#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/52/2205219.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205219_Fobs loop_ _publ_author_name 'Fu, Yun-Long' 'Xu, Zhi-Wei' 'Ren, Jia-Lin' 'Ng, Seik Weng' _publ_section_title ; catena-Poly[diethylenetriaminium [ferrate(III)-tri-\m-sulfato-\k^6^O:O'] monohydrate] ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m593 _journal_page_last m595 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.264 _cell_angle_gamma 90.000 _cell_length_a 9.1329 _cell_length_b 18.8820 _cell_length_c 8.8856 _exptl_crystal_F_000 964.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file bt6605Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 225.85 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1225.99 1438.66 32.77 o 2 0 0 10040.70 9915.55 174.42 o 3 0 0 50.47 19.13 12.44 o 4 0 0 468.20 366.01 38.07 o 5 0 0 14449.55 14655.83 280.65 o 6 0 0 152.74 187.15 31.04 o 7 0 0 522.33 472.70 69.22 o 8 0 0 990.97 886.23 95.70 o 9 0 0 4653.64 4353.27 217.45 o 10 0 0 154.62 170.93 53.02 o 11 0 0 701.15 772.37 117.28 o 1 1 0 26013.52 27153.80 293.66 o 2 1 0 573.15 465.05 15.27 o 3 1 0 909.30 838.14 23.81 o 4 1 0 6773.49 6101.07 86.12 o 5 1 0 3537.83 3458.22 92.29 o 6 1 0 129.24 135.20 19.20 o 7 1 0 1.94 -9.89 16.50 o 8 1 0 8409.66 7991.76 210.66 o 9 1 0 902.60 976.26 77.59 o 10 1 0 408.26 432.97 62.34 o 11 1 0 8.51 -9.03 55.46 o 0 2 0 51007.24 48284.80 1032.92 o 1 2 0 901.92 972.10 15.84 o 2 2 0 706.29 644.27 22.66 o 3 2 0 318.89 356.53 16.76 o 4 2 0 3942.72 3638.52 60.92 o 5 2 0 8523.84 8586.63 117.45 o 6 2 0 524.38 520.33 34.59 o 7 2 0 7.40 -13.88 13.92 o 8 2 0 3.20 -6.24 22.26 o 9 2 0 1740.80 1850.75 156.33 o 10 2 0 206.78 282.18 69.71 o 11 2 0 373.19 502.48 70.89 o 1 3 0 6698.78 6728.52 73.36 o 2 3 0 131.05 124.34 9.10 o 3 3 0 3104.33 3168.08 50.72 o 4 3 0 341.16 278.56 17.88 o 5 3 0 3054.94 3085.20 59.91 o 6 3 0 3615.98 3019.49 71.79 o 7 3 0 383.52 371.00 38.10 o 8 3 0 747.08 697.66 62.28 o 9 3 0 11.12 13.95 40.69 o 10 3 0 303.20 311.89 53.14 o 11 3 0 165.38 117.91 43.86 o 0 4 0 519.19 404.87 28.50 o 1 4 0 1316.87 1289.54 27.45 o 2 4 0 672.56 685.33 17.68 o 3 4 0 536.99 601.30 17.38 o 4 4 0 7.44 17.64 9.48 o 5 4 0 3151.91 3047.37 67.23 o 6 4 0 5.65 -6.22 11.46 o 7 4 0 109.67 96.13 21.08 o 8 4 0 917.56 761.51 64.52 o 9 4 0 4.35 20.55 23.95 o 10 4 0 2.85 24.83 24.67 o 11 4 0 343.86 373.94 61.49 o 1 5 