#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:10:02 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180973 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/53/2205381.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205381_Fobs loop_ _publ_author_name 'K\?ir\?ilm\?i\,s, Cumhur' 'Koca, Murat' 'Ar\?ic\?i, Cengiz' 'Heinemann, Frank W.' 'Ahmedzade, Misir' _publ_section_title ; 3-Butyl-4-(3-methyl-3-phenylcyclobut-1-yl)-1,3-thiazole-2(3H)-thione ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o555 _journal_page_last o556 _journal_volume 61 _journal_year 2005 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.9080 _cell_length_b 10.4420 _cell_length_c 16.6030 _exptl_crystal_F_000 680.00 _reflns_d_resolution_high 0.7695 _cod_data_source_file wn6325Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CK0401 in P2(1)2(1)2(1), C.KRILMIS, Firat Univ, MC1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 130.02 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13141.52 11671.19 495.42 o 4 0 0 6459.19 7056.23 87.82 o 6 0 0 2396.56 2651.60 41.31 o 8 0 0 6317.40 5942.98 70.15 o 10 0 0 25.30 -12.33 18.71 o 12 0 0 2884.12 2865.86 89.51 o 2 1 0 221.24 238.07 13.00 o 3 1 0 7997.00 7803.27 61.64 o 4 1 0 4.64 -5.48 5.48 o 5 1 0 3538.11 3603.83 35.65 o 6 1 0 1948.64 1944.16 23.34 o 7 1 0 15.30 29.99 8.43 o 8 1 0 34.38 26.49 8.75 o 9 1 0 235.87 268.17 12.49 o 10 1 0 44.85 36.06 13.76 o 11 1 0 317.21 321.69 21.55 o 12 1 0 332.66 404.23 94.84 o 0 2 0 3763.49 3518.96 88.13 o 2 2 0 2574.36 2570.44 35.15 o 3 2 0 1647.69 1638.60 15.69 o 4 2 0 146.37 207.11 9.78 o 5 2 0 391.43 383.09 10.15 o 6 2 0 841.79 910.67 19.26 o 7 2 0 183.90 208.19 8.68 o 8 2 0 550.27 534.05 12.86 o 9 2 0 231.62 279.03 12.80 o 10 2 0 198.95 210.32 15.50 o 11 2 0 704.32 660.43 24.64 o 12 2 0 24.47 39.78 21.72 o 1 3 0 1353.83 1410.36 12.55 o 2 3 0 1159.49 1135.59 16.38 o 3 3 0 448.82 463.45 9.72 o 4 3 0 494.88 550.91 19.45 o 5 3 0 850.35 919.26 15.11 o 6 3 0 2777.36 2583.00 27.41 o 7 3 0 92.10 112.02 8.03 o 8 3 0 599.85 587.25 13.35 o 9 3 0 11.90 -2.10 12.64 o 10 3 0 136.22 163.80 17.17 o 11 3 0 2.26 -6.38 17.15 o 12 3 0 69.28 43.78 64.58 o 0 4 0 902.99 805.20 11.64 o 1 4 0 36.17 43.73 4.40 o 2 4 0 0.19 7.83 4.31 o 3 4 0 7021.99 7177.67 69.23 o 4 4 0 