654.82 729.36 45.65 o 10 2 2 43.43 35.57 33.49 o 11 2 2 33.12 27.28 33.92 o 1 3 2 10137.90 10297.35 128.96 o 2 3 2 939.65 854.05 16.16 o 3 3 2 53.60 47.51 8.29 o 4 3 2 1554.26 1470.33 22.09 o 5 3 2 905.31 946.74 24.44 o 6 3 2 231.82 218.52 21.07 o 7 3 2 6.59 6.35 21.12 o 8 3 2 2.01 11.48 24.47 o 9 3 2 3.08 4.05 27.89 o 10 3 2 3.85 11.44 33.81 o 0 4 2 102.80 101.55 10.46 o 1 4 2 4640.49 4567.11 55.20 o 2 4 2 1153.09 1144.92 23.67 o 3 4 2 2439.69 2534.52 33.47 o 4 4 2 589.30 589.88 19.46 o 5 4 2 77.21 87.88 16.35 o 6 4 2 0.68 -0.27 19.84 o 7 4 2 64.18 47.63 24.83 o 8 4 2 3.57 4.22 25.38 o 9 4 2 5.07 -3.03 30.07 o 10 4 2 58.23 51.07 36.40 o 1 5 2 286.56 316.95 11.95 o 2 5 2 105.51 112.02 12.71 o 3 5 2 1153.25 1159.59 26.67 o 4 5 2 494.79 488.04 23.21 o 5 5 2 305.52 307.06 23.49 o 6 5 2 154.51 160.14 22.83 o 7 5 2 40.26 29.26 27.35 o 8 5 2 64.74 57.67 31.27 o 9 5 2 50.23 29.41 33.18 o 0 6 2 58.36 62.30 14.88 o 1 6 2 67.39 71.29 11.94 o 2 6 2 280.40 274.14 18.29 o 3 6 2 1140.12 1172.18 32.41 o 4 6 2 55.90 58.31 17.46 o 5 6 2 24.37 27.41 17.40 o 6 6 2 7.66 9.10 21.18 o 7 6 2 16.24 16.58 25.94 o 8 6 2 62.52 51.86 34.52 o 9 6 2 17.15 12.74 38.01 o 1 7 2 59.49 54.21 17.31 o 2 7 2 277.10 280.25 22.60 o 3 7 2 993.76 907.67 33.48 o 4 7 2 47.86 48.32 21.38 o 5 7 2 121.74 115.07 24.84 o 6 7 2 0.61 1.22 24.12 o 7 7 2 479.02 463.49 37.06 o 8 7 2 3.82 18.84 36.42 o 0 8 2 54.07 75.12 38.95 o 1 8 2 12.58 10.30 25.50 o 2 8 2 0.01 1.62 22.82 o 3 8 2 70.20 64.10 24.17 o 4 8 2 4.99 4.78 23.52 o 5 8 2 91.03 75.21 27.67 o 6 8 2 6.94 11.34 27.42 o 1 9 2 303.83 289.28 40.00 o 2 9 2 21.91 28.82 31.97 o 3 9 2 77.71 79.55 34.31 o 4 9 2 11.54 3.72 30.72 o 5 9 2 62.08 47.83 30.87 o 0 10 2 51.39 30.33 50.49 o 1 10 2 9.15 8.89 36.40 o 1 1 3 720.51 810.13 13.32 o 2 1 3 23695.95 23437.82 382.52 o 3 1 3 3198.79 3224.36 59.15 o 4 1 3 7127.77 7049.85 72.11 o 5 1 3 137.70 134.66 13.56 o 6 1 3 1416.31 1389.21 31.75 o 7 1 3 616.63 621.15 27.61 o 8 1 3 908.65 939.79 35.24 o 9 1 3 100.14 84.31 23.23 o 10 1 3 7.19 5.96 24.56 o 11 1 3 28.24 23.52 29.90 o 0 2 3 1963.22 1817.59 21.33 o 1 2 3 10482.61 10580.87 98.87 o 2 2 3 16461.77 16334.46 300.17 o 3 2 3 381.58 341.97 10.96 o 4 2 3 33.66 45.71 9.59 o 5 2 3 931.27 959.32 24.46 o 6 2 3 13.76 16.07 13.33 o 7 2 3 35.22 22.86 15.78 o 8 2 3 185.89 165.71 24.98 o 9 2 3 160.59 164.38 32.35 o 10 2 3 1.32 0.76 30.89 o 11 2 3 8.63 7.01 33.12 o 1 3 3 2831.26 2816.78 