#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/52/2205253.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205253_Fobs loop_ _publ_author_name 'Fan, Sai-Rong' 'Zhu, Long-Guan' 'Xiao, Hong-Ping' 'Ng, Seik Weng' _publ_section_title ; Poly[[cis-diaqua(2,2'-bipyridine)copper(II)]-\m-3-carboxylato-4-hydroxybenzenesulfonato] ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m509 _journal_page_last m511 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.940 _cell_angle_gamma 90.000 _cell_length_a 14.2339 _cell_length_b 7.7622 _cell_length_c 17.8010 _exptl_crystal_F_000 964.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file dn6199Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I in space group P 21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 247.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2226.42 2385.33 35.03 o 4 0 0 470.79 519.42 15.88 o 6 0 0 137.68 117.35 9.35 o 8 0 0 484.00 389.93 18.12 o 10 0 0 1383.35 1174.62 51.45 o 12 0 0 922.25 935.43 51.24 o 14 0 0 405.49 400.54 37.42 o 16 0 0 109.87 113.51 25.06 o 1 1 0 27458.14 28139.12 467.00 o 2 1 0 52.68 66.59 3.03 o 3 1 0 2387.58 2523.73 28.12 o 4 1 0 1027.28 1112.54 14.80 o 5 1 0 8272.66 8552.38 74.02 o 6 1 0 58.33 63.40 5.39 o 7 1 0 646.84 565.48 14.32 o 8 1 0 527.40 511.10 17.08 o 9 1 0 79.80 79.68 8.67 o 10 1 0 845.75 837.01 24.84 o 11 1 0 3609.83 3474.66 73.74 o 12 1 0 9.95 4.23 7.75 o 13 1 0 1249.29 1135.10 42.16 o 14 1 0 210.58 241.40 22.20 o 15 1 0 488.55 470.94 29.85 o 16 1 0 42.05 56.22 15.08 o 17 1 0 10.86 26.08 19.69 o 0 2 0 13364.68 13327.10 138.66 o 1 2 0 4188.37 4728.72 46.27 o 2 2 0 30874.39 32545.08 330.35 o 3 2 0 11893.06 12110.12 112.05 o 4 2 0 1589.92 1643.86 22.80 o 5 2 0 326.45 261.38 9.76 o 6 2 0 4216.85 4222.35 43.85 o 7 2 0 4134.39 4169.73 44.87 o 8 2 0 2484.56 2429.74 32.12 o 9 2 0 41.86 47.54 5.55 o 10 2 0 982.21 936.83 32.16 o 11 2 0 47.07 34.64 8.70 o 12 2 0 111.81 99.21 14.87 o 13 2 0 498.07 478.27 29.02 o 14 2 0 175.72 198.91 20.84 o 15 2 0 402.59 397.81 29.06 o 16 2 0 33.33 52.09 15.55 o 1 3 0 309.76 286.25 6.52 o 2 3 0 6918.30 7200.75 70.48 o 3 3 0 712.03 899.54 15.17 o 4 3 0 6202.31 6658.15 68.60 o 5 3 0 3456.87 3711.04 44.51 o 6 3 0 210.61 236.33 9.24 o 7 3 0 604.51 648.94 16.34 o 8 3 0 1971.04 1853.20 27.87 o 9 3 0 3367.58 3376.04 42.61 o 10 3 0 117.92 107.18 8.13 o 11 3 0 103.28 98.68 8.50 