61.32 87.05 9.51 o 5 4 0 1117.36 1134.74 21.38 o 6 4 0 335.18 335.49 14.88 o 7 4 0 5.54 9.27 13.38 o 8 4 0 612.23 593.10 15.18 o 9 4 0 293.47 272.74 10.85 o 10 4 0 155.15 196.71 14.28 o 11 4 0 227.81 224.91 25.47 o 1 5 0 452.35 481.70 7.54 o 2 5 0 2103.11 2264.51 20.76 o 3 5 0 3564.02 3433.66 33.53 o 4 5 0 785.44 768.19 15.25 o 5 5 0 660.27 650.30 15.75 o 6 5 0 1388.09 1406.90 23.78 o 7 5 0 724.63 737.28 19.66 o 8 5 0 176.38 161.67 17.06 o 9 5 0 1945.51 1941.29 35.49 o 10 5 0 276.13 292.51 29.21 o 11 5 0 1.08 158.30 54.42 o 0 6 0 1862.19 1761.40 28.74 o 1 6 0 234.63 218.24 6.46 o 2 6 0 715.14 686.73 10.41 o 3 6 0 1265.22 1354.79 19.21 o 4 6 0 933.42 1009.02 17.81 o 5 6 0 802.30 824.32 18.94 o 6 6 0 282.55 288.09 16.06 o 7 6 0 20.30 16.13 14.66 o 8 6 0 79.40 94.77 17.59 o 9 6 0 0.71 -18.18 18.18 o 10 6 0 6.30 39.08 38.70 o 1 7 0 1500.42 1520.89 17.71 o 2 7 0 18.26 15.23 10.41 o 3 7 0 82.42 100.24 7.27 o 4 7 0 17.30 27.66 8.69 o 5 7 0 127.45 143.49 20.11 o 6 7 0 146.20 161.07 14.87 o 7 7 0 952.80 890.98 30.71 o 8 7 0 12.39 14.88 18.23 o 9 7 0 89.71 113.31 26.73 o 0 8 0 552.28 571.12 20.13 o 1 8 0 3.73 4.52 8.48 o 2 8 0 1105.09 1118.16 15.48 o 3 8 0 540.50 579.72 26.21 o 4 8 0 187.65 197.84 10.02 o 5 8 0 730.56 738.86 18.16 o 6 8 0 535.81 499.66 27.12 o 7 8 0 1.74 20.31 18.89 o 8 8 0 126.19 159.19 21.50 o 9 8 0 460.88 462.49 46.32 o 10 8 0 71.17 44.99 49.80 o 1 9 0 1007.57 952.19 19.11 o 2 9 0 341.46 368.45 23.37 o 3 9 0 112.76 75.03 23.83 o 4 9 0 118.83 136.58 23.60 o 5 9 0 0.33 -1.04 18.28 o 6 9 0 2733.86 2614.59 37.58 o 7 9 0 283.02 293.72 19.55 o 8 9 0 71.32 78.90 30.27 o 0 10 0 556.21 547.80 34.95 o 1 10 0 183.91 207.68 20.81 o 2 10 0 21.95 20.83 9.86 o 3 10 0 793.90 799.01 33.96 o 4 10 0 150.29 139.83 18.67 o 5 10 0 53.67 102.18 19.76 o 6 10 0 18.74 -10.21 34.97 o 7 10 0 41.98 14.51 45.96 o 1 11 0 4.68 14.09 15.64 o 2 11 0 21.32 44.73 23.30 o 3 11 0 270.67 300.06 30.64 o 4 11 0 23.07 17.03 21.42 o 5 11 0 400.54 437.89 34.92 o 6 11 0 0.08 32.10 37.77 o 0 12 0 310.47 256.61 42.88 o 1 12 0 355.55 328.38 21.34 o 2 12 0 15.50 28.55 18.93 o 3 12 0 30.13 82.73 57.00 o 4 12 0 2.96 -12.39 52.84 o 5 12 0 83.10 53.61 62.61 o 1 13 0 1.22 4.39 28.72 o 2 13 0 15.46 6.77 40.92 o 3 13 0 754.02 798.15 66.57 o 2 0 1 3258.55 3246.41 34.03 o 3 0 