40.58 o 2 3 3 2216.06 2251.51 35.61 o 3 3 3 1472.22 1465.53 27.30 o 4 3 3 582.64 643.43 15.46 o 5 3 3 37.72 48.97 11.97 o 6 3 3 293.39 320.52 23.24 o 7 3 3 13.27 3.45 20.96 o 8 3 3 151.12 183.07 30.77 o 9 3 3 0.78 -3.62 28.51 o 10 3 3 111.26 138.90 38.63 o 0 4 3 2999.95 3060.85 50.49 o 1 4 3 1405.43 1525.07 18.59 o 2 4 3 865.74 907.36 14.76 o 3 4 3 562.67 605.69 18.45 o 4 4 3 931.46 933.96 23.03 o 5 4 3 0.30 -2.09 13.67 o 6 4 3 15.31 5.45 20.98 o 7 4 3 175.43 162.91 27.71 o 8 4 3 2.15 0.62 25.48 o 9 4 3 48.49 53.95 31.54 o 10 4 3 120.09 154.66 42.08 o 1 5 3 2437.06 2480.22 41.90 o 2 5 3 1503.25 1531.42 31.36 o 3 5 3 393.49 394.00 16.89 o 4 5 3 61.71 73.32 15.21 o 5 5 3 10.10 9.51 14.98 o 6 5 3 383.01 363.82 27.10 o 7 5 3 279.99 306.45 34.16 o 8 5 3 1.63 -1.16 28.04 o 9 5 3 28.54 20.73 32.47 o 0 6 3 1337.26 1309.13 34.71 o 1 6 3 754.25 755.55 20.96 o 2 6 3 555.15 587.06 23.11 o 3 6 3 31.10 25.57 14.92 o 4 6 3 311.43 316.44 22.96 o 5 6 3 56.67 54.27 18.62 o 6 6 3 475.12 428.32 30.28 o 7 6 3 80.77 64.74 27.51 o 8 6 3 36.55 40.78 34.02 o 9 6 3 6.27 8.28 36.90 o 1 7 3 0.67 -1.16 16.07 o 2 7 3 230.03 240.84 20.15 o 3 7 3 25.67 24.07 18.38 o 4 7 3 0.16 3.70 19.89 o 5 7 3 112.59 109.69 24.88 o 6 7 3 16.20 13.83 23.91 o 7 7 3 43.26 46.98 27.62 o 8 7 3 56.36 56.73 38.91 o 0 8 3 269.07 268.16 47.80 o 1 8 3 122.46 129.99 29.05 o 2 8 3 15.38 4.13 23.95 o 3 8 3 297.04 310.43 30.45 o 4 8 3 179.36 166.16 26.43 o 5 8 3 8.66 13.65 25.47 o 6 8 3 236.49 245.24 34.76 o 1 9 3 303.14 314.49 40.25 o 2 9 3 4.55 9.95 31.22 o 3 9 3 1.71 7.92 31.10 o 4 9 3 13.71 17.27 31.32 o 5 9 3 22.68 9.44 30.23 o 0 10 3 162.10 185.68 62.43 o 1 10 3 3.65 2.69 35.78 o 0 0 4 16535.12 15623.50 120.66 o 1 0 4 6030.45 5969.55 180.42 o 2 0 4 12339.20 13321.41 325.49 o 3 0 4 8667.79 8468.38 167.43 o 4 0 4 552.59 514.08 24.19 o 5 0 4 390.70 393.32 26.30 o 6 0 4 97.83 77.50 19.71 o 7 0 4 2.35 4.31 20.20 o 8 0 4 1.87 6.71 21.70 o 9 0 4 622.67 649.40 42.47 o 10 0 4 53.11 53.21 31.61 o 11 0 4 3.89 2.74 40.31 o 1 1 4 15983.09 15900.79 296.64 o 2 1 4 1503.92 1483.73 21.21 o 3 1 4 580.83 599.95 15.56 o 4 1 4 5532.61 5426.89 93.18 o 5 1 4 384.26 402.41 19.09 o 6 1 4 347.42 339.60 19.78 o 7 1 4 68.31 64.10 16.20 o 8 1 4 1.31 2.25 16.31 o 9 1 4 145.59 141.03 24.96 o 10 1 4 35.50 22.50 26.14 o 11 1 4 4.39 1.67 29.57 o 0 2 4 8.21 24.37 5.88 o 1 2 4 16612.56 16432.56 199.72 o 2 2 4 5705.03 5860.57 116.35 o 3 2 4 2687.40 