#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/52/2205233.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205233_Fobs loop_ _publ_author_name 'Lin, Zhi-Dong' 'Liu, Li-Ming' 'Lu, Jin-Yu' 'Meng, Xiang-Gao' _publ_section_title ; Diaquabis(propane-1,2-diamine-\k^2^N,N')copper(II) terephthalate dihydrate ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m590 _journal_page_last m592 _journal_volume 61 _journal_year 2005 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 40.9222 _cell_length_b 6.8025 _cell_length_c 15.1512 _exptl_crystal_F_000 1896.00 _reflns_d_resolution_high 0.7503 _[local]_cod_data_source_file ci6501Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CI6501R in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 457.93 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 113789.38 120938.95 1635.36 o 6 0 0 66.68 56.54 4.67 o 8 0 0 686.75 421.32 10.77 o 10 0 0 156.81 187.48 13.46 o 12 0 0 11944.03 11356.17 286.39 o 14 0 0 3140.36 3262.39 106.93 o 16 0 0 11793.98 11494.62 119.64 o 18 0 0 7884.46 8005.76 114.96 o 20 0 0 11825.59 11206.61 57.20 o 22 0 0 2575.63 2407.83 26.98 o 24 0 0 67.97 40.52 7.77 o 26 0 0 6198.70 5919.31 63.67 o 28 0 0 4176.88 4236.20 148.05 o 30 0 0 16487.88 16718.72 121.16 o 32 0 0 14309.80 15012.10 201.90 o 34 0 0 3872.94 3999.04 112.16 o 36 0 0 1891.24 2023.45 86.74 o 38 0 0 557.69 502.50 56.83 o 40 0 0 95.25 91.23 40.38 o 42 0 0 2634.47 2866.93 112.16 o 44 0 0 12.77 10.47 40.38 o 46 0 0 3415.85 3396.34 130.11 o 48 0 0 1.41 43.37 46.36 o 50 0 0 1563.67 1474.59 100.20 o 52 0 0 61.66 80.76 56.83 o 1 1 0 1777.11 1561.01 337.99 o 3 1 0 26864.23 28980.44 180.81 o 5 1 0 22404.06 24689.13 583.51 o 7 1 0 11445.13 11351.34 395.44 o 9 1 0 9757.63 9838.80 325.42 o 11 1 0 51204.45 55677.55 1774.35 o 13 1 0 86.37 94.59 8.32 o 15 1 0 38180.74 41751.40 937.70 o 17 1 0 4485.52 4804.20 116.13 o 19 1 0 5157.24 4564.39 118.94 o 21 1 0 1267.14 1037.02 21.92 o 23 1 0 9703.73 8818.75 151.75 o 25 1 0 4.35 19.25 6.26 o 27 1 0 11192.05 11391.99 668.91 o 29 1 0 23.51 25.23 9.27 o 31 1 0 8210.39 8537.95 80.61 o 33 1 0 822.43 761.77 22.77 o 35 1 0 3869.98 3827.68 51.29 o 37 1 0 338.08 337.70 34.36 o 39 1 0 476.07 447.60 39.08 o 41 1 0 743.03 721.26 47.05 o 43 1 0 123.26 124.61 32.73 o 45 1 0 303.99 317.27 40.70 o 47 1 0 122.86 158.48 37.53 o 49 1 0 148.91 158.53 39.13 o 51 1 0 146.85 166.24 41.68 o 2 2 0 186.11 