1 1.33 -6.71 6.71 o 4 0 1 5919.39 5938.42 45.23 o 5 0 1 195.43 237.00 11.62 o 6 0 1 7.41 9.32 6.83 o 7 0 1 820.52 825.38 14.21 o 8 0 1 72.42 106.28 10.93 o 9 0 1 3.92 22.09 13.06 o 10 0 1 5.33 19.02 12.94 o 11 0 1 0.02 -16.15 16.15 o 12 0 1 671.46 712.06 36.05 o -12 1 1 55.18 70.71 26.38 o -11 1 1 0.91 2.63 17.14 o -10 1 1 180.09 215.05 15.54 o -9 1 1 257.56 240.40 13.18 o -8 1 1 763.97 755.26 16.32 o -7 1 1 1073.07 1060.69 17.06 o -6 1 1 72.84 73.78 10.29 o -5 1 1 2449.72 2496.55 22.80 o -4 1 1 473.06 466.16 10.61 o -3 1 1 1106.78 1140.51 11.88 o -2 1 1 2714.82 2654.77 28.11 o 2 1 1 2772.39 2739.67 22.57 o 3 1 1 1097.94 1143.34 12.10 o 4 1 1 504.66 484.25 7.93 o 5 1 1 2477.07 2509.73 24.60 o 6 1 1 70.42 78.95 8.73 o 7 1 1 1053.14 1045.85 16.24 o 8 1 1 741.38 734.53 15.33 o 9 1 1 266.42 260.76 11.52 o 10 1 1 179.32 206.02 17.55 o 11 1 1 0.75 -12.86 17.89 o 12 1 1 57.35 92.15 26.19 o -12 2 1 28.89 17.20 20.52 o -11 2 1 179.03 195.66 16.17 o -10 2 1 509.34 496.61 17.70 o -9 2 1 111.52 113.27 18.12 o -8 2 1 78.52 73.71 14.70 o -7 2 1 283.63 257.47 12.79 o -6 2 1 54.33 35.75 9.41 o -5 2 1 2496.79 2771.66 25.97 o -4 2 1 1075.02 1165.56 13.20 o -3 2 1 387.28 393.39 8.03 o -2 2 1 6217.85 6017.32 50.64 o -1 2 1 15088.17 14556.44 94.22 o 0 2 1 334.27 394.88 8.94 o 1 2 1 14899.95 14283.96 194.06 o 2 2 1 6184.87 5947.25 64.44 o 3 2 1 392.59 383.32 7.34 o 4 2 1 1124.66 1215.82 17.48 o 5 2 1 2454.41 2693.42 26.21 o 6 2 1 55.05 53.78 12.91 o 7 2 1 291.81 266.97 13.49 o 8 2 1 81.20 102.56 10.07 o 9 2 1 106.02 98.01 10.27 o 10 2 1 508.91 521.72 17.05 o 11 2 1 179.85 206.17 21.20 o 12 2 1 28.96 25.22 22.03 o -11 3 1 111.43 103.34 15.79 o -10 3 1 632.82 655.87 18.05 o -9 3 1 59.03 64.35 17.02 o -8 3 1 234.74 227.93 24.96 o -7 3 1 2066.83 2045.02 24.47 o -6 3 1 422.14 418.24 9.06 o -5 3 1 2305.34 2297.97 25.39 o -4 3 1 288.75 309.38 11.31 o -3 3 1 556.95 578.63 17.71 o -2 3 1 1486.72 1414.72 14.14 o -1 3 1 1020.31 996.63 10.62 o 0 3 1 1940.89 1919.90 17.80 o 1 3 1 1026.07 1008.96 13.53 o 2 3 1 1414.87 1363.21 28.80 o 3 3 1 572.08 626.69 9.89 o 4 3 1 292.28 304.54 8.14 o 5 3 1 2319.12 2248.96 22.70 o 6 3 1 422.96 443.02 11.18 o 7 3 1 2083.83 2046.07 23.43 o 8 3 1 228.65 226.00 11.45 o 9 3 1 57.38 76.97 10.71 o 10 3 1 645.01 645.67 18.63 o 11 3 1 