#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2205319.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205319_Fobs loop_ _publ_author_name 'Huo, Li-Hua' 'Gao, Shan' 'Xu, Shi-Xiao' 'Zhao, Hui' _publ_section_title ; Hexaaquazinc(II) naphthalene-1,5-disulfonate ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m449 _journal_page_last m450 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.272 _cell_angle_gamma 90.000 _cell_length_a 13.2367 _cell_length_b 6.6598 _cell_length_c 9.6849 _exptl_crystal_F_000 472.00 _reflns_d_resolution_high 0.7712 _[local]_cod_data_source_file ng6100Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 131.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 663.53 526.37 9.42 o 3 0 0 9.89 10.10 1.19 o 4 0 0 9714.81 10689.92 343.94 o 5 0 0 5706.60 6605.40 174.08 o 6 0 0 312.99 337.21 4.86 o 7 0 0 700.32 660.68 10.63 o 8 0 0 6613.74 7304.51 176.49 o 9 0 0 1658.29 1789.73 26.36 o 10 0 0 624.76 631.56 8.85 o 11 0 0 1644.26 1585.94 26.67 o 12 0 0 1184.14 1211.59 21.98 o 13 0 0 13.80 13.54 1.83 o 14 0 0 2.84 2.23 1.36 o 15 0 0 448.38 429.38 9.30 o 16 0 0 1582.28 1578.75 39.10 o 17 0 0 62.05 71.67 3.67 o 1 1 0 595.68 605.51 5.71 o 2 1 0 16.94 16.38 1.36 o 3 1 0 680.24 706.96 11.81 o 4 1 0 36.87 45.66 1.45 o 5 1 0 1539.11 1617.05 21.82 o 6 1 0 2199.55 2314.45 54.56 o 7 1 0 1020.25 961.26 13.70 o 8 1 0 211.75 224.51 6.51 o 9 1 0 27.86 29.34 1.46 o 10 1 0 112.98 113.85 1.93 o 11 1 0 1272.65 1295.37 15.96 o 12 1 0 119.01 123.08 2.19 o 13 1 0 4.22 5.26 1.15 o 14 1 0 2.99 2.32 0.91 o 15 1 0 9.43 8.51 1.23 o 16 1 0 0.01 1.06 1.22 o 17 1 0 23.34 25.69 1.67 o 0 2 0 5405.37 5525.37 158.40 o 1 2 0 3783.30 4017.10 71.90 o 2 2 0 1032.55 999.76 11.78 o 3 2 0 148.72 191.55 2.77 o 4 2 0 2152.79 1980.10 27.78 o 5 2 0 2278.68 2267.18 33.52 o 6 2 0 812.76 818.40 8.93 o 7 2 0 305.39 292.67 5.19 o 8 2 0 1995.25 1939.81 43.67 o 9 2 0 2760.15 2690.28 45.11 o 10 2 0 114.54 117.84 5.24 o 11 2 0 958.71 856.68 15.04 o 12 2 0 177.51 183.02 6.15 o 13 2 0 481.98 467.21 6.63 o 14 2 0 11.46 12.99 1.25 o 15 2 0 485.48 486.15 6.38 o 16 2 0 1169.51 1153.81 16.47 o 1 3 0 140.65 187.80 2.54 o 2 3 0 5.10 4.11 1.03 o 3 3 0 19.86 33.06 1.20 o 4 3 0 168.34 165.52 2.09 o 5 3 0 773.67 823.83 9.51 o 6 3 0 70.80 67.22 1.44 o 7 3 0 7.06 6.34 0.78 o 8 3 0 35.09 34.59 1.02 o 9 3 0 175.09 171.20 5.44 o 10 3 0 19.42 21.55 1.15 o 11 3 0 50.55 61.23 5.33 o 12 