#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:10:02 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180973 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/53/2205355.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205355_Fobs loop_ _publ_author_name 'Wu, Jian-Yi' 'Xie, Lin-Ming' 'He, Hong-Yin' 'Zhou, Xia' 'Zhu, Long-Guan' _publ_section_title ; Aqua(1,10-phenanthroline)(thiodiglycolato)cobalt(II) ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m568 _journal_page_last m570 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.420 _cell_angle_gamma 90.000 _cell_length_a 8.0127 _cell_length_b 22.5238 _cell_length_c 9.7331 _exptl_crystal_F_000 828.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file rz6052Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 232.16 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 493.14 590.38 18.37 o 4 0 0 6186.74 6579.97 157.66 o 6 0 0 296.20 356.33 36.47 o 8 0 0 1185.32 1064.85 90.53 o 1 1 0 6207.99 6272.82 103.26 o 2 1 0 9815.65 10000.19 173.68 o 3 1 0 210.74 263.19 8.81 o 4 1 0 3711.80 3697.68 69.98 o 5 1 0 97.78 122.00 9.20 o 6 1 0 985.57 1059.38 35.56 o 7 1 0 163.24 196.35 32.84 o 8 1 0 10.16 14.68 13.76 o 9 1 0 79.59 67.48 15.35 o 0 2 0 1091.96 1312.90 36.30 o 1 2 0 4380.63 4481.33 78.60 o 2 2 0 53897.02 51541.17 880.59 o 3 2 0 13928.04 14474.06 236.11 o 4 2 0 1860.20 1937.05 37.32 o 5 2 0 972.89 961.82 22.99 o 6 2 0 35.89 41.14 8.94 o 7 2 0 184.95 204.13 21.94 o 8 2 0 81.89 68.70 28.73 o 9 2 0 20.19 30.92 21.59 o 1 3 0 7533.36 7837.84 135.84 o 2 3 0 20058.47 21031.59 361.52 o 3 3 0 1593.92 1496.36 28.78 o 4 3 0 611.13 661.03 16.64 o 5 3 0 386.13 394.59 22.76 o 6 3 0 502.51 487.76 21.75 o 7 3 0 708.94 698.09 39.44 o 8 3 0 0.34 31.36 23.30 o 9 3 0 36.63 40.25 14.42 o 0 4 0 538.40 633.33 17.21 o 1 4 0 231.67 232.29 8.60 o 2 4 0 5157.61 5596.53 106.76 o 3 4 0 6518.47 6509.54 109.00 o 4 4 0 3726.73 3910.67 69.25 o 5 4 0 1680.62 1587.74 60.73 o 6 4 0 1121.93 1095.11 32.89 o 7 4 0 199.79 207.27 22.08 o 8 4 0 993.24 955.68 47.16 o 9 4 0 0.07 27.43 19.34 o 1 5 0 350.54 360.74 9.49 o 2 5 0 148.62 187.53 11.29 o 3 5 0 7969.24 8320.28 147.74 o 4 5 0 22247.84 23131.41 376.53 o 5 5 0 0.47 1.83 6.42 o 6 5 0 142.70 155.64 13.80 o 7 5 0 26.93 55.40 12.59 o 8 5 0 18.37 23.18 13.86 o 9 5 0 34.66 32.28 22.53 o 0 6 0 13609.65 14618.49 334.58 o 1 6 0 22.77 24.68 3.52 o 2 6 0 925.62 899.76 21.62 o 3 6 0 1702.44 