2759.81 40.27 o 4 2 4 2769.83 2756.73 53.39 o 5 2 4 201.91 176.47 14.88 o 6 2 4 110.51 90.21 15.34 o 7 2 4 127.70 126.34 18.41 o 8 2 4 30.97 18.91 21.30 o 9 2 4 127.52 138.83 30.89 o 10 2 4 80.05 57.82 33.36 o 11 2 4 94.27 101.13 36.45 o 1 3 4 473.05 449.12 11.47 o 2 3 4 3.79 14.45 7.36 o 3 3 4 1049.67 1068.40 20.67 o 4 3 4 837.08 842.78 16.56 o 5 3 4 618.38 655.53 21.70 o 6 3 4 22.26 13.92 15.76 o 7 3 4 1331.57 1317.08 70.73 o 8 3 4 168.73 182.18 30.74 o 9 3 4 39.29 31.05 30.37 o 10 3 4 84.13 120.16 37.07 o 0 4 4 114.83 114.04 10.63 o 1 4 4 1350.83 1335.85 17.65 o 2 4 4 2871.84 2896.81 48.94 o 3 4 4 689.63 666.33 19.67 o 4 4 4 31.11 16.15 10.58 o 5 4 4 1814.94 1792.27 39.24 o 6 4 4 371.03 388.06 32.28 o 7 4 4 0.17 5.98 22.84 o 8 4 4 61.24 49.50 28.93 o 9 4 4 313.49 332.39 41.09 o 10 4 4 27.98 28.03 36.42 o 1 5 4 719.07 768.45 16.09 o 2 5 4 271.17 276.53 14.10 o 3 5 4 128.79 122.38 12.74 o 4 5 4 6.87 4.99 13.94 o 5 5 4 11.00 12.23 15.29 o 6 5 4 127.00 149.41 22.93 o 7 5 4 24.62 32.01 26.47 o 8 5 4 86.76 82.93 31.78 o 9 5 4 40.37 30.97 33.79 o 0 6 4 599.56 663.30 28.29 o 1 6 4 2.95 3.84 11.33 o 2 6 4 466.84 469.10 21.26 o 3 6 4 2.10 -0.82 14.51 o 4 6 4 36.40 30.52 16.59 o 5 6 4 186.77 206.11 22.19 o 6 6 4 300.64 322.03 28.41 o 7 6 4 44.96 38.05 26.33 o 8 6 4 75.37 79.90 34.33 o 9 6 4 54.25 57.43 38.63 o 1 7 4 422.57 433.40 24.18 o 2 7 4 807.93 832.36 29.09 o 3 7 4 438.45 426.18 24.61 o 4 7 4 240.77 230.03 26.08 o 5 7 4 165.96 156.99 26.22 o 6 7 4 12.94 8.11 23.43 o 7 7 4 51.99 65.34 27.90 o 8 7 4 10.02 7.64 35.79 o 0 8 4 81.20 93.76 38.75 o 1 8 4 5.86 12.80 25.42 o 2 8 4 165.47 156.76 28.18 o 3 8 4 29.50 29.51 21.83 o 4 8 4 0.01 2.47 21.87 o 5 8 4 9.27 9.76 25.22 o 6 8 4 0.73 5.08 28.25 o 1 9 4 108.69 138.44 35.53 o 2 9 4 92.61 80.65 33.83 o 3 9 4 75.17 83.00 34.90 o 4 9 4 30.13 21.07 32.80 o 0 10 4 9.00 22.05 53.69 o 1 1 5 35334.11 34416.66 487.16 o 2 1 5 2081.15 2211.31 40.83 o 3 1 5 2059.40 2074.09 32.03 o 4 1 5 746.72 766.86 20.21 o 5 1 5 1020.28 1056.32 26.16 o 6 1 5 194.63 213.38 17.99 o 7 1 5 757.22 808.98 30.14 o 8 1 5 3.75 11.95 17.15 o 9 1 5 28.06 25.02 22.29 o 10 1 5 28.93 37.62 26.24 o 11 1 5 0.70 5.32 30.37 o 0 2 5 17607.84 17476.76 137.89 o 1 2 5 2549.72 2714.66 36.56 o 2 2 5 5775.37 6111.79 114.52 o 3 2 5 11.61 15.92 6.12 o 4 2 5 517.52 512.52 17.99 o 5 2 5 370.80 372.91 18.54 o 6 2 5 2028.77 1983.76 37.43 o 7 2 5 7.68 8.06 17.95 o 8 2 5 79.13 