212.03 11.07 o 4 2 0 10947.13 12153.98 56.67 o 6 2 0 702.19 863.81 15.05 o 8 2 0 4672.51 5063.92 58.07 o 10 2 0 38.55 40.77 7.16 o 12 2 0 975.08 1198.07 24.74 o 14 2 0 6799.02 8027.05 282.57 o 16 2 0 292.40 234.86 31.01 o 18 2 0 19680.92 22208.81 660.18 o 20 2 0 125.24 350.50 19.82 o 22 2 0 259.86 197.19 15.76 o 24 2 0 999.56 1040.74 38.74 o 26 2 0 95.88 60.40 13.86 o 28 2 0 341.82 422.56 31.67 o 30 2 0 752.78 644.88 25.26 o 32 2 0 232.41 179.25 14.72 o 34 2 0 67.18 73.77 12.31 o 36 2 0 69.55 40.46 20.31 o 38 2 0 123.51 104.85 15.60 o 40 2 0 62.95 34.96 13.52 o 42 2 0 301.76 319.53 39.56 o 44 2 0 2.35 16.02 29.38 o 46 2 0 64.54 93.59 35.41 o 48 2 0 9.76 6.73 32.78 o 50 2 0 230.82 217.69 41.20 o 1 3 0 176.39 333.50 23.93 o 3 3 0 3375.89 3899.74 55.33 o 5 3 0 2227.49 2835.38 42.62 o 7 3 0 242.59 302.86 13.78 o 9 3 0 1140.63 1043.95 34.88 o 11 3 0 18514.00 20134.08 214.37 o 13 3 0 1178.05 1220.54 29.06 o 15 3 0 9892.25 9918.68 216.71 o 17 3 0 472.66 416.42 22.76 o 19 3 0 4806.42 5248.05 154.34 o 21 3 0 211.83 193.67 16.59 o 23 3 0 4707.40 4651.34 103.69 o 25 3 0 194.77 178.13 18.33 o 27 3 0 2108.75 1913.35 85.44 o 29 3 0 41.54 57.78 21.51 o 31 3 0 807.13 861.85 30.10 o 33 3 0 277.70 262.60 20.81 o 35 3 0 457.98 516.28 24.65 o 37 3 0 76.71 98.73 16.69 o 39 3 0 503.40 490.59 25.60 o 41 3 0 308.28 305.74 22.47 o 43 3 0 655.95 610.73 32.72 o 45 3 0 391.14 414.64 47.05 o 47 3 0 17.98 32.26 34.36 o 49 3 0 5.63 15.60 33.20 o 2 4 0 2968.30 3312.41 51.22 o 4 4 0 25309.57 24832.81 244.52 o 6 4 0 3973.69 4297.56 48.14 o 8 4 0 24231.16 26551.17 160.13 o 10 4 0 1812.08 2040.03 33.73 o 12 4 0 13618.29 14503.19 275.92 o 14 4 0 1126.49 1113.69 62.06 o 16 4 0 1216.29 1284.79 41.24 o 18 4 0 145.49 235.91 29.91 o 20 4 0 7045.42 6951.62 147.79 o 22 4 0 4223.92 4585.89 156.30 o 24 4 0 321.90 381.94 25.79 o 26 4 0 2512.87 2590.34 53.24 o 28 4 0 837.24 1032.87 50.10 o 30 4 0 1671.67 1688.80 97.21 o 32 4 0 526.00 550.99 28.89 o 34 4 0 2478.89 2230.65 65.84 o 36 4 0 138.40 127.01 18.28 o 38 4 0 1223.36 1278.70 36.61 o 40 4 0 360.88 334.40 24.24 o 42 4 0 1223.27 1198.60 37.62 o 44 4 0 9.63 1.39 16.37 o 46 4 0 356.77 346.60 29.25 o 48 4 0 1.07 -25.78 25.78 o 1 5 0 4665.80 4549.39 97.21 o 3 5 0 5521.84 5680.03 75.34 o 5 5 0 4715.98 4829.27 58.10 o 7 5 0 8972.15 9783.24 80.65 o 9 5 0 2310.57 2457.18 57.10 o 11 5 0 2577.85 2818.19 62.06 o 13 5 0 75.74 83.75 19.54 o 15 