1737.47 35.80 o 4 6 0 427.65 455.45 24.64 o 5 6 0 826.95 783.52 29.02 o 6 6 0 1717.05 1593.25 43.11 o 7 6 0 498.53 468.54 34.87 o 8 6 0 685.60 646.58 39.44 o 9 6 0 0.03 30.41 13.39 o 1 7 0 315.66 258.66 9.25 o 2 7 0 2316.69 2413.17 49.57 o 3 7 0 138.72 165.41 11.28 o 4 7 0 371.94 367.15 20.57 o 5 7 0 2939.11 2890.74 76.92 o 6 7 0 2029.71 1937.00 69.62 o 7 7 0 938.97 899.03 32.89 o 8 7 0 18.74 44.55 15.26 o 9 7 0 425.74 542.49 56.99 o 0 8 0 1112.56 1064.47 32.02 o 1 8 0 220.44 230.25 8.81 o 2 8 0 1244.59 1398.16 31.80 o 3 8 0 6393.29 6650.54 120.27 o 4 8 0 30.04 18.06 6.88 o 5 8 0 3318.79 3015.37 68.64 o 6 8 0 829.81 829.23 34.99 o 7 8 0 78.21 100.44 13.54 o 8 8 0 13.38 -8.58 12.55 o 9 8 0 32.18 33.22 14.81 o 1 9 0 205.16 200.11 12.65 o 2 9 0 4117.60 4435.22 80.83 o 3 9 0 21.90 46.67 6.50 o 4 9 0 149.77 114.06 10.87 o 5 9 0 311.78 307.58 18.23 o 6 9 0 1081.59 1014.82 33.03 o 7 9 0 1049.84 1039.72 48.98 o 8 9 0 118.40 96.61 16.76 o 9 9 0 536.82 666.31 69.82 o 0 10 0 10651.73 11393.12 302.93 o 1 10 0 6883.72 7426.61 131.81 o 2 10 0 337.50 307.51 10.68 o 3 10 0 73.61 46.11 6.28 o 4 10 0 118.20 98.34 18.50 o 5 10 0 382.14 401.28 20.71 o 6 10 0 314.16 374.42 24.29 o 7 10 0 675.25 649.97 29.55 o 8 10 0 1601.90 1591.79 54.38 o 1 11 0 2592.58 2772.77 53.17 o 2 11 0 1988.65 1961.95 39.61 o 3 11 0 15.49 25.94 5.74 o 4 11 0 180.41 210.64 16.58 o 5 11 0 222.97 228.51 16.72 o 6 11 0 407.67 412.64 25.38 o 7 11 0 12.94 17.40 10.38 o 8 11 0 91.07 67.59 17.10 o 0 12 0 2150.79 2463.52 73.71 o 1 12 0 1125.03 1274.82 28.07 o 2 12 0 1166.95 1191.97 25.40 o 3 12 0 224.25 209.68 14.33 o 4 12 0 592.27 548.06 22.40 o 5 12 0 556.14 573.31 25.01 o 6 12 0 871.08 904.74 37.10 o 7 12 0 28.21 32.32 11.69 o 8 12 0 366.45 427.15 33.30 o 1 13 0 3942.72 3766.13 71.15 o 2 13 0 697.14 721.27 18.18 o 3 13 0 652.26 614.65 21.72 o 4 13 0 24.65 20.94 10.59 o 5 13 0 46.63 57.64 10.62 o 6 13 0 0.55 4.14 9.65 o 7 13 0 39.38 44.62 12.64 o 8 13 0 225.73 227.46 22.27 o 0 14 0 2897.57 2832.99 74.01 o 1 14 0 13.37 38.81 5.44 o 2 14 0 2860.34 2947.63 58.74 o 3 14 0 1893.47 1760.77 43.64 o 4 14 0 736.05 700.18 26.22 o 5 14 0 1223.74 1220.41 40.32 o 6 14 0 173.60 172.92 18.30 o 7 14 0 216.30 211.63 20.59 o 8 14 0 29.46 33.86 18.50 o 1 15 0 286.49 258.39 11.50 o 2 15 0 946.73 935.76 35.10 o 3 15 0 935.26 936.77 28.43 o 4 15 0 739.92 727.80 30.37 o 5 15 0 108.07 118.83 14.87 o 6 15 0 971.51 984.97 39.44 o 7 15 0 293.24 273.26 