0 3779.72 3561.99 51.12 o 2 5 0 224.16 278.96 13.95 o 3 5 0 111.05 106.68 10.30 o 4 5 0 389.96 383.52 23.00 o 5 5 0 768.07 745.50 33.50 o 6 5 0 9255.91 9276.30 148.49 o 7 5 0 115.44 152.66 24.04 o 8 5 0 226.41 179.29 37.06 o 9 5 0 110.86 129.42 36.28 o 10 5 0 817.77 820.80 77.68 o 11 5 0 954.73 844.03 85.36 o 0 6 0 128.29 172.82 25.71 o 1 6 0 3196.76 3043.79 45.49 o 2 6 0 5329.61 4907.60 58.83 o 3 6 0 2115.39 1954.17 40.16 o 4 6 0 1584.56 1558.79 34.68 o 5 6 0 2058.33 1894.49 52.40 o 6 6 0 1439.69 1396.34 48.71 o 7 6 0 6214.08 6037.58 155.64 o 8 6 0 1.48 -12.92 17.41 o 9 6 0 103.26 117.59 52.46 o 10 6 0 330.44 371.94 54.51 o 11 6 0 1725.76 1661.91 110.82 o 1 7 0 1269.69 1129.22 26.89 o 2 7 0 1542.00 1379.11 25.76 o 3 7 0 5523.66 5323.29 81.52 o 4 7 0 2779.56 2827.07 50.61 o 5 7 0 4945.30 4945.34 92.62 o 6 7 0 15190.45 14966.85 212.03 o 7 7 0 374.00 386.10 38.09 o 8 7 0 615.22 681.09 54.06 o 9 7 0 26.53 69.87 24.98 o 10 7 0 2177.31 2119.52 211.90 o 0 8 0 447.36 477.10 44.85 o 1 8 0 203.68 233.47 16.61 o 2 8 0 11534.10 11083.82 114.80 o 3 8 0 5353.58 5502.93 70.86 o 4 8 0 1790.87 1729.44 35.64 o 5 8 0 8240.44 8059.02 128.54 o 6 8 0 1307.75 1266.53 47.22 o 7 8 0 11031.59 11429.40 209.65 o 8 8 0 40.35 50.03 22.59 o 9 8 0 79.88 93.66 25.85 o 10 8 0 826.29 864.60 77.15 o 1 9 0 1952.97 1637.07 35.15 o 2 9 0 982.41 1035.71 22.48 o 3 9 0 6811.02 6857.70 82.82 o 4 9 0 2899.23 3121.23 119.70 o 5 9 0 1308.85 1312.32 49.81 o 6 9 0 10603.13 10692.14 166.46 o 7 9 0 0.16 26.12 18.13 o 8 9 0 23.04 50.29 23.76 o 9 9 0 67.31 86.55 26.11 o 10 9 0 1858.56 1797.50 105.28 o 0 10 0 457.72 429.67 46.94 o 1 10 0 304.17 296.38 18.93 o 2 10 0 16911.83 17770.23 190.22 o 3 10 0 5369.68 5316.28 69.59 o 4 10 0 778.04 779.47 28.69 o 5 10 0 1107.10 1007.75 61.86 o 6 10 0 93.97 101.49 19.87 o 7 10 0 1669.97 1707.84 86.81 o 8 10 0 16.12 3.00 27.56 o 9 10 0 3.99 -20.04 24.38 o 10 10 0 32.43 92.50 54.38 o 1 11 0 4800.08 4962.05 89.40 o 2 11 0 706.44 666.04 31.56 o 3 11 0 72.48 78.79 12.71 o 4 11 0 3.50 1.77 11.59 o 5 11 0 506.62 533.15 39.27 o 6 11 0 1349.84 1385.83 60.56 o 7 11 0 136.50 131.22 27.29 o 8 11 0 116.17 134.59 29.77 o 9 11 0 20.00 30.00 22.33 o 10 11 0 661.03 688.72 64.23 o 0 12 0 1967.15 1779.10 99.89 o 1 12 0 603.55 593.05 45.01 o 2 12 0 1251.08 1195.80 59.41 o 3 12 0 96.96 99.43 16.63 o 4 12 0 83.27 62.25 20.28 o 5 12 0 654.19 689.40 44.32 o 6 12 0 59.84 36.56 21.59 