5 0 3901.90 3817.96 73.44 o 17 5 0 2.30 15.94 18.30 o 19 5 0 3302.13 3105.13 148.80 o 21 5 0 4.85 46.03 21.51 o 23 5 0 8062.13 8686.21 419.50 o 25 5 0 690.60 685.23 43.20 o 27 5 0 7718.42 8614.24 168.99 o 29 5 0 81.13 71.55 20.79 o 31 5 0 3288.12 3096.67 84.02 o 33 5 0 415.79 378.11 27.16 o 35 5 0 1091.31 997.05 34.46 o 37 5 0 415.36 368.45 25.45 o 39 5 0 369.69 365.83 25.59 o 41 5 0 187.47 205.73 22.89 o 43 5 0 104.21 80.44 20.26 o 45 5 0 39.00 38.88 33.77 o 2 6 0 371.62 405.68 58.33 o 4 6 0 5738.29 5926.10 90.94 o 6 6 0 139.60 121.74 23.78 o 8 6 0 2298.35 2349.69 85.25 o 10 6 0 2743.05 2954.65 68.74 o 12 6 0 121.62 104.16 23.78 o 14 6 0 63.05 96.05 23.78 o 16 6 0 1266.38 1357.68 56.83 o 18 6 0 65.38 69.47 22.98 o 20 6 0 753.65 1117.16 71.79 o 22 6 0 5.47 20.94 35.89 o 24 6 0 600.59 614.32 51.03 o 26 6 0 952.23 977.59 65.45 o 28 6 0 43.13 71.06 21.90 o 30 6 0 110.46 81.16 23.10 o 32 6 0 37.26 26.22 18.79 o 34 6 0 3.77 7.19 18.63 o 36 6 0 439.96 472.75 34.37 o 38 6 0 425.92 415.43 36.24 o 1 7 0 94.47 60.46 16.42 o 3 7 0 29.62 34.67 16.11 o 5 7 0 96.29 83.93 18.54 o 7 7 0 427.43 365.69 26.92 o 9 7 0 17.88 52.08 18.22 o 11 7 0 102.63 93.21 20.28 o 13 7 0 69.66 87.55 20.20 o 15 7 0 0.14 10.31 17.87 o 17 7 0 20.35 77.63 21.66 o 19 7 0 18.44 -1.75 21.66 o 21 7 0 19.59 35.10 23.78 o 23 7 0 211.71 222.87 33.84 o 25 7 0 13.70 -16.60 21.07 o 27 7 0 17.08 20.01 24.83 o 29 7 0 53.49 35.96 22.08 o 31 7 0 9.72 -6.50 21.80 o 6 8 0 189.60 177.95 29.07 o 8 8 0 375.64 370.90 41.13 o 10 8 0 111.33 131.88 28.55 o 12 8 0 982.00 978.62 53.90 o 14 8 0 215.94 318.11 37.01 o 16 8 0 394.50 382.83 40.70 o 18 8 0 38.85 29.16 25.38 o 20 8 0 679.91 712.35 52.34 o 22 8 0 196.85 151.02 33.30 o -51 1 1 15.21 5.23 34.90 o -49 1 1 90.59 99.99 36.97 o -47 1 1 561.55 618.29 52.84 o -45 1 1 3.01 7.02 33.65 o -43 1 1 141.33 205.28 35.95 o -41 1 1 660.72 700.43 67.30 o -39 1 1 1567.72 1575.86 59.19 o -37 1 1 103.54 110.93 19.21 o -35 1 1 171.69 190.02 17.37 o -33 1 1 42.63 25.85 10.25 o -31 1 1 6616.41 6506.44 54.24 o -29 1 1 616.47 528.87 60.17 o -27 1 1 13312.18 12444.65 753.20 o -25 1 1 34.08 17.45 8.20 o -23 1 1 8242.05 6362.46 489.34 o -21 1 1 4685.52 5008.70 83.05 o -19 1 1 17989.02 18805.80 251.36 o -17 1 1 13311.91 14332.32 221.41 o -15 1 1 32202.02 34430.85 562.88 o -13 1 1 40546.34 44142.13 715.97 o -11 1 1 32164.15 31586.55 500.00 o -9 1 1 36.00 36.39 3.23 o -7 1 