o 12 3 0 648.03 683.81 32.21 o 13 3 0 651.88 559.16 30.66 o 14 3 0 439.54 459.53 29.45 o 15 3 0 550.44 569.36 33.91 o 16 3 0 188.59 203.22 24.02 o 0 4 0 980.97 892.89 18.07 o 1 4 0 842.31 806.86 13.52 o 2 4 0 8.87 6.18 2.18 o 3 4 0 8805.55 9036.83 81.88 o 4 4 0 952.83 1017.22 18.28 o 5 4 0 3.07 3.74 3.05 o 6 4 0 21.14 23.84 5.13 o 7 4 0 3111.26 2891.17 40.93 o 8 4 0 468.17 459.50 16.91 o 9 4 0 42.43 55.26 8.92 o 10 4 0 25.35 40.24 7.13 o 11 4 0 681.68 659.43 21.34 o 12 4 0 358.13 328.71 16.90 o 13 4 0 400.66 428.75 27.30 o 14 4 0 17.14 26.73 10.70 o 15 4 0 638.27 624.43 36.05 o 1 5 0 1598.66 1655.66 23.44 o 2 5 0 651.35 534.57 14.93 o 3 5 0 1020.09 1045.78 20.79 o 4 5 0 561.75 476.12 13.83 o 5 5 0 461.32 425.19 14.16 o 6 5 0 260.68 235.02 13.81 o 7 5 0 2707.76 2563.58 46.70 o 8 5 0 2385.48 2204.96 55.81 o 9 5 0 166.93 176.71 20.88 o 10 5 0 601.13 620.22 20.64 o 11 5 0 487.69 469.54 18.80 o 12 5 0 41.54 63.59 9.16 o 13 5 0 130.50 171.59 13.73 o 14 5 0 157.77 211.24 32.99 o 0 6 0 1262.14 1270.64 35.00 o 1 6 0 821.84 865.68 19.98 o 2 6 0 629.98 609.41 24.65 o 3 6 0 2089.18 1782.50 60.10 o 4 6 0 629.95 598.44 16.97 o 5 6 0 217.28 205.87 10.46 o 6 6 0 1631.57 1513.78 28.99 o 7 6 0 216.52 238.34 14.08 o 8 6 0 7.20 4.07 5.15 o 9 6 0 97.48 107.02 11.12 o 10 6 0 246.43 242.15 16.64 o 11 6 0 383.68 350.49 19.83 o 12 6 0 319.51 343.75 21.06 o 13 6 0 169.28 214.87 18.69 o 1 7 0 1694.56 1674.68 31.52 o 2 7 0 653.81 663.40 19.00 o 3 7 0 213.65 198.53 11.14 o 4 7 0 102.36 92.47 10.25 o 5 7 0 5.88 12.35 7.23 o 6 7 0 314.33 311.32 20.51 o 7 7 0 165.88 164.15 23.66 o 8 7 0 464.58 430.58 24.99 o 9 7 0 274.17 337.52 22.92 o 10 7 0 105.20 129.29 24.23 o 11 7 0 670.11 725.52 29.94 o 12 7 0 0.12 -1.52 9.48 o 0 8 0 934.79 919.56 53.41 o 1 8 0 456.86 417.94 26.09 o 2 8 0 448.55 436.39 25.95 o 3 8 0 178.17 187.31 18.89 o 4 8 0 94.82 91.98 14.54 o 5 8 0 135.14 138.60 15.48 o 6 8 0 176.97 188.89 28.81 o 7 8 0 115.43 137.27 15.84 o 8 8 0 142.22 191.89 18.75 o 9 8 0 0.98 9.69 16.19 o 10 8 0 12.62 25.57 18.45 o 1 9 0 83.11 105.62 15.92 o 2 9 0 3.21 13.66 9.53 o 3 9 0 26.69 36.81 14.43 o 4 9 0 363.77 389.31 41.24 o 5 9 0 117.28 110.93 27.63 o 6 9 0 194.32 210.53 35.57 o 0 10 0 1.75 3.81 19.39 o 1 10 0 152.68 134.14 21.57 o 2 10 0 26.36 48.04 20.62 o -17 0 1 715.04 615.30 51.86 o -15 0 1 495.59 506.74 42.38 o -13 0 1 139.55 172.28 26.08 o -11 0 1 