#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:10:02 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180973 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/53/2205373.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205373_Fobs loop_ _publ_author_name 'Burrows, Andrew D.' 'Harrington, Ross W.' 'Mahon, Mary F.' _publ_section_title ; Diaquabis(1,1,4-trimethylthiosemicarbazide)nickel(II) dinitrate ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m551 _journal_page_last m553 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 117.767 _cell_angle_gamma 90.000 _cell_length_a 9.4640 _cell_length_b 12.3580 _cell_length_c 9.7750 _exptl_crystal_F_000 508.00 _reflns_d_resolution_high 0.7699 _cod_data_source_file wk6043Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' K00rwh14' _shelx_refln_list_code 4 _shelx_f_calc_maximum 147.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 393.22 337.82 10.94 o 3 0 0 5086.47 4842.53 109.55 o 4 0 0 6676.24 6870.57 141.41 o 5 0 0 1676.26 1663.61 33.18 o 6 0 0 93.58 82.26 3.17 o 7 0 0 96.79 100.89 2.98 o 8 0 0 71.51 73.69 3.07 o 9 0 0 128.74 119.65 4.72 o 10 0 0 48.90 50.61 4.79 o 2 1 0 3361.09 3305.66 89.12 o 3 1 0 610.31 635.36 10.48 o 4 1 0 1003.01 1018.51 14.88 o 5 1 0 199.17 202.37 3.00 o 6 1 0 345.94 351.46 4.71 o 7 1 0 35.54 36.21 1.15 o 8 1 0 1.47 1.21 1.27 o 9 1 0 17.41 17.98 1.31 o 10 1 0 0.75 0.62 1.17 o 2 2 0 335.01 324.56 5.06 o 3 2 0 6619.45 6793.22 109.98 o 4 2 0 3411.59 3365.59 51.20 o 5 2 0 763.36 708.81 10.40 o 6 2 0 1421.58 1448.25 20.86 o 7 2 0 325.41 335.04 5.86 o 8 2 0 149.94 141.59 3.74 o 9 2 0 166.03 173.94 5.28 o 10 2 0 28.91 29.09 3.20 o 1 3 0 1911.82 1868.95 30.84 o 2 3 0 4954.82 4736.63 77.29 o 3 3 0 580.19 645.44 9.88 o 4 3 0 274.71 266.98 4.27 o 5 3 0 62.39 57.51 2.16 o 6 3 0 388.61 397.11 6.13 o 7 3 0 204.10 222.36 4.78 o 8 3 0 3.34 1.99 0.88 o 9 3 0 112.09 101.91 3.27 o 10 3 0 6.28 3.20 1.45 o 0 4 0 8689.08 8898.56 292.84 o 1 4 0 3326.66 3206.98 51.25 o 2 4 0 14314.88 14420.74 328.67 o 3 4 0 6189.29 6369.23 93.58 o 4 4 0 1156.95 1096.55 15.17 o 5 4 0 331.81 320.00 4.75 o 6 4 0 463.60 488.51 8.24 o 7 4 0 7.95 5.67 1.35 o 8 4 0 98.18 92.92 2.33 o 9 4 0 131.71 120.23 3.61 o 10 4 0 53.77 45.78 2.55 o 1 5 0 396.37 353.35 5.64 o 2 5 0 200.14 224.41 3.52 o 3 5 0 96.60 94.25 1.68 o 4 5 0 19.78 11.66 0.74 o 5 5 0 153.77 150.70 2.59 o 6 5 0 119.17 138.76 2.65 o 7 5 0 170.80 161.06 3.23 o 8 5 0 232.73 242.33 5.58 o 9 5 0 196.70 181.25 5.21 o 10 5 0 163.12 