#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:09:42 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180972 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/52/2205224.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205224_Fobs loop_ _publ_author_name 'Shallard-Brown, Howard A.' 'Watkin, David J.' 'Cowley, Andrew R.' _publ_section_title ; n-Butyl acetate ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o561 _journal_page_last o562 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _audit_creation_date 04-12-09 _audit_creation_method CRYSTALS _cell_angle_alpha 100.7426(13) _cell_angle_beta 96.0038(15) _cell_angle_gamma 99.3371(18) _cell_length_a 4.72720(10) _cell_length_b 7.6955(3) _cell_length_c 10.1387(4) _cod_data_source_file cf6393Isup2.hkl _cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 2 0 0 289.20 302.12 10.48 o 3 0 0 246.30 231.78 4.90 o 4 0 0 154.00 149.36 4.30 o 5 0 0 7.60 8.54 1.70 o -6 1 0 -2.30 7.96 4.70 o -5 1 0 84.00 84.18 3.10 o -4 1 0 3.70 2.27 0.90 o -3 1 0 391.30 366.22 8.10 o -2 1 0 1070.80 1036.80 21.50 o 1 1 0 1306.25 1468.75 30.45 o 2 1 0 97.35 99.80 3.21 o 3 1 0 142.65 138.15 7.29 o 4 1 0 22.60 26.53 1.40 o 5 1 0 93.40 92.63 4.20 o -6 2 0 4.50 1.83 6.20 o -5 2 0 48.70 46.79 2.80 o -4 2 0 117.60 107.51 3.10 o -3 2 0 35.80 57.21 1.40 o -2 2 0 1049.70 1033.34 27.63 o 0 2 0 2216.40 2231.20 54.38 o 1 2 0 79.85 76.77 2.55 o 2 2 0 488.00 490.16 13.34 o 3 2 0 218.35 202.41 6.04 o 4 2 0 116.30 120.65 5.39 o 5 2 0 3.90 2.86 3.50 o -6 3 0 0.80 0.65 6.08 o -5 3 0 66.30 63.21 3.50 o -4 3 0 49.40 45.77 2.30 o -3 3 0 65.65 82.50 2.84 o -2 3 0 143.75 126.07 4.16 o -1 3 0 283.15 300.03 7.08 o 0 3 0 184.00 183.02 4.70 o 1 3 0 47.20 48.10 1.50 o 2 3 0 5.90 3.84 1.36 o 3 3 0 891.55 909.33 26.33 o 4 3 0 -1.00 0.01 0.92 o 5 3 0 8.80 13.38 4.20 o -5 4 0 79.30 66.10 4.90 o -4 4 0 1.40 2.04 2.69 o -3 4 0 65.20 61.34 2.94 o -2 4 0 2444.10 2512.40 55.28 o -1 4 0 44.50 46.11 1.67 o 0 4 0 307.35 317.24 7.98 o 1 4 0 38.60 32.14 1.57 o 2 4 0 2063.75 2015.90 49.81 o 3 4 0 51.85 52.54 2.86 o 4 4 0 49.35 51.45 4.73 o 5 4 0 22.60 25.02 6.10 o -5 5 0 14.00 16.74 3.10 o -4 5 0 12.35 12.98 2.75 o -3 5 0 571.85 560.32 16.41 o -2 5 0 176.25 162.50 5.18 o -1 5 0 185.25 159.80 5.05 o 0 5 0 69.50 82.09 2.65 o 1 5 0 13.30 16.22 1.45 o 2 5 0 396.10 367.41 11.73 o 3 5 0 5.45 3.24 2.72 o 4 5 0 24.80 24.02 5.93 o -5 6 0 4.90 0.11 2.80 o -4 6 0 1.05 0.05 2.33 o -3 6 0 315.90 330.83 