#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:10:23 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180974 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/54/2205467.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205467_Fobs loop_ _publ_author_name 'Nagaraj, Basavegowda' 'Yathirajan, Hemmige S.' 'Bolte, Michael' _publ_section_title ; 2-(3-Chloropropyl)-2,3-dihydro-1H-isoindole-1,3-dione ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o928 _journal_page_last o929 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.605 _cell_angle_gamma 90.000 _cell_length_a 4.5421 _cell_length_b 15.3996 _cell_length_c 15.3471 _exptl_crystal_F_000 464.00 _reflns_d_resolution_high 0.7847 _cod_data_source_file cv6468Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' yat24 in P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 73.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 381.29 375.65 14.91 o 4 0 0 87.24 91.76 1.55 o 1 1 0 399.60 381.77 5.13 o 2 1 0 1893.64 1834.11 38.76 o 3 1 0 891.62 899.16 19.71 o 4 1 0 188.37 195.99 2.62 o 5 1 0 19.74 20.04 1.13 o 1 2 0 4403.02 4175.30 20.44 o 2 2 0 1034.00 1022.47 25.39 o 3 2 0 520.27 527.64 8.73 o 4 2 0 1.92 2.26 1.19 o 5 2 0 122.34 123.13 1.40 o 1 3 0 1272.41 1265.80 16.04 o 2 3 0 0.02 2.08 0.95 o 3 3 0 193.47 226.63 2.58 o 4 3 0 5.46 9.04 1.24 o 5 3 0 61.74 63.90 1.05 o 0 4 0 183.29 137.68 1.99 o 2 4 0 25.01 27.18 1.06 o 3 4 0 922.59 996.07 10.92 o 4 4 0 19.14 18.99 1.35 o 5 4 0 9.17 9.92 0.91 o 1 5 0 2612.57 2758.66 92.18 o 2 5 0 365.99 338.73 6.88 o 3 5 0 66.96 76.00 1.29 o 4 5 0 0.56 0.71 0.91 o 5 5 0 340.82 325.20 5.38 o 0 6 0 1202.46 1176.47 22.26 o 1 6 0 833.19 800.91 7.32 o 2 6 0 307.67 343.94 5.55 o 3 6 0 91.36 97.11 1.83 o 4 6 0 510.90 528.54 8.39 o 5 6 0 4.23 4.31 1.04 o 1 7 0 147.90 147.52 1.82 o 2 7 0 1285.58 1341.12 22.98 o 3 7 0 13.19 16.55 1.25 o 4 7 0 484.65 490.51 9.76 o 5 7 0 45.65 45.58 1.36 o 0 8 0 1004.72 1068.50 11.58 o 1 8 0 179.49 182.51 1.64 o 2 8 0 487.60 479.59 5.15 o 3 8 0 441.12 430.76 11.32 o 4 8 0 37.25 39.61 2.03 o 5 8 0 34.35 32.23 1.40 o 1 9 0 408.84 386.51 2.65 o 2 9 0 229.55 218.33 3.78 o 3 9 0 8.63 9.89 0.98 o 4 9 0 3.07 2.16 0.83 o 5 9 0 1.08 1.00 1.78 o 0 10 0 138.48 156.74 1.80 o 1 10 0 434.48 465.18 5.84 o 2 10 0 77.27 83.66 0.96 o 3 10 0 6.26 5.32 1.29 o 