350.34 378.96 23.71 o -9 0 1 9219.27 9380.41 142.26 o -7 0 1 384.19 422.84 20.21 o -5 0 1 169.07 122.60 11.28 o -3 0 1 6044.15 6281.55 58.24 o 1 0 1 41006.87 36777.28 679.74 o 3 0 1 3721.69 4421.99 89.70 o 5 0 1 168.01 93.61 11.76 o 7 0 1 573.10 718.82 33.61 o 9 0 1 1155.13 1049.26 46.91 o 11 0 1 138.71 146.30 21.96 o 13 0 1 151.08 206.41 28.97 o 15 0 1 412.21 459.73 42.58 o -17 1 1 15.76 36.83 14.88 o -16 1 1 234.71 274.52 32.37 o -15 1 1 8.86 16.52 10.68 o -14 1 1 1303.58 1231.51 45.10 o -13 1 1 538.87 473.52 26.49 o -12 1 1 245.81 265.25 16.64 o -11 1 1 853.79 804.14 25.33 o -10 1 1 1533.60 1449.78 32.83 o -9 1 1 144.03 155.33 10.85 o -8 1 1 2139.96 2134.71 29.07 o -7 1 1 2.55 7.97 2.46 o -6 1 1 1195.04 1266.87 16.60 o -5 1 1 2168.82 2021.68 26.16 o -4 1 1 643.45 570.50 9.76 o -3 1 1 1375.37 1690.12 18.36 o -2 1 1 1173.71 1098.82 12.32 o -1 1 1 12014.30 12864.36 95.10 o 0 1 1 10.87 2.95 0.92 o 1 1 1 3603.69 3895.30 37.91 o 2 1 1 1336.08 1339.33 19.29 o 3 1 1 144.38 131.48 4.46 o 4 1 1 6196.68 6652.37 58.71 o 5 1 1 87.00 60.20 4.18 o 6 1 1 4103.59 4294.76 63.60 o 7 1 1 252.97 224.35 16.77 o 8 1 1 183.62 131.39 12.43 o 9 1 1 166.15 157.60 14.28 o 10 1 1 1443.37 1357.76 40.89 o 11 1 1 251.87 244.88 19.85 o 12 1 1 1338.58 1211.54 42.75 o 13 1 1 24.28 21.85 10.50 o 14 1 1 661.83 682.25 34.83 o 15 1 1 59.25 88.88 16.33 o 16 1 1 0.39 -6.05 9.96 o -17 2 1 463.82 460.96 48.87 o -16 2 1 21.31 34.89 12.87 o -15 2 1 147.92 186.12 20.73 o -14 2 1 307.13 358.36 26.29 o -13 2 1 233.59 231.67 20.52 o -12 2 1 219.50 238.64 15.76 o -11 2 1 606.59 564.73 18.25 o -10 2 1 32.54 31.20 5.07 o -9 2 1 2917.04 2789.08 35.99 o -8 2 1 114.79 106.55 6.58 o -7 2 1 524.57 486.66 23.54 o -6 2 1 5211.75 5310.59 58.30 o -5 2 1 1709.82 1817.32 30.59 o -4 2 1 1539.89 1662.79 22.69 o -3 2 1 5431.56 5806.26 57.81 o -2 2 1 40205.37 41736.64 366.44 o -1 2 1 3460.05 3786.81 34.28 o 0 2 1 227.64 270.07 5.05 o 1 2 1 10733.92 11405.52 104.78 o 2 2 1 2497.58 2845.13 31.16 o 3 2 1 196.85 197.85 6.41 o 4 2 1 125.53 233.31 7.58 o 5 2 1 83.75 109.75 5.43 o 6 2 1 1869.96 1783.92 24.30 o 7 2 1 959.18 890.70 17.03 o 8 2 1 153.21 116.42 7.39 o 9 2 1 2218.72 2214.63 52.89 o 10 2 1 477.78 447.26 23.76 o 11 2 1 334.71 320.98 21.99 o 12 2 1 949.36 900.71 37.36 o 13 2 1 121.41 118.64 16.27 o 14 2 1 0.14 13.89 11.24 o 15 2 1 924.14 913.40 42.90 o 16 2 1 179.19 232.92 