#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2205391.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205391_Fobs loop_ _publ_author_name 'Liu, Bing-Xin' 'Xu, Duan-Jun' _publ_section_title ; 2,2'-Diamino-4,4'-bi-1,3-thiazolium (2R,3R)-tartrate ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o753 _journal_page_last o755 _journal_volume 61 _journal_year 2005 _space_group_IT_number 154 _symmetry_space_group_name_Hall 'P 32 2"' _symmetry_space_group_name_H-M 'P 32 2 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 11.0122 _cell_length_b 11.0122 _cell_length_c 18.8285 _exptl_crystal_F_000 1080.00 _reflns_d_resolution_high 0.7702 _[local]_cod_data_source_file ww6361Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bx-291 in P 3221' _shelx_refln_list_code 4 _shelx_f_calc_maximum 408.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z+2/3' '-x+y, -x, z+1/3' 'x-y, -y, -z+1/3' '-x, -x+y, -z+2/3' 'y, x, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 765.48 273.14 76.61 o 1 1 0 6624.10 6336.40 129.39 o -1 2 0 6614.99 6459.87 42.62 o 0 2 0 5607.81 5199.76 34.74 o 1 2 0 53.39 30.09 0.99 o 2 2 0 5740.00 5527.08 84.50 o -1 3 0 55.45 32.06 1.31 o 0 3 0 673.16 702.16 3.35 o 1 3 0 719.55 814.99 7.47 o 2 3 0 1478.43 1471.10 16.69 o 3 3 0 610.63 664.43 15.00 o -2 4 0 5762.51 5654.75 71.96 o -1 4 0 726.02 805.92 8.51 o 0 4 0 2662.33 2857.63 24.98 o 1 4 0 1928.55 1974.58 19.53 o 2 4 0 411.02 391.32 7.21 o 3 4 0 1118.48 1117.41 10.10 o 4 4 0 888.89 908.66 14.20 o -2 5 0 1511.05 1502.33 17.43 o -1 5 0 1885.41 1958.36 5.35 o 0 5 0 264.81 240.74 1.78 o 1 5 0 114.03 136.34 1.98 o 2 5 0 865.96 899.57 9.20 o 3 5 0 119.38 123.24 2.02 o 4 5 0 173.81 169.11 1.99 o 5 5 0 1121.73 1103.69 14.32 o -3 6 0 574.85 672.43 6.72 o -2 6 0 424.02 409.64 2.33 o -1 6 0 104.67 130.32 2.44 o 0 6 0 1226.21 1117.06 7.98 o 1 6 0 799.96 779.42 11.69 o 2 6 0 1618.50 1615.59 13.66 o 3 6 0 516.14 483.61 6.70 o 4 6 0 874.87 791.99 7.35 o 5 6 0 0.39 2.25 2.34 o 6 6 0 131.58 127.22 4.39 o -3 7 0 1112.83 1088.32 21.34 o -2 7 0 856.40 887.41 7.21 o -1 7 0 781.06 742.59 9.32 o 0 7 0 1161.91 1077.79 6.18 o 1 7 0 25.30 30.32 2.09 o 2 7 0 2188.67 2189.77 11.02 o 3 7 0 505.08 514.83 3.15 o 4 7 0 210.99 195.37 3.34 o 5 7 0 172.84 174.93 3.28 o 6 7 0 77.21 74.50 3.11 o 7 7 0 164.70 171.78 5.46 o -4 8 0 864.20 883.23 6.03 o -3 8 0 124.06 130.59 3.43 o -2 8 0 1591.41 1587.14 12.58 o -1 8 0 23.96 29.95 2.36 o 0 8 0 251.21 255.44 