4 10 0 31.12 28.56 1.22 o 1 11 0 454.75 511.22 3.89 o 2 11 0 0.60 1.44 0.85 o 3 11 0 94.06 96.27 2.18 o 4 11 0 1.32 -0.16 1.05 o 0 12 0 474.33 486.61 5.30 o 1 12 0 771.72 778.22 5.61 o 2 12 0 4.35 2.03 0.92 o 3 12 0 2.70 2.86 1.11 o 4 12 0 71.75 72.02 2.43 o 1 13 0 94.81 90.81 0.95 o 2 13 0 708.25 685.15 15.97 o 3 13 0 67.31 62.61 1.67 o 4 13 0 6.28 6.76 0.91 o 0 14 0 195.26 199.42 3.94 o 1 14 0 693.68 684.18 7.35 o 2 14 0 50.78 53.22 1.28 o 3 14 0 2.17 5.60 1.36 o 4 14 0 2.86 0.01 0.87 o 1 15 0 1.45 1.96 0.91 o 2 15 0 0.30 0.69 0.91 o 3 15 0 106.38 111.90 1.51 o 0 16 0 28.78 30.96 1.25 o 1 16 0 2.32 1.33 0.92 o 2 16 0 13.67 11.90 0.97 o 3 16 0 48.87 45.39 1.61 o 1 17 0 134.59 141.11 2.05 o 2 17 0 5.95 9.10 1.13 o 0 18 0 106.86 116.76 1.84 o 1 18 0 64.91 60.80 1.58 o 2 18 0 0.02 0.85 0.95 o 1 19 0 19.25 21.14 1.29 o -5 0 1 12.85 16.81 2.00 o -3 0 1 117.04 103.01 1.54 o -1 0 1 1053.66 964.19 7.90 o 1 0 1 868.41 889.75 27.12 o 3 0 1 28.93 32.00 1.64 o 5 0 1 679.18 680.16 16.92 o -5 1 1 177.34 181.58 1.80 o -4 1 1 100.83 101.51 2.25 o -3 1 1 116.57 105.78 1.75 o -2 1 1 1729.74 1645.68 50.11 o -1 1 1 2345.63 2106.43 40.16 o 1 1 1 1432.25 1373.67 8.78 o 2 1 1 568.75 565.94 10.77 o 3 1 1 743.82 752.27 15.04 o 4 1 1 26.93 28.26 1.25 o 5 1 1 18.36 18.94 1.15 o -5 2 1 67.50 67.52 1.22 o -4 2 1 353.59 369.01 6.16 o -3 2 1 0.57 2.80 1.03 o -2 2 1 856.28 876.02 16.63 o 1 2 1 4500.75 4585.62 24.50 o 2 2 1 2670.71 2729.15 38.47 o 3 2 1 269.14 275.03 4.89 o 4 2 1 41.25 36.53 1.22 o 5 2 1 0.77 2.00 0.96 o -5 3 1 92.58 90.44 1.26 o -4 3 1 261.39 272.42 5.25 o -3 3 1 57.62 57.64 2.07 o -2 3 1 136.88 151.50 4.83 o -1 3 1 211.96 188.99 2.04 o 0 3 1 439.77 496.37 4.27 o 1 3 1 3.05 3.12 1.25 o 2 3 1 21.38 19.78 0.97 o 3 3 1 107.82 107.75 1.44 o 4 3 1 579.98 572.34 15.72 o 5 3 1 286.19 284.19 2.96 o -5 4 1 184.36 183.91 4.89 o -4 4 1 7.68 9.51 1.00 o -3 4 1 18.26 20.15 0.88 o -2 4 1 136.82 138.65 1.86 o -1 4 1 380.14 359.92 6.01 o 0 4 1 583.38 521.87 5.08 o 1 4 1 667.31 602.73 8.02 o 2 4 1 2175.24 2332.57 14.46 o 3 4 1 177.45 182.52 2.71 o 4 4 1 440.07 452.51 4.77 o 5 4 1 64.21 63.55 0.88 o -5 5 1 0.22 2.71 1.19 o -4 5 1 20.39 17.70 0.87 o -3 5 1 693.32 729.27 19.70 o -2 5 1 0.74 3.76 0.99 o -1 5 1 77.86 79.64 2.02 o 0 5 1 164.01 182.81 2.55 o 1 5 1 5.41 7.79 1.03 o 2 5 1 191.83 218.91 3.01 