157.37 7.75 o 0 6 0 1784.52 1753.09 43.77 o 1 6 0 2406.27 2273.12 36.35 o 2 6 0 1910.94 1830.21 28.93 o 3 6 0 2599.13 2518.79 33.52 o 4 6 0 1412.51 1378.55 19.37 o 5 6 0 675.24 647.07 9.82 o 6 6 0 207.29 232.53 4.89 o 7 6 0 1007.01 1025.45 20.31 o 8 6 0 183.61 177.95 4.30 o 9 6 0 7.92 9.77 1.32 o 10 6 0 1.56 1.64 1.42 o 1 7 0 127.01 120.71 2.37 o 2 7 0 291.08 281.99 4.61 o 3 7 0 542.28 541.68 9.11 o 4 7 0 1086.25 1093.30 14.44 o 5 7 0 1237.46 1269.52 18.35 o 6 7 0 6.36 6.50 0.82 o 7 7 0 0.04 1.29 0.83 o 8 7 0 510.96 514.35 12.45 o 9 7 0 5.03 3.41 1.25 o 0 8 0 2056.91 2118.06 50.83 o 1 8 0 2539.79 2598.28 46.03 o 2 8 0 1942.71 1929.49 30.66 o 3 8 0 1037.70 1021.25 18.04 o 4 8 0 309.57 325.39 5.89 o 5 8 0 309.55 328.42 5.31 o 6 8 0 629.48 629.67 12.75 o 7 8 0 323.89 321.38 7.76 o 8 8 0 160.63 152.78 5.04 o 9 8 0 2.11 1.80 1.78 o 1 9 0 370.45 372.00 6.54 o 2 9 0 30.63 28.01 2.03 o 3 9 0 823.96 835.32 15.61 o 4 9 0 833.58 850.78 14.69 o 5 9 0 101.03 93.16 2.72 o 6 9 0 150.33 143.24 3.55 o 7 9 0 157.33 153.57 4.37 o 8 9 0 77.37 82.62 4.32 o 9 9 0 32.92 27.55 4.16 o 0 10 0 259.66 268.61 7.22 o 1 10 0 517.18 542.72 10.51 o 2 10 0 508.06 492.46 11.04 o 3 10 0 222.31 213.86 4.87 o 4 10 0 1094.08 1109.46 26.30 o 5 10 0 456.16 427.99 10.30 o 6 10 0 262.74 273.37 6.20 o 7 10 0 350.47 336.08 10.44 o 8 10 0 206.34 203.13 9.97 o 1 11 0 118.43 110.65 2.62 o 2 11 0 342.89 349.03 9.15 o 3 11 0 63.24 55.10 2.97 o 4 11 0 412.28 427.40 9.21 o 5 11 0 461.97 495.67 11.65 o 6 11 0 65.28 65.51 3.35 o 7 11 0 138.81 142.94 6.59 o 0 12 0 141.98 154.11 7.85 o 1 12 0 198.44 196.53 4.40 o 2 12 0 533.03 536.02 17.55 o 3 12 0 392.68 413.05 13.11 o 4 12 0 35.93 33.85 2.29 o 5 12 0 485.40 484.05 15.62 o 6 12 0 92.91 82.83 3.60 o 7 12 0 149.22 142.94 9.93 o 1 13 0 452.19 465.67 11.75 o 2 13 0 8.28 5.26 1.57 o 3 13 0 36.60 34.50 2.21 o 4 13 0 17.69 11.58 3.89 o 5 13 0 20.38 19.08 2.48 o 6 13 0 172.36 216.71 33.74 o 0 14 0 5.83 6.14 3.20 o 1 14 0 105.65 97.00 4.02 o 2 14 0 134.75 123.36 10.55 o 3 14 0 3.76 6.27 2.24 o 4 14 0 204.19 196.92 21.03 o 5 14 0 127.66 113.93 12.99 o 1 15 0 65.05 58.98 8.43 o 2 15 0 81.43 60.25 7.48 o 3 15 0 0.95 4.41 2.22 o 0 16 0 36.13 25.00 5.35 o -11 1 1 109.26 104.34 5.32 o -10 1 1 37.16 34.04 2.40 o -9 1 1 123.13 119.31 3.11 o -8 1 1 18.70 20.33 1.19 o -7 1 1 6.51 5.61 1.04 o -6 1 1 101.00 102.53 1.70 o -5 1 1 826.42 787.49 10.58 o -4 1 1 539.33 572.95 8.14 o -3 1 1 8.44 5.60 0.57 o -2 1 1 628.73 611.23 11.10 o 2 1 1 593.32 599.89 12.22 o 