#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/54/2205462.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205462_Fobs loop_ _publ_author_name 'Li, Zhengkai' 'Zhao, Jin' 'Liang, Lei' 'Zhou, Xiangge' _publ_section_title ; Bis(pyrimidine-2-thiolato)bis(triphenylphosphine)ruthenium(II) chloroform solvate ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m714 _journal_page_last m716 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.382 _cell_angle_gamma 90.000 _cell_length_a 11.7340 _cell_length_b 10.3824 _cell_length_c 36.1625 _exptl_crystal_F_000 1968.00 _reflns_d_resolution_high 0.7684 _[local]_cod_data_source_file cv6463Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ZJ3 in P2(1)/n Ru(C4H3N2S)2[P(C6H5)3]2.CHCl3' _shelx_refln_list_code 4 _shelx_f_calc_maximum 470.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 10300.22 9682.33 139.75 o 6 0 0 18897.58 20194.45 247.48 o 8 0 0 360.52 391.98 55.14 o 10 0 0 9778.81 9231.17 330.53 o 12 0 0 2656.32 2524.53 209.75 o 14 0 0 812.98 749.26 189.06 o 1 1 0 46992.45 46044.13 540.80 o 2 1 0 1347.40 1385.89 50.54 o 3 1 0 2732.93 3362.66 94.40 o 4 1 0 4187.74 4383.53 76.61 o 5 1 0 38.99 -6.27 18.12 o 6 1 0 2713.86 2813.48 75.44 o 7 1 0 1849.52 1900.95 68.75 o 8 1 0 85.54 89.78 29.45 o 9 1 0 3259.30 3012.89 104.76 o 10 1 0 28.46 8.41 42.76 o 11 1 0 29.77 17.31 60.85 o 12 1 0 3301.20 3260.64 138.46 o 13 1 0 1632.83 1628.18 143.86 o 14 1 0 282.48 315.42 104.31 o 15 1 0 11.76 -56.89 96.47 o 0 2 0 3.95 160.31 63.24 o 1 2 0 75049.93 77712.35 338.44 o 2 2 0 678.66 689.93 28.88 o 3 2 0 14829.59 15011.12 216.61 o 4 2 0 384.02 462.23 49.85 o 5 2 0 25253.84 26059.05 203.68 o 6 2 0 257.36 232.68 24.25 o 7 2 0 66.76 38.65 19.86 o 8 2 0 20.11 23.20 42.74 o 9 2 0 361.07 385.07 69.06 o 10 2 0 3.40 -7.85 50.81 o 11 2 0 3374.00 3272.54 111.12 o 12 2 0 185.28 177.36 103.97 o 13 2 0 312.99 329.91 127.77 o 14 2 0 1.57 51.99 140.18 o 15 2 0 128.73 122.44 107.81 o 1 3 0 23674.06 23548.27 165.75 o 2 3 0 23650.38 25422.99 360.05 o 3 3 0 2831.51 2953.49 60.58 o 4 3 0 2529.79 2547.02 152.98 o 5 3 0 375.55 338.13 41.25 o 6 3 0 98.60 40.58 31.44 o 7 3 0 6370.53 5961.55 137.81 o 8 3 0 109.54 95.96 40.34 o 9 3 0 4606.40 4538.85 144.80 o 10 3 0 2.57 -15.63 45.70 o 11 3 0 2.25 -31.98 48.55 o 12 3 0 1538.08 1670.63 109.90 o 13 3 0 847.49 1024.27 128.83 o 0 4 0 87274.12 90051.16 590.36 o 1 4 0 2375.96 2434.86 61.20 o 2 4 0 2603.65 2789.73 62.62 o 3 4 0 2661.35 2722.98 62.79 o 4 4 0 6135.65 6043.02 99.90 o 5 4 0 15891.74 16304.84 200.63 o 6 4 0 2829.75 2698.62 123.13 o 7 4 0 23.26 32.75 36.72 o 8 4 0 4.11 -3.84 37.20 o 9 4 0 44.38 