#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2205520.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205520_Fobs loop_ _publ_author_name 'Nagaraj, Basavegowda' 'Yathirajan, Hemmige S.' 'Nagaraja, Padmarajaiah' 'Lynch, Daniel E.' _publ_section_title ; 1-(Carbamoylmethyl)cyclohexanecarboxylic acid ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o884 _journal_page_last o885 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.627 _cell_angle_gamma 90.000 _cell_length_a 13.4973 _cell_length_b 8.0905 _cell_length_c 8.8358 _exptl_crystal_F_000 400.00 _reflns_d_resolution_high 0.8108 _[local]_cod_data_source_file is6057Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title '1-(Carbamoylmethyl)cyclohexanecarboxylic acid' _shelx_refln_list_code 4 _shelx_f_calc_maximum 93.36 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 209.54 194.08 3.59 o 4 0 0 1269.09 1162.65 18.78 o 5 0 0 38.27 55.82 1.37 o 6 0 0 5.89 4.66 0.69 o 7 0 0 161.38 166.21 2.87 o 8 0 0 4.30 4.12 0.55 o 9 0 0 21.68 23.08 1.19 o 10 0 0 206.73 221.13 4.30 o 11 0 0 440.79 465.35 9.05 o 12 0 0 10.61 8.22 1.12 o 13 0 0 88.20 80.78 4.54 o 14 0 0 80.61 72.12 5.85 o 15 0 0 12.60 8.54 2.49 o 16 0 0 163.28 154.20 12.96 o 2 1 0 253.72 209.77 7.17 o 3 1 0 180.05 162.82 2.51 o 4 1 0 1597.65 1604.49 15.57 o 5 1 0 1383.55 1459.23 15.84 o 6 1 0 31.12 24.94 0.71 o 7 1 0 201.48 202.82 2.61 o 8 1 0 119.61 112.03 1.54 o 9 1 0 149.40 160.76 2.48 o 10 1 0 6.65 4.54 0.56 o 11 1 0 0.52 1.78 0.62 o 12 1 0 403.57 419.39 7.18 o 13 1 0 0.02 0.00 1.03 o 14 1 0 73.50 67.78 2.96 o 15 1 0 132.59 139.66 5.44 o 16 1 0 176.19 174.77 14.00 o 0 2 0 824.09 821.55 15.72 o 1 2 0 1337.08 1280.97 15.27 o 2 2 0 1405.70 1342.07 11.79 o 3 2 0 2663.06 2695.45 27.28 o 4 2 0 295.63 311.50 3.64 o 5 2 0 1570.69 1611.23 15.83 o 6 2 0 10.47 18.33 0.58 o 7 2 0 17.13 23.62 0.72 o 8 2 0 523.29 532.19 6.08 o 9 2 0 164.07 159.56 2.13 o 10 2 0 0.08 -0.02 0.52 o 11 2 0 123.49 129.92 2.61 o 12 2 0 11.64 15.19 1.06 o 13 2 0 14.08 10.35 1.28 o 14 2 0 104.07 102.99 3.87 o 15 2 0 31.76 20.50 3.28 o 1 3 0 83.15 70.37 1.11 o 2 3 0 0.14 1.18 0.25 o 3 3 0 1092.40 1050.02 9.47 o 4 3 0 272.64 240.31 2.78 o 5 3 0 4.20 10.07 0.93 o 6 3 0 6.80 6.52 0.49 o 7 3 0 980.75 