1 41543.81 45352.89 725.13 o -5 1 1 14105.24 14657.12 281.85 o -3 1 1 242.74 160.86 5.61 o -1 1 1 14303.39 14674.24 125.87 o 1 1 1 19815.71 20582.84 757.50 o 3 1 1 30151.72 38396.78 860.64 o 5 1 1 5986.62 5623.54 1260.62 o 7 1 1 55.90 43.24 4.84 o 9 1 1 610.16 630.58 23.04 o 11 1 1 1260.45 1824.43 48.32 o 13 1 1 331.18 307.95 17.95 o 15 1 1 10036.97 10679.89 248.44 o 17 1 1 10786.12 11979.52 355.24 o 19 1 1 2119.86 2281.60 21.29 o 21 1 1 1272.31 1348.09 26.08 o 23 1 1 1877.13 1544.69 19.14 o 25 1 1 447.01 355.14 11.65 o 27 1 1 12369.13 11070.11 557.60 o 29 1 1 1609.96 1552.67 45.19 o 31 1 1 2954.22 2975.41 77.77 o 33 1 1 2459.30 2241.11 34.39 o 35 1 1 4145.47 4223.96 53.89 o 37 1 1 29.56 29.28 23.78 o 39 1 1 206.11 151.64 29.61 o 41 1 1 9.35 1.69 24.83 o 43 1 1 1346.23 1317.15 62.06 o 45 1 1 185.93 210.04 44.12 o 47 1 1 497.19 525.03 48.11 o 49 1 1 372.25 367.18 45.33 o 51 1 1 63.55 112.66 38.03 o -52 2 1 35.38 26.92 52.34 o -50 2 1 655.45 778.38 63.56 o -48 2 1 0.49 -3.74 33.84 o -46 2 1 3324.39 3497.19 121.89 o -44 2 1 292.71 389.96 42.82 o -42 2 1 4330.58 4192.44 196.66 o -40 2 1 498.27 445.29 36.26 o -38 2 1 2823.08 2554.37 48.01 o -36 2 1 1913.72 1514.66 226.67 o -34 2 1 2741.77 2693.41 40.66 o -32 2 1 11.80 18.19 10.74 o -30 2 1 3942.59 4007.17 114.34 o -28 2 1 1837.09 1984.48 47.55 o -26 2 1 6419.47 6081.86 92.47 o -24 2 1 4798.02 4229.36 81.36 o -22 2 1 325.82 256.89 14.93 o -20 2 1 7837.64 6758.98 107.48 o -18 2 1 5129.29 5104.04 229.56 o -16 2 1 48816.84 54293.02 1280.07 o -14 2 1 23675.88 25043.97 786.46 o -12 2 1 59595.96 65692.85 1913.29 o -10 2 1 5669.45 5249.90 107.93 o -8 2 1 41788.50 45342.61 463.25 o -6 2 1 1864.37 2213.30 24.12 o -4 2 1 48334.79 55527.16 483.70 o -2 2 1 37.13 26.84 7.48 o 0 2 1 22273.54 19603.38 128.62 o 2 2 1 998.66 1066.31 31.41 o 4 2 1 51165.56 56187.22 840.56 o 6 2 1 9980.33 11721.38 163.41 o 8 2 1 38994.92 39616.73 869.33 o 10 2 1 7873.18 8524.82 261.83 o 12 2 1 51202.49 51541.41 1306.11 o 14 2 1 6925.09 6838.10 160.61 o 16 2 1 75555.74 83117.51 2653.83 o 18 2 1 12014.96 13033.57 465.64 o 20 2 1 10823.60 11747.59 396.51 o 22 2 1 5287.37 5714.44 179.77 o 24 2 1 39.35 99.50 13.60 o 26 2 1 1293.12 1273.84 46.26 o 28 2 1 320.77 290.79 20.85 o 30 2 1 877.42 776.53 31.40 o 32 2 1 162.80 187.15 20.22 o 34 2 1 117.55 168.34 28.01 o 36 2 1 239.19 230.17 19.92 o 38 2 1 3645.46 3439.95 133.68 o 40 2 1 634.42 