3 1 1 3906.42 3703.09 59.96 o 4 1 1 8302.92 8438.45 130.46 o 5 1 1 4780.79 4797.22 74.15 o 6 1 1 1456.05 1449.44 21.81 o 7 1 1 1693.69 1743.18 34.20 o 8 1 1 428.40 452.71 10.48 o 9 1 1 150.40 155.43 5.68 o 10 1 1 307.52 312.26 12.81 o -11 2 1 46.55 48.86 3.04 o -10 2 1 3.27 2.72 1.41 o -9 2 1 486.25 499.30 12.95 o -8 2 1 30.04 23.74 1.03 o -7 2 1 63.55 64.65 1.45 o -6 2 1 305.73 307.38 4.21 o -5 2 1 440.56 453.46 6.05 o -4 2 1 402.99 418.06 6.81 o -3 2 1 3654.66 3665.95 54.51 o -2 2 1 105.87 103.84 2.25 o -1 2 1 703.61 606.91 13.95 o 0 2 1 240.93 228.61 8.77 o 1 2 1 4276.74 4221.58 84.39 o 2 2 1 797.01 811.59 14.76 o 3 2 1 272.41 299.69 4.73 o 4 2 1 80.05 65.62 1.50 o 5 2 1 41.63 28.86 1.16 o 6 2 1 307.86 302.79 5.64 o 7 2 1 12.45 14.20 1.19 o 8 2 1 3.48 2.17 0.91 o 9 2 1 1.11 1.27 1.49 o 10 2 1 185.95 188.18 12.50 o -11 3 1 87.94 78.47 4.75 o -10 3 1 71.92 66.92 2.90 o -9 3 1 348.98 351.00 10.01 o -8 3 1 92.41 96.15 2.89 o -7 3 1 71.68 65.99 1.64 o -6 3 1 183.24 201.73 3.27 o -5 3 1 289.99 294.39 4.63 o -4 3 1 1304.18 1310.11 18.93 o -3 3 1 1802.96 1776.65 25.80 o -2 3 1 2916.28 2787.12 48.71 o -1 3 1 1325.90 1277.89 20.70 o 0 3 1 606.96 616.20 10.00 o 2 3 1 3518.25 3333.29 56.95 o 3 3 1 1480.05 1454.44 21.62 o 4 3 1 7789.88 7817.65 110.87 o 5 3 1 2589.15 2539.81 35.18 o 6 3 1 1632.71 1653.54 25.59 o 7 3 1 458.92 481.09 9.35 o 8 3 1 1086.61 1126.48 30.28 o 9 3 1 565.86 578.69 22.88 o 10 3 1 61.86 54.50 4.04 o -10 4 1 241.12 228.55 10.24 o -9 4 1 49.94 50.22 2.13 o -8 4 1 60.27 64.92 2.07 o -7 4 1 19.37 26.27 1.21 o -6 4 1 77.16 79.55 1.86 o -5 4 1 1.18 1.39 0.67 o -4 4 1 61.50 60.82 1.25 o -3 4 1 2.41 0.74 0.80 o -2 4 1 6400.91 6620.85 109.95 o -1 4 1 292.13 272.03 5.44 o 0 4 1 49.72 59.73 1.25 o 1 4 1 46.32 46.92 0.90 o 2 4 1 309.71 303.84 4.69 o 3 4 1 533.40 541.24 7.98 o 4 4 1 5.56 4.05 0.77 o 5 4 1 186.12 185.00 2.88 o 6 4 1 151.79 145.13 3.20 o 7 4 1 39.43 43.94 1.48 o 8 4 1 12.78 12.33 1.01 o 9 4 1 397.73 411.80 13.47 o 10 4 1 15.46 12.87 2.35 o -10 5 1 159.34 147.42 6.21 o -9 5 1 522.80 507.62 13.47 o -8 5 1 12.91 9.91 1.06 o -7 5 1 2.79 5.82 1.62 o -6 5 1 2.27 4.01 0.74 o -5 5 1 794.20 828.11 10.97 o -4 5 1 310.33 347.21 4.73 o -3 5 1 2458.15 2468.26 36.89 o -2 5 1 3183.61 3265.48 61.19 o -1 5 1 960.34 908.94 16.21 o 0 5 1 81.46 86.38 1.65 o 1 5 1 4060.30 3845.95 54.98 o 2 5 1 10626.41 10951.61 153.79 o 3 5 1 3980.17 3984.08 58.74 o 4 5 1 457.78 442.28 6.09 o 5 5 1 1775.00 1785.77 25.71 o 6 5 1 1213.75 1228.67 21.47 o 7 5 1 