976.22 9.39 o 8 3 0 256.69 265.43 3.03 o 9 3 0 15.62 21.46 1.15 o 10 3 0 466.51 471.09 6.31 o 11 3 0 252.16 260.64 5.91 o 12 3 0 379.45 372.12 7.53 o 13 3 0 6.37 7.82 1.46 o 14 3 0 0.69 -0.51 2.03 o 15 3 0 40.53 43.62 4.13 o 0 4 0 41.62 51.15 1.74 o 1 4 0 65.83 72.01 1.57 o 2 4 0 111.15 123.34 2.00 o 3 4 0 352.61 368.48 3.85 o 4 4 0 77.56 97.98 3.99 o 5 4 0 72.22 85.99 1.39 o 6 4 0 28.00 27.31 0.94 o 7 4 0 114.08 117.96 1.79 o 8 4 0 513.99 549.71 8.17 o 9 4 0 5.99 8.27 0.91 o 10 4 0 40.63 42.44 1.42 o 11 4 0 3.93 5.73 1.26 o 12 4 0 10.43 8.12 1.09 o 13 4 0 16.87 12.83 2.54 o 14 4 0 11.85 7.22 2.09 o 1 5 0 180.06 185.71 3.65 o 2 5 0 82.90 90.59 2.82 o 3 5 0 245.03 259.15 5.60 o 4 5 0 222.08 227.56 2.80 o 5 5 0 26.63 32.00 0.86 o 6 5 0 489.78 493.42 9.67 o 7 5 0 835.27 879.11 10.18 o 8 5 0 741.57 784.09 10.82 o 9 5 0 2.81 2.13 0.74 o 10 5 0 4.41 5.34 0.86 o 11 5 0 0.00 1.26 0.93 o 12 5 0 322.22 335.35 12.48 o 13 5 0 46.46 43.62 2.88 o 14 5 0 3.03 0.35 4.06 o 0 6 0 44.43 40.92 1.68 o 1 6 0 5.66 7.88 0.82 o 2 6 0 11.29 12.53 0.69 o 3 6 0 69.96 64.48 1.52 o 4 6 0 7.35 8.82 0.92 o 5 6 0 7.75 10.84 0.64 o 6 6 0 514.99 528.77 6.57 o 7 6 0 348.74 368.63 5.10 o 8 6 0 262.24 280.13 4.74 o 9 6 0 525.55 561.09 10.22 o 10 6 0 25.59 23.22 1.40 o 11 6 0 2.64 2.16 1.40 o 12 6 0 213.16 214.29 12.68 o 1 7 0 201.43 197.53 3.50 o 2 7 0 304.95 310.35 5.68 o 3 7 0 471.39 472.51 7.12 o 4 7 0 2.93 3.85 0.73 o 5 7 0 30.28 26.92 1.32 o 6 7 0 17.64 16.77 1.08 o 7 7 0 2.72 2.29 0.76 o 8 7 0 27.97 33.40 1.50 o 9 7 0 53.36 47.85 2.06 o 10 7 0 252.10 261.97 10.57 o 11 7 0 144.83 148.94 10.76 o 0 8 0 382.17 407.94 9.61 o 1 8 0 2.18 4.00 1.00 o 2 8 0 99.41 93.36 2.62 o 3 8 0 16.30 14.91 1.24 o 4 8 0 6.95 5.85 0.94 o 5 8 0 59.42 55.90 2.07 o 6 8 0 17.53 15.26 1.38 o 7 8 0 97.19 88.73 4.48 o 8 8 0 26.93 30.16 4.00 o 9 8 0 0.04 -0.74 2.24 o 1 9 0 37.34 33.59 2.22 o 2 9 0 150.47 148.82 4.69 o 3 9 0 6.24 9.90 1.28 o 4 9 0 24.02 22.14 1.86 o 5 9 0 3.62 3.22 1.89 o 6 9 0 94.65 87.57 4.85 o 7 9 0 16.56 21.16 2.94 o -16 1 1 41.31 37.71 3.70 o -15 1 1 42.45 37.83 2.41 o -14 1 1 367.63 374.61 10.48 o -13 1 1 4.26 6.03 1.03 o -12 1 1 4.37 4.42 0.85 o -11 1 1 24.47 19.26 1.21 o -10 1 1 47.16 47.15 1.14 o -9 1 1 183.11 189.41 2.61 o -8 1 1 1367.72 1416.52 11.62 o -7 1 1 1041.43 1061.75 10.86 o -6 1 1 4.96 3.30 0.34 o -5 1 1 728.48 685.28 8.41 o -4 1 1 1254.61 1177.64 12.84 o -3 1 1 290.06 293.90 3.34 o -2 1 1 1259.84 1100.98 20.76 o -1 1 1 7417.96 3650.26 314.54 o 0 1 1 654.86 588.76 11.31 o 2 1 1 109.28 100.58 1.50 o 3 1 1 41.38 37.93 0.84 o 4 1 1 4962.01 5357.56 51.64 o 5 1 1 41.78 54.99 0.84 o 6 1 1 127.79 150.73 1.75 o 7 1 1 0.86 1.94 0.46 o 8 1 1 101.67 96.90 1.54 o 9 1 1 183.12 186.42 2.69 o 10 1 1 59.90 60.71 1.42 o 11 1 1 203.45 215.38 3.96 o 12 1 1 359.86 386.70 7.23 o 13 1 1 11.73 12.42 1.40 o 14 1 1 5.63 4.58 1.91 o 15 1 1 65.75 57.51 4.66 o -16 2 1 13.31 15.62 2.40 o -15 2 1 33.06 27.88 2.39 o -14 2 1 15.06 16.49 1.83 o -13 2 1 180.04 186.62 4.46 o -12 2 1 0.79 1.58 0.92 o -11 2 1 293.77 301.14 5.71 o -10 2 1 0.85 1.42 0.62 o -9 2 1 12.02 11.50 0.77 o -8 2 1 20.72 20.09 0.77 o -7 2 1 1.71 3.32 0.52 o -6 2 1 124.18 136.93 1.88 o -5 2 1 1132.27 1163.97 10.65 o -4 2 1 4179.92 4483.75 60.62 o -3 2 1 3948.86 4193.49 53.58 o -2 2 1 552.35 510.28 6.20 o -1 2 1 6.52 9.68 0.34 o 0 2 1 176.69 130.22 1.09 o 1 2 1 421.96 341.38 2.62 o 2 2 1 972.79 973.38 7.94 o 3 2 1 912.32 899.25 9.12 o 4 2 1 353.97 347.17 4.24 o 5 2 1 37.41 39.06 1.57 o 6 2 1 31.13 25.84 0.88 o 7 2 1 1249.49 1282.62 10.72 o 8 2 1 195.48 196.39 2.85 o 9 2 1 76.58 88.07 1.60 o 10 2 1 802.65 775.43 9.94 o 11 2 1 126.85 123.01 2.64 o 12 2 1 71.17 70.54 2.10 o 13 2 1 150.93 135.68 4.47 o 14 2 1 10.95 10.71 2.08 o 15 2 1 28.81 27.49 3.35 o -15 3 1 39.95 36.20 3.10 o -14 3 1 0.53 -0.04 1.86 o -13 3 1 32.97 30.71 1.47 o -12 3 1 3.22 7.20 1.33 o -11 3 1 408.74 440.19 6.94 o -10 3 1 208.73 226.62 5.09 o -9 3 1 245.08 259.32 4.64 o -8 3 1 416.18 435.12 4.78 o -7 3 1 11.74 12.01 0.82 o -6 3 1 29.62 27.85 0.84 o -5 3 1 5.47 8.48 0.52 o -4 3 1 293.61 279.83 3.78 o -3 3 1 58.12 61.30 1.60 o -2 3 1 5.79 4.32 0.32 o -1 3 1 1082.40 1025.47 8.89 o 0 3 1 1657.01 1634.61 13.24 o 1 3 1 146.12 159.84 1.43 o 2 3 1 5.23 8.19 0.43 o 3 3 1 553.68 569.59 9.04 o 4 3 1 5139.19 5767.32 43.38 o 5 3 1 403.16 416.54 4.45 o 6 3 1 1054.59 1112.41 9.66 o 7 3 1 232.38 221.83 2.63 o 8 3 1 17.53 21.99 0.92 o 9 3 1 157.38 171.05 2.70 o 10 3 1 96.36 88.39 1.88 o 11 3 1 222.76 236.59 