608.63 45.99 o 42 2 1 3153.47 3100.05 145.07 o 44 2 1 0.46 11.96 29.55 o 46 2 1 1827.38 2004.08 139.08 o 48 2 1 17.08 32.90 33.84 o 50 2 1 928.68 927.83 62.15 o -51 3 1 56.54 58.33 55.33 o -49 3 1 140.08 116.71 38.59 o -47 3 1 196.76 227.04 41.68 o -45 3 1 127.75 133.71 26.79 o -43 3 1 288.01 311.22 26.64 o -41 3 1 780.40 709.22 29.47 o -39 3 1 2887.94 2794.80 47.65 o -37 3 1 167.34 201.46 18.98 o -35 3 1 2503.25 2401.15 48.22 o -33 3 1 225.72 275.46 18.71 o -31 3 1 2623.41 2654.33 49.18 o -29 3 1 17.90 15.07 10.58 o -27 3 1 3535.60 3471.45 64.87 o -25 3 1 293.83 263.31 17.47 o -23 3 1 9990.16 10080.79 198.86 o -21 3 1 123.93 190.23 21.66 o -19 3 1 27527.08 28626.51 878.99 o -17 3 1 1338.86 1341.22 32.52 o -15 3 1 50502.30 54385.08 1559.40 o -13 3 1 12530.33 14709.92 73.02 o -11 3 1 50041.89 54274.60 489.37 o -9 3 1 19033.42 21098.11 105.92 o -7 3 1 33473.78 38205.96 306.39 o -5 3 1 19802.30 21871.24 91.81 o -3 3 1 181.51 142.28 13.46 o -1 3 1 32.41 47.97 82.25 o 1 3 1 4201.23 4287.68 73.28 o 3 3 1 856.39 861.47 41.13 o 5 3 1 5349.20 4778.58 60.98 o 7 3 1 1697.65 1639.30 21.51 o 9 3 1 3930.06 3685.80 34.75 o 11 3 1 13914.94 14146.50 337.17 o 13 3 1 32.73 97.47 13.74 o 15 3 1 13684.11 14571.42 404.55 o 17 3 1 295.57 437.64 21.55 o 19 3 1 3702.66 3725.47 67.30 o 21 3 1 7.56 2.41 10.49 o 23 3 1 3615.42 3216.43 175.79 o 25 3 1 165.60 121.43 16.59 o 27 3 1 2801.21 2982.24 73.99 o 29 3 1 1081.44 930.57 34.81 o 31 3 1 2258.98 2351.73 53.05 o 33 3 1 494.90 473.79 30.49 o 35 3 1 5060.13 4734.58 179.46 o 37 3 1 563.13 486.93 27.94 o 39 3 1 1603.26 1412.31 36.58 o 41 3 1 293.28 294.05 22.35 o 43 3 1 1748.96 1680.55 46.14 o 45 3 1 772.22 733.20 55.51 o 47 3 1 733.68 800.15 59.22 o 49 3 1 280.93 321.65 46.53 o -48 4 1 6.59 -2.28 27.93 o -46 4 1 98.12 81.96 26.32 o -44 4 1 48.32 83.09 18.95 o -42 4 1 49.02 45.11 18.26 o -40 4 1 34.04 60.38 17.51 o -38 4 1 181.67 184.44 20.57 o -36 4 1 165.86 164.85 19.10 o -34 4 1 435.06 434.58 24.25 o -32 4 1 638.17 559.26 26.03 o -30 4 1 410.24 358.91 20.74 o -28 4 1 293.14 195.42 17.36 o -26 4 1 252.45 268.85 20.09 o -24 4 1 199.74 258.67 21.15 o -22 4 1 1851.05 2033.10 42.54 o -20 4 1 4209.84 4340.02 101.70 o -18 4 1 530.64 544.35 38.88 o -16 4 1 1690.58 1676.56 45.44 o -14 4 1 150.00 98.66 16.82 o -12 4 1 104.80 137.34 11.63 o -10 4 1 4293.92 4155.60 68.98 o -8 4 1 556.33 489.99 19.55 o -6 4 1 1956.76 1881.78 32.88 