24.61 44.86 o 10 4 0 2303.75 2013.43 110.90 o 11 4 0 398.42 437.18 73.89 o 12 4 0 1034.82 1069.62 129.73 o 13 4 0 161.66 70.98 103.45 o 14 4 0 1044.94 1116.27 206.39 o 1 5 0 7241.84 7113.40 113.34 o 2 5 0 3306.54 2847.07 73.04 o 3 5 0 13290.53 13704.61 147.51 o 4 5 0 9537.08 9886.27 127.11 o 5 5 0 729.58 845.09 51.07 o 6 5 0 2069.92 1768.62 80.52 o 7 5 0 300.54 276.12 50.66 o 8 5 0 818.43 894.10 76.75 o 9 5 0 1261.35 1339.23 195.92 o 10 5 0 7.72 20.92 68.16 o 11 5 0 141.43 63.72 75.23 o 12 5 0 1875.38 2121.54 160.15 o 13 5 0 1531.84 1836.02 173.92 o 14 5 0 462.48 474.85 178.46 o 0 6 0 200.35 254.36 52.95 o 1 6 0 6389.86 6213.35 115.55 o 2 6 0 588.07 642.45 46.99 o 3 6 0 754.46 790.54 49.72 o 4 6 0 2720.58 2667.38 71.53 o 5 6 0 2546.80 2092.13 99.01 o 6 6 0 291.00 224.69 72.14 o 7 6 0 498.55 341.70 140.70 o 8 6 0 226.56 155.56 75.42 o 9 6 0 620.26 622.12 103.14 o 10 6 0 101.73 103.09 78.18 o 11 6 0 1423.13 1602.76 154.84 o 12 6 0 276.90 285.59 108.23 o 13 6 0 141.16 105.12 103.22 o 1 7 0 1823.19 1927.96 76.51 o 2 7 0 2014.45 1892.11 74.29 o 3 7 0 30.30 41.70 29.35 o 4 7 0 1150.54 1364.05 90.96 o 5 7 0 65.71 29.82 46.12 o 6 7 0 585.71 594.53 74.19 o 7 7 0 2531.99 2563.16 156.70 o 8 7 0 94.87 89.61 73.11 o 9 7 0 0.99 2.94 73.68 o 10 7 0 7.57 15.95 76.34 o 11 7 0 257.27 202.23 96.41 o 12 7 0 334.47 330.93 114.94 o 0 8 0 2415.83 2207.25 122.93 o 1 8 0 76.80 50.45 37.79 o 2 8 0 3711.38 3231.28 102.43 o 3 8 0 349.36 184.06 57.42 o 4 8 0 1476.20 1561.47 102.03 o 5 8 0 5666.56 5344.04 177.98 o 6 8 0 803.52 830.26 86.73 o 7 8 0 1162.35 1046.18 127.28 o 8 8 0 198.73 105.35 157.38 o 9 8 0 190.27 271.91 101.38 o 10 8 0 1292.08 1288.06 152.88 o 11 8 0 29.18 -23.19 90.07 o 12 8 0 301.69 358.61 124.24 o 1 9 0 604.59 591.68 65.28 o 2 9 0 633.66 582.57 81.28 o 3 9 0 2947.89 2743.79 128.57 o 4 9 0 1192.62 1247.21 105.95 o 5 9 0 3.29 8.41 52.50 o 6 9 0 42.65 28.79 55.56 o 7 9 0 110.70 79.57 63.54 o 8 9 0 1052.20 1264.79 193.20 o 9 9 0 298.06 451.41 119.04 o 10 9 0 48.56 18.68 95.24 o 11 9 0 486.42 478.71 135.33 o 0 10 0 33.88 85.72 71.14 o 1 10 0 5852.12 5383.63 148.05 o 2 10 0 0.04 -36.07 53.95 o 3 10 0 16.70 29.08 57.88 o 4 10 0 168.49 66.96 64.30 o 5 10 0 3045.69 2907.89 145.06 o 6 10 0 68.50 75.62 63.56 o 7 10 0 248.23 188.31 76.64 o 8 10 0 534.82 553.46 125.38 o 9 10 0 1160.03 1176.02 260.70 o 10 10 0 5.46 42.64 107.01 o 1 11 0 30.82 49.27 59.08 o 2 11 0 719.52 685.41 94.75 o 3 11 0 7.02 -41.55 64.96 o 4 11 0 44.39 39.91 67.81 o 5 11 0 15.25 11.65 65.73 o 6 11 0 241.40 297.68 85.11 o 7 11 0 993.13 1187.08 179.62 o 8 11 0 1406.19 1726.44 234.06 o 0 12 0 126.85 106.30 137.33 