109.09 104.92 19.38 o 12 3 1 46.59 46.87 35.16 o -11 4 1 180.23 211.29 47.96 o -10 4 1 617.80 635.21 17.65 o -9 4 1 139.39 146.04 15.62 o -8 4 1 81.77 95.02 12.25 o -7 4 1 1366.78 1344.52 24.28 o -6 4 1 402.30 417.23 16.79 o -5 4 1 428.98 423.11 13.01 o -4 4 1 1106.63 1094.54 17.71 o -3 4 1 590.78 679.47 22.14 o -2 4 1 651.43 709.17 14.52 o -1 4 1 7518.45 7354.60 61.98 o 0 4 1 34.14 23.16 5.92 o 1 4 1 7537.37 7429.07 57.37 o 2 4 1 690.01 755.34 8.51 o 3 4 1 587.15 672.42 16.09 o 4 4 1 1125.14 1131.08 20.84 o 5 4 1 436.98 420.69 13.12 o 6 4 1 402.38 413.96 15.41 o 7 4 1 1396.55 1363.55 17.47 o 8 4 1 85.67 91.80 17.02 o 9 4 1 136.39 146.28 10.58 o 10 4 1 633.20 676.96 16.93 o 11 4 1 183.28 190.20 20.00 o -11 5 1 6.90 -25.45 50.14 o -10 5 1 480.92 514.61 21.86 o -9 5 1 396.71 429.10 16.53 o -8 5 1 47.01 53.00 15.88 o -7 5 1 1023.02 980.29 23.99 o -6 5 1 299.29 333.10 15.74 o -5 5 1 1065.74 1037.33 18.87 o -4 5 1 613.78 619.00 13.26 o -3 5 1 826.35 826.72 11.07 o -2 5 1 2184.77 2224.89 20.09 o -1 5 1 2889.37 2935.13 27.24 o 0 5 1 13.93 72.41 10.62 o 1 5 1 2865.34 2889.70 23.38 o 2 5 1 2218.78 2249.61 20.42 o 3 5 1 825.05 853.44 20.42 o 4 5 1 618.31 636.44 16.56 o 5 5 1 1075.16 1028.08 18.89 o 6 5 1 288.60 321.07 14.61 o 7 5 1 1027.76 951.90 21.91 o 8 5 1 49.71 83.94 23.17 o 9 5 1 395.71 399.87 45.20 o 10 5 1 483.58 532.64 27.29 o -11 6 1 238.95 254.38 56.26 o -10 6 1 28.87 -26.10 42.54 o -9 6 1 147.71 213.21 29.93 o -8 6 1 226.73 234.05 18.80 o -7 6 1 646.48 617.16 19.39 o -6 6 1 15.58 11.05 14.61 o -5 6 1 589.16 588.02 15.51 o -4 6 1 1167.14 1136.73 18.33 o -3 6 1 617.86 637.16 10.01 o -2 6 1 44.27 46.05 7.20 o -1 6 1 764.08 699.25 12.03 o 0 6 1 72.57 89.35 9.48 o 1 6 1 753.42 702.91 8.78 o 2 6 1 45.15 60.47 9.63 o 3 6 1 629.71 670.65 16.70 o 4 6 1 1137.48 1080.41 18.61 o 5 6 1 569.90 562.54 16.07 o 6 6 1 15.25 18.37 12.14 o 7 6 1 664.12 633.48 19.74 o 8 6 1 234.39 256.35 22.05 o 9 6 1 151.09 168.99 20.89 o 10 6 1 26.36 11.19 36.22 o 11 6 1 242.45 357.23 63.39 o -9 7 1 173.19 148.70 32.42 o -8 7 1 474.28 427.72 21.76 o -7 7 1 400.90 387.22 19.01 o -6 7 1 120.91 164.87 15.72 o -5 7 1 960.74 939.23 23.79 o -4 7 1 783.81 805.91 15.79 o -3 7 1 445.48 466.61 10.34 o -2 7 1 549.74 544.42 9.30 o -1 7 1 429.66 419.60 7.73 o 0 7 1 66.68 45.37 