1386.60 1475.52 28.69 o 8 5 1 301.34 309.17 7.77 o 9 5 1 221.51 202.82 8.74 o -10 6 1 145.87 134.01 6.37 o -9 6 1 171.72 174.06 4.42 o -8 6 1 7.43 5.83 0.88 o -7 6 1 14.70 16.69 0.94 o -6 6 1 24.70 16.29 0.92 o -5 6 1 13.41 12.48 1.06 o -4 6 1 14.34 22.55 1.06 o -3 6 1 676.96 650.24 9.68 o -2 6 1 1495.09 1535.13 25.55 o -1 6 1 1001.98 980.83 17.32 o 0 6 1 55.76 71.08 1.62 o 1 6 1 1470.87 1383.14 20.11 o 2 6 1 574.65 578.69 7.90 o 3 6 1 15.56 15.50 1.04 o 4 6 1 10.68 11.17 0.68 o 5 6 1 52.69 58.64 2.07 o 6 6 1 18.61 17.93 1.39 o 7 6 1 69.50 66.73 2.43 o 8 6 1 601.12 639.81 16.42 o 9 6 1 141.95 142.28 6.19 o -10 7 1 12.88 10.52 1.92 o -9 7 1 5.69 7.46 1.56 o -8 7 1 500.27 486.49 14.38 o -7 7 1 167.76 154.19 4.02 o -6 7 1 225.10 254.37 5.15 o -5 7 1 134.73 152.33 2.85 o -4 7 1 919.33 883.71 13.33 o -3 7 1 62.67 52.53 3.65 o -2 7 1 1007.99 989.20 16.96 o -1 7 1 569.02 565.74 8.24 o 0 7 1 2871.01 2886.81 47.94 o 1 7 1 780.54 764.87 12.78 o 2 7 1 1763.72 1645.23 22.76 o 3 7 1 967.58 896.58 12.97 o 4 7 1 1151.93 1183.13 17.09 o 5 7 1 1106.17 1096.22 18.21 o 6 7 1 1294.46 1317.91 28.42 o 7 7 1 718.84 737.57 18.65 o 8 7 1 468.86 483.18 13.48 o 9 7 1 68.82 56.63 3.97 o -9 8 1 150.48 141.46 5.92 o -8 8 1 50.28 48.39 1.58 o -7 8 1 182.85 187.21 4.51 o -6 8 1 66.20 62.86 1.73 o -5 8 1 217.63 227.98 4.37 o -4 8 1 761.69 788.51 14.08 o -3 8 1 412.11 414.40 7.61 o -2 8 1 21.23 25.89 0.83 o -1 8 1 426.84 442.82 7.43 o 0 8 1 2006.97 1965.71 32.37 o 1 8 1 717.30 719.50 13.31 o 2 8 1 459.01 456.51 6.22 o 3 8 1 155.29 151.14 2.57 o 4 8 1 45.66 50.78 1.35 o 5 8 1 136.99 123.04 2.49 o 6 8 1 43.00 41.13 1.34 o 7 8 1 3.36 5.92 0.99 o 8 8 1 96.52 97.85 3.45 o -9 9 1 17.01 15.17 2.00 o -8 9 1 8.58 5.55 1.19 o -7 9 1 643.02 615.38 17.43 o -6 9 1 246.17 248.11 6.23 o -5 9 1 80.98 93.76 2.44 o -4 9 1 374.47 372.29 7.22 o -3 9 1 504.78 504.91 8.90 o -2 9 1 251.96 268.24 4.15 o -1 9 1 2745.09 2894.11 47.77 o 0 9 1 433.95 437.97 8.59 o 1 9 1 1398.26 1436.08 24.69 o 2 9 1 313.20 317.65 6.59 o 3 9 1 894.43 901.88 18.61 o 4 9 1 882.82 878.93 15.66 o 5 9 1 343.15 355.64 6.80 o 6 9 1 254.68 246.75 6.44 o 7 9 1 229.24 233.24 6.48 o 8 9 1 333.20 308.30 14.45 o -8 10 1 149.97 157.87 7.51 o -7 10 1 1.08 4.05 1.03 o -6 10 1 12.31 13.41 1.22 o -5 10 1 20.64 19.24 1.59 o -4 10 1 283.81 278.17 6.29 o -3 10 1 98.43 90.52 2.21 o -2 10 1 138.01 146.73 4.19 o -1 10 1 27.64 28.68 1.69 o 0 10 1 720.47 707.27 13.41 o 1 10 1 1470.62 1480.87 28.28 o 2 10 1 23.03 24.42 1.85 o 3 10 1 259.56 