2.32 o 1 8 0 676.90 668.42 6.87 o 2 8 0 63.53 68.14 2.67 o 3 8 0 1.08 3.29 2.48 o 4 8 0 32.90 31.86 2.40 o 5 8 0 31.40 39.18 2.61 o 6 8 0 124.91 126.56 3.69 o -4 9 0 177.75 176.52 3.24 o -3 9 0 500.46 479.71 6.06 o -2 9 0 2164.50 2155.40 18.22 o -1 9 0 664.75 653.22 4.96 o 0 9 0 754.89 722.03 8.08 o 1 9 0 224.53 234.37 3.99 o 2 9 0 159.40 182.31 2.93 o 3 9 0 8.99 11.83 2.85 o 4 9 0 185.29 185.40 4.17 o 5 9 0 10.15 13.71 3.34 o -5 10 0 1105.03 1095.84 15.00 o -4 10 0 886.72 825.48 4.53 o -3 10 0 515.49 536.87 5.44 o -2 10 0 61.09 66.78 3.12 o -1 10 0 230.13 236.63 3.43 o 0 10 0 5.22 15.60 3.51 o 1 10 0 2.40 9.34 3.49 o 2 10 0 397.77 378.77 6.07 o 3 10 0 25.27 24.58 3.46 o -5 11 0 0.46 3.82 3.11 o -4 11 0 203.56 196.42 3.50 o -3 11 0 1.68 8.54 3.39 o -2 11 0 160.52 179.93 4.21 o -1 11 0 2.48 4.37 3.16 o 0 11 0 1268.81 1286.36 11.57 o 1 11 0 14.36 19.75 4.12 o 2 11 0 94.46 95.40 4.26 o -6 12 0 127.09 117.06 6.53 o -5 12 0 176.94 165.18 5.77 o -4 12 0 33.76 34.67 3.44 o -3 12 0 8.86 5.77 3.32 o -2 12 0 398.06 378.68 5.66 o -1 12 0 14.15 17.66 3.83 o 0 12 0 4.77 9.92 4.76 o -6 13 0 77.79 74.08 5.69 o -5 13 0 31.91 44.12 4.24 o -4 13 0 184.18 188.21 4.04 o -3 13 0 25.68 26.23 3.69 o -2 13 0 97.31 96.69 4.02 o -7 14 0 166.30 164.55 21.69 o -6 14 0 123.99 121.74 8.89 o -5 14 0 10.23 17.11 4.11 o -1 1 1 448.43 386.46 15.88 o 0 1 1 132.22 101.06 3.37 o 1 1 1 6272.61 5916.65 69.19 o -3 2 1 237.26 178.57 0.92 o -2 2 1 7406.53 7476.35 71.40 o -1 2 1 6323.71 5941.95 56.45 o 0 2 1 1193.00 976.73 9.29 o 1 2 1 5763.36 5906.41 36.98 o 2 2 1 12330.76 12280.87 74.26 o -5 3 1 6145.16 6427.94 58.74 o -4 3 1 1626.77 1611.12 8.82 o -3 3 1 2942.24 3300.54 21.91 o -2 3 1 268.57 208.29 1.63 o -1 3 1 5727.52 5818.82 35.99 o 0 3 1 484.84 505.17 2.71 o 1 3 1 2005.12 2113.12 18.08 o 2 3 1 1530.39 1605.01 20.16 o 3 3 1 3061.41 3313.65 21.74 o -7 4 1 955.98 968.46 5.62 o -6 4 1 668.31 664.14 5.76 o -5 4 1 1046.70 1107.18 6.89 o -4 4 1 11285.29 12367.23 31.82 o -3 4 1 1659.58 1644.49 11.02 o -2 4 1 12318.12 11853.68 251.77 o -1 4 1 2019.57 2104.07 18.93 o 0 4 1 5576.88 5692.94 20.98 o 1 4 1 324.18 348.97 4.07 o 2 4 1 1363.22 1379.54 15.74 o 3 4 1 2076.55 2103.48 21.63 o 4 4 1 2383.96 2369.88 16.90 o -9 5 1 424.24 392.42 2.87 o -8 5 1 41.17 51.02 1.64 o -7 5 1 134.37 126.87 2.12 o -6 5 1 2363.81 2484.74 16.71 o -5 5 1 3362.55 3496.72 32.00 o -4 5 1 1075.02 1105.28 20.65 o -3 5 1 6131.97 6463.90 33.36 o -2 5 1 1511.85 1579.37 16.92 