23.17 o 8 15 0 91.23 76.19 19.74 o 0 16 0 3653.55 3538.91 91.68 o 1 16 0 524.12 523.18 16.36 o 2 16 0 4134.06 3914.06 76.44 o 3 16 0 185.35 171.61 14.85 o 4 16 0 1676.09 1606.81 47.70 o 5 16 0 279.10 228.04 19.57 o 6 16 0 96.74 105.11 19.69 o 7 16 0 96.23 94.98 16.44 o 1 17 0 179.39 178.75 11.91 o 2 17 0 742.30 756.47 24.33 o 3 17 0 729.99 679.76 32.66 o 4 17 0 207.84 195.77 17.18 o 5 17 0 3.03 12.98 9.88 o 6 17 0 649.91 579.15 32.36 o 7 17 0 18.84 40.03 14.39 o 0 18 0 1260.65 1191.54 39.57 o 1 18 0 71.78 82.66 8.78 o 2 18 0 1905.78 1828.25 45.17 o 3 18 0 474.46 491.51 24.99 o 4 18 0 30.50 50.87 11.49 o 5 18 0 2086.91 1937.94 57.85 o 6 18 0 1.23 6.98 12.12 o 7 18 0 142.84 199.68 24.75 o 1 19 0 1269.03 1265.91 34.57 o 2 19 0 2.57 8.66 7.94 o 3 19 0 682.16 604.26 28.25 o 4 19 0 0.86 17.55 10.13 o 5 19 0 5.47 23.88 11.47 o 6 19 0 142.93 160.44 19.30 o 7 19 0 90.53 97.38 17.95 o 0 20 0 8.76 3.53 9.35 o 1 20 0 34.37 30.72 8.68 o 2 20 0 22.44 27.99 9.02 o 3 20 0 2010.18 1801.76 52.61 o 4 20 0 17.39 23.63 10.82 o 5 20 0 305.26 376.28 26.09 o 6 20 0 68.60 70.40 15.93 o 1 21 0 415.43 393.50 21.65 o 2 21 0 502.87 498.79 41.27 o 3 21 0 161.90 176.20 19.53 o 4 21 0 352.90 341.09 26.29 o 5 21 0 17.58 43.39 13.07 o 6 21 0 251.91 284.33 26.62 o 0 22 0 1700.87 1744.14 77.16 o 1 22 0 132.84 113.34 13.19 o 2 22 0 395.75 378.73 25.99 o 3 22 0 42.81 43.05 15.56 o 4 22 0 14.56 11.57 12.32 o 5 22 0 10.98 6.04 11.85 o 6 22 0 138.89 171.75 21.01 o 1 23 0 574.53 555.27 26.80 o 2 23 0 360.10 340.93 25.07 o 3 23 0 122.38 121.31 17.48 o 4 23 0 238.71 246.04 23.89 o 5 23 0 114.38 160.21 20.93 o 0 24 0 461.78 495.08 40.41 o 1 24 0 478.63 413.64 27.27 o 2 24 0 181.90 217.68 22.97 o 3 24 0 360.68 338.21 27.18 o 4 24 0 37.53 63.86 15.82 o 5 24 0 180.72 199.70 23.29 o 1 25 0 641.32 646.26 37.83 o 2 25 0 66.57 58.90 14.46 o 3 25 0 1.84 7.95 13.45 o 4 25 0 3.62 7.27 13.33 o 0 26 0 171.33 144.50 27.52 o 1 26 0 82.74 49.54 16.34 o 2 26 0 3.95 1.71 11.94 o 3 26 0 295.44 322.66 44.86 o 4 26 0 168.82 156.48 21.21 o 1 27 0 17.63 25.26 16.38 o 2 27 0 166.23 168.62 21.13 o 3 27 0 1.40 6.01 13.46 o 0 28 0 60.61 94.14 31.22 o 1 28 0 5.57 -2.89 14.44 o 2 28 0 0.71 -17.63 11.75 o 1 29 0 111.77 106.56 27.70 o -9 0 1 289.76 334.84 50.79 o -7 0 1 44.63 59.91 37.10 o -5 0 1 217.63 219.71 17.02 o -3 0 1 162.33 200.57 10.37 o -1 0 1 3275.04 3432.28 80.37 o 1 0 1 2047.71 2155.20 52.51 o 3 0 1 7636.19 7696.43 182.14 o 5 0 1 