o 3 5 1 861.77 890.88 9.01 o 4 5 1 263.69 255.27 2.76 o 5 5 1 47.85 48.20 1.10 o -5 6 1 21.17 20.87 1.76 o -4 6 1 0.82 2.79 1.31 o -3 6 1 53.29 56.78 1.47 o -2 6 1 185.64 201.08 3.48 o -1 6 1 1466.41 1495.40 12.95 o 0 6 1 2.14 2.69 0.98 o 1 6 1 121.64 121.53 1.10 o 2 6 1 66.84 57.17 1.56 o 3 6 1 432.22 474.60 9.89 o 4 6 1 19.63 19.01 0.77 o 5 6 1 147.10 144.47 3.21 o -5 7 1 4.93 4.80 1.40 o -4 7 1 6.86 9.54 0.77 o -3 7 1 218.84 223.86 5.71 o -2 7 1 340.81 325.65 7.51 o -1 7 1 1787.41 1822.06 35.13 o 0 7 1 140.50 130.93 1.35 o 1 7 1 203.27 182.51 2.25 o 2 7 1 310.41 306.40 4.47 o 3 7 1 567.40 560.46 12.43 o 4 7 1 80.65 86.05 1.16 o 5 7 1 20.38 21.05 1.40 o -5 8 1 25.39 28.71 2.64 o -4 8 1 2.04 3.98 1.10 o -3 8 1 246.16 240.30 3.62 o -2 8 1 704.10 742.13 20.42 o -1 8 1 107.42 99.38 0.96 o 0 8 1 289.62 291.21 2.78 o 1 8 1 492.12 543.75 5.32 o 2 8 1 843.05 850.22 10.11 o 3 8 1 22.46 23.69 0.98 o 4 8 1 70.23 70.58 1.27 o 5 8 1 85.84 95.46 2.17 o -5 9 1 1.79 2.00 0.91 o -4 9 1 365.47 388.62 8.73 o -3 9 1 877.18 855.97 20.44 o -2 9 1 123.21 117.09 2.59 o -1 9 1 278.64 283.85 2.58 o 0 9 1 1192.58 1264.51 15.17 o 1 9 1 213.33 237.62 1.87 o 2 9 1 833.26 838.10 12.72 o 3 9 1 135.40 149.73 1.73 o 4 9 1 405.53 419.78 11.86 o 5 9 1 2.37 3.69 1.09 o -4 10 1 78.54 77.79 1.69 o -3 10 1 46.30 40.62 1.20 o -2 10 1 854.45 860.29 12.78 o -1 10 1 40.47 38.02 0.98 o 0 10 1 52.76 50.80 0.93 o 1 10 1 486.03 500.57 3.84 o 2 10 1 60.98 64.82 1.30 o 3 10 1 158.17 148.02 2.35 o 4 10 1 0.05 0.29 1.11 o -4 11 1 124.94 132.79 2.48 o -3 11 1 536.29 520.21 6.49 o -2 11 1 541.06 549.85 6.81 o -1 11 1 396.57 401.50 4.94 o 0 11 1 827.69 838.89 4.80 o 1 11 1 64.76 67.48 1.17 o 2 11 1 69.02 61.38 1.14 o 3 11 1 7.82 11.49 1.01 o 4 11 1 0.04 1.05 1.07 o -4 12 1 15.55 13.75 0.90 o -3 12 1 93.94 97.39 1.71 o -2 12 1 4.57 5.98 0.85 o -1 12 1 99.88 92.16 1.09 o 0 12 1 352.07 338.99 3.88 o 1 12 1 292.19 295.14 1.93 o 2 12 1 1.30 2.09 1.06 o 3 12 1 0.33 -0.05 0.84 o 4 12 1 21.29 22.88 1.05 o -4 13 1 3.54 4.44 0.88 o -3 13 1 535.14 525.40 11.45 o -2 13 1 38.82 41.98 1.11 o -1 13 1 73.71 79.15 0.96 o 0 13 1 0.00 -0.46 0.85 o 1 13 1 20.84 22.72 0.85 o 2 13 1 39.00 41.69 1.14 o 3 13 1 545.71 520.10 12.17 o 4 13 1 51.35 49.77 1.48 o -4 14 1 41.01 37.16 1.25 o -3 14 1 166.29 164.74 3.54 o -2 14 1 320.26 332.69 6.50 o -1 14 1 134.06 135.24 1.13 o 0 14 1 960.82 978.17 9.56 o 1 14 1 304.72 285.57 3.38 o 2 14 1 97.50 97.27 1.15 o 3 14 1 1.04 -0.37 0.98 o -3 15 1 71.10 69.36 2.40 o -2 15 1 24.48 27.21 1.17 o -1 15 1 166.91 156.22 1.35 o 0 15 1 160.58 160.23 1.34 o 1 15 1 42.16 44.85 1.00 o 2 15 1 163.64 169.03 1.86 o 3 15 1 41.57 44.19 1.22 o -3 16 1 6.60 8.65 0.95 o -2 16 1 324.11 310.91 5.68 o -1 16 1 0.40 0.81 0.96 o 0 16 1 27.81 25.51 1.19 o 1 16 1 0.03 0.22 0.80 o 2 16 1 235.26 222.72 2.77 o 3 16 1 22.82 25.29 0.88 o -2 17 1 1.47 2.31 1.13 o -1 17 1 137.14 122.65 1.98 o 0 17 1 103.06 105.12 1.20 o 1 17 1 68.45 74.04 1.21 o 2 17 1 3.52 3.35 0.85 o -2 18 1 129.32 135.39 3.38 o -1 18 1 9.97 10.75 1.08 o 0 18 1 7.53 6.31 1.09 o 1 18 1 178.25 177.96 3.14 o 2 18 1 43.21 42.25 0.91 o -1 19 1 77.85 73.09 1.25 o 0 19 1 8.24 7.30 1.12 o 1 19 1 2.79 5.10 0.99 o -4 0 2 11.30 12.16 1.11 o -2 0 2 715.66 695.07 12.25 o 2 0 2 170.85 162.54 2.86 o 4 0 2 267.35 251.45 8.07 o -5 1 2 0.02 1.98 3.50 o -4 1 2 0.97 3.30 0.85 o -3 1 2 5.14 7.70 1.01 o -2 1 2 465.78 410.77 14.89 o -1 1 2 5333.50 4913.54 112.02 o 1 1 2 2668.26 2672.28 24.52 o 2 1 2 59.53 54.02 0.94 o 3 1 2 12.15 19.13 0.95 o 4 1 2 0.36 1.41 1.52 o 5 1 2 36.12 37.54 1.66 o -5 2 2 33.22 32.72 1.40 o -4 2 2 236.42 241.21 2.96 o -3 2 2 61.86 68.70 2.20 o -2 2 2 86.73 81.24 2.13 o -1 2 2 6.21 5.55 1.09 o 1 2 2 579.37 538.69 3.30 o 2 2 2 111.78 105.80 1.05 o 3 2 2 789.51 782.39 7.19 o 4 2 2 57.68 60.39 1.23 o 5 2 2 27.49 26.10 1.25 o -5 3 2 416.70 418.45 8.40 o -4 3 2 23.30 25.99 1.10 o -3 3 2 1048.23 1088.34 15.92 o -2 3 2 463.16 461.12 4.36 o -1 3 2 451.55 446.12 7.18 o 0 3 2 434.56 342.71 3.40 o 1 3 2 214.19 233.77 2.05 o 2 3 2 387.17 375.99 5.59 o 3 3 2 103.30 101.19 1.87 o 4 3 2 69.73 69.13 1.71 o 5 3 2 111.59 99.92 1.80 o -5 4 2 42.72 42.32 1.48 o -4 4 2 122.80 117.91 2.55 o -3 4 2 125.27 147.72 2.22 o -2 4 2 274.05 266.85 7.31 o -1 4 2 3290.93 3451.78 64.53 o 0 4 2 7.36 2.88 1.01 o 1 4 2 1201.10 1160.13 13.04 o 2 4 2 212.04 199.29 1.69 o 3 4 2 2.99 4.71 0.84 o 4 4 2 816.82 792.92 18.47 o 5 4 2 5.93 6.30 0.89 o -5 5 2 10.19 10.53 1.36 o -4 5 2 6.34 9.99 1.39 o -3 5 2 16.69 15.30 0.93 o -2 5 2 339.10 304.44 3.74 o -1 5 2 4.15 3.24 0.96 o 0 5 2 2932.25 2925.32 47.25 o 1 5 2 269.27 249.44 2.93 o 2 5 2 851.32 805.51 12.19 o 3 5 2 74.21 63.60 