o -1 5 1 315.74 344.90 4.11 o 0 5 1 751.03 810.30 9.20 o 1 5 1 163.10 153.83 2.84 o 2 5 1 946.98 904.26 6.45 o 3 5 1 661.91 672.92 4.52 o 4 5 1 254.21 231.35 2.47 o 5 5 1 725.76 727.67 8.14 o -11 6 1 130.58 134.60 2.68 o -10 6 1 1558.53 1525.62 12.93 o -9 6 1 130.06 134.21 2.09 o -8 6 1 310.24 273.27 4.23 o -7 6 1 451.40 448.56 5.43 o -6 6 1 173.78 203.31 3.61 o -5 6 1 2352.98 2409.30 32.77 o -4 6 1 685.58 686.55 6.42 o -3 6 1 3090.71 3403.31 15.40 o -2 6 1 1382.03 1364.14 20.21 o -1 6 1 154.14 144.15 1.73 o 0 6 1 512.08 463.85 3.02 o 1 6 1 1283.67 1305.68 9.56 o 2 6 1 566.64 568.11 6.19 o 3 6 1 157.29 156.81 2.95 o 4 6 1 274.13 279.77 3.85 o 5 6 1 124.47 124.29 2.46 o 6 6 1 87.80 88.07 2.77 o -13 7 1 104.82 105.79 4.26 o -12 7 1 182.80 188.24 3.92 o -11 7 1 114.51 128.11 2.56 o -10 7 1 413.47 414.79 3.66 o -9 7 1 853.81 903.77 8.08 o -8 7 1 1439.78 1452.92 17.94 o -7 7 1 1091.08 1040.84 8.18 o -6 7 1 451.10 461.03 3.09 o -5 7 1 133.52 127.80 3.14 o -4 7 1 993.66 1032.99 13.69 o -3 7 1 2064.93 2125.70 6.32 o -2 7 1 958.60 896.48 10.41 o -1 7 1 1276.76 1280.69 5.71 o 0 7 1 1.22 8.94 2.74 o 1 7 1 307.30 284.13 6.49 o 2 7 1 1371.13 1371.59 9.21 o 3 7 1 242.48 242.07 3.80 o 4 7 1 114.88 119.55 4.15 o 5 7 1 33.73 34.74 2.96 o 6 7 1 1.14 5.57 3.56 o 7 7 1 248.13 269.41 4.73 o -14 8 1 5.73 8.51 3.26 o -13 8 1 113.86 123.11 3.33 o -12 8 1 19.22 16.66 2.36 o -11 8 1 457.86 453.45 4.79 o -10 8 1 233.40 236.87 8.33 o -9 8 1 77.10 73.58 2.51 o -8 8 1 8.81 10.51 2.33 o -7 8 1 1467.15 1485.88 4.17 o -6 8 1 319.71 275.61 3.49 o -5 8 1 41.94 46.55 3.32 o -4 8 1 2386.08 2445.40 21.10 o -3 8 1 667.58 678.83 7.52 o -2 8 1 557.08 546.93 2.80 o -1 8 1 298.77 282.66 4.31 o 0 8 1 602.43 580.18 6.08 o 1 8 1 123.75 119.00 2.54 o 2 8 1 49.66 47.04 3.11 o 3 8 1 157.55 170.42 3.23 o 4 8 1 115.69 127.32 3.55 o 5 8 1 298.18 320.59 4.59 o 6 8 1 53.30 56.90 4.00 o -14 9 1 77.32 77.08 3.98 o -13 9 1 393.13 398.36 10.92 o -12 9 1 97.60 108.17 2.92 o -11 9 1 207.63 223.62 3.63 o -10 9 1 316.23 320.96 2.78 o -9 9 1 78.23 72.68 2.77 o -8 9 1 82.16 72.97 3.24 o -7 9 1 859.68 914.15 4.62 o -6 9 1 139.62 151.03 3.13 o -5 9 1 418.71 389.44 3.69 o -4 9 1 258.86 245.67 3.66 o -3 9 1 160.40 164.22 3.95 o -2 9 1 1374.40 1391.04 14.43 o -1 9 1 126.79 117.57 2.54 o 0 9 1 95.82 111.65 2.63 o 1 9 1 153.33 144.05 2.76 o 2 9 1 79.96 91.24 2.91 o 3 9 1 214.69 212.91 3.49 o 4 9 1 179.75 188.55 3.00 o 5 9 1 195.34 201.73 3.71 o -13 10 1 52.20 