39.90 o -16 3 1 7.81 36.08 21.71 o -15 3 1 80.79 122.02 17.54 o -14 3 1 912.35 908.39 68.98 o -13 3 1 480.45 505.75 27.18 o -12 3 1 642.64 626.12 25.20 o -11 3 1 34.77 45.84 6.47 o -10 3 1 61.03 51.67 6.44 o -9 3 1 2849.37 2813.38 37.39 o -8 3 1 207.34 192.33 9.90 o -7 3 1 649.82 628.68 15.76 o -6 3 1 596.48 589.23 15.69 o -5 3 1 1169.46 1279.31 21.26 o -4 3 1 1947.41 1825.74 50.47 o -3 3 1 5544.57 6076.02 55.06 o -2 3 1 3528.87 3924.44 37.71 o -1 3 1 5974.44 6160.60 54.83 o 0 3 1 18.59 13.37 1.74 o 1 3 1 1457.42 1381.00 18.09 o 2 3 1 27.75 39.89 3.85 o 3 3 1 46.60 38.48 3.55 o 4 3 1 915.41 810.64 15.41 o 5 3 1 2247.96 2257.99 31.41 o 6 3 1 883.64 874.41 21.13 o 7 3 1 431.77 402.33 11.69 o 8 3 1 33.78 41.49 5.49 o 9 3 1 1928.70 1849.65 29.53 o 10 3 1 602.14 523.48 17.89 o 11 3 1 1960.62 1931.74 54.77 o 12 3 1 142.27 134.95 21.13 o 13 3 1 48.74 81.50 15.83 o 14 3 1 468.23 444.15 29.26 o 15 3 1 3.00 17.62 12.03 o 16 3 1 30.98 11.96 18.45 o -16 4 1 184.71 230.53 34.54 o -15 4 1 46.14 77.13 25.52 o -14 4 1 730.96 708.85 35.89 o -13 4 1 91.10 90.26 10.71 o -12 4 1 593.45 596.77 20.86 o -11 4 1 200.21 195.58 12.66 o -10 4 1 1024.92 952.26 21.15 o -9 4 1 894.51 868.12 21.52 o -8 4 1 399.59 361.30 13.28 o -7 4 1 704.39 706.52 17.39 o -6 4 1 4575.07 4418.36 56.65 o -5 4 1 2034.81 1958.45 28.93 o -4 4 1 2777.34 2824.08 40.72 o -3 4 1 17.73 18.12 3.01 o -2 4 1 9422.37 9979.32 86.73 o -1 4 1 798.98 841.04 12.33 o 0 4 1 7473.34 7774.93 63.25 o 1 4 1 51.63 44.38 3.01 o 2 4 1 273.96 245.17 7.59 o 3 4 1 138.53 186.48 7.02 o 4 4 1 2550.84 2366.06 31.72 o 5 4 1 8.46 8.83 3.14 o 6 4 1 889.11 823.17 18.27 o 7 4 1 335.97 271.17 13.91 o 8 4 1 0.79 -3.79 3.79 o 9 4 1 231.54 221.40 12.56 o 10 4 1 189.26 217.31 13.01 o 11 4 1 504.57 485.13 19.89 o 12 4 1 1939.43 1913.39 57.81 o 13 4 1 310.27 349.14 27.01 o 14 4 1 6.24 27.03 10.94 o 15 4 1 114.83 140.15 40.11 o -14 5 1 11.12 14.54 25.36 o -13 5 1 277.03 311.80 20.15 o -12 5 1 523.04 505.39 20.11 o -11 5 1 574.81 536.58 23.54 o -10 5 1 149.25 166.20 16.22 o -9 5 1 24.97 21.01 6.50 o -8 5 1 106.74 99.99 9.62 o -7 5 1 1565.43 1504.17 36.56 o -6 5 1 326.08 306.49 11.76 o -5 5 1 896.22 797.63 39.25 o -4 5 1 1057.10 967.26 19.89 o -3 5 1 1347.70 1392.79 24.37 o -2 5 1 2364.54 2242.48 25.38 o -1 5 1 3528.59 3654.76 48.54 o 0 5 1 58.36 70.49 6.05 o 1 5 1 247.52 212.46 7.87 o 2 5 1 314.75 261.57 12.62 