89.93 23.18 o 9 2 5 546.36 494.46 41.64 o 10 2 5 1.50 12.42 29.27 o 11 2 5 4.29 1.38 33.28 o 1 3 5 360.69 352.51 10.69 o 2 3 5 254.81 253.05 11.45 o 3 3 5 621.23 615.70 17.29 o 4 3 5 2208.75 2014.57 22.95 o 5 3 5 2.77 2.92 12.12 o 6 3 5 139.18 179.07 21.11 o 7 3 5 1413.17 1384.60 50.28 o 8 3 5 182.61 187.60 31.69 o 9 3 5 47.34 52.34 31.47 o 10 3 5 124.95 143.45 37.92 o 0 4 5 174.78 200.36 12.20 o 1 4 5 620.47 636.30 13.79 o 2 4 5 686.63 693.27 18.60 o 3 4 5 990.40 1017.56 22.86 o 4 4 5 19.40 19.44 10.64 o 5 4 5 161.73 155.66 15.52 o 6 4 5 202.11 250.61 28.89 o 7 4 5 24.19 21.53 23.48 o 8 4 5 30.03 52.96 29.00 o 9 4 5 25.56 29.46 31.22 o 10 4 5 28.23 27.43 34.88 o 1 5 5 187.50 209.26 10.75 o 2 5 5 209.07 216.43 14.73 o 3 5 5 303.82 318.33 17.07 o 4 5 5 1757.66 1743.75 36.56 o 5 5 5 821.25 791.99 29.83 o 6 5 5 285.40 276.72 25.27 o 7 5 5 33.64 47.86 27.88 o 8 5 5 143.06 131.68 34.80 o 9 5 5 32.45 37.69 35.39 o 0 6 5 860.62 849.72 31.17 o 1 6 5 450.02 463.84 19.64 o 2 6 5 0.96 2.82 12.74 o 3 6 5 33.16 24.07 15.00 o 4 6 5 298.21 305.48 22.72 o 5 6 5 284.42 277.45 24.41 o 6 6 5 207.55 158.66 25.79 o 7 6 5 61.38 31.78 26.58 o 8 6 5 15.83 3.70 32.63 o 1 7 5 25.04 29.97 16.65 o 2 7 5 41.68 30.63 16.26 o 3 7 5 246.52 233.44 21.39 o 4 7 5 4.84 7.52 19.10 o 5 7 5 46.60 46.99 23.99 o 6 7 5 8.27 8.48 23.93 o 7 7 5 119.92 111.83 29.71 o 8 7 5 62.90 93.99 39.84 o 0 8 5 118.63 141.73 43.29 o 1 8 5 900.35 866.14 41.70 o 2 8 5 73.60 66.92 23.04 o 3 8 5 47.30 45.87 21.84 o 4 8 5 69.65 80.59 24.04 o 5 8 5 422.19 391.64 35.64 o 6 8 5 0.06 -0.03 27.71 o 1 9 5 17.60 18.80 31.22 o 2 9 5 2.37 3.36 31.13 o 3 9 5 125.81 116.93 35.50 o 4 9 5 3.86 2.85 30.99 o 0 10 5 55.11 34.36 53.20 o 0 0 6 5617.59 5421.91 75.21 o 1 0 6 1827.07 1777.39 62.79 o 2 0 6 976.32 1017.47 21.16 o 3 0 6 3749.77 3921.08 89.56 o 4 0 6 132.87 124.92 15.53 o 5 0 6 26.57 18.99 15.03 o 6 0 6 7820.42 7821.16 187.62 o 7 0 6 8.01 9.93 21.57 o 8 0 6 1689.02 1653.21 51.73 o 9 0 6 12.61 2.66 26.56 o 10 0 6 694.16 685.05 54.91 o 11 0 6 4.23 8.41 42.37 o 1 1 6 2337.35 2332.27 38.79 o 2 1 6 4244.62 4452.63 85.07 o 3 1 6 3096.29 3193.48 46.22 o 4 1 6 489.89 514.99 17.65 o 5 1 6 70.73 83.28 12.74 o 6 1 6 71.69 67.74 14.85 o 7 1 6 93.01 97.65 17.96 o 8 1 6 770.52 736.38 30.68 o 9 1 6 0.12 -5.34 21.68 o 10 1 6 159.26 156.38 32.35 o 11 1 6 9.16 7.47 29.18 o 0 2 6 4386.38 4299.36 45.03 o 1 2 6 359.43 418.03 9.77 o 2 2 6 1704.67 