#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:09:23 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180971 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/51/2205196.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205196_Fobs loop_ _publ_author_name 'Baber, R. Angharad' 'Bull, Andrew E. A.' 'Charmant, Jonathan P. H.' 'Norman, Nicholas C.' 'Orpen, A. Guy' _publ_section_title ; N-Imidazole--boron trichloride adduct ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o553 _journal_page_last o554 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 84.484 _cell_angle_beta 81.333 _cell_angle_gamma 71.076 _cell_length_a 6.0390 _cell_length_b 7.2210 _cell_length_c 8.5610 _exptl_crystal_F_000 184.00 _reflns_d_resolution_high 0.7701 _cod_data_source_file ac6154Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' smelly in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 107.44 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 298.26 324.71 6.16 o 2 0 0 1242.96 1289.48 10.94 o 3 0 0 788.35 831.49 9.59 o 4 0 0 193.99 198.91 4.62 o 5 0 0 30.65 35.52 3.85 o 6 0 0 357.10 362.07 10.78 o 7 0 0 440.04 451.50 13.29 o -7 1 0 357.25 372.85 18.42 o -6 1 0 262.98 275.88 10.00 o -5 1 0 377.86 357.10 10.06 o -4 1 0 1084.83 1097.77 16.42 o -3 1 0 0.02 0.11 1.17 o -2 1 0 0.21 -0.85 0.85 o -1 1 0 354.44 359.97 4.16 o 0 1 0 464.83 499.78 3.95 o 1 1 0 217.62 216.03 3.19 o 2 1 0 1446.86 1556.83 12.30 o 3 1 0 965.83 1021.76 10.46 o 4 1 0 296.22 293.35 5.53 o 5 1 0 35.32 30.17 3.29 o 6 1 0 65.95 70.43 4.50 o 7 1 0 225.32 241.84 14.19 o -6 2 0 65.53 66.92 8.60 o -5 2 0 64.92 65.01 5.92 o -4 2 0 142.73 132.66 5.87 o -3 2 0 849.42 839.86 18.41 o -2 2 0 9.78 7.17 1.05 o -1 2 0 2680.22 2770.69 17.29 o 0 2 0 4688.33 4990.42 27.19 o 1 2 0 0.78 0.66 0.74 o 2 2 0 882.73 916.17 12.97 o 3 2 0 2.96 3.61 0.82 o 4 2 0 1048.28 1070.64 11.74 o 5 2 0 210.65 211.82 6.47 o 6 2 0 626.69 645.65 26.17 o 7 2 0 355.26 367.47 12.46 o -6 3 0 8.47 9.86 3.68 o -5 3 0 578.80 568.93 16.13 o -4 3 0 86.85 89.31 5.18 o -3 3 0 254.88 246.78 9.51 o -2 3 0 19.42 24.39 1.83 o -1 3 0 2058.02 2219.92 15.93 o 0 3 0 589.35 590.76 6.39 o 1 3 0 1312.32 1366.55 10.44 o 2 3 0 944.40 934.78 10.70 o 3 3 0 49.51 43.93 2.87 o 4 3 0 6.11 6.89 2.22 o 5 3 0 3.38 