o -4 4 1 13589.48 15118.50 88.10 o -2 4 1 347.40 310.63 20.44 o 0 4 1 9336.75 9131.69 119.64 o 2 4 1 57.69 91.23 19.44 o 4 4 1 916.25 789.64 41.87 o 6 4 1 294.38 328.99 14.44 o 8 4 1 4404.38 4578.38 74.69 o 10 4 1 64.38 89.03 8.28 o 12 4 1 2717.36 2817.91 86.56 o 14 4 1 926.90 867.04 73.28 o 16 4 1 683.39 594.46 49.35 o 18 4 1 8.81 24.25 12.59 o 20 4 1 863.44 748.70 29.90 o 22 4 1 148.28 153.39 24.17 o 24 4 1 259.34 245.20 22.02 o 26 4 1 2148.10 2181.15 49.47 o 28 4 1 9.19 2.76 15.54 o 30 4 1 499.57 496.71 30.87 o 32 4 1 9.48 7.59 17.48 o 34 4 1 179.74 195.87 32.14 o 36 4 1 64.95 68.06 28.95 o 38 4 1 57.67 29.79 18.40 o 40 4 1 59.79 62.50 17.98 o 42 4 1 248.16 226.59 22.80 o 44 4 1 0.11 5.45 16.97 o 46 4 1 174.67 140.84 23.99 o 48 4 1 3.66 -23.93 49.35 o -45 5 1 13.38 -10.47 40.38 o -43 5 1 2.88 -9.22 17.16 o -41 5 1 55.92 26.83 17.52 o -39 5 1 323.15 328.41 25.13 o -37 5 1 34.73 42.22 17.48 o -35 5 1 286.16 280.17 23.02 o -33 5 1 22.73 19.23 17.07 o -31 5 1 253.42 221.39 23.02 o -29 5 1 20.53 36.70 16.40 o -27 5 1 326.48 319.98 27.55 o -25 5 1 1152.05 1207.08 45.52 o -23 5 1 266.33 308.59 34.66 o -21 5 1 2674.45 2669.15 110.95 o -19 5 1 4450.03 4759.21 168.95 o -17 5 1 11.95 13.46 25.42 o -15 5 1 207.56 291.63 37.39 o -13 5 1 751.79 737.29 52.34 o -11 5 1 5.44 35.89 23.93 o -9 5 1 144.54 143.17 14.97 o -7 5 1 420.98 401.79 21.78 o -5 5 1 1005.66 1067.87 36.20 o -3 5 1 1064.23 1052.85 49.35 o -1 5 1 1325.38 0.00 4.49 o 1 5 1 117.05 107.08 12.89 o 3 5 1 768.77 804.44 25.82 o 5 5 1 35.57 74.39 10.38 o 7 5 1 895.22 937.80 23.98 o 9 5 1 1015.32 980.45 39.13 o 11 5 1 75.43 66.95 17.88 o 13 5 1 1708.08 1947.57 53.93 o 15 5 1 3575.17 3561.41 71.89 o 17 5 1 5315.18 5218.60 87.75 o 19 5 1 37.08 56.37 20.44 o 21 5 1 42.02 97.90 22.98 o 23 5 1 485.25 534.75 69.54 o 25 5 1 14.45 48.64 22.62 o 27 5 1 1087.44 1066.27 51.22 o 29 5 1 86.52 73.02 21.45 o 31 5 1 548.75 588.97 35.84 o 33 5 1 28.31 43.72 27.25 o 35 5 1 241.15 258.68 25.31 o 37 5 1 11.65 22.33 18.89 o 39 5 1 60.31 68.58 18.96 o 41 5 1 132.31 120.39 21.05 o 43 5 1 31.11 24.49 18.38 o 45 5 1 5.66 13.05 31.97 o -38 6 1 266.86 272.82 32.49 o -36 6 1 54.35 64.16 23.10 o -34 6 1 755.42 720.67 42.01 o -32 6 1 62.85 57.17 22.20 o -30 6 1 1047.92 933.85 43.71 o -28 6 1 377.76 351.59 31.06 o -26 6 1 1702.65 1644.50 51.86 o -24 6 1 1484.31 1578.28 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