1073.17 1089.40 36.72 o 7 0 1 1028.59 1019.54 83.30 o 9 0 1 9.46 45.85 19.82 o -9 1 1 18.97 36.04 14.52 o -8 1 1 18.79 41.49 15.53 o -7 1 1 9.97 17.72 11.85 o -6 1 1 170.85 178.53 17.66 o -5 1 1 161.87 201.84 11.64 o -4 1 1 2101.93 2135.17 39.86 o -3 1 1 7930.45 7961.28 131.42 o -2 1 1 755.02 766.27 15.13 o -1 1 1 16767.52 17195.44 294.59 o 0 1 1 32.27 39.70 3.28 o 1 1 1 19596.44 20240.11 326.06 o 2 1 1 461.59 479.39 15.69 o 3 1 1 1291.61 1320.56 26.76 o 4 1 1 4602.94 4536.33 79.82 o 5 1 1 1.20 6.99 5.80 o 6 1 1 525.50 514.07 30.12 o 7 1 1 1346.09 1270.15 49.03 o 8 1 1 123.04 137.34 19.82 o 9 1 1 279.54 311.51 28.11 o -9 2 1 211.25 193.52 23.14 o -8 2 1 881.04 874.45 57.85 o -7 2 1 63.40 54.14 14.64 o -6 2 1 103.23 112.24 19.41 o -5 2 1 249.55 273.15 13.15 o -4 2 1 23.88 16.77 4.30 o -3 2 1 1.68 6.03 2.76 o -2 2 1 1077.39 1112.22 22.69 o -1 2 1 9824.16 9889.58 159.90 o 0 2 1 23734.79 23732.64 407.37 o 1 2 1 1052.73 1127.72 22.05 o 2 2 1 3583.72 3717.86 68.37 o 3 2 1 4751.00 4917.64 84.28 o 4 2 1 139.74 157.02 9.06 o 5 2 1 687.93 691.20 21.46 o 6 2 1 181.04 216.20 20.02 o 7 2 1 29.55 58.19 15.03 o 8 2 1 1073.11 1035.42 73.61 o 9 2 1 74.98 127.95 33.66 o -9 3 1 102.06 102.85 18.73 o -8 3 1 1.39 9.36 12.97 o -7 3 1 344.79 347.99 30.46 o -6 3 1 619.85 703.17 25.45 o -5 3 1 115.50 112.99 12.61 o -4 3 1 4023.46 3988.50 69.49 o -3 3 1 12467.19 13680.40 223.05 o -2 3 1 2671.80 2815.05 62.27 o -1 3 1 3451.70 3529.55 58.54 o 0 3 1 1274.19 1362.28 27.96 o 1 3 1 87.83 93.08 4.50 o 2 3 1 2731.35 2633.54 46.40 o 3 3 1 2066.82 2203.52 41.04 o 4 3 1 10083.76 9979.20 166.87 o 5 3 1 185.87 208.80 20.32 o 6 3 1 3053.93 2870.35 70.82 o 7 3 1 2.37 -2.42 10.94 o 8 3 1 58.38 55.97 18.17 o 9 3 1 26.18 60.66 20.34 o -9 4 1 111.75 116.82 23.69 o -8 4 1 391.91 339.23 29.22 o -7 4 1 50.97 52.76 12.16 o -6 4 1 220.31 213.91 18.12 o -5 4 1 1185.72 1138.13 34.84 o -4 4 1 166.34 167.69 14.12 o -3 4 1 4378.52 4488.24 82.49 o -2 4 1 589.44 585.30 13.97 o -1 4 1 298.40 269.94 6.87 o 0 4 1 9013.01 9319.26 173.35 o 1 4 1 12838.29 13381.87 216.91 o 2 4 1 151.02 138.85 6.34 o 3 4 1 1970.08 1951.57 36.95 o 4 4 1 12.64 24.05 5.43 o 5 4 1 476.97 461.26 20.35 o 6 4 1 390.98 436.21 29.30 o 7 4 1 33.77 32.97 13.12 o 8 4 1 280.55 293.85 26.94 o 9 4 1 1.71 22.28 13.72 o -9 5 1 375.56 322.03 29.15 o -8 5 1 202.03 258.72 26.46 o -7 5 1 870.75 873.96 43.50 o -6 5 1 49.83 57.26 13.63 o -5 5 1 1615.92 1597.97 48.81 o -4 