3.35 2.87 o 6 3 0 57.95 51.54 5.35 o 7 3 0 117.83 123.53 15.56 o -5 4 0 65.71 80.58 12.72 o -4 4 0 62.62 66.93 6.50 o -3 4 0 30.17 33.25 4.30 o -2 4 0 0.97 2.82 1.13 o -1 4 0 915.72 910.85 9.81 o 0 4 0 77.79 68.85 2.95 o 1 4 0 72.95 79.89 4.97 o 2 4 0 99.93 95.56 3.67 o 3 4 0 0.44 -0.37 1.11 o 4 4 0 152.34 151.57 7.34 o 5 4 0 142.62 128.21 6.97 o 6 4 0 560.49 536.65 14.02 o 7 4 0 46.04 38.10 5.26 o -4 5 0 22.00 23.75 5.16 o -3 5 0 23.32 28.41 4.25 o -2 5 0 176.76 171.21 5.80 o -1 5 0 488.73 486.03 8.59 o 0 5 0 1.83 3.69 1.20 o 1 5 0 1592.81 1575.94 13.97 o 2 5 0 266.42 246.66 4.57 o 3 5 0 79.90 74.21 4.18 o 4 5 0 8.24 8.26 2.50 o 5 5 0 87.66 93.73 5.54 o 6 5 0 9.38 11.86 2.82 o 7 5 0 58.10 67.76 9.89 o -4 6 0 32.36 31.75 8.00 o -3 6 0 150.81 153.35 9.56 o -2 6 0 16.20 16.32 3.40 o -1 6 0 108.73 94.80 5.27 o 0 6 0 310.83 293.08 6.26 o 1 6 0 111.94 114.01 6.39 o 2 6 0 111.06 109.32 4.90 o 3 6 0 1.02 2.83 1.61 o 4 6 0 79.98 85.05 8.76 o 5 6 0 55.02 54.20 4.71 o 6 6 0 276.02 281.68 9.85 o 7 6 0 0.15 -0.43 3.09 o -3 7 0 11.74 19.29 4.53 o -2 7 0 229.38 221.58 12.10 o -1 7 0 84.18 86.14 7.88 o 0 7 0 112.65 102.16 6.87 o 1 7 0 592.51 609.82 15.54 o 2 7 0 145.14 145.27 7.65 o 3 7 0 27.48 29.58 3.38 o 4 7 0 18.98 22.92 3.33 o 5 7 0 390.01 390.49 10.63 o 6 7 0 9.98 13.14 3.23 o -1 8 0 7.64 5.94 2.98 o 0 8 0 505.78 584.86 16.61 o 1 8 0 230.65 245.62 29.36 o 2 8 0 101.43 99.96 8.00 o 3 8 0 73.56 72.08 5.39 o 4 8 0 80.02 80.91 5.88 o 5 8 0 37.30 47.07 4.89 o 1 9 0 133.77 141.38 9.84 o 2 9 0 7.38 18.77 4.09 o 3 9 0 0.56 1.74 2.87 o 4 9 0 75.72 89.71 6.52 o -3 -9 1 11.80 10.72 3.58 o -2 -9 1 42.62 51.81 6.52 o -1 -9 1 104.57 118.89 9.64 o -5 -8 1 257.62 292.07 13.73 o -4 -8 1 637.06 632.88 13.81 o -3 -8 1 95.54 112.88 8.72 o -2 -8 1 144.19 173.52 10.20 o -1 -8 1 153.11 152.47 9.62 o 0 -8 1 171.03 188.00 10.07 o 1 -8 1 69.56 78.25 5.84 o -6 -7 1 30.94 42.63 5.88 o -5 -7 1 390.38 410.68 11.07 o -4 -7 1 20.12 22.61 3.36 o -3 -7 1 74.83 74.93 5.10 o -2 -7 1 436.83 435.03 9.79 o -1 -7 1 72.65 71.38 6.52 o 0 -7 1 0.13 -0.58 1.53 o 1 -7 1 3.33 4.29 2.10 o 2 -7 1 0.61 3.68 2.75 o 3 -7 1 0.55 2.21 4.20 o -7 -6 1 71.06 65.49 5.75 o -6 -6 1 163.42 173.39 13.47 o -5 -6 1 255.28 239.11 8.08 o -4 -6 1 84.76 84.31 7.61 o -3 -6 1 272.39 270.79 