16.49 o -2 6 0 39.45 38.94 2.62 o -1 6 0 163.45 160.46 5.55 o 0 6 0 7.75 13.71 1.60 o 1 6 0 551.80 530.31 16.40 o 2 6 0 579.95 535.08 22.90 o 3 6 0 0.65 0.23 5.54 o 4 6 0 29.40 29.84 6.79 o -5 7 0 4.10 4.04 3.50 o -4 7 0 14.10 19.22 2.60 o -3 7 0 10.40 13.48 1.36 o -2 7 0 1.70 0.09 5.24 o -1 7 0 54.25 56.96 3.75 o 0 7 0 45.80 41.03 3.54 o 1 7 0 42.90 38.59 3.50 o 2 7 0 7.50 5.55 3.87 o 3 7 0 5.00 6.65 5.71 o -4 8 0 2.30 2.59 2.50 o -3 8 0 46.70 51.76 3.70 o -2 8 0 29.20 38.63 3.60 o -1 8 0 0.00 0.05 3.41 o 0 8 0 626.75 576.57 31.30 o 1 8 0 14.70 17.35 4.15 o 2 8 0 29.05 37.63 7.21 o -3 9 0 18.70 35.23 5.60 o -2 9 0 22.50 27.22 4.40 o -1 9 0 27.65 30.16 5.89 o 0 9 0 77.40 86.77 9.31 o 1 9 0 45.85 48.57 7.72 o -1 -9 1 7.30 0.02 6.86 o 0 -9 1 104.95 108.53 11.00 o 1 -9 1 5.10 7.24 3.80 o 2 -9 1 26.80 35.61 4.50 o 3 -9 1 20.70 32.63 4.20 o -2 -8 1 15.60 5.37 7.70 o -1 -8 1 299.70 312.21 16.06 o 0 -8 1 40.05 25.76 5.17 o 1 -8 1 6.40 10.19 2.80 o 2 -8 1 33.80 31.26 2.80 o 3 -8 1 8.00 6.53 3.10 o 4 -8 1 14.70 17.90 3.40 o -3 -7 1 9.30 14.47 5.35 o -2 -7 1 0.30 0.43 4.35 o -1 -7 1 171.85 167.27 7.20 o 0 -7 1 3.25 2.85 2.30 o 1 -7 1 79.15 76.11 4.47 o 2 -7 1 484.00 494.90 22.74 o 3 -7 1 61.25 76.83 3.05 o 4 -7 1 70.10 68.10 3.90 o 5 -7 1 5.40 0.00 3.20 o -4 -6 1 6.55 5.15 5.87 o -3 -6 1 20.05 16.25 4.90 o -2 -6 1 273.25 271.08 10.77 o -1 -6 1 653.90 616.28 19.40 o 0 -6 1 2.40 2.38 1.60 o 1 -6 1 434.95 428.37 12.36 o 2 -6 1 0.75 0.85 2.74 o 3 -6 1 60.40 57.01 4.62 o 4 -6 1 55.15 54.09 5.13 o 5 -6 1 -2.00 0.56 2.80 o -4 -5 1 6.60 3.54 4.50 o -3 -5 1 79.15 71.01 5.54 o -2 -5 1 101.50 101.62 4.15 o -1 -5 1 10.10 10.45 1.45 o 0 -5 1 375.15 373.66 9.87 o 1 -5 1 250.45 234.10 7.10 o 2 -5 1 178.80 189.54 4.55 o 3 -5 1 89.80 96.29 3.79 o 4 -5 1 3.90 2.07 2.53 o 5 -5 1 19.50 17.07 2.90 o -5 -4 1 11.20 7.72 6.00 o -4 -4 1 1.65 0.24 5.70 o -3 -4 1 1663.85 1588.50 51.37 o -2 -4 1 312.50 306.63 8.75 o -1 -4 1 1.05 4.87 1.23 o 0 -4 1 501.80 497.92 11.81 o 1 -4 1 1013.00 960.83 25.83 o 2 -4 1 25.95 20.14 1.35 o 3 -4 1 16.15 6.85 1.73 o 4 -4 1 4.90 5.72 2.31 o 5 -4 1 73.30 69.06 4.80 o -5 -3 1 57.30 53.49 6.50 o -4 -3 1 95.80 100.39 4.28 o -3 -3 1 501.90 499.04 13.62 o -2 -3 1 259.05 291.08 5.65 o -1 -3 1 552.85 593.37 13.90 o 0 -3 1 456.80 417.49 11.85 o 1 -3 1 296.45 334.56 8.55 o 2 -3 1 1570.80 1552.35 37.20 o 3 -3 1 45.75 44.94 2.26 o 4 -3 1 534.40 517.26 12.70 o 5 -3 1 11.70 13.65 2.00 o -5 -2 1 -0.60 0.18 2.79 o -4 -2 1 1050.55 1006.39 46.07 o -3 -2 1 307.05 303.61 8.47 o -2 -2 1 0.10 0.01 0.78 o -1 -2 1 1826.35 1765.26 47.20 o 0 -2 1 756.35 853.35 19.45 o 1 -2 1 7183.40 7641.70 464.20 o 2 -2 1 2.70 2.81 1.37 o 3 -2 1 44.45 61.22 2.31 o 4 -2 1 20.70 18.88 1.10 o 5 -2 1 33.90 36.91 2.00 o 6 -2 1 46.10 33.22 7.00 o -5 -1 1 5.90 5.79 1.70 o -4 -1 1 4.80 4.68 0.90 o -3 -1 1 1.50 1.05 0.90 o -2 -1 1 -0.05 1.20 1.06 o -1 -1 1 2703.40 2914.32 98.49 o 1 -1 1 4450.90 5301.86 160.02 o 2 -1 1 366.35 392.07 11.58 o 3 -1 1 876.70 872.82 15.80 o 4 -1 1 97.70 79.63 2.90 o 5 -1 1 5.20 4.40 1.50 o -6 0 1 5.10 5.07 4.30 o -5 0 1 219.20 211.35 6.40 o -4 0 1 131.30 135.62 3.00 o -3 0 1 148.95 135.43 5.25 o -2 0 1 1.90 6.14 1.53 o 1 0 1 2865.15 3391.24 103.36 o 2 0 1 29.25 18.09 1.42 o 3 0 1 164.80 178.56 3.70 o 4 0 1 40.60 40.60 1.80 o 5 0 1 80.80 72.31 3.60 o -6 1 1 56.30 61.84 5.90 o -5 1 1 37.40 34.13 2.00 o -4 1 1 41.70 44.84 1.50 o -3 1 1 0.70 2.00 0.96 o -2 1 1 194.10 191.56 6.03 o 1 1 1 1481.55 1576.30 43.39 o 2 1 1 3021.80 3064.49 79.39 o 3 1 1 5.20 4.63 1.33 o 4 1 1 322.80 320.31 11.62 o 5 1 1 6.80 8.43 3.10 o -6 2 1 140.30 139.75 9.70 o -5 2 1 5.60 4.86 1.10 o -4 2 1 231.30 214.40 5.10 o -3 2 1 2.60 0.54 1.39 o -2 2 1 1237.05 1167.11 27.03 o -1 2 1 9694.70 10338.94 405.00 o 0 2 1 249.30 241.32 5.80 o 1 2 1 1627.50 1501.46 38.04 o 2 2 1 181.70 159.35 4.64 o 3 2 1 818.70 807.25 22.87 o 4 2 1 261.30 270.52 11.20 o 5 2 1 -1.80 0.50 2.90 o -6 3 1 11.40 9.92 4.10 o -5 3 1 8.70 10.70 2.20 o -4 3 1 2.00 1.23 0.90 o -3 3 1 286.70 253.91 10.45 o -2 3 1 125.50 145.14 2.90 o -1 3 1 1374.10 1369.76 28.05 o 0 3 1 445.60 409.41 9.80 o 1 3 1 1825.40 1748.54 37.72 o 2 3 1 0.60 0.13 1.95 o 3 3 1 540.45 530.35 14.92 o 4 3 1 -0.25 3.08 5.31 o 5 3 1 3.00 11.96 4.30 o -5 4 1 34.00 34.52 3.30 o -4 4 1 0.25 3.50 1.71 o -3 4 1 395.60 355.36 10.04 o -2 4 1 1605.75 1620.90 35.27 o -1 4 1 406.00 385.73 9.47 o 0 4 1 95.90 87.41 2.55 o 1 4 1 152.70 139.18 3.96 o 2 4 1 32.25 27.69 2.47 o 3 4 1 3.20 0.00 3.03 o 4 4 1 4.35 2.55 3.79 o -5 5 1 10.70 16.06 2.50 o -4 5 1 -0.05 0.41 1.89 o -3 5 1 256.55 270.76 7.38 o -2 5 1 64.05 66.65 3.00 o -1 5 1 17.45 19.49 1.60 o 0 5 1 93.70 94.27 3.35 o 1 5 1 371.55 378.51 8.28 o 2 5 1 632.75 626.72 21.25 o 3 5 1 4.90 2.82 2.90 o 4 5 1 88.45 95.01 9.40 o -5 6 1 3.00 1.28 2.40 o -4 6 1 290.35 323.68 13.64 o -3 6 1 19.05 16.24 1.70 o -2 6 1 202.75 199.75 7.89 o -1 6 1 0.45 1.12 1.94 o 0 6 1 -2.35 0.46 1.71 o 1 