o 3 5 1 236.62 223.94 10.71 o 4 5 1 240.29 297.62 12.78 o 5 5 1 2522.15 2436.80 43.13 o 6 5 1 873.82 726.71 25.89 o 7 5 1 3900.68 3637.73 59.80 o 8 5 1 2.75 -5.03 6.03 o 9 5 1 332.47 314.25 14.65 o 10 5 1 0.49 11.20 5.89 o 11 5 1 910.67 918.44 26.30 o 12 5 1 29.30 45.87 8.05 o 13 5 1 21.87 36.55 18.66 o 14 5 1 5.78 37.96 33.56 o -14 6 1 327.54 345.70 40.00 o -13 6 1 4.64 22.90 9.97 o -12 6 1 204.64 239.85 18.13 o -11 6 1 53.64 79.22 11.45 o -10 6 1 91.21 119.46 21.96 o -9 6 1 12.00 26.90 10.26 o -8 6 1 82.32 70.93 11.72 o -7 6 1 64.26 61.11 10.94 o -6 6 1 639.13 604.21 37.05 o -5 6 1 1678.26 1618.55 55.88 o -4 6 1 83.72 92.00 8.05 o -3 6 1 459.89 451.97 14.30 o -2 6 1 2675.78 2664.71 39.24 o -1 6 1 183.34 221.53 13.20 o 0 6 1 24.40 49.54 5.88 o 1 6 1 5.91 10.57 4.95 o 2 6 1 289.26 295.52 11.67 o 3 6 1 740.06 724.23 18.48 o 4 6 1 3864.16 3638.74 49.50 o 5 6 1 24.83 22.16 5.45 o 6 6 1 323.41 304.33 13.00 o 7 6 1 186.20 172.74 12.89 o 8 6 1 100.53 98.72 10.74 o 9 6 1 62.17 80.51 9.04 o 10 6 1 2.02 19.73 6.18 o 11 6 1 122.94 154.48 17.54 o 12 6 1 533.83 489.46 24.02 o 13 6 1 382.43 428.03 25.18 o -12 7 1 1.68 13.20 10.34 o -11 7 1 3.02 1.24 11.24 o -10 7 1 448.32 458.26 48.51 o -9 7 1 198.10 216.45 19.74 o -8 7 1 151.39 173.99 19.43 o -7 7 1 367.35 378.67 22.51 o -6 7 1 175.14 167.16 16.13 o -5 7 1 3.11 6.48 5.69 o -4 7 1 63.84 84.71 11.53 o -3 7 1 332.11 329.96 16.50 o -2 7 1 761.25 804.16 25.26 o -1 7 1 811.37 786.79 24.84 o 0 7 1 502.93 493.11 19.48 o 1 7 1 97.68 97.84 8.60 o 2 7 1 1436.85 1425.68 38.12 o 3 7 1 243.66 255.22 12.32 o 4 7 1 132.11 157.65 10.16 o 5 7 1 69.41 76.66 7.95 o 6 7 1 1.66 10.53 12.22 o 7 7 1 480.93 457.76 25.06 o 8 7 1 1361.59 1255.78 43.53 o 9 7 1 1.86 24.64 14.22 o 10 7 1 126.28 135.88 14.07 o 11 7 1 54.74 78.93 12.23 o 12 7 1 131.36 139.36 16.85 o -10 8 1 123.08 159.19 39.85 o -9 8 1 220.07 302.00 24.52 o -8 8 1 136.59 167.40 17.53 o -7 8 1 88.51 132.42 15.64 o -6 8 1 336.36 350.64 23.13 o -5 8 1 32.66 66.91 15.26 o -4 8 1 71.66 99.36 14.84 o -3 8 1 687.50 674.64 24.91 o -2 8 1 93.52 102.72 16.96 o -1 8 1 1.26 2.70 7.76 o 0 8 1 269.83 287.41 22.71 o 1 8 1 975.99 973.20 53.04 o 2 8 1 515.92 520.33 28.14 o 3 8 1 1851.13 1755.76 53.60 o 4 8 1 328.73 343.68 24.30 o 5 8 1 1.26 27.32 13.71 o 6 8 1 20.85 41.97 17.94 o 7 8 1 73.00 75.47 21.13 o 8 8 1 44.47 47.64 19.18 o 9 8 1 297.03 304.15 37.84 