48.99 2.89 o -12 10 1 0.13 5.60 2.94 o -11 10 1 106.23 103.86 3.53 o -10 10 1 157.21 160.86 3.68 o -9 10 1 310.14 309.86 4.06 o -8 10 1 219.29 230.51 3.40 o -7 10 1 410.86 428.79 4.34 o -6 10 1 1551.68 1516.44 14.46 o -5 10 1 710.48 714.42 11.70 o -4 10 1 284.69 296.34 5.69 o -3 10 1 232.39 223.93 3.59 o -2 10 1 49.63 52.50 3.40 o -1 10 1 145.26 141.58 3.70 o 0 10 1 408.89 431.65 7.53 o 1 10 1 164.20 167.19 3.51 o 2 10 1 160.29 163.69 4.61 o 3 10 1 42.78 46.11 2.91 o -13 11 1 296.50 304.85 9.18 o -12 11 1 82.75 77.83 3.89 o -11 11 1 81.42 88.05 4.60 o -10 11 1 100.07 99.32 3.31 o -9 11 1 212.94 225.36 9.21 o -8 11 1 456.83 471.51 5.47 o -7 11 1 109.92 119.68 3.45 o -6 11 1 129.47 133.27 3.45 o -5 11 1 121.54 111.79 4.69 o -4 11 1 115.50 119.37 3.21 o -3 11 1 163.33 162.94 7.56 o -2 11 1 81.27 87.66 3.13 o -1 11 1 163.02 165.74 6.05 o 0 11 1 0.40 6.50 3.14 o 1 11 1 25.36 22.55 3.86 o 2 11 1 148.31 161.44 4.62 o -12 12 1 4.73 4.25 3.53 o -11 12 1 81.54 81.65 3.75 o -10 12 1 0.28 9.11 3.41 o -9 12 1 98.85 108.66 4.38 o -8 12 1 17.40 17.15 3.73 o -7 12 1 175.96 185.57 3.92 o -6 12 1 88.02 85.56 3.98 o -5 12 1 33.32 25.87 5.86 o -4 12 1 115.99 112.66 3.91 o -3 12 1 211.30 210.75 3.82 o -2 12 1 158.50 153.75 6.14 o -1 12 1 26.48 36.44 3.48 o 0 12 1 36.76 28.38 3.63 o -11 13 1 296.65 306.64 17.87 o -10 13 1 52.66 57.16 4.56 o -9 13 1 389.38 408.41 11.28 o -8 13 1 114.31 113.24 3.86 o -7 13 1 103.19 103.27 6.69 o -6 13 1 1.05 8.50 4.93 o -5 13 1 299.01 317.45 8.86 o -4 13 1 178.16 190.04 4.86 o -3 13 1 42.64 41.34 3.85 o -2 13 1 148.69 171.14 6.79 o -9 14 1 78.79 80.62 6.07 o -8 14 1 5.56 10.36 6.91 o -7 14 1 247.00 266.36 9.53 o -6 14 1 53.93 57.07 5.10 o -5 14 1 197.08 214.28 8.08 o -1 1 2 92.22 76.81 1.19 o 0 1 2 5.28 14.89 0.46 o 1 1 2 542.99 495.29 6.99 o -3 2 2 1909.85 1899.15 11.76 o -2 2 2 22446.13 21363.52 120.42 o -1 2 2 538.56 490.88 5.75 o 0 2 2 1210.14 1228.30 10.60 o 1 2 2 2476.19 2370.87 17.25 o 2 2 2 866.76 932.48 7.53 o -5 3 2 1968.64 2144.23 16.92 o -4 3 2 1904.33 1873.82 11.56 o -3 3 2 1172.81 1089.65 6.56 o -2 3 2 1932.47 1948.23 21.37 o -1 3 2 2404.56 2350.70 16.14 o 0 3 2 6.37 19.64 1.22 o 1 3 2 2337.02 2265.63 22.31 o 2 3 2 3273.22 3349.81 14.71 o 3 3 2 25.43 39.82 1.87 o -7 4 2 105.44 147.09 1.92 o -6 4 2 2635.66 2671.58 8.44 o -5 4 2 514.45 567.08 3.81 o -4 4 2 6572.17 7335.06 23.82 o -3 4 2 1793.70 1760.48 20.47 o -2 4 2 861.11 913.43 10.32 o -1 4 2 2372.87 2286.40 12.94 o 0 4 2 