7.52 o -2 -6 1 0.00 1.51 1.44 o -1 -6 1 390.47 378.17 6.67 o 0 -6 1 200.17 179.33 7.27 o 1 -6 1 1102.80 1021.43 29.84 o 2 -6 1 583.60 561.52 11.77 o 3 -6 1 14.45 10.68 3.42 o 4 -6 1 193.50 192.52 11.39 o -7 -5 1 90.00 81.70 7.52 o -6 -5 1 222.19 219.89 7.97 o -5 -5 1 874.26 868.47 14.80 o -4 -5 1 110.37 102.81 8.56 o -3 -5 1 1534.18 1463.84 17.45 o -2 -5 1 263.38 246.30 6.34 o -1 -5 1 272.60 264.76 7.30 o 0 -5 1 0.79 1.30 0.98 o 1 -5 1 57.23 49.42 4.38 o 2 -5 1 189.73 168.38 8.12 o 3 -5 1 325.48 297.40 11.03 o 4 -5 1 127.38 118.10 8.76 o -7 -4 1 99.84 92.02 7.88 o -6 -4 1 12.61 11.74 2.70 o -5 -4 1 162.44 153.70 5.89 o -4 -4 1 9.95 8.02 1.98 o -3 -4 1 19.49 19.62 2.33 o -2 -4 1 184.90 191.48 3.21 o -1 -4 1 22.01 25.09 1.89 o 0 -4 1 58.09 58.14 2.80 o 1 -4 1 1127.37 1083.80 10.45 o 2 -4 1 292.88 277.18 7.06 o 3 -4 1 115.75 105.97 4.94 o 4 -4 1 169.91 139.94 13.97 o 5 -4 1 19.09 13.33 3.72 o -7 -3 1 53.67 61.23 12.18 o -6 -3 1 826.17 840.08 17.92 o -5 -3 1 88.37 89.68 4.77 o -4 -3 1 620.21 628.87 10.79 o -3 -3 1 2247.65 2273.55 21.01 o -2 -3 1 1.52 2.54 1.12 o -1 -3 1 612.18 631.86 6.33 o 0 -3 1 1078.39 1118.26 9.79 o 1 -3 1 510.83 458.31 9.82 o 2 -3 1 100.24 102.39 3.01 o 3 -3 1 1309.22 1291.47 14.01 o 4 -3 1 185.32 185.25 15.85 o 5 -3 1 1.17 2.32 2.66 o 6 -3 1 75.91 76.45 7.74 o -7 -2 1 35.58 29.56 6.80 o -6 -2 1 196.65 203.79 22.01 o -5 -2 1 254.11 247.11 5.30 o -4 -2 1 1126.22 1120.66 12.85 o -3 -2 1 391.46 402.91 5.24 o -2 -2 1 328.05 364.79 4.00 o -1 -2 1 85.45 80.73 2.66 o 0 -2 1 487.78 497.48 4.94 o 1 -2 1 414.44 414.29 4.54 o 2 -2 1 723.81 759.26 9.42 o 3 -2 1 45.18 49.82 2.74 o 4 -2 1 169.61 167.59 5.92 o 5 -2 1 0.27 0.51 2.35 o 6 -2 1 9.91 9.62 3.59 o -7 -1 1 101.33 109.93 11.43 o -6 -1 1 372.75 374.68 10.67 o -5 -1 1 1.54 2.75 1.50 o -4 -1 1 247.70 228.92 4.55 o -3 -1 1 465.45 450.09 5.73 o -2 -1 1 2.89 1.43 0.64 o -1 -1 1 904.52 967.64 6.94 o 0 -1 1 496.61 548.61 4.31 o 1 -1 1 2374.79 2529.75 15.26 o 2 -1 1 1729.26 1837.36 12.98 o 3 -1 1 1610.44 1598.86 17.97 o 4 -1 1 112.45 108.89 10.03 o 5 -1 1 13.57 14.39 3.45 o 6 -1 1 5.28 9.33 3.86 o 7 -1 1 111.30 122.77 20.24 o -7 0 1 182.91 204.27 14.68 o -6 0 1 38.30 38.58 4.65 o -5 0 1 555.42 530.54 12.01 o -4 0 1 1252.60 1228.99 17.30 o -3 0 1 133.85 127.78 8.77 