1738.52 23.73 o 3 2 6 735.21 758.15 15.68 o 4 2 6 9781.99 9933.93 134.07 o 5 2 6 450.75 535.76 21.09 o 6 2 6 18.63 12.03 13.70 o 7 2 6 610.43 625.03 31.49 o 8 2 6 79.45 63.31 22.10 o 9 2 6 103.84 102.96 30.11 o 10 2 6 116.59 151.40 33.17 o 1 3 6 9310.59 9463.05 68.71 o 2 3 6 2447.27 2308.81 27.08 o 3 3 6 5567.34 5770.70 69.48 o 4 3 6 24.44 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7 4 8 10.48 2.20 24.33 o 8 4 8 68.86 61.36 29.14 o 9 4 8 183.96 184.80 37.50 o 10 4 8 9.29 5.56 36.59 o 1 5 8 180.17 190.93 12.27 o 2 5 8 454.82 458.57 18.28 o 3 5 8 614.20 595.24 22.08 o 4 5 8 18.14 21.28 13.69 o 5 5 8 143.94 139.32 19.40 o 6 5 8 296.49 281.79 26.04 o 7 5 8 2.39 2.35 25.91 o 8 5 8 0.63 3.12 29.53 o 9 5 8 150.26 111.76 38.68 o 0 6 8 1169.12 1117.54 40.24 o 1 6 8 0.03 1.18 11.89 o 2 6 8 161.68 156.93 15.84 o 3 6 8 49.92 58.68 16.40 o 4 6 8 298.09 311.02 23.65 o 5 6 8 44.76 55.09 19.34 o 6 6 8 15.50 16.68 20.13 o 7 6 8 0.01 -0.78 26.67 o 8 6 8 13.36 9.06 33.38 o 1 7 8 1317.99 1309.25 35.82 o 2 7 8 161.37 160.10 19.91 o 3 7 8 353.92 377.60 24.45 o 4 7 8 3.54 1.95 19.48 o 5 7 8 5.27 12.03 20.84 o 6 7 8 31.14 20.32 23.50 o 7 7 8 13.26 14.54 29.46 o 0 8 8 347.26 306.53 40.16 o 1 8 8 50.41 47.19 22.09 o 2 8 8 32.62 33.04 21.28 o 3 8 8 23.18 7.63 22.89 o 4 8 8 0.25 2.52 22.70 o 5 8 8 3.26 -1.47 23.87 o 6 8 8 1.25 -2.84 30.89 o 1 9 8 295.93 300.68 39.85 o 2 9 8 17.25 10.12 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4 9 166.94 179.54 13.98 o 4 4 9 320.58 313.06 17.60 o 5 4 9 80.30 97.68 16.23 o 6 4 9 1132.48 1171.79 47.66 o 7 4 9 54.60 64.75 26.71 o 8 4 9 23.26 17.54 28.03 o 9 4 9 4.25 2.47 32.38 o 10 4 9 83.82 92.09 39.36 o 1 5 9 27.51 36.26 10.74 o 2 5 9 3.77 2.28 10.43 o 3 5 9 446.01 460.71 20.43 o 4 5 9 1627.56 1635.45 33.40 o 5 5 9 288.71 249.40 21.88 o 6 5 9 92.67 97.60 21.99 o 7 5 9 166.84 145.10 32.16 o 8 5 9 245.53 230.06 37.84 o 9 5 9 22.50 19.82 34.11 o 0 6 9 4169.73 4119.35 111.34 o 1 6 9 0.05 -3.16 11.83 o 2 6 9 134.58 133.85 15.17 o 3 6 9 2.23 -0.46 14.14 o 4 6 9 648.30 649.36 29.59 o 5 6 9 0.08 -2.32 17.77 o 6 6 9 73.77 73.36 21.92 o 7 6 9 7.46 6.84 27.58 o 8 6 9 10.72 -0.13 33.28 o 1 7 9 24.32 17.37 17.49 o 2 7 9 714.78 666.45 28.20 o 3 7 9 37.65 35.74 17.83 o 4 7 9 70.50 85.97 20.29 o 5 7 9 0.29 -0.98 20.56 o 6 7 9 0.81 0.81 25.23 o 7 7 9 49.31 26.81 31.18 o 0 8 9 32.92 40.49 31.45 o 1 8 9 29.84 25.23 20.33 o 2 8 9 2.15 -0.06 20.22 o 3 