o 7 12 0 59.22 68.31 23.66 o 8 12 0 124.67 142.79 30.90 o 9 12 0 655.54 746.04 60.20 o 10 12 0 28.39 27.10 47.99 o 1 13 0 11064.65 11320.92 238.82 o 2 13 0 16.32 35.23 22.68 o 3 13 0 183.77 233.11 27.46 o 4 13 0 2108.25 2127.93 91.03 o 5 13 0 1752.38 1674.60 84.66 o 6 13 0 127.53 107.01 26.26 o 7 13 0 33.02 48.75 21.96 o 8 13 0 538.12 504.39 53.89 o 9 13 0 1.30 3.38 21.89 o 0 14 0 15790.08 16339.70 454.05 o 1 14 0 170.54 136.93 42.47 o 2 14 0 74.34 65.85 26.92 o 3 14 0 1450.19 1357.00 99.12 o 4 14 0 2164.85 2249.90 96.49 o 5 14 0 1138.64 1256.86 76.29 o 6 14 0 72.79 73.24 29.13 o 7 14 0 26.03 4.47 24.32 o 8 14 0 439.80 446.73 59.17 o 9 14 0 2099.89 2026.57 114.39 o 1 15 0 6048.14 5872.76 224.09 o 2 15 0 39.46 29.83 39.12 o 3 15 0 1391.54 1397.21 77.01 o 4 15 0 6982.79 6570.56 182.99 o 5 15 0 819.46 856.98 114.28 o 6 15 0 5.28 37.67 28.96 o 7 15 0 9.96 -1.12 22.96 o 8 15 0 3222.21 3199.83 178.37 o 9 15 0 450.43 461.31 97.38 o 0 16 0 14325.23 13382.31 404.17 o 1 16 0 169.61 216.08 38.64 o 2 16 0 478.42 475.17 39.90 o 3 16 0 49.09 92.69 47.57 o 4 16 0 4499.06 4344.85 145.90 o 5 16 0 4803.94 4830.47 160.37 o 6 16 0 443.11 416.57 56.91 o 7 16 0 1904.88 1926.67 101.50 o 8 16 0 1.72 11.24 36.01 o 1 17 0 3340.20 3406.77 123.03 o 2 17 0 51.74 71.53 23.53 o 3 17 0 1896.78 1839.73 149.45 o 4 17 0 537.23 535.08 60.52 o 5 17 0 3.72 30.43 27.93 o 6 17 0 69.51 143.12 35.38 o 7 17 0 4.66 90.07 32.60 o 8 17 0 3792.86 3884.69 162.14 o 0 18 0 1049.83 1060.45 105.34 o 1 18 0 926.71 893.26 70.60 o 2 18 0 7.49 8.87 25.00 o 3 18 0 1.24 14.75 33.18 o 4 18 0 530.96 629.62 66.37 o 5 18 0 1440.13 1394.92 91.34 o 6 18 0 19.10 76.25 30.25 o 7 18 0 904.13 912.75 83.47 o 1 19 0 18.67 0.39 25.38 o 2 19 0 1443.79 1301.31 128.95 o 3 19 0 575.42 500.97 60.15 o 4 19 0 20.70 32.07 29.60 o 5 19 0 6.89 35.57 50.40 o 6 19 0 198.98 243.43 95.59 o 7 19 0 384.77 334.33 63.37 o 0 20 0 219.92 84.87 48.69 o 1 20 0 186.44 217.37 44.89 o 2 20 0 113.94 149.41 38.73 o 3 20 0 79.56 100.50 33.78 o 4 20 0 310.35 327.36 53.28 o 5 20 0 128.55 201.96 55.39 o 6 20 0 5.14 67.46 38.99 o 1 21 0 8.89 33.61 27.82 o 2 21 0 627.97 554.99 65.94 o 3 21 0 855.04 876.56 78.90 o 4 21 0 413.19 509.44 65.74 o 5 21 0 84.33 131.03 46.07 o 0 22 0 25.12 31.22 39.33 o 1 22 0 70.37 186.68 42.27 o 2 22 0 2057.23 2129.41 112.66 o 3 22 0 83.23 125.58 51.97 o 4 22 0 609.51 653.52 77.56 o 5 22 0 148.96 126.02 63.50 o 1 23 