o -2 0 1 1866.02 1966.84 14.69 o -1 0 1 481.21 500.80 7.10 o 0 0 1 15.67 15.63 0.63 o 1 0 1 1313.28 1399.70 12.11 o 2 0 1 1875.18 2005.46 18.20 o 3 0 1 292.45 284.63 6.36 o 4 0 1 32.57 33.03 2.55 o 5 0 1 149.27 153.91 5.09 o 6 0 1 49.00 59.98 5.31 o 7 0 1 132.44 135.30 14.68 o -6 1 1 1.88 -0.28 5.10 o -5 1 1 154.92 152.15 8.07 o -4 1 1 26.16 33.44 3.64 o -3 1 1 317.48 314.04 6.42 o -2 1 1 16.68 17.79 4.03 o -1 1 1 1127.92 1215.01 9.71 o 0 1 1 135.32 154.04 2.11 o 1 1 1 1051.25 1146.03 10.17 o 2 1 1 1389.60 1542.36 14.59 o 3 1 1 1070.99 1098.58 13.29 o 4 1 1 32.05 41.03 3.26 o 5 1 1 271.22 263.59 5.62 o 6 1 1 347.33 359.81 8.53 o 7 1 1 182.38 215.82 13.21 o -6 2 1 32.88 36.68 4.93 o -5 2 1 481.04 458.14 12.21 o -4 2 1 365.06 347.66 9.55 o -3 2 1 88.72 86.48 4.72 o -2 2 1 429.82 411.20 12.85 o -1 2 1 1.67 1.55 0.70 o 0 2 1 1091.64 1158.38 8.83 o 1 2 1 617.96 662.21 5.83 o 2 2 1 3916.64 3995.35 30.68 o 3 2 1 117.70 126.01 2.92 o 4 2 1 322.04 309.20 5.97 o 5 2 1 353.12 352.89 7.24 o 6 2 1 19.03 17.02 2.67 o 7 2 1 53.11 46.58 5.50 o -6 3 1 0.00 2.10 2.85 o -5 3 1 199.61 206.19 7.35 o -4 3 1 16.74 16.32 2.54 o -3 3 1 372.27 353.08 9.12 o -2 3 1 445.16 430.01 6.13 o -1 3 1 7.62 10.77 1.27 o 0 3 1 268.69 292.43 4.53 o 1 3 1 262.84 284.56 4.18 o 2 3 1 643.42 661.52 6.57 o 3 3 1 9.63 5.53 0.89 o 4 3 1 13.59 20.44 1.61 o 5 3 1 11.73 10.02 5.00 o 6 3 1 415.41 414.97 11.85 o 7 3 1 10.20 9.69 2.97 o -5 4 1 239.73 248.49 11.24 o -4 4 1 150.02 136.16 8.55 o -3 4 1 436.23 426.93 9.20 o -2 4 1 81.17 73.00 4.91 o -1 4 1 91.83 86.47 3.16 o 0 4 1 107.95 110.00 3.21 o 1 4 1 1060.40 1039.88 10.00 o 2 4 1 2723.69 2844.48 19.24 o 3 4 1 26.95 23.87 1.98 o 4 4 1 2086.76 2132.74 27.07 o 5 4 1 122.54 119.15 5.48 o 6 4 1 201.97 204.67 8.75 o 7 4 1 36.31 39.26 7.06 o -4 5 1 81.69 114.89 8.66 o -3 5 1 581.03 555.30 15.08 o -2 5 1 754.83 727.19 11.95 o -1 5 1 221.22 213.42 5.08 o 0 5 1 46.18 45.15 2.82 o 1 5 1 14.69 17.25 2.16 o 2 5 1 3.51 4.26 1.55 o 3 5 1 253.08 220.81 8.09 o 4 5 1 187.21 168.98 5.80 o 5 5 1 194.25 185.18 6.58 o 6 5 1 9.09 13.18 3.41 o 7 5 1 103.03 105.47 11.03 o -3 6 1 19.65 12.12 3.66 o -2 6 1 0.60 1.73 2.18 o -1 6 1 71.48 71.43 3.72 o 0 6 1 208.89 198.14 5.20 o 1 6 1 1509.59 1446.75 19.23 o 2 6 1 359.36 361.98 6.51 o 3 6 1 