10.12 o 1 7 1 447.04 422.79 11.15 o 2 7 1 551.53 534.27 8.48 o 3 7 1 451.28 464.40 17.09 o 4 7 1 788.20 758.67 16.10 o 5 7 1 931.10 881.01 19.44 o 6 7 1 123.09 134.55 15.07 o 7 7 1 416.43 382.53 17.70 o 8 7 1 467.01 468.07 22.61 o 9 7 1 174.94 155.37 27.09 o 10 7 1 124.87 97.56 51.67 o 11 7 1 6.77 104.78 54.73 o -10 8 1 508.27 572.01 54.86 o -9 8 1 21.89 35.00 43.70 o -8 8 1 244.81 247.60 26.84 o -7 8 1 481.07 490.98 19.73 o -6 8 1 165.72 149.45 13.99 o -5 8 1 905.55 865.47 26.63 o -4 8 1 2170.98 2195.64 46.55 o -3 8 1 1070.39 1059.86 16.76 o -2 8 1 2122.80 2088.78 29.23 o -1 8 1 270.46 274.69 9.00 o 0 8 1 975.60 1013.54 17.02 o 1 8 1 275.01 262.53 11.26 o 2 8 1 2124.39 2054.52 24.66 o 3 8 1 1050.66 1034.88 17.49 o 4 8 1 2192.41 2139.11 29.15 o 5 8 1 923.34 903.11 23.57 o 6 8 1 162.24 188.80 14.95 o 7 8 1 474.42 460.93 21.84 o 8 8 1 242.35 249.03 23.61 o 9 8 1 20.97 64.69 51.35 o 10 8 1 506.81 575.37 56.14 o -8 9 1 25.09 35.19 25.05 o -7 9 1 7.15 29.61 20.75 o -6 9 1 429.86 456.39 21.11 o -5 9 1 240.36 279.74 20.19 o -4 9 1 20.54 -1.45 18.16 o -3 9 1 53.63 74.85 20.32 o -2 9 1 1894.76 1892.38 26.85 o -1 9 1 240.89 251.93 11.93 o 0 9 1 278.46 298.40 13.36 o 1 9 1 252.83 264.60 15.52 o 2 9 1 1896.58 1839.29 23.43 o 3 9 1 59.38 64.13 10.35 o 4 9 1 20.58 11.69 19.10 o 5 9 1 251.43 257.18 26.96 o 6 9 1 429.06 473.46 57.59 o 7 9 1 4.87 -3.98 20.57 o 8 9 1 24.93 60.06 49.92 o -7 10 1 282.13 329.11 53.89 o -6 10 1 981.08 1004.96 93.88 o -5 10 1 74.06 53.93 25.65 o -4 10 1 133.87 127.84 27.09 o -3 10 1 198.82 195.01 14.01 o -2 10 1 9.16 10.71 9.47 o -1 10 1 400.97 436.56 18.22 o 0 10 1 879.08 911.13 20.88 o 1 10 1 398.68 425.69 22.55 o 2 10 1 12.07 31.35 11.10 o 3 10 1 195.85 179.08 14.67 o 4 10 1 138.05 171.84 27.49 o 5 10 1 72.26 81.57 21.29 o 6 10 1 981.74 934.16 23.59 o 7 10 1 272.00 304.81 25.83 o -6 11 1 101.89 123.98 43.82 o -5 11 1 250.15 249.14 28.91 o -4 11 1 99.90 110.09 35.59 o -3 11 1 153.64 89.92 29.57 o -2 11 1 482.99 465.60 16.33 o -1 11 1 437.75 444.14 21.43 o 0 11 1 76.92 79.28 20.59 o 1 11 1 443.00 439.45 17.32 o 2 11 1 466.63 473.65 15.98 o 3 11 1 150.11 151.36 29.57 o 4 11 1 102.57 92.88 33.92 o 5 11 1 249.47 307.34 71.31 o 6 11 1 104.17 102.13 58.43 o -5 12 1 29.86 310.25 62.87 o -4 12 1 84.04 117.51 51.41 o -3 12 1 