0 1400.16 1386.80 191.08 o 2 23 0 887.32 937.49 93.60 o 3 23 0 3086.28 3126.38 146.58 o 0 24 0 225.94 216.27 80.26 o 1 24 0 103.36 132.25 65.31 o 2 24 0 3361.16 3253.01 210.82 o -11 1 1 412.23 505.50 70.24 o -10 1 1 351.18 413.89 56.38 o -9 1 1 0.74 28.43 17.79 o -8 1 1 3.48 -20.07 13.38 o -7 1 1 2809.40 2603.77 70.53 o -6 1 1 580.21 565.88 36.24 o -5 1 1 11.98 5.10 14.80 o -4 1 1 262.75 220.55 24.98 o -3 1 1 636.85 538.09 35.61 o -2 1 1 3028.12 3624.58 61.78 o 0 1 1 234.50 220.48 12.83 o 1 1 1 4.52 40.42 6.21 o 2 1 1 39662.20 41063.14 519.11 o 3 1 1 911.43 898.89 40.64 o 4 1 1 1273.70 1078.27 58.43 o 5 1 1 1418.12 1470.51 64.90 o 6 1 1 276.12 280.81 38.83 o 7 1 1 444.82 476.53 51.20 o 8 1 1 17.81 22.98 24.60 o 9 1 1 75.78 154.90 37.70 o 10 1 1 881.78 858.85 83.37 o 11 1 1 70.31 69.12 43.62 o -11 2 1 267.63 248.12 54.16 o -10 2 1 28.38 44.00 26.98 o -9 2 1 71.51 76.76 25.74 o -8 2 1 23.91 34.55 17.14 o -7 2 1 555.83 565.99 37.98 o -6 2 1 5700.17 5315.35 98.86 o -5 2 1 254.49 218.57 28.22 o -4 2 1 2855.32 3160.22 70.15 o -3 2 1 5340.31 5186.92 94.62 o -2 2 1 1994.73 2142.13 43.86 o -1 2 1 2.47 -14.29 9.53 o 0 2 1 153.68 112.00 7.58 o 1 2 1 1617.20 2040.26 39.76 o 2 2 1 30172.47 30748.94 395.11 o 3 2 1 0.20 -9.85 7.86 o 4 2 1 1137.17 1237.39 43.47 o 5 2 1 156.74 172.00 39.96 o 6 2 1 3374.66 3227.99 110.27 o 7 2 1 145.19 168.29 35.74 o 8 2 1 400.80 420.65 54.06 o 9 2 1 148.14 162.59 39.73 o 10 2 1 351.80 385.62 67.76 o 11 2 1 880.39 773.66 127.27 o -11 3 1 192.59 219.84 47.94 o -10 3 1 274.87 282.17 46.78 o -9 3 1 2451.54 2339.31 88.69 o -8 3 1 229.34 176.69 26.51 o -7 3 1 5266.15 5430.64 96.75 o -6 3 1 26.95 50.19 12.86 o -5 3 1 2.01 -1.42 9.89 o -4 3 1 252.72 338.36 38.40 o -3 3 1 2237.62 2278.33 51.76 o -1 3 1 208.59 135.97 9.21 o 0 3 1 1974.00 2451.55 32.42 o 2 3 1 14122.83 14616.73 174.65 o 3 3 1 1352.05 1534.40 75.19 o 4 3 1 835.64 810.84 35.84 o 5 3 1 1185.54 1184.89 47.40 o 6 3 1 490.03 519.43 49.27 o 7 3 1 18.61 19.16 27.91 o 8 3 1 493.74 503.10 58.99 o 9 3 1 4.05 -8.60 26.82 o 10 3 1 1048.33 1109.48 129.65 o 11 3 1 488.12 485.41 98.91 o -11 4 1 144.56 158.50 43.00 o -10 4 1 54.74 93.75 31.65 o -9 4 1 359.72 326.55 42.09 o -8 4 1 1019.70 945.37 49.54 o -7 4 1 466.51 410.12 29.26 o -6 4 1 1070.49 1118.70 37.57 o -5 4 1 2.32 12.03 9.84 o -4 4 1 753.71 977.67 37.65 o -2 4 1 422.93 485.87 20.81 o -1 4 1 4889.60 5692.22 72.72 o 0 4 1 1627.23 