8 9 17.37 24.89 22.33 o 4 8 9 158.99 200.40 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15.67 o 2 6 10 133.01 150.76 15.92 o 3 6 10 429.41 452.69 22.98 o 4 6 10 317.06 323.30 23.80 o 5 6 10 22.74 18.38 18.52 o 6 6 10 5.32 -0.81 21.94 o 7 6 10 19.04 14.43 27.25 o 8 6 10 1.16 9.62 35.04 o 1 7 10 21.84 21.55 16.41 o 2 7 10 10.74 5.02 17.75 o 3 7 10 446.81 475.98 26.20 o 4 7 10 437.36 425.35 26.58 o 5 7 10 0.54 -3.78 23.14 o 6 7 10 100.09 108.21 29.01 o 7 7 10 140.75 142.53 35.23 o 0 8 10 31.42 23.94 31.53 o 1 8 10 17.66 17.48 20.86 o 2 8 10 1.31 4.28 20.87 o 3 8 10 83.42 47.57 22.47 o 4 8 10 20.50 10.17 24.17 o 5 8 10 26.06 23.38 25.20 o 6 8 10 64.30 56.07 35.25 o 1 9 10 230.99 230.68 35.51 o 2 9 10 64.01 41.29 29.89 o 3 9 10 75.41 75.02 31.38 o 4 9 10 14.54 8.51 32.32 o 1 1 11 363.24 388.56 9.73 o 2 1 11 2252.84 2365.99 35.94 o 3 1 11 454.54 443.78 14.06 o 4 1 11 988.54 999.83 21.09 o 5 1 11 0.71 1.06 10.69 o 6 1 11 837.16 804.66 26.21 o 7 1 11 2340.98 2431.96 46.56 o 8 1 11 270.32 284.80 26.40 o 9 1 11 0.33 -3.38 23.18 o 10 1 11 108.07 113.55 32.76 o 0 2 11 9369.13 9538.74 182.84 o 1 2 11 5598.64 5578.04 55.70 o 2 2 11 0.14 4.86 6.99 o 3 2 11 4772.47 4807.86 74.28 o 4 2 11 545.30 577.02 19.43 o 5 2 11 34.59 39.36 12.56 o 6 2 11 558.73 533.24 29.24 o 7 2 11 226.60 205.39 24.74 o 8 2 11 487.25 463.62 30.31 o 9 2 11 188.91 202.25 31.70 o 10 2 11 0.56 0.16 33.97 o 1 3 11 5388.53 5646.83 47.60 o 2 3 11 891.50 936.18 17.98 o 3 3 11 3205.62 3281.68 46.04 o 4 3 11 8.50 11.25 11.78 o 5 3 11 323.82 317.32 21.66 o 6 3 11 30.41 36.13 18.31 o 7 3 11 3.89 13.78 20.80 o 8 3 11 40.22 35.51 27.02 o 9 3 11 144.32 126.55 35.91 o 10 3 11 10.91 0.97 37.75 o 0 4 11 3449.73 3210.80 50.29 o 1 4 11 756.56 726.23 17.47 o 2 4 11 2.02 1.73 9.23 o 3 4 11 184.80 200.66 14.79 o 4 4 11 2.04 8.13 11.94 o 5 4 11 722.59 664.90 27.79 o 6 4 11 484.57 465.75 28.10 o 7 4 11 14.94 31.46 26.02 o 8 4 11 5.17 -2.81 27.76 o 9 4 11 28.60 7.67 32.86 o 1 5 11 1088.36 1070.13 24.51 o 2 5 11 1000.75 1016.02 24.58 o 3 5 11 451.90 443.65 20.53 o 4 5 11 425.73 396.50 21.23 o 5 5 11 0.31 5.22 16.64 o 6 5 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68.69 76.69 28.03 o 6 1 28 4.09 1.10 35.95 o 7 1 28 115.22 86.13 37.72 o 0 2 28 428.59 470.35 53.19 o 1 2 28 391.77 400.14 28.16 o 2 2 28 23.68 16.00 19.58 o 3 2 28 230.09 263.26 26.82 o 4 2 28 32.77 42.08 25.69 o 5 2 28 1.14 2.72 26.44 o 6 2 28 134.22 