47.40 62.05 74.71 o -2 12 1 10.90 12.33 14.54 o -1 12 1 386.15 377.00 18.80 o 0 12 1 64.30 87.30 17.05 o 1 12 1 387.34 396.55 22.72 o 2 12 1 10.34 22.46 18.03 o 3 12 1 51.76 45.30 33.66 o 4 12 1 86.19 14.32 52.20 o 5 12 1 31.87 55.85 57.67 o -3 13 1 72.21 22.22 57.26 o -2 13 1 47.99 50.55 39.52 o -1 13 1 65.46 64.00 51.12 o 0 13 1 829.17 868.08 37.76 o 1 13 1 59.39 23.24 50.84 o 2 13 1 47.30 21.47 36.18 o 3 13 1 70.78 68.52 52.99 o 2 0 2 147.06 177.84 9.70 o 3 0 2 2.49 -5.47 5.47 o 4 0 2 0.93 5.53 5.56 o 5 0 2 1054.61 1071.69 14.22 o 6 0 2 1.16 10.64 7.69 o 7 0 2 1002.10 1074.54 17.43 o 8 0 2 86.20 67.07 13.96 o 9 0 2 52.89 72.33 13.71 o 10 0 2 234.37 228.24 18.11 o 11 0 2 52.26 63.28 16.79 o 12 0 2 0.24 -15.76 32.43 o -12 1 2 585.49 604.55 25.56 o -11 1 2 202.53 199.16 18.96 o -10 1 2 51.68 64.81 24.05 o -9 1 2 316.70 291.56 15.80 o -8 1 2 2172.12 2062.93 26.85 o -7 1 2 155.67 141.94 8.89 o -6 1 2 135.82 139.14 7.62 o -5 1 2 443.69 419.73 10.73 o -4 1 2 2113.02 2163.00 22.77 o -3 1 2 24.05 9.12 4.33 o -2 1 2 159.29 183.12 5.39 o -1 1 2 1727.62 1531.08 178.65 o 1 1 2 1772.94 1370.69 35.92 o 2 1 2 161.24 177.14 6.42 o 3 1 2 19.20 21.38 6.85 o 4 1 2 2115.85 2182.63 22.58 o 5 1 2 440.31 405.15 11.56 o 6 1 2 130.49 121.95 9.29 o 7 1 2 160.18 141.57 11.10 o 8 1 2 2178.91 2066.02 27.47 o 9 1 2 308.17 338.72 14.24 o 10 1 2 52.43 76.92 14.72 o 11 1 2 194.48 190.84 16.53 o 12 1 2 596.66 611.91 32.54 o -12 2 2 14.21 36.49 29.64 o -11 2 2 149.06 168.74 18.01 o -10 2 2 79.61 122.54 13.82 o -9 2 2 84.31 105.83 11.67 o -8 2 2 583.66 591.47 14.61 o -7 2 2 626.77 650.98 12.89 o -6 2 2 2181.34 2099.48 22.49 o -5 2 2 277.49 260.27 7.68 o -4 2 2 341.15 388.53 7.48 o -3 2 2 373.70 373.63 9.75 o -2 2 2 7045.75 6987.39 60.59 o -1 2 2 4510.04 4493.51 37.48 o 0 2 2 1965.13 2011.15 19.99 o 1 2 2 4527.70 4564.45 32.59 o 2 2 2 7073.55 7012.19 49.13 o 3 2 2 353.76 359.54 9.97 o 4 2 2 342.94 390.33 7.98 o 5 2 2 286.40 266.33 10.04 o 6 2 2 2196.94 2101.21 22.98 o 7 2 2 617.40 629.58 13.08 o 8 2 2 585.95 597.21 15.27 o 9 2 2 82.34 96.21 14.59 o 10 2 2 75.54 75.34 12.63 o 11 2 2 150.37 155.02 18.67 o 12 2 2 12.94 19.79 21.25 o -11 3 2 1574.28 1604.69 30.29 o -10 3 2 118.91 134.82 21.17 o -9 3 2 306.03 324.18 19.94 o -8 3 2 95.76 96.49 9.95 o -7 3 2 368.56 402.73 