5 1 38.01 46.83 5.51 o -3 5 1 206.70 183.12 13.18 o -2 5 1 159.62 166.24 6.96 o -1 5 1 170.36 166.03 8.37 o 0 5 1 9683.16 10015.70 163.09 o 1 5 1 14.56 10.24 3.05 o 2 5 1 50.55 50.64 6.39 o 3 5 1 5059.92 5220.55 89.44 o 4 5 1 1195.81 1190.66 26.24 o 5 5 1 1259.13 1281.11 35.43 o 6 5 1 180.12 200.38 15.78 o 7 5 1 480.26 497.92 32.58 o 8 5 1 84.06 76.38 15.60 o 9 5 1 143.68 151.80 30.21 o -9 6 1 1.52 17.08 14.27 o -8 6 1 290.10 275.16 27.07 o -7 6 1 282.39 312.01 22.34 o -6 6 1 2.90 10.17 7.78 o -5 6 1 2656.40 2530.53 82.10 o -4 6 1 93.74 117.16 9.87 o -3 6 1 2447.23 2408.22 51.83 o -2 6 1 334.36 337.87 9.03 o -1 6 1 1609.89 1569.81 30.37 o 0 6 1 4815.69 5021.19 83.57 o 1 6 1 45.61 52.26 4.10 o 2 6 1 1223.04 1262.14 25.30 o 3 6 1 1641.36 1626.28 34.05 o 4 6 1 1479.35 1524.68 34.83 o 5 6 1 1399.13 1303.65 38.41 o 6 6 1 116.80 131.06 13.42 o 7 6 1 51.33 61.48 13.51 o 8 6 1 133.14 154.56 21.03 o -9 7 1 153.14 214.84 55.33 o -8 7 1 391.85 425.42 53.65 o -7 7 1 410.04 437.30 23.29 o -6 7 1 2714.32 2712.79 87.23 o -5 7 1 439.75 402.22 21.19 o -4 7 1 6545.49 6653.65 132.63 o -3 7 1 2180.04 2199.93 48.26 o -2 7 1 5415.41 5516.70 92.37 o -1 7 1 4071.46 3971.13 72.09 o 0 7 1 2393.94 2388.29 41.82 o 1 7 1 1765.12 1903.84 34.52 o 2 7 1 450.97 428.60 11.53 o 3 7 1 145.93 212.95 8.58 o 4 7 1 1991.82 2156.61 45.91 o 5 7 1 47.03 33.58 8.96 o 6 7 1 350.16 353.55 20.43 o 7 7 1 491.52 513.93 26.15 o 8 7 1 73.32 103.13 18.63 o -9 8 1 109.90 131.02 21.69 o -8 8 1 892.57 910.41 47.08 o -7 8 1 505.95 475.97 27.82 o -6 8 1 611.79 594.58 25.29 o -5 8 1 6.81 18.15 9.24 o -4 8 1 4.80 -5.94 5.59 o -3 8 1 4.14 3.83 5.62 o -2 8 1 2475.18 2419.45 43.21 o -1 8 1 990.93 1003.13 21.69 o 0 8 1 4099.30 4022.11 68.42 o 1 8 1 7588.59 8370.85 138.38 o 2 8 1 3034.19 3169.35 55.99 o 3 8 1 776.81 775.39 20.64 o 4 8 1 107.54 122.12 11.25 o 5 8 1 269.24 295.43 17.98 o 6 8 1 159.16 147.16 14.60 o 7 8 1 372.68 376.10 23.02 o 8 8 1 410.41 463.03 34.12 o -9 9 1 52.32 54.56 17.29 o -8 9 1 273.74 240.89 22.45 o -7 9 1 343.08 314.79 23.14 o -6 9 1 2521.05 2376.56 58.29 o -5 9 1 35.04 27.04 9.49 o -4 9 1 5601.56 5451.39 111.12 o -3 9 1 580.91 682.57 20.13 o -2 9 1 3809.15 3922.10 67.79 o -1 9 1 93.69 87.56 5.57 o 0 9 1 14.31 17.06 3.41 o 1 9 1 1516.55 1551.14 29.65 o 2 9 1 3170.27 3431.72 60.48 o 3 9 1 11.22 20.69 5.76 o 4 9 1 68.10 77.82 11.57 o 5 9 1 58.25 64.98 10.59 o 6 9 1 270.41 306.04 21.87 o 7 9 1 356.56 325.62 