376.86 376.38 8.73 o 4 6 1 731.21 707.26 12.73 o 5 6 1 0.84 1.80 1.84 o 6 6 1 211.48 201.29 7.87 o 7 6 1 169.39 148.67 9.94 o -2 7 1 22.21 16.26 10.98 o -1 7 1 133.60 131.17 8.14 o 0 7 1 0.03 1.81 1.78 o 1 7 1 278.67 294.92 8.14 o 2 7 1 11.77 13.19 2.43 o 3 7 1 1453.83 1439.50 19.38 o 4 7 1 266.00 254.47 8.12 o 5 7 1 1.75 4.17 2.20 o 6 7 1 133.84 135.07 7.53 o -1 8 1 66.05 76.83 7.18 o 0 8 1 117.94 124.51 6.55 o 1 8 1 298.04 327.51 11.93 o 2 8 1 34.40 38.79 4.02 o 3 8 1 72.25 71.65 5.34 o 4 8 1 6.49 10.84 2.77 o 5 8 1 3.33 3.98 2.65 o 6 8 1 1.28 4.08 2.58 o 1 9 1 142.78 182.01 10.59 o 2 9 1 134.13 152.81 14.08 o 3 9 1 553.66 548.97 28.05 o 4 9 1 67.09 70.04 7.61 o -2 -9 2 216.14 238.04 12.37 o -5 -8 2 149.13 148.25 8.04 o -4 -8 2 29.67 30.84 5.23 o -3 -8 2 344.82 362.32 13.73 o -2 -8 2 263.67 267.98 11.59 o -1 -8 2 0.75 0.99 2.34 o 0 -8 2 87.75 97.61 8.34 o 1 -8 2 23.28 23.41 3.42 o -6 -7 2 0.17 2.53 2.22 o -5 -7 2 62.34 63.06 5.37 o -4 -7 2 0.66 -1.03 2.05 o -3 -7 2 9.08 12.13 2.54 o -2 -7 2 125.32 128.39 8.52 o -1 -7 2 61.80 64.53 9.08 o 0 -7 2 2.69 2.62 1.89 o 1 -7 2 1.16 3.01 1.97 o 2 -7 2 169.01 189.30 8.11 o -6 -6 2 0.00 0.38 1.94 o -5 -6 2 79.52 85.75 5.83 o -4 -6 2 12.52 13.32 2.70 o -3 -6 2 837.12 810.79 13.55 o -2 -6 2 331.80 328.92 7.94 o -1 -6 2 318.92 313.32 7.52 o 0 -6 2 384.63 376.75 8.85 o 1 -6 2 6.06 5.08 1.88 o 2 -6 2 5.66 9.55 2.41 o 3 -6 2 17.08 15.30 6.53 o -7 -5 2 335.51 342.31 29.18 o -6 -5 2 0.86 2.55 1.76 o -5 -5 2 43.94 50.29 15.48 o -4 -5 2 41.04 48.91 4.11 o -3 -5 2 55.52 56.70 3.90 o -2 -5 2 374.31 358.65 8.42 o -1 -5 2 138.93 134.34 4.17 o 0 -5 2 379.67 346.88 21.78 o 1 -5 2 0.82 1.34 1.48 o 2 -5 2 68.14 61.34 4.50 o 3 -5 2 94.72 107.95 6.01 o 4 -5 2 302.00 325.11 12.62 o -7 -4 2 8.62 2.52 3.68 o -6 -4 2 17.42 11.04 3.25 o -5 -4 2 2.07 3.29 1.83 o -4 -4 2 385.98 377.00 14.31 o -3 -4 2 1095.78 1044.90 14.04 o -2 -4 2 266.59 258.65 4.28 o -1 -4 2 622.78 608.43 7.20 o 0 -4 2 1033.64 1052.08 9.83 o 1 -4 2 250.73 247.54 6.38 o 2 -4 2 2.84 5.30 1.67 o 3 -4 2 407.78 395.50 9.20 o 4 -4 2 683.45 659.12 28.99 o 5 -4 2 38.59 45.78 5.93 o -7 -3 2 109.90 108.37 12.12 o -6 -3 2 7.34 6.82 2.82 o -5 -3 2 139.80 140.01 5.71 o -4 -3 2 418.58 393.62 7.80 o -3 -3 2 300.32 297.02 4.53 o -2 -3 2 551.35 553.13 