4.65 o 12 3 1 24.49 29.73 2.05 o 13 3 1 1.05 0.25 1.77 o 14 3 1 9.25 7.05 2.01 o 15 3 1 6.20 6.72 2.46 o -15 4 1 84.92 84.52 6.40 o -14 4 1 17.00 18.22 2.32 o -13 4 1 11.68 9.67 1.39 o -12 4 1 283.35 291.67 6.97 o -11 4 1 530.77 539.26 8.95 o -10 4 1 47.12 45.39 1.31 o -9 4 1 127.72 126.40 2.37 o -8 4 1 1719.65 1789.27 20.96 o -7 4 1 586.87 607.79 6.94 o -6 4 1 952.45 958.61 10.76 o -5 4 1 71.86 74.38 2.14 o -4 4 1 90.41 79.26 1.60 o -3 4 1 0.17 2.88 0.48 o -2 4 1 214.33 225.11 4.46 o -1 4 1 539.51 509.14 5.17 o 0 4 1 697.38 682.90 6.67 o 1 4 1 230.08 229.15 4.48 o 2 4 1 0.01 1.99 0.37 o 3 4 1 92.37 104.80 2.67 o 4 4 1 2117.16 2205.50 20.63 o 5 4 1 425.96 421.87 4.34 o 6 4 1 129.13 133.00 2.46 o 7 4 1 122.88 117.47 2.51 o 8 4 1 166.92 180.78 2.86 o 9 4 1 66.05 68.05 1.64 o 10 4 1 22.94 17.46 1.02 o 11 4 1 236.37 223.95 4.88 o 12 4 1 130.50 122.67 4.26 o 13 4 1 20.13 17.56 2.23 o 14 4 1 0.02 0.07 1.90 o -14 5 1 30.21 39.08 4.92 o -13 5 1 1.01 -1.52 1.30 o -12 5 1 45.53 41.02 2.06 o -11 5 1 1.87 2.22 0.88 o -10 5 1 59.42 57.77 1.54 o -9 5 1 3.44 4.24 0.68 o -8 5 1 105.43 111.81 2.11 o -7 5 1 30.90 35.19 1.66 o -6 5 1 229.68 228.51 3.39 o -5 5 1 0.31 2.28 0.52 o -4 5 1 24.45 21.47 0.62 o -3 5 1 377.53 372.66 5.21 o -2 5 1 907.96 958.74 12.05 o -1 5 1 609.34 615.49 6.87 o 0 5 1 196.88 192.95 2.78 o 1 5 1 51.46 43.74 1.11 o 2 5 1 18.11 21.57 0.86 o 3 5 1 91.86 97.36 1.51 o 4 5 1 356.00 347.37 4.32 o 5 5 1 129.00 137.44 1.88 o 6 5 1 0.15 0.47 0.57 o 7 5 1 52.13 52.61 1.32 o 8 5 1 61.55 63.15 2.50 o 9 5 1 22.93 25.70 1.18 o 10 5 1 2.20 2.52 0.90 o 11 5 1 7.86 7.03 1.68 o 12 5 1 9.67 7.27 1.67 o 13 5 1 117.66 118.15 5.89 o -13 6 1 43.16 41.32 4.56 o -12 6 1 1.55 2.89 1.44 o -11 6 1 17.51 19.27 1.62 o -10 6 1 91.95 88.96 2.78 o -9 6 1 94.71 92.49 2.30 o -8 6 1 209.06 209.21 3.36 o -7 6 1 689.06 730.89 11.78 o -6 6 1 925.86 986.61 12.41 o -5 6 1 11.81 11.49 0.76 o -4 6 1 181.94 164.49 2.86 o -3 6 1 352.00 368.86 5.35 o -2 6 1 3.60 4.82 0.80 o -1 6 1 60.98 63.78 1.52 o 0 6 1 150.31 153.40 2.81 o 1 6 1 0.02 2.02 0.47 o 2 6 1 45.77 45.95 1.23 o 3 6 1 129.33 142.43 3.32 o 4 6 1 7.91 7.81 1.03 o 5 6 1 17.75 17.48 0.84 o 6 6 1 37.22 35.76 1.15 o 7 6 1 46.20 39.53 1.31 o 8 6 1 9.15 10.44 1.03 o 9 6 1 