0.95 o 4 5 2 241.19 242.41 4.43 o 5 5 2 91.50 90.65 1.70 o -5 6 2 40.63 43.60 2.49 o -4 6 2 197.62 206.91 2.15 o -3 6 2 0.06 0.77 1.16 o -2 6 2 440.67 459.93 8.48 o -1 6 2 165.01 162.28 3.73 o 0 6 2 3588.49 3864.18 32.16 o 1 6 2 2.86 6.61 1.12 o 2 6 2 47.32 57.23 1.00 o 3 6 2 11.27 5.75 0.87 o 4 6 2 24.60 24.02 0.95 o 5 6 2 70.06 65.92 1.75 o -5 7 2 1.04 0.13 1.43 o -4 7 2 69.28 72.08 1.75 o -3 7 2 102.81 101.86 3.20 o -2 7 2 1027.48 1065.49 33.83 o -1 7 2 505.81 526.45 2.96 o 0 7 2 343.93 342.74 3.71 o 1 7 2 18.97 33.59 1.00 o 2 7 2 43.12 40.25 0.96 o 3 7 2 78.76 81.74 1.33 o 4 7 2 103.68 104.27 2.49 o 5 7 2 3.12 2.78 1.18 o -5 8 2 0.01 -0.37 1.40 o -4 8 2 1.07 -0.52 1.66 o -3 8 2 273.17 257.57 4.30 o -2 8 2 0.01 1.24 1.01 o -1 8 2 228.96 226.72 2.47 o 0 8 2 484.02 466.32 4.35 o 1 8 2 1260.82 1335.20 10.02 o 2 8 2 7.55 4.39 1.09 o 3 8 2 5.06 4.70 1.05 o 4 8 2 69.34 84.04 1.86 o 5 8 2 63.54 58.31 4.73 o -5 9 2 187.41 184.35 3.59 o -4 9 2 58.19 65.42 1.99 o -3 9 2 4.40 6.34 1.36 o -2 9 2 1.26 2.68 0.96 o -1 9 2 629.73 670.73 9.58 o 0 9 2 123.01 138.88 1.46 o 1 9 2 2855.07 3031.47 37.32 o 2 9 2 659.36 677.10 17.25 o 3 9 2 0.04 0.27 0.79 o 4 9 2 2.49 1.98 1.00 o -4 10 2 34.55 38.86 1.54 o -3 10 2 90.75 93.59 3.39 o -2 10 2 288.52 308.36 2.52 o -1 10 2 1398.24 1420.26 17.19 o 0 10 2 1100.12 1087.16 13.12 o 1 10 2 233.39 237.09 1.74 o 2 10 2 3.44 1.58 0.91 o 3 10 2 661.77 672.49 8.99 o 4 10 2 0.84 1.68 1.47 o -4 11 2 43.04 45.59 1.54 o -3 11 2 17.61 12.11 1.60 o -2 11 2 334.57 348.60 4.13 o -1 11 2 681.55 664.62 5.88 o 0 11 2 42.16 33.94 0.87 o 1 11 2 641.53 643.01 4.68 o 2 11 2 811.09 748.18 7.76 o 3 11 2 15.85 14.99 0.88 o 4 11 2 76.41 77.38 2.33 o -4 12 2 97.07 93.38 2.11 o -3 12 2 86.79 80.81 1.22 o -2 12 2 8.68 9.32 1.23 o -1 12 2 229.68 219.39 2.30 o 0 12 2 645.25 636.82 5.78 o 1 12 2 0.02 0.72 0.98 o 2 12 2 807.02 769.98 11.74 o 3 12 2 21.68 25.47 0.87 o 4 12 2 15.88 13.05 1.04 o -4 13 2 240.90 234.33 7.46 o -3 13 2 0.69 0.19 1.73 o -2 13 2 201.07 195.72 2.94 o -1 13 2 18.52 18.81 0.83 o 0 13 2 417.09 429.73 3.64 o 1 13 2 14.65 12.66 0.96 o 2 13 2 380.06 404.33 5.75 o 3 13 2 49.81 50.36 1.57 o 4 13 2 130.38 121.65 3.79 o -4 14 2 48.25 43.31 2.62 o -3 14 2 20.14 19.18 1.38 o -2 14 2 3.24 5.72 0.91 o -1 14 2 23.33 25.73 1.02 o 0 14 2 796.29 790.87 8.00 o 1 14 2 2.65 