251.55 6.49 o 4 10 1 15.44 12.07 0.98 o 5 10 1 0.27 0.30 0.47 o 6 10 1 47.32 42.02 1.69 o 7 10 1 27.58 28.82 1.80 o 8 10 1 100.11 96.05 10.14 o -8 11 1 61.14 60.68 5.73 o -7 11 1 236.84 248.30 8.98 o -6 11 1 509.15 511.32 14.06 o -5 11 1 645.18 666.70 15.78 o -4 11 1 367.93 368.25 9.06 o -3 11 1 288.52 292.69 6.93 o -2 11 1 1022.95 1048.99 29.95 o -1 11 1 375.56 379.55 8.23 o 0 11 1 328.66 326.72 7.28 o 1 11 1 23.98 20.76 1.26 o 2 11 1 689.51 710.37 16.92 o 3 11 1 547.64 534.58 17.06 o 4 11 1 209.54 201.42 5.64 o 5 11 1 315.01 293.50 8.74 o 6 11 1 60.41 56.95 2.80 o 7 11 1 121.85 119.20 6.21 o -7 12 1 4.76 3.69 1.98 o -6 12 1 62.82 60.96 3.79 o -5 12 1 24.84 23.37 1.90 o -4 12 1 1.50 1.41 1.57 o -3 12 1 770.61 766.82 24.07 o -2 12 1 494.61 492.49 13.62 o -1 12 1 278.26 289.75 6.83 o 0 12 1 239.00 249.75 5.80 o 1 12 1 79.14 83.69 2.92 o 2 12 1 97.60 95.76 4.05 o 3 12 1 11.17 7.87 1.32 o 4 12 1 93.24 84.19 3.37 o 5 12 1 0.35 -0.31 1.19 o 6 12 1 42.33 40.25 2.04 o -6 13 1 217.44 245.49 19.60 o -5 13 1 309.82 332.41 17.42 o -4 13 1 407.12 398.45 17.18 o -3 13 1 203.18 195.27 7.91 o -2 13 1 291.91 301.38 10.51 o -1 13 1 997.93 1039.07 25.49 o 0 13 1 174.39 173.39 4.82 o 1 13 1 139.63 142.99 4.81 o 2 13 1 149.27 145.87 5.01 o 3 13 1 163.22 143.84 7.06 o 4 13 1 46.49 37.78 3.98 o 5 13 1 20.32 11.26 4.83 o -5 14 1 0.87 2.50 2.94 o -4 14 1 11.94 9.87 4.48 o -3 14 1 13.40 14.11 3.31 o -2 14 1 35.60 26.15 2.64 o -1 14 1 213.34 216.57 5.88 o 0 14 1 253.81 255.88 7.43 o 1 14 1 3.96 2.72 1.44 o 2 14 1 9.19 6.25 2.40 o 3 14 1 349.74 349.49 27.07 o 4 14 1 157.35 132.58 11.40 o -4 15 1 292.39 269.85 29.12 o -3 15 1 173.34 183.50 22.93 o -2 15 1 273.99 270.84 22.85 o -1 15 1 203.95 198.87 12.68 o 0 15 1 54.68 61.82 5.20 o 1 15 1 16.85 16.44 5.61 o 2 15 1 60.58 47.69 6.94 o 3 15 1 22.81 17.22 4.94 o -11 0 2 1050.03 1113.15 55.44 o -10 0 2 666.14 712.88 19.84 o -9 0 2 3.74 3.83 1.07 o -8 0 2 3945.24 4110.37 106.38 o -7 0 2 1636.08 1634.58 34.49 o -6 0 2 222.30 234.52 5.39 o -5 0 2 251.42 217.15 4.85 o -4 0 2 699.09 700.71 17.13 o -3 0 2 535.26 526.56 12.27 o -2 0 2 3426.96 3460.95 182.71 o -1 0 2 10.44 19.76 0.96 o 0 0 2 4472.21 4435.80 123.66 o 1 0 2 7.38 7.90 1.17 o 2 0 2 1047.06 1005.73 23.32 o 3 0 2 96.68 70.14 2.47 o 4 0 2 1022.00 987.53 23.29 o 5 0 2 4415.15 4572.02 107.36 o 6 0 2 674.29 655.16 17.75 o 7 0 2 775.71 776.76 30.42 o 8 0 2 875.56 943.35 29.42 o 9 0 2 689.94 729.69 34.72 o -11 1 2 75.37 69.18 3.35 o -10 1 2 55.54 50.05 1.97 o -9 1 2 