111.49 118.33 3.12 o 10 6 1 27.23 23.67 1.68 o 11 6 1 114.30 125.58 5.05 o 12 6 1 3.74 2.90 1.93 o -11 7 1 1.02 3.31 1.91 o -10 7 1 27.47 25.45 2.14 o -9 7 1 34.04 31.35 1.52 o -8 7 1 1.23 1.56 0.67 o -7 7 1 11.90 11.78 0.84 o -6 7 1 4.73 5.37 0.76 o -5 7 1 29.45 27.62 1.28 o -4 7 1 0.17 0.21 0.54 o -3 7 1 1.17 2.10 0.66 o -2 7 1 0.18 0.60 0.54 o -1 7 1 19.58 19.73 1.05 o 0 7 1 19.30 17.89 1.34 o 1 7 1 50.75 46.23 2.20 o 2 7 1 130.30 132.79 2.49 o 3 7 1 0.56 1.47 0.64 o 4 7 1 455.93 473.31 7.57 o 5 7 1 2.41 2.19 1.03 o 6 7 1 80.93 80.93 2.12 o 7 7 1 2.25 2.46 0.90 o 8 7 1 81.11 79.33 2.50 o 9 7 1 0.11 0.59 1.22 o 10 7 1 8.21 7.59 2.31 o 11 7 1 46.79 41.83 3.91 o -9 8 1 63.39 63.25 3.66 o -8 8 1 1.79 6.71 3.36 o -7 8 1 14.86 16.96 1.46 o -6 8 1 4.51 4.41 1.10 o -5 8 1 23.51 24.20 1.61 o -4 8 1 210.83 225.05 5.05 o -3 8 1 68.08 72.63 2.98 o -2 8 1 103.42 116.65 3.36 o -1 8 1 2.17 1.86 0.94 o 0 8 1 28.92 27.92 1.46 o 1 8 1 364.11 381.10 7.85 o 2 8 1 103.14 100.06 2.68 o 3 8 1 35.98 33.41 1.25 o 4 8 1 41.01 34.44 1.47 o 5 8 1 21.75 21.37 1.49 o 6 8 1 5.78 5.15 1.71 o 7 8 1 26.67 23.19 2.20 o 8 8 1 18.59 15.96 2.63 o 9 8 1 8.29 8.21 2.68 o -7 9 1 18.95 20.45 2.65 o -6 9 1 1.22 -1.06 1.77 o -5 9 1 14.21 12.62 2.39 o -4 9 1 4.20 2.70 1.71 o -3 9 1 17.55 15.63 1.57 o -2 9 1 0.31 1.26 1.11 o -1 9 1 335.41 325.75 7.77 o 0 9 1 72.78 71.63 2.47 o 1 9 1 194.24 217.83 6.34 o 2 9 1 26.69 26.30 2.09 o 3 9 1 12.01 13.36 2.84 o 4 9 1 24.71 25.52 2.10 o 5 9 1 0.95 -0.41 1.52 o 6 9 1 17.66 16.25 3.76 o -16 0 2 0.11 0.89 2.02 o -15 0 2 769.48 843.75 36.54 o -14 0 2 137.00 137.67 5.30 o -13 0 2 923.65 962.50 21.37 o -12 0 2 24.16 22.51 1.96 o -11 0 2 62.84 57.80 1.97 o -10 0 2 4.57 7.90 0.95 o -9 0 2 0.82 1.02 0.65 o -8 0 2 304.93 325.69 6.87 o -7 0 2 1233.58 1285.64 20.18 o -6 0 2 847.74 876.42 13.55 o -5 0 2 96.25 78.75 1.47 o -4 0 2 3429.11 3299.87 53.82 o -3 0 2 1192.57 1069.82 16.57 o -2 0 2 34.03 18.82 0.68 o -1 0 2 3275.56 3295.77 41.25 o 0 0 2 4604.29 4742.73 58.53 o 1 0 2 2217.62 2161.69 23.23 o 2 0 2 4694.56 4953.21 63.92 o 3 0 2 3665.46 3686.30 32.10 o 4 0 2 3928.75 4234.96 40.36 o 5 0 2 1781.98 1852.12 17.90 o 6 0 2 42.42 48.69 1.37 o 7 0 2 35.93 33.59 1.25 o 8 0 2 1045.13 1080.36 15.43 o 9 0 2 