24.95 o 8 9 1 116.18 160.71 24.56 o -9 10 1 25.41 47.82 17.32 o -8 10 1 249.72 269.08 23.60 o -7 10 1 152.40 179.47 16.40 o -6 10 1 164.75 159.11 14.78 o -5 10 1 2246.03 2001.79 54.05 o -4 10 1 85.00 68.60 13.86 o -3 10 1 3633.93 3294.25 63.37 o -2 10 1 57.83 63.32 7.29 o -1 10 1 2928.81 3188.58 60.16 o 0 10 1 120.33 119.47 9.57 o 1 10 1 139.57 145.10 8.41 o 2 10 1 19.89 42.02 5.10 o 3 10 1 34.81 44.67 6.80 o 4 10 1 406.55 449.85 22.37 o 5 10 1 36.54 62.22 10.59 o 6 10 1 1.14 0.95 8.35 o 7 10 1 23.40 23.26 11.03 o 8 10 1 13.58 10.10 16.70 o -9 11 1 775.34 755.80 54.63 o -8 11 1 30.07 42.68 14.25 o -7 11 1 822.63 823.64 45.47 o -6 11 1 54.09 54.65 10.51 o -5 11 1 424.33 376.50 21.74 o -4 11 1 93.42 119.37 15.25 o -3 11 1 1203.83 1222.80 28.25 o -2 11 1 90.44 117.52 7.04 o -1 11 1 5580.20 5700.93 103.72 o 0 11 1 672.02 821.80 21.47 o 1 11 1 2524.38 2419.72 44.44 o 2 11 1 210.28 245.48 9.71 o 3 11 1 630.61 635.11 19.62 o 4 11 1 150.97 143.49 12.82 o 5 11 1 1253.89 1230.14 36.66 o 6 11 1 355.89 334.45 23.07 o 7 11 1 4.95 -0.16 10.54 o 8 11 1 47.35 45.99 19.54 o -9 12 1 22.73 49.50 33.05 o -8 12 1 162.85 166.82 19.82 o -7 12 1 527.04 533.17 27.48 o -6 12 1 18.47 23.00 9.40 o -5 12 1 3086.16 2738.26 70.02 o -4 12 1 50.57 45.72 9.13 o -3 12 1 4328.12 4485.06 84.71 o -2 12 1 2075.47 1904.58 36.90 o -1 12 1 2571.64 2474.41 49.03 o 0 12 1 3503.51 3666.28 64.64 o 1 12 1 120.45 141.52 7.75 o 2 12 1 389.26 357.12 12.25 o 3 12 1 10.84 14.58 6.08 o 4 12 1 269.74 240.69 16.24 o 5 12 1 2.32 8.74 8.44 o 6 12 1 153.88 159.34 17.37 o 7 12 1 74.55 53.85 13.73 o 8 12 1 116.49 137.15 23.84 o -8 13 1 8.35 24.70 12.82 o -7 13 1 370.75 380.94 23.82 o -6 13 1 1042.36 985.17 32.89 o -5 13 1 331.40 368.38 20.38 o -4 13 1 292.57 300.97 32.15 o -3 13 1 512.87 549.22 20.55 o -2 13 1 2367.01 2386.97 45.17 o -1 13 1 663.15 718.13 22.45 o 0 13 1 42.28 52.76 5.56 o 1 13 1 25.28 17.12 6.16 o 2 13 1 3464.32 3355.50 65.77 o 3 13 1 156.51 145.84 11.99 o 4 13 1 290.63 291.21 23.85 o 5 13 1 76.92 88.06 13.31 o 6 13 1 237.95 277.33 22.16 o 7 13 1 98.10 79.80 19.53 o 8 13 1 151.15 155.30 28.66 o -8 14 1 261.50 236.73 27.56 o -7 14 1 85.02 103.81 16.04 o -6 14 1 277.02 287.26 19.95 o -5 14 1 186.68 189.66 15.32 o -4 14 1 12.39 15.68 8.49 o -3 14 1 9.41 7.62 6.62 o -2 14 1 3510.42 3606.17 65.30 o -1 14 1 2769.54 2933.36 58.02 o 0 14 1 798.47 766.21 20.42 o 1 14 1 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