o -7 9 1 34.32 25.06 19.18 o -6 9 1 290.33 306.31 39.59 o -5 9 1 134.44 185.06 31.86 o -4 9 1 124.59 109.80 25.16 o -3 9 1 198.63 221.97 21.45 o -2 9 1 339.34 343.64 25.54 o -1 9 1 7.42 24.69 10.77 o 0 9 1 366.02 386.86 34.18 o 1 9 1 72.50 88.83 14.90 o 2 9 1 301.57 338.10 26.52 o 3 9 1 70.26 59.00 14.00 o 4 9 1 114.38 130.11 27.63 o 5 9 1 253.84 246.93 35.15 o 6 9 1 7.05 11.55 17.83 o -2 10 1 6.07 29.08 18.97 o -1 10 1 16.77 17.63 13.98 o 0 10 1 197.55 164.96 23.22 o 1 10 1 126.64 116.73 20.92 o -16 0 2 215.30 212.49 30.41 o -14 0 2 571.10 475.91 38.87 o -12 0 2 1135.91 1098.87 48.82 o -10 0 2 433.95 425.09 22.22 o -8 0 2 12991.56 13112.00 183.23 o -6 0 2 443.83 529.29 17.05 o -4 0 2 114.98 98.62 5.19 o -2 0 2 16052.43 17642.88 319.10 o 0 0 2 14.43 34.55 4.59 o 2 0 2 8414.74 8904.81 164.34 o 4 0 2 131.91 179.39 14.54 o 6 0 2 4580.13 4559.33 106.50 o 8 0 2 3431.88 3280.35 91.04 o 10 0 2 5788.44 5884.16 148.05 o 12 0 2 275.18 200.84 27.73 o 14 0 2 3.27 16.19 13.71 o 16 0 2 1075.75 993.79 66.71 o -17 1 2 292.59 332.64 29.52 o -16 1 2 185.00 227.51 23.27 o -15 1 2 256.83 229.59 21.75 o -14 1 2 67.01 105.20 12.51 o -13 1 2 905.86 854.11 28.37 o -12 1 2 21.85 24.72 7.74 o -11 1 2 324.42 326.74 13.84 o -10 1 2 767.66 727.88 19.16 o -9 1 2 587.98 548.86 14.04 o -8 1 2 438.28 436.94 10.18 o -7 1 2 7019.23 6937.61 59.08 o -6 1 2 245.14 216.35 6.77 o -5 1 2 7.30 8.66 2.10 o -4 1 2 16832.16 18189.54 188.00 o -3 1 2 60822.38 58166.33 463.30 o -2 1 2 1922.86 2134.55 20.05 o -1 1 2 1009.90 986.89 12.12 o 0 1 2 5262.06 5645.94 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173.11 172.28 31.03 o -12 0 20 883.95 895.74 59.80 o -10 0 20 488.97 481.28 42.79 o -8 0 20 358.54 398.38 38.25 o -6 0 20 2257.99 1986.85 87.94 o -4 0 20 829.54 775.94 52.27 o -2 0 20 773.38 728.00 49.80 o 0 0 20 95.64 138.47 24.03 o 2 0 20 291.55 276.10 34.23 o -14 1 20 408.26 501.17 46.08 o -13 1 20 73.88 120.49 30.88 o -12 1 20 53.74 81.07 22.53 o -11 1 20 639.50 734.77 37.49 o -10 1 20 10.44 19.83 25.00 o -9 1 20 454.28 450.64 64.49 o -8 1 20 203.06 270.75 23.29 o -7 1 20 642.21 594.35 32.42 o -6 1 20 211.21 253.34 22.88 o -5 1 20 330.33 343.92 24.37 o -4 1 20 5.09 31.84 9.99 o -3 1 20 986.54 887.59 39.75 o -2 1 20 86.00 127.43 24.12 o -1 1 20 342.47 329.10 37.63 o 0 1 20 164.00 194.04 28.87 o 1 1 20 379.22 396.42 41.76 o 2 1 20 8.97 43.92 18.45 o -13 