0.96 5.93 1.24 o 1 4 2 1518.12 1467.82 11.38 o 2 4 2 3976.31 4233.75 30.36 o 3 4 2 1265.18 1303.93 12.30 o 4 4 2 1144.86 1111.43 5.66 o -9 5 2 2038.64 1989.10 13.92 o -8 5 2 349.82 300.61 2.79 o -7 5 2 549.01 539.96 3.36 o -6 5 2 452.03 490.55 4.28 o -5 5 2 694.42 712.43 8.59 o -4 5 2 499.63 552.64 2.97 o -3 5 2 1936.06 2126.37 14.66 o -2 5 2 3315.88 3418.19 26.44 o -1 5 2 1540.64 1487.20 14.44 o 0 5 2 253.51 210.50 3.21 o 1 5 2 1668.29 1758.67 12.96 o 2 5 2 193.89 180.66 2.23 o 3 5 2 46.41 44.02 2.43 o 4 5 2 303.59 300.26 2.83 o 5 5 2 731.10 661.54 8.05 o -11 6 2 116.23 121.41 3.40 o -10 6 2 153.18 154.95 3.57 o -9 6 2 547.34 523.59 3.06 o -8 6 2 133.54 137.75 3.49 o -7 6 2 227.09 222.94 2.93 o -6 6 2 11113.66 11779.37 99.07 o -5 6 2 435.47 464.02 6.02 o -4 6 2 2611.10 2625.56 26.53 o -3 6 2 29.38 49.87 3.19 o -2 6 2 3957.78 4161.99 54.34 o -1 6 2 1720.16 1725.51 23.96 o 0 6 2 1045.99 1015.22 6.55 o 1 6 2 89.32 80.06 3.80 o 2 6 2 592.50 591.47 3.35 o 3 6 2 781.86 795.19 4.72 o 4 6 2 186.78 180.88 3.51 o 5 6 2 78.32 86.81 2.56 o 6 6 2 67.14 65.44 3.09 o -13 7 2 69.60 78.84 3.13 o -12 7 2 251.59 263.47 6.50 o -11 7 2 207.90 224.63 4.34 o -10 7 2 526.23 494.94 3.89 o -9 7 2 1051.96 1019.84 11.50 o -8 7 2 1104.58 1089.90 11.03 o -7 7 2 499.06 519.65 5.17 o -6 7 2 234.15 230.70 3.01 o -5 7 2 550.69 539.65 8.49 o -4 7 2 97.37 146.19 2.37 o -3 7 2 1292.47 1322.27 3.69 o -2 7 2 186.06 170.63 2.99 o -1 7 2 88.73 78.97 3.61 o 0 7 2 2252.34 2204.26 11.72 o 1 7 2 499.52 522.19 4.82 o 2 7 2 505.51 514.03 11.77 o 3 7 2 176.85 176.48 3.36 o 4 7 2 15.34 19.92 2.93 o 5 7 2 39.23 40.66 2.40 o 6 7 2 300.81 287.78 3.53 o 7 7 2 49.68 57.84 3.29 o -14 8 2 81.34 84.34 3.06 o -13 8 2 19.72 19.73 2.72 o -12 8 2 110.22 109.87 2.77 o -11 8 2 88.39 90.20 3.19 o -10 8 2 108.48 113.50 2.21 o -9 8 2 348.22 363.18 3.24 o -8 8 2 142.35 140.32 3.05 o -7 8 2 1119.00 1102.67 10.14 o -6 8 2 136.60 134.10 3.43 o -5 8 2 340.69 286.63 3.83 o -4 8 2 1134.00 1078.31 15.48 o -3 8 2 45.00 38.20 2.19 o -2 8 2 584.44 570.74 6.45 o -1 8 2 491.59 521.25 5.94 o 0 8 2 694.40 693.62 4.13 o 1 8 2 677.24 664.05 7.63 o 2 8 2 46.25 47.06 3.02 o 3 8 2 36.35 36.99 2.71 o 4 8 2 392.75 380.66 6.94 o 5 8 2 74.90 81.11 2.92 o 6 8 2 98.81 101.88 4.39 o -14 9 2 78.06 85.62 6.99 o -13 9 2 57.93 54.23 3.44 o -12 9 2 27.32 24.28 2.54 o -11 9 2 946.32 954.87 12.73 o -10 9 2 3.11 7.70 2.94 o -9 9 2 1257.54 1306.71 10.76 o -8 9 2 355.52 367.44 3.44 o -7 9 2 1059.31 