3 0 53.49 46.28 3.57 o 13 3 0 475.46 460.80 8.46 o 14 3 0 71.12 73.39 1.70 o 15 3 0 16.94 19.04 1.20 o 16 3 0 17.77 23.14 3.18 o 0 4 0 9779.04 10627.24 430.16 o 1 4 0 805.44 721.96 9.40 o 2 4 0 198.67 193.65 3.08 o 3 4 0 1669.56 1609.87 22.43 o 4 4 0 3916.21 3919.28 74.30 o 5 4 0 2356.12 2337.36 37.16 o 6 4 0 14.47 17.46 0.94 o 7 4 0 2465.79 2436.86 39.28 o 8 4 0 2482.37 2428.63 38.40 o 9 4 0 602.43 590.65 7.56 o 10 4 0 2.97 3.65 1.06 o 11 4 0 249.48 238.24 4.56 o 12 4 0 513.07 511.08 8.96 o 13 4 0 46.23 49.40 2.01 o 14 4 0 6.70 7.27 1.75 o 15 4 0 280.48 292.42 11.31 o 1 5 0 404.08 374.38 5.31 o 2 5 0 185.65 175.03 4.04 o 3 5 0 2381.21 2385.79 41.53 o 4 5 0 301.10 309.69 4.45 o 5 5 0 1422.49 1411.27 22.80 o 6 5 0 211.91 200.87 3.55 o 7 5 0 30.74 34.02 1.52 o 8 5 0 2.70 2.94 1.24 o 9 5 0 349.23 346.73 5.15 o 10 5 0 4.36 2.20 1.03 o 11 5 0 851.22 844.18 14.57 o 12 5 0 41.26 40.83 2.90 o 13 5 0 61.55 59.85 7.54 o 0 6 0 313.99 321.60 8.73 o 1 6 0 874.00 843.21 12.17 o 2 6 0 612.58 576.38 9.57 o 3 6 0 119.53 112.06 2.86 o 4 6 0 679.34 697.24 11.13 o 5 6 0 12.57 11.82 1.91 o 6 6 0 374.22 369.27 5.58 o 7 6 0 100.70 99.31 2.70 o 8 6 0 361.33 355.32 5.01 o 9 6 0 454.61 454.71 6.78 o 10 6 0 249.30 271.30 13.14 o 11 6 0 120.08 111.09 6.04 o 12 6 0 513.76 528.74 21.12 o 1 7 0 339.49 336.07 6.38 o 2 7 0 3.75 3.83 1.81 o 3 7 0 181.37 183.95 5.07 o 4 7 0 62.47 70.65 4.19 o 5 7 0 411.16 398.95 7.32 o 6 7 0 156.14 161.48 3.65 o 7 7 0 22.55 23.15 2.50 o 8 7 0 3.80 5.99 1.66 o 9 7 0 15.99 16.04 4.30 o 10 7 0 0.41 0.35 4.17 o 0 8 0 204.94 225.09 16.93 o 1 8 0 369.11 359.38 7.23 o 2 8 0 89.78 93.33 3.51 o 3 8 0 261.86 262.83 6.26 o 4 8 0 190.07 198.44 5.33 o 5 8 0 257.57 274.30 6.55 o 6 8 0 39.22 41.47 4.27 o -17 1 1 190.60 197.93 3.55 o -16 1 1 55.73 57.39 2.11 o -15 1 1 361.21 353.45 4.48 o -14 1 1 795.01 791.76 9.50 o -13 1 1 63.95 60.10 2.16 o -12 1 1 259.00 253.89 4.26 o -11 1 1 641.83 653.77 7.49 o -10 1 1 4074.23 4091.20 71.21 o -9 1 1 717.43 695.65 10.71 o -8 1 1 1444.40 1435.79 34.70 o -7 1 1 4537.45 4540.69 71.76 o -6 1 1 2472.66 2309.11 42.60 o -5 1 1 1572.48 1760.15 31.21 o -4 1 1 126.11 110.42 1.83 o -3 1 1 7012.66 7502.13 141.63 o -2 1 1 16275.11 16745.71 569.11 o -1 1 1 2900.55 3029.30 68.72 o 0 1 1 1269.70 1402.25 24.63 o 1 1 1 15684.88 15916.93 822.92 o 2 1 1 11500.04 11728.39 476.58 o 3 1 1 528.28 594.30 25.26 o 4 1 1 131.41 141.49 1.79 o 5 1 1 336.74 