1749.46 26.66 o 1 4 1 365.13 397.75 13.87 o 2 4 1 1927.70 1745.94 35.84 o 3 4 1 90.00 136.41 13.08 o 4 4 1 259.93 209.91 22.04 o 5 4 1 429.39 423.34 32.10 o 6 4 1 558.73 568.85 40.61 o 7 4 1 0.13 1.92 22.91 o 8 4 1 4833.96 4660.98 154.27 o 9 4 1 339.50 331.71 52.17 o 10 4 1 169.30 166.43 41.05 o 11 4 1 715.93 845.72 117.42 o -11 5 1 6.04 96.61 36.76 o -10 5 1 499.02 582.97 67.94 o -9 5 1 4847.56 4748.72 131.49 o -8 5 1 59.54 47.30 16.95 o -7 5 1 512.07 529.56 32.51 o -6 5 1 467.87 475.04 29.52 o -5 5 1 1942.85 2002.24 51.14 o -4 5 1 93.45 184.35 25.49 o -3 5 1 169.56 144.15 15.80 o -2 5 1 620.85 537.00 19.20 o -1 5 1 201.16 206.69 10.85 o 0 5 1 43410.93 45200.88 487.57 o 1 5 1 8.73 8.58 5.85 o 2 5 1 27.22 8.16 5.59 o 3 5 1 1540.68 1680.88 39.29 o 4 5 1 11.46 2.18 10.55 o 5 5 1 2195.70 2283.88 67.85 o 6 5 1 35.52 31.18 18.42 o 7 5 1 1161.11 1003.01 55.15 o 8 5 1 112.12 115.87 54.94 o 9 5 1 211.26 228.77 54.66 o 10 5 1 7.28 28.86 25.60 o 11 5 1 19.44 62.38 52.81 o -11 6 1 0.80 46.82 31.84 o -10 6 1 20.95 -1.80 27.63 o -9 6 1 26.60 0.67 18.25 o -8 6 1 881.56 826.05 47.17 o -7 6 1 96.84 119.90 19.47 o -6 6 1 2023.21 1818.86 53.80 o -5 6 1 676.97 668.49 30.41 o -4 6 1 57.77 40.08 10.65 o -3 6 1 1852.13 1896.36 34.11 o -2 6 1 1523.22 1704.71 34.90 o -1 6 1 12467.72 12649.91 149.06 o 0 6 1 141.04 177.15 9.87 o 1 6 1 1476.77 1632.95 29.46 o 2 6 1 1176.44 1350.18 29.05 o 3 6 1 896.59 1007.56 30.14 o 4 6 1 601.39 528.11 25.06 o 5 6 1 578.13 559.64 36.15 o 6 6 1 31.79 44.62 17.75 o 7 6 1 209.21 203.79 31.90 o 8 6 1 1667.53 1624.38 151.72 o 9 6 1 218.82 281.23 47.87 o 10 6 1 75.29 58.09 49.04 o -11 7 1 49.78 58.40 46.98 o -10 7 1 797.59 800.54 75.55 o -9 7 1 163.56 232.41 40.43 o -8 7 1 0.06 -0.49 17.44 o -7 7 1 1350.39 1256.07 54.74 o -6 7 1 5.04 17.33 12.36 o -5 7 1 4694.88 4491.94 83.40 o -4 7 1 1063.61 1142.86 26.24 o -3 7 1 4256.38 4198.29 54.18 o -2 7 1 985.37 1122.77 27.57 o -1 7 1 1.88 14.28 7.50 o 0 7 1 6979.75 7312.75 92.46 o 1 7 1 711.98 710.15 19.08 o 2 7 1 2030.49 2069.28 38.24 o 3 7 1 322.02 360.92 20.04 o 4 7 1 198.77 190.25 17.58 o 5 7 1 2515.59 2298.96 142.89 o 6 7 1 30.18 21.86 17.17 o 7 7 1 354.35 358.31 37.76 o 8 7 1 53.47 49.49 22.82 o 9 7 1 1.97 -4.86 22.89 o 10 7 1 2.29 5.33 24.25 o -11 8 1 29.42 -27.10 48.69 o -10 8 1 187.51 196.62 35.56 o -9 8 1 0.19 2.89 17.34 o -8 8 1 284.51 251.35 30.69 o -7 8 1 56.33 57.84 18.49 o -6 8 1 296.78 