21.42 18.77 1.25 o -8 1 2 251.41 245.79 4.50 o -7 1 2 283.64 268.91 4.26 o -6 1 2 77.57 74.83 1.50 o -5 1 2 327.84 332.62 4.86 o -4 1 2 7.29 15.75 0.79 o -3 1 2 90.60 104.59 1.94 o -2 1 2 4534.06 4591.78 112.85 o -1 1 2 58.38 63.02 1.08 o 0 1 2 665.53 697.25 14.19 o 1 1 2 966.37 922.32 15.31 o 2 1 2 4038.12 4065.12 82.42 o 3 1 2 98.14 99.46 1.89 o 4 1 2 638.55 611.85 9.40 o 5 1 2 111.95 111.55 2.35 o 6 1 2 0.66 0.97 0.82 o 7 1 2 79.85 76.69 2.19 o 8 1 2 66.24 57.99 2.46 o 9 1 2 61.43 55.70 3.46 o -11 2 2 943.18 1000.06 44.47 o -10 2 2 134.91 130.35 4.04 o -9 2 2 1557.04 1611.58 35.29 o -8 2 2 861.66 872.68 15.11 o -7 2 2 1394.62 1371.37 19.67 o -6 2 2 589.25 573.36 7.72 o -5 2 2 1356.98 1389.63 18.81 o -4 2 2 870.42 806.59 12.28 o -3 2 2 232.95 251.89 3.88 o -2 2 2 90.19 100.23 1.75 o -1 2 2 2612.17 2527.60 40.32 o 0 2 2 7035.25 7067.97 114.13 o 1 2 2 81.76 79.26 1.41 o 2 2 2 473.63 465.60 8.11 o 3 2 2 487.31 473.59 7.50 o 4 2 2 1956.55 1954.40 29.74 o 5 2 2 966.01 932.61 14.83 o 6 2 2 1730.55 1750.16 32.16 o 7 2 2 1516.50 1561.51 33.38 o 8 2 2 1014.87 1077.05 25.44 o 9 2 2 553.25 603.61 25.84 o -11 3 2 0.09 1.20 1.55 o -10 3 2 0.01 -1.16 1.16 o -9 3 2 349.59 350.16 7.15 o -8 3 2 373.60 383.45 7.01 o -7 3 2 135.90 142.45 4.35 o -6 3 2 361.73 353.75 5.31 o -5 3 2 419.28 440.07 6.74 o -4 3 2 312.50 341.55 5.11 o -3 3 2 216.02 235.59 3.54 o -2 3 2 2957.57 2779.99 43.01 o -1 3 2 73.87 68.75 2.79 o 0 3 2 4854.84 4810.76 72.53 o 1 3 2 3115.34 3011.01 46.13 o 2 3 2 790.22 845.24 13.45 o 3 3 2 390.55 416.71 6.46 o 4 3 2 443.79 469.13 6.59 o 5 3 2 12.35 9.89 0.94 o 6 3 2 74.60 87.99 2.27 o 7 3 2 96.62 88.63 2.70 o 8 3 2 42.76 39.46 1.94 o 9 3 2 5.03 3.30 1.55 o -11 4 2 496.31 524.20 21.27 o -10 4 2 930.97 984.67 30.44 o -9 4 2 699.37 688.62 19.12 o -8 4 2 1595.64 1659.20 36.72 o -7 4 2 34.49 36.07 1.30 o -6 4 2 22.71 18.62 1.80 o -5 4 2 491.51 535.91 7.32 o -4 4 2 1378.09 1418.58 20.30 o -3 4 2 124.80 115.35 1.81 o -2 4 2 683.63 647.15 10.66 o -1 4 2 651.06 644.24 10.07 o 0 4 2 278.23 232.11 3.46 o 1 4 2 2115.44 2118.01 30.20 o 2 4 2 2689.58 2755.75 41.88 o 3 4 2 1050.07 1058.68 15.91 o 4 4 2 98.82 91.32 2.22 o 5 4 2 1013.35 1047.07 16.14 o 6 4 2 1135.08 1139.86 23.54 o 7 4 2 503.38 498.47 11.41 o 8 4 2 705.21 767.46 17.84 o 9 4 2 629.29 642.38 28.64 o -11 5 2 3.32 5.85 1.31 o -10 5 2 13.61 13.32 1.74 o -9 5 2 42.49 43.57 2.89 o -8 5 2 32.45 31.02 1.68 o -7 5 2 17.59 19.61 1.02 o -6 5 2 240.25 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