170.17 34.25 o 7 2 28 9.69 9.45 42.75 o 1 3 28 4.60 5.44 20.28 o 2 3 28 163.96 183.20 28.59 o 3 3 28 347.40 324.11 29.96 o 4 3 28 144.06 167.86 31.59 o 5 3 28 0.42 -3.78 28.26 o 6 3 28 34.48 18.20 30.46 o 7 3 28 3.82 4.98 36.35 o 0 4 28 5.43 6.77 38.66 o 1 4 28 370.82 394.02 33.83 o 2 4 28 13.92 13.73 22.40 o 3 4 28 2.30 1.48 24.32 o 4 4 28 268.49 271.92 32.05 o 5 4 28 92.04 71.27 32.76 o 6 4 28 47.26 46.38 34.24 o 1 5 28 79.68 102.99 28.57 o 2 5 28 86.57 77.36 26.97 o 3 5 28 12.91 4.89 25.74 o 4 5 28 47.18 28.93 29.38 o 5 5 28 0.09 -6.08 29.22 o 0 6 28 233.38 250.93 47.25 o 1 6 28 11.22 15.24 31.08 o 2 6 28 52.73 29.62 31.49 o 3 6 28 51.22 64.14 34.09 o 4 6 28 3.77 3.27 32.00 o 1 7 28 17.53 14.12 31.59 o 1 1 29 522.46 647.89 30.30 o 2 1 29 80.12 64.74 19.63 o 3 1 29 101.87 113.75 21.91 o 4 1 29 376.86 411.22 29.37 o 5 1 29 22.39 10.56 27.04 o 6 1 29 3.62 -0.39 33.19 o 7 1 29 55.95 29.17 43.43 o 0 2 29 150.81 165.53 33.98 o 1 2 29 164.43 163.07 24.61 o 2 2 29 588.97 562.26 32.99 o 3 2 29 77.84 75.64 27.05 o 4 2 29 73.89 60.36 27.50 o 5 2 29 32.84 38.61 28.09 o 6 2 29 179.82 181.15 36.23 o 7 2 29 1.08 -6.38 43.55 o 1 3 29 103.83 121.10 23.84 o 2 3 29 11.18 13.74 24.73 o 3 3 29 153.24 157.97 29.88 o 4 3 29 223.11 231.25 34.07 o 5 3 29 15.16 21.86 29.91 o 6 3 29 0.81 4.29 31.60 o 0 4 29 545.58 469.17 58.59 o 1 4 29 96.63 86.15 27.31 o 2 4 29 16.32 8.99 26.68 o 3 4 29 137.55 102.73 27.67 o 4 4 29 7.62 11.01 27.26 o 5 4 29 42.32 48.44 33.21 o 6 4 29 5.92 0.02 34.74 o 1 5 29 407.17 394.76 43.23 o 2 5 29 237.00 246.44 33.10 o 3 5 29 14.77 9.02 27.46 o 4 5 29 128.02 113.27 31.39 o 5 5 29 0.39 3.22 33.35 o 0 6 29 39.92 35.70 51.22 o 1 6 29 2.23 6.54 31.27 o 2 6 29 62.11 58.49 32.48 o 3 6 29 1.69 0.12 33.64 o 0 0 30 718.78 667.14 58.12 o 1 0 30 685.17 735.44 42.92 o 2 0 30 152.64 148.30 29.81 o 3 0 30 161.00 189.21 31.56 o 4 0 30 189.38 233.59 35.30 o 5 0 30 99.30 88.01 39.16 o 6 0 30 3.78 -5.15 62.45 o 7 0 30 51.23 32.91 80.81 o 1 1 30 251.72 278.92 26.88 o 2 1 30 25.41 16.65 19.42 o 3 1 30 5.88 0.50 20.81 o 4 1 30 15.23 17.88 22.04 o 5 1 30 10.93 18.15 28.39 o 6 1 30 9.64 4.86 32.65 o 7 1 30 131.43 103.87 48.09 o 0 2 30 2291.76 2269.23 118.83 o 1 2 30 14.36 11.18 20.64 o 2 2 30 213.21 210.14 27.07 o 3 2 30 4.39 -1.34 24.76 o 4 2 30 106.31 97.02 30.29 o 5 2 30 91.46 87.38 31.67 o 6 2 30 27.38 23.45 32.49 o 7 2 30 7.62 7.96 38.88 o 1 3 30 9.89 6.89 22.64 o 2 3 30 