6.19 o -1 -3 2 1778.69 1791.02 13.18 o 0 -3 2 993.65 1011.09 8.72 o 1 -3 2 12.79 19.40 2.08 o 2 -3 2 83.67 93.31 2.42 o 3 -3 2 174.97 153.39 5.32 o 4 -3 2 13.53 15.10 3.46 o 5 -3 2 107.28 126.63 8.70 o 6 -3 2 3.90 1.47 3.07 o -7 -2 2 19.37 19.99 5.61 o -6 -2 2 0.58 3.92 3.25 o -5 -2 2 0.84 0.56 1.57 o -4 -2 2 652.42 650.60 7.53 o -3 -2 2 1048.73 1076.96 9.13 o -2 -2 2 0.50 1.58 0.67 o -1 -2 2 680.09 707.57 5.85 o 0 -2 2 17.88 15.25 1.37 o 1 -2 2 323.79 325.11 5.84 o 2 -2 2 21.23 14.81 1.18 o 3 -2 2 2538.10 2607.28 19.33 o 4 -2 2 672.30 624.72 14.25 o 5 -2 2 674.55 648.79 16.06 o 6 -2 2 341.59 347.18 12.86 o -7 -1 2 16.90 26.04 6.70 o -6 -1 2 75.85 84.47 9.68 o -5 -1 2 9.72 14.53 2.67 o -4 -1 2 1043.74 1080.28 12.23 o -3 -1 2 376.16 376.52 6.05 o -2 -1 2 477.66 473.33 5.87 o -1 -1 2 11543.67 11437.12 128.10 o 0 -1 2 0.03 0.14 0.54 o 1 -1 2 599.75 627.15 5.38 o 2 -1 2 22.81 29.96 1.52 o 3 -1 2 212.03 209.29 3.87 o 4 -1 2 2.16 2.92 1.03 o 5 -1 2 479.99 478.65 9.60 o 6 -1 2 383.02 366.66 12.48 o 7 -1 2 1.64 1.22 3.08 o -7 0 2 16.79 5.62 4.72 o -6 0 2 87.31 91.35 6.75 o -5 0 2 135.78 131.33 6.82 o -4 0 2 18.34 19.72 2.88 o -3 0 2 87.95 92.84 4.64 o -2 0 2 62.36 61.04 1.98 o -1 0 2 218.14 216.65 3.08 o 0 0 2 1695.93 1737.84 10.81 o 1 0 2 290.53 315.31 4.20 o 2 0 2 972.97 1060.46 11.80 o 3 0 2 1282.70 1374.57 15.86 o 4 0 2 3.00 1.57 1.44 o 5 0 2 339.31 327.95 8.39 o 6 0 2 107.48 109.33 5.25 o 7 0 2 86.23 111.54 10.96 o -6 1 2 151.18 154.38 8.57 o -5 1 2 100.17 104.54 6.63 o -4 1 2 921.71 918.72 15.90 o -3 1 2 49.70 47.15 3.76 o -2 1 2 2513.17 2448.37 24.15 o -1 1 2 2718.02 2856.66 25.29 o 0 1 2 1111.27 1200.59 15.39 o 1 1 2 1272.86 1338.78 13.00 o 2 1 2 465.01 481.20 8.54 o 3 1 2 1475.31 1665.94 17.95 o 4 1 2 871.89 873.16 15.39 o 5 1 2 949.51 973.93 15.71 o 6 1 2 46.88 59.36 4.19 o 7 1 2 130.69 123.49 7.71 o -6 2 2 218.22 237.18 10.03 o -5 2 2 23.32 24.89 4.03 o -4 2 2 93.27 83.86 5.77 o -3 2 2 53.90 53.58 6.19 o -2 2 2 885.99 894.46 13.56 o -1 2 2 7.35 8.02 1.11 o 0 2 2 1369.26 1424.41 10.65 o 1 2 2 683.33 748.98 7.22 o 2 2 2 33.42 31.14 1.63 o 3 2 2 118.85 131.11 4.23 o 4 2 2 45.35 41.26 3.10 o 5 2 2 11.71 15.25 2.09 o 6 2 2 182.38 187.65 13.69 o 7 2 2 2.86 2.90 2.60 o -5 3 2 122.45 115.83 6.47 o -4 3 2 0.02 0.52 1.69 o -3 3 2 129.88 114.37 5.09 o -2 3 2 1617.95 1671.97 13.75 o -1 3 2 7.54 4.37 1.03 o 0 3 2 77.20 72.46 2.46 o 1 3 2 11.51 15.44 1.85 o 2 3 2 184.18 161.13 3.22 o 3 3 2 0.18 1.23 0.90 o 4 3 2 1333.38 1306.61 14.02 o 5 3 2 666.78 684.63 10.48 o 6 3 2 101.76 92.44 11.11 o 7 3 2 203.10 229.06 13.57 o -5 4 2 51.34 52.88 6.31 o -4 4 2 3.10 0.04 1.73 o -3 4 2 899.25 854.18 13.68 o -2 4 2 293.39 288.13 7.22 o -1 4 2 186.92 184.75 4.90 o 0 4 2 2522.63 2600.21 19.25 o 1 4 2 6.45 3.25 0.99 o 2 4 2 109.61 107.80 3.05 o 3 4 2 282.01 300.27 4.94 o 4 4 2 239.78 232.52 6.26 o 5 4 2 37.35 33.15 4.05 o 6 4 2 407.88 396.98 12.15 o 7 4 2 93.35 102.71 7.84 o -4 5 2 47.29 55.68 8.18 o -3 5 2 8.42 6.45 2.25 o -2 5 2 245.73 233.24 6.93 o -1 5 2 345.03 333.75 6.52 o 0 5 2 131.71 128.70 4.00 o 1 5 2 3.26 5.75 1.40 o 2 5 2 2.73 2.97 1.14 o 3 5 2 345.12 315.21 5.54 o 4 5 2 475.29 471.02 9.53 o 5 5 2 272.15 257.12 7.60 o 6 5 2 14.85 17.55 3.65 o 7 5 2 99.58 97.33 8.10 o -3 6 2 627.59 615.05 17.24 o -2 6 2 6.86 7.55 3.17 o -1 6 2 342.76 356.13 8.71 o 0 6 2 328.68 304.22 14.32 o 1 6 2 26.87 23.98 2.33 o 2 6 2 13.58 12.38 2.52 o 3 6 2 253.97 250.70 8.01 o 4 6 2 806.47 809.52 17.16 o 5 6 2 275.03 255.96 8.06 o 6 6 2 459.02 437.51 11.15 o 7 6 2 129.08 129.45 11.82 o -2 7 2 79.26 88.35 7.79 o -1 7 2 580.27 629.94 21.36 o 0 7 2 130.42 128.44 5.12 o 1 7 2 99.36 94.83 5.90 o 2 7 2 0.28 3.53 1.78 o 3 7 2 33.72 36.58 3.62 o 4 7 2 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0 -3 9 14.29 26.15 4.53 o 1 -3 9 395.26 375.06 14.57 o 2 -3 9 196.22 220.17 11.53 o 3 -3 9 91.92 107.58 9.14 o -3 -2 9 79.98 97.43 12.47 o -2 -2 9 47.40 48.74 9.25 o -1 -2 9 146.49 138.72 8.44 o 0 -2 9 7.66 11.44 4.18 o 1 -2 9 197.57 217.80 11.34 o 2 -2 9 71.64 79.37 7.30 o 3 -2 9 49.13 35.58 7.34 o -3 -1 9 169.46 181.21 9.83 o -2 -1 9 139.35 137.14 8.28 o -1 -1 9 73.90 75.46 5.19 o 0 -1 9 325.79 321.50 12.21 o 1 -1 9 636.32 623.93 21.80 o 2 -1 9 14.02 12.50 4.55 o 3 -1 9 232.64 243.98 14.58 o 4 -1 9 71.01 79.04 10.61 o -3 0 9 77.79 66.92 6.72 o -2 0 9 4.31 7.42 3.38 o -1 0 9 3.71 1.85 2.25 o 0 0 9 15.60 15.98 3.45 o 1 0 9 0.13 0.26 2.08 o 2 0 9 235.89 207.19 12.71 o 3 0 9 10.05 14.40 4.45 o 4 0 9 3.18 7.85 4.50 o 5 0 9 18.07 16.49 6.48 o -3 1 9 1.46 5.52 3.17 o -2 1 9 3.55 3.07 