2 20 307.05 386.73 38.46 o -12 2 20 398.70 441.77 30.86 o -11 2 20 122.72 198.90 46.96 o -10 2 20 4.55 26.61 9.61 o -9 2 20 288.57 387.56 41.97 o -8 2 20 468.20 417.97 40.62 o -7 2 20 137.09 169.30 29.28 o -6 2 20 956.87 886.36 59.59 o -5 2 20 11.86 24.85 15.46 o -4 2 20 1063.21 991.42 62.89 o -3 2 20 661.78 698.92 52.38 o -2 2 20 168.50 210.63 31.75 o -1 2 20 298.22 340.13 39.17 o 0 2 20 7.31 37.22 16.50 o 1 2 20 13.38 23.50 19.59 o 2 2 20 545.26 502.30 48.77 o -11 3 20 18.34 25.47 21.34 o -10 3 20 115.15 102.59 28.14 o -9 3 20 227.93 244.86 34.95 o -8 3 20 422.79 406.42 42.06 o -7 3 20 37.53 61.13 17.73 o -6 3 20 242.90 334.77 40.73 o -5 3 20 13.22 79.87 15.46 o -4 3 20 475.05 532.83 31.34 o -3 3 20 144.91 180.17 27.52 o -2 3 20 714.55 733.51 37.55 o -1 3 20 13.06 61.46 26.81 o 0 3 20 103.98 170.61 57.48 o 1 3 20 122.63 135.37 27.52 o -10 4 20 42.68 98.98 25.16 o -9 4 20 1392.58 1443.20 70.32 o -8 4 20 586.42 595.84 35.48 o -7 4 20 834.06 880.53 42.47 o -6 4 20 34.05 90.84 34.54 o -5 4 20 51.52 59.15 23.50 o -4 4 20 0.03 20.45 25.06 o -3 4 20 490.28 550.83 69.28 o -2 4 20 162.50 183.59 23.44 o -1 4 20 470.71 481.69 48.25 o -7 5 20 62.28 51.14 25.26 o -6 5 20 707.55 678.30 56.91 o -5 5 20 96.96 96.81 29.80 o -13 0 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21 91.83 95.98 25.57 o -9 3 21 181.13 220.94 35.98 o -8 3 21 7.24 20.62 17.11 o -7 3 21 165.35 161.56 30.72 o -6 3 21 7.75 25.06 19.59 o -5 3 21 713.38 637.26 54.65 o -4 3 21 6.21 22.68 15.88 o -3 3 21 25.87 47.94 21.34 o -7 4 21 81.86 101.24 26.19 o -6 4 21 303.07 359.62 41.14 o -5 4 21 61.82 80.83 25.98 o -4 4 21 101.53 123.10 29.70 o -10 0 22 44.12 94.34 25.68 o -8 0 22 117.64 141.04 26.49 o -6 0 22 1667.82 1491.86 78.05 o -4 0 22 200.23 277.86 35.15 o -2 0 22 3.21 30.11 15.46 o -11 1 22 462.92 537.57 48.04 o -10 1 22 20.82 51.90 12.79 o -9 1 22 92.89 126.07 24.07 o -8 1 22 46.80 87.18 15.18 o -7 1 22 391.24 429.02 29.41 o -6 1 22 233.73 235.37 32.89 o -5 1 22 170.38 178.98 31.86 o -4 1 22 48.22 69.49 21.24 o -3 1 22 118.95 167.33 30.62 o -2 1 22 0.89 30.21 17.63 o -8 2 22 81.20 140.63 30.21 o -7 2 22 8.52 62.37 21.45 o -6 2 22 935.58 856.15 61.96 o -5 2 22 111.03 149.60 30.00 o -4 2 22 61.07 103.00 25.47 o -3 2 22 322.86 350.64 43.00 o -7 0 23 10.60 31.65 17.22 o -5 0 23 859.00 866.46 59.80 o -7 1 23 284.42 241.05 37.42 o -6 1 23 2.04 23.41 18.45 o