254.72 2.56 o 6 1 1 8205.08 9022.39 208.71 o 7 1 1 1292.74 1337.32 20.91 o 8 1 1 541.21 554.32 14.68 o 9 1 1 968.58 908.12 33.15 o 10 1 1 1357.04 1308.36 36.83 o 11 1 1 5.31 4.42 0.90 o 12 1 1 385.57 363.85 4.88 o 13 1 1 896.83 907.85 12.65 o 14 1 1 1415.71 1401.14 19.91 o 15 1 1 37.31 40.67 2.56 o 16 1 1 3.10 1.18 1.41 o -16 2 1 5.63 7.89 2.11 o -15 2 1 19.01 16.86 1.41 o -14 2 1 8.89 9.49 1.13 o -13 2 1 5.17 7.18 1.07 o -12 2 1 267.63 250.67 4.12 o -11 2 1 156.44 171.20 3.61 o -10 2 1 199.11 210.54 4.35 o -9 2 1 233.69 241.80 6.80 o -8 2 1 324.36 331.59 6.52 o -7 2 1 69.35 61.45 3.48 o -6 2 1 68.54 94.94 3.25 o -5 2 1 3846.49 4272.71 71.64 o -4 2 1 433.04 474.05 4.27 o -3 2 1 667.77 651.01 7.00 o -2 2 1 1211.48 1239.87 17.21 o -1 2 1 85.10 90.91 1.67 o 0 2 1 859.45 794.76 10.60 o 1 2 1 600.28 573.44 8.95 o 2 2 1 318.62 369.17 4.30 o 3 2 1 477.55 452.24 7.23 o 4 2 1 229.43 233.47 2.98 o 5 2 1 604.13 577.42 14.18 o 6 2 1 1308.11 1341.53 25.78 o 7 2 1 9.12 7.50 0.68 o 8 2 1 553.45 524.70 10.57 o 9 2 1 196.15 197.46 3.32 o 10 2 1 9.03 10.60 0.96 o 11 2 1 184.16 204.01 3.09 o 12 2 1 203.97 217.16 3.79 o 13 2 1 22.86 20.28 2.01 o 14 2 1 115.12 113.01 2.70 o 15 2 1 147.71 157.82 3.40 o 16 2 1 0.07 -0.17 1.22 o -16 3 1 34.49 24.73 3.58 o -15 3 1 336.61 322.17 8.43 o -14 3 1 528.82 488.53 10.87 o -13 3 1 37.32 42.06 1.66 o -12 3 1 103.55 97.39 1.92 o -11 3 1 606.28 636.16 13.75 o -10 3 1 1062.55 968.03 12.67 o -9 3 1 85.45 85.97 3.49 o -8 3 1 114.98 115.57 2.02 o -7 3 1 2902.30 2878.14 42.36 o -6 3 1 2503.59 2419.87 33.72 o -5 3 1 505.57 532.75 5.48 o -4 3 1 179.76 177.87 2.10 o -3 3 1 6444.86 6671.30 150.05 o -2 3 1 9603.76 10217.04 279.90 o -1 3 1 3981.09 4283.24 79.76 o 0 3 1 9.61 19.53 1.07 o 1 3 1 2617.96 2590.85 40.92 o 2 3 1 1815.94 1666.84 22.68 o 3 3 1 1396.29 1388.15 19.40 o 4 3 1 38.22 28.57 2.26 o 5 3 1 2637.00 2647.96 43.36 o 6 3 1 3317.97 3140.55 55.04 o 7 3 1 3119.28 3109.06 96.75 o 8 3 1 1002.47 964.42 11.54 o 9 3 1 2233.34 2175.56 30.58 o 10 3 1 1189.77 1176.02 17.22 o 11 3 1 6.24 8.20 0.99 o 12 3 1 24.01 21.74 2.65 o 13 3 1 472.56 451.53 8.74 o 14 3 1 661.71 656.07 10.66 o 15 3 1 74.10 76.91 2.29 o -15 4 1 130.88 153.07 5.01 o -14 4 1 79.42 73.41 3.49 o -13 4 1 132.07 138.95 4.79 o -12 4 1 0.26 1.52 1.04 o -11 4 1 13.22 11.88 1.58 o -10 4 1 469.83 465.10 7.17 o -9 4 1 83.87 89.56 2.33 o -8 4 1 205.91 207.13 2.83 o -7 4 1 817.76 834.59 