6 1 410.50 415.58 13.35 o 2 6 1 21.00 18.87 3.45 o 3 6 1 16.80 22.90 4.66 o -4 7 1 8.40 6.88 2.60 o -3 7 1 0.60 0.47 2.62 o -2 7 1 5.35 3.16 2.63 o -1 7 1 93.60 95.57 5.57 o 0 7 1 17.65 17.35 3.01 o 1 7 1 827.55 771.87 29.10 o 2 7 1 15.75 16.76 5.87 o 3 7 1 72.40 69.18 10.76 o -4 8 1 32.30 34.43 3.20 o -3 8 1 3.50 5.97 3.30 o -2 8 1 6.10 13.88 3.00 o -1 8 1 1.70 3.10 4.49 o 0 8 1 206.50 181.68 12.59 o 1 8 1 31.25 29.72 5.02 o 2 8 1 8.30 1.82 5.60 o -3 9 1 3.60 0.87 7.80 o -2 9 1 7.10 7.36 4.50 o -1 9 1 127.85 114.41 10.70 o 0 9 1 26.80 34.23 5.52 o 1 9 1 3.30 2.73 4.81 o -1 -9 2 8.70 1.80 8.20 o 0 -9 2 66.70 75.25 5.60 o 1 -9 2 -1.30 0.51 3.30 o 2 -9 2 0.40 0.64 4.05 o 3 -9 2 46.40 41.14 4.70 o -2 -8 2 14.40 14.14 6.24 o -1 -8 2 -1.05 2.39 4.14 o 0 -8 2 18.15 15.49 3.92 o 1 -8 2 21.50 13.60 3.20 o 2 -8 2 7.35 9.74 3.07 o 3 -8 2 11.80 14.98 2.50 o 4 -8 2 0.50 0.65 3.96 o -3 -7 2 5.65 17.72 5.80 o -2 -7 2 51.35 52.77 6.53 o -1 -7 2 259.85 262.79 12.61 o 0 -7 2 2.05 0.10 2.20 o 1 -7 2 312.40 304.02 17.25 o 2 -7 2 15.95 15.34 1.97 o 3 -7 2 46.90 43.19 2.80 o 4 -7 2 19.00 19.13 5.70 o -4 -6 2 18.15 25.79 5.60 o -3 -6 2 13.65 12.34 3.49 o -2 -6 2 303.95 287.43 12.18 o -1 -6 2 14.30 18.25 1.63 o 0 -6 2 2.85 3.01 1.41 o 1 -6 2 178.00 172.82 5.89 o 2 -6 2 199.50 205.72 6.31 o 3 -6 2 76.50 81.93 4.81 o 4 -6 2 11.50 7.32 2.30 o 5 -6 2 11.70 10.13 3.20 o -4 -5 2 128.45 123.76 9.49 o -3 -5 2 4.50 6.04 2.46 o -2 -5 2 1441.85 1379.19 39.34 o -1 -5 2 5.80 8.01 1.36 o 0 -5 2 1594.80 1549.05 42.70 o 1 -5 2 382.45 354.73 11.42 o 2 -5 2 22.25 17.85 1.45 o 3 -5 2 42.60 41.28 3.02 o 4 -5 2 1.15 2.57 2.85 o 5 -5 2 35.40 29.50 3.40 o -5 -4 2 12.20 5.89 5.60 o -4 -4 2 19.25 20.30 2.72 o -3 -4 2 513.45 499.43 13.07 o -2 -4 2 80.50 88.50 2.71 o -1 -4 2 23.85 24.70 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10.30 o 4 -1 2 4.70 1.51 1.10 o 5 -1 2 -0.80 0.03 3.22 o -5 0 2 463.70 420.04 12.40 o -4 0 2 7.05 6.88 2.39 o -3 0 2 4.00 0.01 2.40 o -2 0 2 20.85 12.02 1.49 o -1 0 2 1070.55 1076.42 34.60 o 1 0 2 256.75 199.57 9.79 o 2 0 2 -0.60 4.66 1.17 o 3 0 2 427.20 410.35 8.00 o 4 0 2 76.50 75.17 2.50 o 5 0 2 31.00 42.00 4.00 o -6 1 2 -3.40 2.53 5.60 o -5 1 2 57.10 58.86 2.90 o -4 1 2 2.05 1.18 1.96 o -3 1 2 123.20 155.69 4.82 o -2 1 2 1266.95 1268.06 31.79 o -1 1 2 4081.10 4399.67 100.96 o 0 1 2 2244.80 2593.48 55.65 o 1 1 2 709.90 657.94 27.53 o 2 1 2 2389.10 2437.97 93.83 o 3 1 2 85.55 86.87 3.55 o 4 1 2 15.30 18.33 