1010.63 12.48 o -6 9 2 555.76 515.50 6.09 o -5 9 2 2023.09 1999.22 10.66 o -4 9 2 300.59 301.25 2.79 o -3 9 2 796.52 816.45 6.39 o -2 9 2 501.59 505.44 9.09 o -1 9 2 682.15 673.11 3.57 o 0 9 2 379.60 410.03 4.30 o 1 9 2 114.86 117.82 3.06 o 2 9 2 123.55 123.51 2.97 o 3 9 2 90.48 87.21 3.29 o 4 9 2 21.81 23.75 3.22 o 5 9 2 32.98 31.58 3.14 o -13 10 2 98.08 93.14 4.36 o -12 10 2 227.85 206.48 3.28 o -11 10 2 23.82 26.93 3.90 o -10 10 2 408.91 409.33 5.60 o -9 10 2 2.82 9.75 3.18 o -8 10 2 114.49 121.20 3.71 o -7 10 2 503.98 472.36 5.24 o -6 10 2 148.53 145.35 3.34 o -5 10 2 761.19 691.63 4.11 o -4 10 2 190.13 181.31 3.51 o -3 10 2 186.69 179.84 3.19 o -2 10 2 52.18 50.38 2.84 o -1 10 2 112.44 113.79 2.84 o 0 10 2 62.66 73.89 3.18 o 1 10 2 60.08 68.85 3.80 o 2 10 2 13.80 21.37 3.43 o 3 10 2 72.07 72.62 3.41 o -13 11 2 56.55 63.81 3.43 o -12 11 2 105.05 96.56 6.15 o -11 11 2 172.62 173.02 4.82 o -10 11 2 25.34 23.92 3.76 o -9 11 2 934.64 964.96 10.86 o -8 11 2 86.71 93.15 3.37 o -7 11 2 208.13 226.42 6.47 o -6 11 2 120.75 134.78 4.22 o -5 11 2 75.88 84.94 4.74 o -4 11 2 14.03 17.03 2.80 o -3 11 2 37.34 31.87 3.65 o -2 11 2 126.27 124.04 4.14 o -1 11 2 59.04 63.97 3.89 o 0 11 2 0.44 0.43 3.39 o 1 11 2 61.57 64.82 3.30 o 2 11 2 309.16 309.70 8.63 o -12 12 2 115.48 107.74 5.84 o -11 12 2 104.13 102.99 6.03 o -10 12 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734.29 680.41 10.07 o -4 3 3 826.89 768.18 8.00 o -3 3 3 501.52 462.57 3.58 o -2 3 3 5512.64 5462.19 37.72 o -1 3 3 1324.08 1315.54 3.02 o 0 3 3 3279.91 3556.90 15.08 o 1 3 3 717.29 732.96 6.28 o 2 3 3 2430.07 2433.16 26.73 o 3 3 3 2235.70 2375.41 13.74 o -7 4 3 281.99 248.12 3.88 o -6 4 3 1305.51 1348.39 8.93 o -5 4 3 2021.69 2090.34 9.95 o -4 4 3 1519.45 1434.78 16.46 o -3 4 3 805.48 756.56 10.54 o -2 4 3 304.66 353.35 9.06 o -1 4 3 730.90 749.93 5.00 o 0 4 3 150.94 163.06 1.54 o 1 4 3 2434.73 2433.52 46.71 o 2 4 3 994.22 1055.64 9.41 o 3 4 3 463.26 426.38 3.71 o 4 4 3 231.17 222.22 3.94 o -9 5 3 281.06 273.15 4.10 o -8 5 3 173.38 169.10 2.81 o -7 5 3 2055.64 2110.21 33.95 o -6 5 3 284.54 345.19 2.85 o -5 5 3 1060.82 1025.60 12.09 o -4 5 3 2010.60 2055.83 32.41 o -3 5 3 722.94 690.78 6.56 o -2 5 3 2401.71 2397.14 21.73 o -1 5 3 2435.18 2518.21 15.78 o 0 5 3 4242.57 4674.00 23.88 o 1 5 3 1411.68 1433.20 9.48 o 2 5 3 662.33 670.95 6.18 o 3 5 3 104.13 98.81 3.61 o 4 5 3 145.74 151.13 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