10.15 o -6 4 1 39.13 40.07 2.79 o -5 4 1 1029.90 952.36 11.91 o -4 4 1 68.32 67.53 1.63 o -3 4 1 105.22 98.10 2.21 o -2 4 1 802.04 801.27 10.86 o -1 4 1 602.60 560.40 7.29 o 0 4 1 154.63 163.48 2.71 o 1 4 1 371.35 354.94 5.73 o 2 4 1 67.79 86.02 2.10 o 3 4 1 71.74 71.58 1.81 o 4 4 1 0.03 1.93 1.42 o 5 4 1 322.26 306.91 4.29 o 6 4 1 602.93 581.97 7.94 o 7 4 1 54.05 46.88 2.47 o 8 4 1 38.76 37.38 1.45 o 9 4 1 396.57 387.40 8.28 o 10 4 1 64.70 65.89 1.65 o 11 4 1 211.09 210.08 5.67 o 12 4 1 59.27 55.30 4.91 o 13 4 1 107.17 106.87 2.84 o 14 4 1 59.07 56.31 3.87 o 15 4 1 66.20 59.78 5.38 o -13 5 1 66.17 69.19 3.82 o -12 5 1 146.06 141.90 5.04 o -11 5 1 749.15 750.66 19.43 o -10 5 1 1015.70 959.71 17.67 o -9 5 1 32.10 36.24 1.40 o -8 5 1 250.81 255.77 3.62 o -7 5 1 718.85 721.49 8.85 o -6 5 1 2070.08 2058.35 33.19 o -5 5 1 55.55 52.34 1.54 o -4 5 1 4.35 3.77 0.99 o -3 5 1 1075.67 1091.04 14.82 o -2 5 1 2113.75 2142.11 37.24 o -1 5 1 957.55 909.08 12.31 o 0 5 1 94.55 84.73 3.21 o 1 5 1 410.78 414.27 6.31 o 2 5 1 847.23 861.99 14.15 o 3 5 1 256.94 236.26 3.91 o 4 5 1 297.45 292.78 5.33 o 5 5 1 459.61 441.93 6.81 o 6 5 1 1022.67 1028.22 15.28 o 7 5 1 10.78 10.92 2.41 o 8 5 1 578.26 572.77 8.62 o 9 5 1 490.44 478.33 9.40 o 10 5 1 504.58 491.02 13.71 o 11 5 1 9.54 10.26 1.12 o 12 5 1 5.38 4.56 1.75 o 13 5 1 476.26 498.30 16.10 o -12 6 1 1.35 3.11 2.10 o -11 6 1 173.76 176.58 5.39 o -10 6 1 125.69 129.10 7.45 o -9 6 1 43.16 40.22 4.65 o -8 6 1 513.97 508.64 9.08 o -7 6 1 343.10 339.12 4.46 o -6 6 1 95.62 95.56 3.74 o -5 6 1 695.95 696.26 10.52 o -4 6 1 647.05 671.81 10.00 o -3 6 1 110.74 111.02 4.04 o -2 6 1 256.05 249.47 4.21 o -1 6 1 492.41 487.09 7.69 o 0 6 1 251.99 238.00 4.62 o 1 6 1 1082.50 1037.71 16.97 o 2 6 1 28.47 26.95 1.74 o 3 6 1 257.06 249.06 5.23 o 4 6 1 23.66 28.46 2.70 o 5 6 1 350.93 361.51 9.97 o 6 6 1 252.27 241.72 4.40 o 7 6 1 154.11 155.70 5.23 o 8 6 1 53.93 53.72 3.13 o 9 6 1 69.54 74.07 2.15 o 10 6 1 21.81 16.98 2.05 o 11 6 1 347.54 333.78 9.32 o 12 6 1 86.43 90.73 20.62 o -10 7 1 76.67 74.61 22.10 o -9 7 1 176.10 187.09 8.34 o -8 7 1 234.34 268.00 12.43 o -7 7 1 273.84 274.60 7.08 o -6 7 1 234.24 227.85 6.13 o -5 7 1 216.44 217.36 4.45 o -4 7 1 64.91 74.81 5.47 o -3 7 1 273.77 277.35 5.21 o -2 7 1 503.65 518.03 8.18 o -1 7 1 389.71 376.13 9.93 o 0 7 1 949.55 913.92 14.88 o 1 7 1 172.53 187.60 4.43 o 2 7 1 870.23 859.14 13.42 o 3 7 1 