254.93 259.64 32.71 o 3 3 30 13.59 6.05 26.89 o 4 3 30 285.71 310.73 36.09 o 5 3 30 0.19 -4.97 30.06 o 6 3 30 54.83 50.58 34.47 o 0 4 30 248.05 252.48 53.89 o 1 4 30 23.04 15.64 26.99 o 2 4 30 37.02 35.69 27.82 o 3 4 30 0.08 3.26 28.62 o 4 4 30 9.98 10.01 30.01 o 5 4 30 11.87 3.77 32.74 o 1 5 30 0.01 -1.49 31.47 o 2 5 30 237.29 250.51 41.49 o 3 5 30 2.25 0.96 28.91 o 4 5 30 0.03 -1.86 30.53 o 0 6 30 34.70 38.75 53.91 o 1 6 30 51.43 47.86 38.37 o 2 6 30 22.51 10.56 33.06 o 3 6 30 131.07 143.52 38.58 o 1 1 31 15.34 31.53 22.49 o 2 1 31 209.97 181.82 26.81 o 3 1 31 28.97 25.93 21.77 o 4 1 31 92.61 103.90 25.04 o 5 1 31 363.41 361.78 37.90 o 6 1 31 45.41 31.63 36.14 o 0 2 31 4.17 56.77 32.18 o 1 2 31 119.70 111.96 25.10 o 2 2 31 5.51 11.94 23.51 o 3 2 31 534.85 528.47 38.90 o 4 2 31 18.57 20.23 28.71 o 5 2 31 296.08 327.78 39.30 o 6 2 31 27.85 9.76 33.58 o 1 3 31 16.82 3.69 23.60 o 2 3 31 19.25 22.86 27.21 o 3 3 31 247.41 271.22 36.17 o 4 3 31 6.10 -0.46 31.05 o 5 3 31 6.20 -5.16 31.06 o 6 3 31 20.13 21.40 31.33 o 0 4 31 248.19 246.16 55.50 o 1 4 31 0.10 2.41 27.66 o 2 4 31 2.00 1.12 27.76 o 3 4 31 20.66 16.86 30.95 o 4 4 31 31.42 15.51 31.90 o 5 4 31 82.44 74.39 36.11 o 1 5 31 68.05 39.36 34.89 o 2 5 31 148.27 155.03 40.39 o 3 5 31 127.60 111.05 35.87 o 4 5 31 0.73 2.15 32.45 o 0 6 31 8.52 -1.22 55.61 o 1 6 31 1.61 -0.69 39.16 o 2 6 31 1.57 7.76 38.09 o 0 0 32 1629.30 1538.57 236.50 o 1 0 32 1.31 3.88 26.54 o 2 0 32 6.06 -7.91 31.96 o 3 0 32 176.72 192.24 39.38 o 4 0 32 5.20 7.95 37.08 o 5 0 32 624.15 697.88 59.02 o 6 0 32 5.68 14.55 71.18 o 1 1 32 95.60 107.24 25.93 o 2 1 32 173.36 146.44 26.52 o 3 1 32 53.69 34.56 23.90 o 4 1 32 6.85 11.45 27.98 o 5 1 32 63.80 39.55 32.16 o 6 1 32 35.69 15.45 37.49 o 0 2 32 33.61 20.19 34.50 o 1 2 32 223.31 250.16 29.11 o 2 2 32 0.24 0.65 23.53 o 3 2 32 7.56 14.74 27.57 o 4 2 32 51.72 47.20 29.78 o 5 2 32 129.66 120.99 34.60 o 6 2 32 13.78 19.43 34.57 o 1 3 32 163.25 154.01 31.55 o 2 3 32 46.41 42.93 29.17 o 3 3 32 23.79 27.57 29.54 o 4 3 32 0.43 9.50 30.83 o 5 3 32 132.06 128.47 36.76 o 0 4 32 129.89 161.50 51.12 o 1 4 32 186.80 198.96 34.30 o 2 4 32 15.61 9.80 29.60 o 3 4 32 250.37 295.62 39.12 o 4 4 32 1.48 -2.32 32.89 o 1 5 32 16.85 -1.60 37.91 o 2 5 32 16.49 10.13 36.62 o 3 5 32 20.41 20.39 34.60 o 1 1 33 2.59 6.41 23.80 o 2 1 33 25.70 12.21 23.81 o 3 1 33 159.69 135.25 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