319.81 24.20 o -5 8 1 8.33 13.65 14.04 o -4 8 1 1148.04 1220.93 32.36 o -3 8 1 1016.57 1092.14 23.75 o -2 8 1 66.13 79.19 7.74 o -1 8 1 198.41 161.63 14.27 o 0 8 1 1978.09 2331.18 37.85 o 1 8 1 915.17 977.40 36.53 o 2 8 1 16.04 16.67 6.77 o 3 8 1 54.24 43.73 9.24 o 4 8 1 341.47 394.36 21.29 o 5 8 1 0.66 14.88 14.06 o 6 8 1 283.61 261.50 46.16 o 7 8 1 274.29 262.05 34.02 o 8 8 1 208.80 244.45 36.47 o 9 8 1 39.72 50.93 46.31 o 10 8 1 30.74 21.23 26.74 o -10 9 1 21.18 28.54 28.93 o -9 9 1 1383.11 1357.49 62.39 o -8 9 1 55.24 69.31 21.74 o -7 9 1 270.60 318.39 30.92 o -6 9 1 43.24 45.24 15.90 o -5 9 1 221.95 180.79 18.59 o -4 9 1 58.94 62.82 10.49 o -3 9 1 363.02 359.61 16.37 o -2 9 1 2093.18 2166.91 49.92 o -1 9 1 2780.43 2678.51 57.40 o 0 9 1 403.46 551.65 22.31 o 1 9 1 2667.13 2666.68 42.76 o 2 9 1 135.04 156.98 12.15 o 3 9 1 3908.37 3770.28 62.05 o 4 9 1 766.82 774.48 31.19 o 5 9 1 459.18 500.19 30.96 o 6 9 1 6.68 16.46 16.08 o 7 9 1 546.99 581.38 45.07 o 8 9 1 150.54 159.55 31.61 o 9 9 1 1509.64 1476.29 85.70 o 10 9 1 0.77 5.80 37.51 o -10 10 1 630.28 714.57 76.95 o -9 10 1 144.43 154.48 40.08 o -8 10 1 1400.64 1407.27 70.05 o -7 10 1 41.69 55.13 18.59 o -6 10 1 320.07 336.88 30.51 o -5 10 1 637.57 563.63 51.59 o -4 10 1 88.86 68.10 12.98 o -3 10 1 0.88 6.17 7.38 o -2 10 1 0.80 5.91 7.17 o -1 10 1 1225.49 1108.14 37.12 o 0 10 1 8.29 27.26 10.21 o 1 10 1 799.12 955.85 23.25 o 2 10 1 289.08 316.60 16.07 o 3 10 1 204.48 222.59 16.27 o 4 10 1 8364.68 8468.40 115.59 o 5 10 1 331.17 306.30 25.82 o 6 10 1 15.51 14.60 13.87 o 7 10 1 730.19 736.72 43.39 o 8 10 1 1611.28 1654.80 99.82 o 9 10 1 764.60 882.96 78.15 o 10 10 1 115.05 109.81 55.74 o -10 11 1 7.46 79.74 33.35 o -9 11 1 3646.83 3625.07 117.16 o -8 11 1 6.26 2.07 18.25 o -7 11 1 674.38 676.17 43.05 o -6 11 1 42.33 59.15 19.28 o -5 11 1 730.70 769.42 40.99 o -4 11 1 1270.23 1152.89 90.86 o -3 11 1 146.02 159.04 20.27 o -2 11 1 5.67 19.99 9.95 o -1 11 1 644.04 702.32 49.13 o 0 11 1 1573.76 1586.52 63.60 o 1 11 1 2578.11 2686.13 84.41 o 2 11 1 1709.01 1555.47 41.34 o 3 11 1 105.31 102.81 15.95 o 4 11 1 926.30 890.67 44.88 o 5 11 1 1962.46 1996.17 69.77 o 6 11 1 17.01 34.68 20.31 o 7 11 1 207.18 201.44 32.51 o 8 11 1 202.53 259.14 37.06 o 9 11 1 1190.12 1192.34 211.62 o 10 11 1 98.50 97.38 59.45 o -10 12 1 0.32 -3.22 31.38 o -9 12 1 84.65 94.04 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