840.93 841.63 14.00 o 4 7 1 363.43 358.75 7.73 o 5 7 1 506.61 505.51 8.56 o 6 7 1 66.63 69.89 3.58 o 7 7 1 291.67 285.38 6.57 o 8 7 1 216.09 214.61 7.04 o 9 7 1 126.69 130.04 4.91 o -6 8 1 110.78 113.52 7.64 o -5 8 1 146.29 144.16 5.46 o -4 8 1 15.62 20.69 2.53 o -3 8 1 16.70 16.76 1.82 o -2 8 1 62.29 72.65 4.97 o -1 8 1 219.19 233.16 6.14 o 0 8 1 222.92 219.53 5.33 o 1 8 1 264.57 260.97 5.51 o 2 8 1 11.10 9.00 1.79 o 3 8 1 280.17 292.03 5.98 o 4 8 1 18.46 15.78 2.04 o 5 8 1 62.27 67.94 3.11 o 6 8 1 46.88 53.82 5.66 o -17 0 2 401.81 396.10 8.13 o -16 0 2 822.20 831.55 16.11 o -15 0 2 327.73 338.40 5.80 o -14 0 2 66.54 66.36 2.70 o -13 0 2 1375.48 1370.14 20.91 o -12 0 2 241.50 236.26 5.94 o -11 0 2 409.81 385.87 7.85 o -10 0 2 80.87 76.67 8.37 o -9 0 2 7387.30 7454.14 282.61 o -8 0 2 2751.51 2797.36 53.91 o -7 0 2 254.47 283.34 4.21 o -6 0 2 52.72 56.57 1.89 o -5 0 2 5277.41 5323.37 128.80 o -4 0 2 2455.33 2334.28 34.38 o -3 0 2 353.55 360.75 3.78 o -2 0 2 349.55 366.37 8.08 o -1 0 2 14104.98 15228.77 494.90 o 0 0 2 12746.82 13411.66 470.09 o 1 0 2 4795.93 5039.52 136.25 o 2 0 2 5744.83 6260.79 189.26 o 3 0 2 17309.88 18069.87 920.97 o 4 0 2 9750.56 10409.36 407.36 o 5 0 2 4541.57 5223.13 225.36 o 6 0 2 1211.13 1255.43 83.13 o 7 0 2 12176.78 12648.01 925.81 o 8 0 2 855.14 825.32 70.19 o 9 0 2 37.97 32.65 1.40 o 10 0 2 333.63 328.86 8.14 o 11 0 2 2011.56 1995.68 35.58 o 12 0 2 1027.24 1057.74 25.16 o 13 0 2 43.12 47.37 1.82 o 14 0 2 658.63 661.28 16.27 o 15 0 2 1659.87 1685.71 49.75 o 16 0 2 553.17 531.39 13.16 o -16 1 2 0.51 0.18 0.89 o -15 1 2 38.19 44.23 2.11 o -14 1 2 57.39 60.15 1.78 o -13 1 2 0.86 0.38 0.94 o -12 1 2 0.30 1.10 1.12 o -11 1 2 85.09 90.73 2.43 o -10 1 2 1087.78 1078.93 20.99 o -9 1 2 13.47 12.67 0.80 o -8 1 2 349.67 376.03 6.44 o -7 1 2 586.26 606.24 9.62 o -6 1 2 14.50 16.81 0.73 o -5 1 2 0.59 1.75 1.09 o -4 1 2 9413.53 10168.60 226.55 o -3 1 2 2893.15 3044.67 75.13 o -2 1 2 449.41 505.77 5.89 o -1 1 2 854.58 846.85 7.48 o 0 1 2 1519.05 1593.75 20.43 o 1 1 2 3998.90 4295.05 122.54 o 2 1 2 2255.86 2346.83 33.38 o 3 1 2 1619.29 1639.24 34.46 o 4 1 2 1278.40 1222.02 50.72 o 5 1 2 109.87 106.92 2.13 o 6 1 2 2.35 5.35 1.00 o 7 1 2 679.49 689.60 10.16 o 8 1 2 94.35 88.89 2.84 o 9 1 2 57.14 53.35 1.86 o 10 1 2 581.38 563.56 15.12 o 11 1 2 0.51 2.87 3.14 o 12 1 2 9.37 11.01 1.42 o 13 1 2 41.27 42.05 1.79 o 14 1 2 250.85 248.69 4.19 o 15 