1.71 0.92 o 2 14 2 13.08 15.32 0.92 o 3 14 2 368.72 353.82 7.41 o -3 15 2 20.30 22.65 1.17 o -2 15 2 202.63 202.60 1.53 o -1 15 2 553.70 558.66 7.18 o 0 15 2 192.90 175.74 1.87 o 1 15 2 465.48 486.44 3.53 o 2 15 2 107.33 100.43 0.96 o 3 15 2 96.72 96.88 1.51 o -3 16 2 362.17 344.54 10.90 o -2 16 2 25.03 25.68 1.04 o -1 16 2 761.16 770.55 8.29 o 0 16 2 0.03 -0.13 0.95 o 1 16 2 78.57 71.13 0.91 o 2 16 2 63.39 58.13 0.89 o 3 16 2 112.47 110.96 3.53 o -2 17 2 155.94 147.72 3.35 o -1 17 2 9.19 7.45 1.11 o 0 17 2 64.18 60.31 0.90 o 1 17 2 144.15 146.40 1.20 o 2 17 2 137.59 132.74 1.36 o -2 18 2 0.54 0.24 1.05 o -1 18 2 226.59 232.27 5.86 o 0 18 2 292.93 277.87 2.27 o 1 18 2 114.74 124.19 1.31 o 2 18 2 99.77 103.95 1.70 o -1 19 2 0.35 0.59 1.00 o 0 19 2 0.69 0.14 0.91 o 1 19 2 22.65 26.42 0.93 o -5 0 3 115.31 107.51 2.00 o -3 0 3 1076.96 1057.84 4.13 o 1 0 3 2310.79 2211.86 12.98 o 3 0 3 205.39 191.87 1.60 o 5 0 3 37.95 30.42 1.33 o -5 1 3 49.94 51.81 1.02 o -4 1 3 724.17 765.74 8.56 o -3 1 3 564.72 555.67 14.50 o -2 1 3 21.61 15.58 1.36 o 0 1 3 278.47 254.31 2.62 o 1 1 3 248.65 213.57 2.67 o 2 1 3 384.13 422.67 4.03 o 3 1 3 682.89 730.21 6.33 o 4 1 3 0.38 -0.41 1.04 o 5 1 3 2.98 3.39 0.95 o -5 2 3 5.75 6.69 1.28 o -4 2 3 1.08 3.94 1.31 o -3 2 3 100.45 111.82 1.81 o -2 2 3 1780.00 1783.44 39.53 o 0 2 3 190.75 183.18 2.80 o 1 2 3 1849.52 1820.69 26.59 o 2 2 3 230.15 246.87 3.61 o 3 2 3 142.29 135.33 1.00 o 4 2 3 7.40 7.74 1.07 o 5 2 3 0.34 0.11 1.51 o -5 3 3 32.11 35.52 1.06 o -4 3 3 253.61 267.73 4.07 o -3 3 3 23.06 23.72 0.95 o -2 3 3 563.54 543.37 12.61 o 0 3 3 1057.26 1061.78 5.00 o 1 3 3 82.04 77.01 1.07 o 2 3 3 4027.24 4251.98 63.40 o 3 3 3 54.52 52.87 1.93 o 4 3 3 54.14 53.62 1.15 o 5 3 3 41.79 45.51 1.20 o -5 4 3 35.52 40.03 1.63 o -4 4 3 66.48 69.76 2.41 o -3 4 3 66.56 68.76 2.39 o -2 4 3 2987.70 3028.22 170.88 o -1 4 3 109.24 94.85 2.47 o 0 4 3 277.32 247.20 2.00 o 1 4 3 11.93 10.91 1.04 o 2 4 3 0.52 -0.52 0.96 o 3 4 3 7.53 6.76 0.80 o 4 4 3 365.50 360.51 3.88 o 5 4 3 0.31 0.14 0.91 o -5 5 3 24.03 25.85 2.14 o -4 5 3 483.37 497.48 5.28 o -3 5 3 956.35 975.55 15.75 o -2 5 3 318.65 333.79 6.00 o -1 5 3 600.70 572.58 6.56 o 0 5 3 333.66 303.08 1.55 o 1 5 3 1012.01 1006.92 15.79 o 2 5 3 439.67 432.78 4.60 o 3 5 3 33.35 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