2.17 o 5 1 2 51.10 43.28 4.60 o -6 2 2 27.90 26.17 6.60 o -5 2 2 47.00 46.18 2.80 o -4 2 2 -1.80 0.07 1.88 o -3 2 2 1.75 0.01 1.66 o -2 2 2 238.95 234.25 5.18 o -1 2 2 10.95 7.01 0.73 o 0 2 2 1028.60 1065.31 23.80 o 1 2 2 907.35 910.62 20.72 o 2 2 2 295.80 331.05 7.26 o 3 2 2 75.85 69.42 3.64 o 4 2 2 16.60 22.70 3.40 o 5 2 2 2.30 4.16 3.20 o -6 3 2 4.90 0.01 4.80 o -5 3 2 10.70 9.45 2.20 o -4 3 2 54.70 53.97 2.00 o -3 3 2 54.50 49.36 1.80 o -2 3 2 5352.10 5300.79 191.58 o -1 3 2 89.50 100.02 2.22 o 0 3 2 1293.75 1295.51 28.57 o 1 3 2 291.70 281.75 6.75 o 2 3 2 646.30 606.77 17.05 o 3 3 2 15.30 16.52 2.06 o 4 3 2 11.45 10.64 3.37 o 5 3 2 22.00 26.20 4.87 o -5 4 2 2.40 2.49 1.80 o -4 4 2 84.75 85.66 4.87 o -3 4 2 711.10 650.88 16.77 o -2 4 2 39.05 41.54 1.40 o -1 4 2 504.25 425.55 11.91 o 0 4 2 15.05 10.78 1.20 o 1 4 2 3.55 2.38 1.20 o 2 4 2 0.35 0.79 2.18 o 3 4 2 117.65 145.64 6.71 o 4 4 2 7.60 4.25 4.67 o -4 5 2 20.90 21.63 2.56 o -3 5 2 736.50 724.79 22.44 o -2 5 2 37.75 37.83 1.91 o -1 5 2 152.70 131.50 4.66 o 0 5 2 601.05 559.57 13.83 o 1 5 2 43.55 45.47 1.92 o 2 5 2 157.25 162.74 6.84 o 3 5 2 6.65 1.62 3.35 o 4 5 2 44.50 39.85 7.34 o -5 6 2 11.80 0.11 7.50 o -4 6 2 43.85 49.74 4.14 o -3 6 2 99.25 112.61 4.89 o -2 6 2 8.40 8.14 1.95 o -1 6 2 0.40 0.13 2.36 o 0 6 2 0.00 0.12 1.82 o 1 6 2 80.65 79.26 3.85 o 2 6 2 2.45 5.70 3.51 o 3 6 2 25.40 16.86 7.20 o -4 7 2 77.30 77.98 4.00 o -3 7 2 0.50 0.78 5.33 o -2 7 2 24.05 20.65 3.21 o -1 7 2 0.50 0.03 3.08 o 0 7 2 550.15 522.57 21.15 o 1 7 2 9.90 10.86 2.97 o 2 7 2 6.80 8.61 4.75 o -4 8 2 4.30 0.89 5.20 o -3 8 2 16.10 15.65 4.20 o -2 8 2 26.60 29.98 4.14 o -1 8 2 37.15 39.43 5.12 o 0 8 2 110.65 98.43 8.96 o 1 8 2 7.40 6.44 5.66 o 2 8 2 3.80 11.46 8.70 o -2 9 2 0.80 0.49 6.03 o -1 9 2 117.90 120.80 11.22 o 0 9 2 90.40 95.31 10.04 o 0 -9 3 4.30 6.37 3.70 o 1 -9 3 3.85 5.55 3.60 o 2 -9 3 19.20 22.51 3.90 o 3 -9 3 117.40 103.88 7.10 o -2 -8 3 -1.10 3.02 5.84 o -1 -8 3 1.40 1.76 5.45 o 0 -8 3 31.40 31.15 4.00 o 1 -8 3 28.10 34.32 3.67 o 2 -8 3 340.25 360.24 21.16 o 3 -8 3 28.50 22.91 3.70 o 4 -8 3 9.90 9.35 4.40 o -3 -7 3 179.15 172.80 13.96 o -2 -7 3 3.85 2.06 5.27 o -1 -7 3 13.35 17.48 2.63 o 0 -7 3 6.30 7.96 1.10 o 1 -7 3 109.10 113.46 5.60 o 2 -7 3 44.75 43.14 3.24 o 3 -7 3 5.20 0.73 2.20 o 4 -7 3 58.30 49.28 4.40 o -4 -6 3 2.95 1.67 3.36 o -3 -6 3 0.05 0.14 3.22 o -2 -6 3 28.50 27.76 2.75 o -1 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