1 2 0.00 2.60 1.49 o 16 1 2 0.61 0.55 1.37 o -16 2 2 238.25 234.02 5.72 o -15 2 2 46.55 52.43 2.88 o -14 2 2 272.66 253.68 4.39 o -13 2 2 1028.68 1011.74 13.33 o -12 2 2 1150.45 1114.44 13.71 o -11 2 2 385.50 360.94 4.09 o -10 2 2 1167.17 1169.12 13.06 o -9 2 2 3063.17 3029.35 42.44 o -8 2 2 1622.15 1573.57 17.77 o -7 2 2 133.68 143.76 2.45 o -6 2 2 292.16 287.26 4.86 o -5 2 2 3993.26 3938.54 85.24 o -4 2 2 5603.55 5721.96 142.02 o -3 2 2 3158.12 3464.82 51.31 o -2 2 2 2319.50 2367.76 34.59 o -1 2 2 3872.24 3876.27 71.00 o 0 2 2 7303.56 8194.42 233.17 o 1 2 2 7.09 17.70 5.17 o 2 2 2 140.58 152.34 4.89 o 3 2 2 176.93 121.52 7.84 o 4 2 2 2172.05 1937.14 70.05 o 5 2 2 796.38 801.91 21.44 o 6 2 2 711.34 687.93 10.22 o 7 2 2 1401.43 1315.63 16.87 o 8 2 2 1742.30 1723.75 26.56 o 9 2 2 5.91 6.13 0.86 o 10 2 2 8.51 10.53 0.73 o 11 2 2 1808.22 1783.25 45.44 o 12 2 2 204.81 192.84 9.07 o 13 2 2 216.81 211.50 4.74 o 14 2 2 5.35 6.99 1.30 o 15 2 2 945.20 916.19 13.55 o 16 2 2 736.89 745.73 12.05 o -15 3 2 9.98 13.79 2.68 o -14 3 2 2.35 4.68 1.98 o -13 3 2 12.23 10.98 0.81 o -12 3 2 218.59 210.77 2.36 o -11 3 2 87.57 71.94 1.51 o -10 3 2 191.22 197.71 3.60 o -9 3 2 74.40 67.82 4.73 o -8 3 2 40.83 43.34 2.97 o -7 3 2 0.86 0.81 2.03 o -6 3 2 431.79 425.87 9.07 o -5 3 2 389.46 385.16 7.39 o -4 3 2 87.60 105.37 2.12 o -3 3 2 583.85 558.36 8.81 o -2 3 2 217.44 190.99 2.28 o -1 3 2 3613.59 3942.14 71.19 o 0 3 2 944.43 1059.50 16.16 o 1 3 2 402.12 464.03 7.17 o 2 3 2 350.70 440.82 5.83 o 3 3 2 590.48 584.47 8.32 o 4 3 2 124.80 116.35 2.45 o 5 3 2 377.39 364.77 7.81 o 6 3 2 165.37 157.61 5.84 o 7 3 2 144.15 132.84 3.22 o 8 3 2 20.92 22.81 1.44 o 9 3 2 1.34 1.21 0.89 o 10 3 2 46.22 49.47 2.37 o 11 3 2 90.87 90.44 2.47 o 12 3 2 607.70 609.52 8.72 o 13 3 2 113.52 112.23 6.36 o 14 3 2 64.81 71.05 2.88 o 15 3 2 53.38 61.18 2.50 o -15 4 2 2.52 0.35 3.53 o -14 4 2 100.47 110.98 4.50 o -13 4 2 882.62 848.54 17.37 o -12 4 2 178.46 196.52 7.35 o -11 4 2 45.91 44.86 3.39 o -10 4 2 48.01 61.88 4.56 o -9 4 2 2085.01 2036.69 42.51 o -8 4 2 433.61 431.43 10.69 o -7 4 2 569.91 544.74 11.86 o -6 4 2 5.23 6.20 0.71 o -5 4 2 3278.41 3155.22 59.37 o -4 4 2 4085.58 4040.38 68.43 o -3 4 2 157.02 176.73 10.45 o -2 4 2 585.29 576.42 7.42 o -1 4 2 4170.47 4229.39 82.34 o 0 4 2 4719.42 4909.37 101.91 o 1 4 2 107.92 90.34 3.53 o 2 4 2 498.86 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