10.73 o -6 3 2 1039.98 1089.84 16.92 o -5 3 2 1623.79 1627.18 30.18 o -4 3 2 180.95 161.89 6.96 o -3 3 2 5583.20 5745.47 50.36 o -2 3 2 2970.63 2944.63 26.95 o -1 3 2 4252.34 4199.26 33.52 o 0 3 2 701.65 720.70 9.49 o 1 3 2 4266.63 4192.68 39.23 o 2 3 2 2983.23 2967.75 22.13 o 3 3 2 5559.68 5727.93 42.51 o 4 3 2 183.96 178.06 9.75 o 5 3 2 1627.18 1611.65 17.28 o 6 3 2 1024.52 1075.67 15.32 o 7 3 2 367.90 407.58 11.43 o 8 3 2 98.69 82.18 11.01 o 9 3 2 309.41 310.59 14.08 o 10 3 2 122.65 158.73 12.30 o 11 3 2 1575.07 1596.63 30.33 o 12 3 2 246.14 221.68 62.53 o -11 4 2 537.27 543.97 60.98 o -10 4 2 8.31 42.64 34.02 o -9 4 2 162.77 142.39 21.02 o -8 4 2 49.26 71.08 13.96 o -7 4 2 67.32 55.24 20.72 o -6 4 2 1543.30 1456.47 23.64 o -5 4 2 1277.22 1288.82 17.04 o -4 4 2 341.86 404.19 11.60 o -3 4 2 361.24 362.87 15.56 o -2 4 2 665.81 636.26 10.25 o -1 4 2 337.90 361.60 11.68 o 0 4 2 39.54 27.08 4.12 o 1 4 2 336.54 362.32 7.64 o 2 4 2 673.25 664.21 10.64 o 3 4 2 355.88 365.58 14.75 o 4 4 2 343.26 423.31 7.77 o 5 4 2 1268.74 1282.60 14.21 o 6 4 2 1536.58 1444.09 15.71 o 7 4 2 72.86 72.61 9.23 o 8 4 2 50.05 46.59 8.30 o 9 4 2 162.94 142.98 14.84 o 10 4 2 8.85 34.35 12.08 o 11 4 2 530.14 519.37 20.28 o -11 5 2 63.46 59.43 54.59 o -10 5 2 81.65 116.00 45.28 o -9 5 2 34.92 61.66 22.16 o -8 5 2 845.55 852.65 26.64 o -7 5 2 246.28 240.79 15.63 o -6 5 2 157.07 156.72 18.38 o -5 5 2 237.64 234.39 11.85 o -4 5 2 22.98 2.96 10.74 o -3 5 2 7.47 6.61 9.37 o -2 5 2 242.98 253.28 6.61 o -1 5 2 675.63 680.78 9.85 o 0 5 2 2830.60 2895.26 30.42 o 1 5 2 667.06 668.23 11.38 o 2 5 2 235.15 241.48 7.94 o 3 5 2 6.48 6.98 7.43 o 4 5 2 25.90 0.76 6.18 o 5 5 2 237.87 251.56 15.47 o 6 5 2 157.04 154.56 13.02 o 7 5 2 239.16 273.52 16.06 o 8 5 2 846.26 863.19 25.57 o 9 5 2 32.10 60.41 20.89 o 10 5 2 81.39 89.67 23.26 o 11 5 2 65.32 147.02 39.95 o -11 6 2 111.29 176.23 53.16 o -9 6 2 879.59 852.20 53.22 o -8 6 2 130.92 158.75 26.53 o -7 6 2 57.33 105.10 16.67 o -6 6 2 493.39 500.52 16.36 o -5 6 2 1299.42 1242.51 21.39 o -4 6 2 574.74 580.82 13.23 o -3 6 2 1502.29 1380.77 26.81 o -2 6 2 967.43 984.32 11.65 o -1 6 2 1180.04 1169.42 14.10 o 0 6 2 103.28 80.85 6.40 o 1 6 2 1167.30 1139.75 13.94 o 2 6 2 959.32 975.34 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