o 1 12 0 105.04 51.43 105.91 o 2 12 0 196.76 240.39 84.40 o 3 12 0 0.56 1.52 70.22 o 4 12 0 1007.99 1138.04 184.58 o 5 12 0 488.90 533.07 103.97 o 6 12 0 304.41 254.01 112.61 o 1 13 0 29.28 -104.57 104.90 o 2 13 0 778.40 1002.81 166.86 o 3 13 0 754.67 829.26 120.39 o 4 13 0 656.27 715.53 116.45 o -15 0 1 240.38 300.27 149.49 o -13 0 1 1980.14 1971.57 194.49 o -11 0 1 2248.97 1804.49 172.25 o -9 0 1 211.00 152.95 49.41 o -7 0 1 1.53 -7.12 30.63 o -5 0 1 23569.06 23754.14 459.33 o -3 0 1 1430.75 1432.06 66.99 o 3 0 1 18127.26 20522.95 255.01 o 5 0 1 2397.66 2556.68 82.53 o 7 0 1 1117.93 1015.50 67.42 o 9 0 1 11.94 6.07 42.99 o 11 0 1 6755.11 6543.96 290.96 o 13 0 1 370.95 478.47 163.20 o 15 0 1 49.61 241.05 168.11 o -15 1 1 111.12 203.30 111.72 o -14 1 1 3.84 83.54 116.90 o -13 1 1 108.60 74.22 78.17 o -12 1 1 3996.87 3680.66 218.80 o -11 1 1 4307.88 3897.47 266.78 o -10 1 1 130.20 29.74 45.30 o -9 1 1 0.35 -24.56 24.81 o -8 1 1 799.46 831.06 58.43 o -7 1 1 6.13 6.41 26.04 o -6 1 1 11655.26 11458.18 146.81 o -5 1 1 117.43 78.22 25.09 o -4 1 1 99.39 134.40 20.67 o -3 1 1 3269.67 3196.05 44.73 o -2 1 1 56379.14 59305.35 347.78 o -1 1 1 54978.68 56707.61 801.77 o 1 1 1 2340.16 1649.06 499.68 o 2 1 1 9554.74 9510.73 331.05 o 3 1 1 60.56 90.56 22.99 o 4 1 1 5009.01 5196.86 79.44 o 5 1 1 624.55 653.92 78.07 o 6 1 1 1008.09 1056.79 51.98 o 7 1 1 1864.67 1952.87 69.43 o 8 1 1 6022.21 5904.81 106.64 o 9 1 1 45.71 42.51 37.55 o 10 1 1 2897.90 3090.45 111.21 o 11 1 1 522.83 613.40 74.82 o 12 1 1 80.89 88.43 77.33 o 13 1 1 2252.99 2437.63 173.89 o 14 1 1 408.01 427.71 118.70 o 15 1 1 60.70 -47.28 99.23 o -15 2 1 7.24 81.83 102.56 o -14 2 1 791.76 1211.70 215.70 o -13 2 1 49.79 4.83 76.84 o -12 2 1 7.40 -2.24 52.74 o -11 2 1 40.42 -44.75 44.75 o -10 2 1 4444.73 4263.26 400.11 o -9 2 1 307.48 331.56 67.35 o -8 2 1 2578.61 2633.41 65.22 o -7 2 1 326.90 409.23 30.71 o -6 2 1 2325.84 2246.84 62.98 o -5 2 1 339.31 340.83 29.90 o -4 2 1 3536.89 3103.50 100.34 o -3 2 1 520.07 560.75 101.90 o -2 2 1 16369.18 18275.04 133.64 o -1 2 1 47.19 121.28 15.55 o 0 2 1 56833.28 58620.58 589.23 o 2 2 1 337.54 339.70 23.43 o 3 2 1 3010.26 3366.90 71.70 o 4 2 1 7058.13 7263.95 114.38 o 5 2 1 1726.66 1948.84 90.10 o 6 2 1 6399.44 6567.11 101.39 o 7 2 1 348.56 398.41 58.69 o 8 2 1 72.78 58.50 56.25 o 9 2 1 1277.83 1252.26 79.31 o 10 2 1 153.75 180.34 43.23 o 11 2 1 177.10 96.08 46.77 o 12 2 1 2892.91 2962.14 167.66 o 13 2 1 492.43 489.88 99.93 o 14 2 1 543.97 695.91 125.46 o 15 2 1 0.85 69.09 100.26 o -14 3 1 132.83 193.46 135.78 o -13 3 1 393.96 417.01 102.00 o -12 3 1 1683.13 1789.30 120.29 o -11 3 1 797.47 961.78 90.18 o -10 3 1 0.17 -40.81 40.81 o -9 3 1 46.71 0.80 42.50 o -8 3 1 648.27 636.03 95.05 o -7 3 1 18.90 -26.79 37.27 o -6 3 1 14567.07 13753.35 252.52 o -5 3 1 64.91 65.85 39.46 o -4 3 1 369.95 363.97 64.58 o -3 3 1 1776.51 2098.48 50.97 o -2 3 1 10955.19 11334.99 108.02 o -1 3 1 6784.66 7013.15 86.22 o 0 3 1 3968.82 3701.97 64.05 o 1 3 1 316.84 376.03 26.48 o 2 3 1 24756.40 26982.88 261.77 o 3 3 1 11076.96 12916.17 155.26 o 4 3 1 57.31 10.03 22.51 o 5 3 1 373.75 314.63 42.00 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2598.86 2583.12 118.72 o -5 7 1 2342.01 2498.42 135.94 o -4 7 1 8.80 0.14 40.90 o -3 7 1 34.53 14.26 29.54 o -2 7 1 421.64 428.04 46.13 o -1 7 1 3509.39 3362.10 96.08 o 0 7 1 21.16 26.42 30.94 o 1 7 1 84.12 96.21 34.79 o 2 7 1 350.92 351.37 42.78 o 3 7 1 1165.55 1129.91 60.91 o 4 7 1 3027.40 2954.08 119.26 o 5 7 1 117.06 82.32 49.59 o 6 7 1 160.12 72.28 50.14 o 7 7 1 16.52 -52.79 63.18 o 8 7 1 902.04 1114.62 127.52 o 9 7 1 296.09 364.71 100.11 o 10 7 1 415.97 443.40 105.22 o 11 7 1 60.95 124.68 88.84 o 12 7 1 386.40 297.18 108.03 o -12 8 1 41.33 -47.30 99.10 o -11 8 1 193.46 266.47 107.15 o -10 8 1 119.49 82.85 88.97 o -9 8 1 2859.76 2656.39 179.21 o -8 8 1 585.94 487.24 104.70 o -7 8 1 54.35 90.21 70.63 o -6 8 1 119.44 91.76 59.42 o -5 8 1 3180.46 3291.49 138.62 o -4 8 1 1314.63 1164.28 96.63 o -3 8 1 5569.41 5416.53 163.49 o -2 8 1 183.85 162.46 42.48 o -1 8 1 1461.96 1346.66 73.37 o 0 8 1 3.42 40.06 34.23 o 1 8 1 3932.79 3946.72 111.30 o 2 8 1 403.26 427.77 52.31 o 3 8 1 171.95 165.63 54.89 o 4 8 1 123.91 101.66 51.60 o 5 8 1 1262.96 1350.97 99.96 o 6 8 1 2485.10 2578.43 126.68 o 7 8 1 1543.50 1672.02 153.37 o 8 8 1 529.91 442.04 105.11 o 9 8 1 517.93 538.72 112.54 o 10 8 1 26.45 -4.44 123.89 o 11 8 1 1582.02 1880.98 183.19 o 12 8 1 11.72 -15.98 100.81 o -11 9 1 446.36 352.02 125.84 o -10 9 1 1033.36 1187.08 157.56 o -9 9 1 265.31 248.81 105.34 o -8 9 1 568.90 589.07 118.12 o -7 9 1 2276.41 2114.47 129.79 o -6 9 1 18.46 68.76 59.71 o -5 9 1 712.82 714.43 90.05 o -4 9 1 581.08 511.97 75.38 o -3 9 1 1616.37 1551.40 105.56 o -2 9 1 6835.04 6583.47 190.31 o -1 9 1 4275.52 4336.52 127.33 o 0 9 1 2930.53 2579.67 103.39 o 1 9 1 54.41 -3.87 40.25 o 2 9 1 72.03 35.99 52.60 o 3 9 1 2313.71 2352.64 122.92 o 4 9 1 893.79 1002.51 97.01 o 5 9 1 3124.58 2955.40 139.53 o 6 9 1 1.54 25.65 54.99 o 7 9 1 256.36 208.01 72.71 o 8 9 1 40.41 -24.75 77.33 o 9 9 1 929.25 1100.61 280.62 o 10 9 1 132.48 48.95 92.51 o 11 9 1 8.23 -23.50 103.57 o -10 10 1 563.40 421.46 148.84 o -9 10 1 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