4.34 o -1 1 9 33.92 32.58 4.44 o 0 1 9 436.42 434.40 12.67 o 1 1 9 333.41 326.88 22.70 o 2 1 9 285.19 272.92 9.51 o 3 1 9 147.67 153.24 12.51 o 4 1 9 17.77 12.21 4.82 o 5 1 9 30.68 45.32 8.00 o -2 2 9 23.54 26.89 4.67 o -1 2 9 64.41 63.48 7.90 o 0 2 9 52.76 64.04 6.69 o 1 2 9 133.10 129.65 7.85 o 2 2 9 542.73 539.61 13.99 o 3 2 9 109.57 107.75 7.25 o 4 2 9 5.91 12.47 5.38 o 5 2 9 17.44 10.59 5.21 o -2 3 9 52.19 49.18 5.97 o -1 3 9 75.76 84.06 7.70 o 0 3 9 212.48 199.09 17.41 o 1 3 9 113.29 114.05 7.85 o 2 3 9 12.96 17.56 3.56 o 3 3 9 149.61 152.51 8.56 o 4 3 9 4.38 8.73 4.26 o 5 3 9 1.45 6.12 2.75 o -1 4 9 93.23 91.62 7.92 o 0 4 9 133.08 141.59 9.53 o 1 4 9 390.82 371.38 12.69 o 2 4 9 518.70 502.80 14.51 o 3 4 9 48.71 51.43 5.74 o 4 4 9 13.14 22.59 7.28 o 5 4 9 7.23 7.21 3.27 o 0 5 9 158.41 178.10 10.77 o 1 5 9 31.71 31.80 5.25 o 2 5 9 35.40 40.98 4.81 o 3 5 9 64.54 64.12 5.27 o 4 5 9 4.16 5.01 2.67 o 2 6 9 348.47 361.92 13.52 o 3 6 9 0.00 3.14 2.34 o -1 -3 10 95.69 104.59 8.23 o 0 -3 10 11.03 10.51 3.85 o 1 -3 10 0.21 6.98 3.27 o -1 -2 10 36.37 55.83 6.33 o 0 -2 10 0.00 3.80 2.85 o 1 -2 10 137.14 149.71 9.59 o 2 -2 10 0.12 0.74 3.22 o -2 -1 10 77.20 80.90 14.99 o -1 -1 10 287.33 300.04 17.11 o 0 -1 10 0.01 5.29 3.92 o 1 -1 10 14.20 12.95 4.34 o 2 -1 10 0.22 1.06 3.32 o 3 -1 10 55.90 51.33 8.42 o -2 0 10 29.13 35.66 9.21 o -1 0 10 0.60 5.54 2.71 o 0 0 10 4.97 5.03 2.69 o 1 0 10 45.67 53.33 8.29 o 2 0 10 21.96 20.36 5.82 o 3 0 10 755.89 757.93 26.50 o 4 0 10 87.56 104.35 12.19 o -2 1 10 166.64 197.39 15.44 o -1 1 10 407.48 419.57 13.88 o 0 1 10 4.73 9.20 2.85 o 1 1 10 0.27 1.06 3.54 o 2 1 10 44.95 49.01 8.09 o 3 1 10 230.87 236.88 15.12 o 4 1 10 14.36 15.05 5.65 o -1 2 10 45.02 47.17 6.01 o 0 2 10 62.01 64.63 6.46 o 1 2 10 1.76 3.21 6.11 o 2 2 10 157.43 162.85 18.12 o 3 2 10 384.17 407.99 15.65 o 4 2 10 23.10 20.31 6.53 o -1 3 10 68.07 78.27 12.26 o 0 3 10 13.23 16.81 5.77 o 1 3 10 12.14 9.23 3.93 o 2 3 10 522.81 534.63 15.36 o 3 3 10 294.30 313.61 11.76 o 4 3 10 179.18 208.78 9.88 o 0 4 10 12.86 15.01 4.45 o 1 4 10 3.49 2.49 3.10 o 2 4 10 49.09 49.21 5.98 o 3 4 10 12.97 21.90 4.37 o 1 0 11 282.52 267.89 16.07 o 1 1 11 202.92 194.86 15.55 o 2 1 11 62.24 59.57 9.47 o 1 2 11 17.12 18.76 4.15 o 2 2 11 8.31 10.26 3.22 o