514.47 488.18 9.55 o 10 0 2 503.41 511.50 10.90 o 11 0 2 8.08 8.69 1.99 o 12 0 2 0.27 -2.55 2.28 o 13 0 2 74.11 68.35 5.15 o 14 0 2 1.02 2.16 3.14 o 15 0 2 2.27 -0.05 3.31 o -16 1 2 23.03 19.35 2.72 o -15 1 2 202.39 214.68 6.69 o -14 1 2 332.62 383.43 9.12 o -13 1 2 378.22 391.69 7.66 o -12 1 2 195.23 195.12 3.75 o -11 1 2 97.86 93.21 2.07 o -10 1 2 0.08 0.93 0.55 o -9 1 2 103.07 103.96 1.83 o -8 1 2 124.17 134.06 1.65 o -7 1 2 0.65 3.59 0.45 o -6 1 2 267.90 261.93 2.74 o -5 1 2 783.18 771.48 9.20 o -4 1 2 3123.85 3349.39 35.31 o -3 1 2 773.45 676.50 9.81 o -2 1 2 550.68 463.27 6.07 o -1 1 2 2790.79 2850.92 24.31 o 0 1 2 243.75 225.34 2.07 o 1 1 2 2617.94 2595.66 19.47 o 2 1 2 3834.37 3954.29 30.64 o 3 1 2 1168.48 1095.85 8.58 o 4 1 2 137.98 128.40 1.40 o 5 1 2 498.59 532.75 4.05 o 6 1 2 112.77 113.98 1.47 o 7 1 2 261.77 262.78 2.73 o 8 1 2 947.91 985.44 10.96 o 9 1 2 10.07 9.85 0.84 o 10 1 2 31.35 31.05 1.37 o 11 1 2 61.32 54.31 1.75 o 12 1 2 140.59 144.15 4.87 o 13 1 2 56.47 57.92 3.20 o 14 1 2 4.25 3.79 2.39 o 15 1 2 0.75 -2.47 2.36 o -16 2 2 0.04 1.35 2.11 o -15 2 2 154.69 157.17 7.14 o -14 2 2 73.95 67.84 2.51 o -13 2 2 107.00 106.96 3.00 o -12 2 2 42.00 38.58 1.40 o -11 2 2 1.41 1.26 0.61 o -10 2 2 447.53 465.56 5.90 o -9 2 2 47.35 47.38 1.21 o -8 2 2 19.71 22.50 0.71 o -7 2 2 1.24 7.64 0.66 o -6 2 2 85.99 78.86 2.79 o -5 2 2 10.60 19.57 1.42 o -4 2 2 24.64 33.13 2.32 o -3 2 2 0.18 8.10 0.79 o -2 2 2 787.67 795.78 9.71 o -1 2 2 7.16 10.54 0.33 o 0 2 2 127.52 122.59 1.24 o 1 2 2 2336.96 2399.26 17.80 o 2 2 2 17.79 21.00 0.62 o 3 2 2 3189.64 3484.96 27.51 o 4 2 2 186.45 218.55 2.55 o 5 2 2 2094.02 2295.22 21.67 o 6 2 2 109.62 114.40 1.79 o 7 2 2 122.50 124.08 1.83 o 8 2 2 416.48 431.52 5.56 o 9 2 2 12.62 13.96 0.88 o 10 2 2 1.91 2.87 0.76 o 11 2 2 18.86 20.54 1.20 o 12 2 2 0.00 1.96 1.16 o 13 2 2 3.20 1.31 1.56 o 14 2 2 2.04 5.11 2.24 o -15 3 2 2.34 4.02 1.82 o -14 3 2 26.21 23.06 1.82 o -13 3 2 3.39 2.57 1.01 o -12 3 2 2.18 0.95 0.76 o -11 3 2 66.40 75.50 2.82 o -10 3 2 1.54 2.32 0.66 o -9 3 2 183.44 194.83 3.05 o -8 3 2 6.78 8.10 0.85 o -7 3 2 483.66 478.14 8.37 o -6 3 2 171.92 169.90 2.37 o -5 3 2 53.74 52.48 1.12 o -4 3 2 221.87 216.19 2.87 o -3 3 2 1591.78 1736.55 25.02 o -2 3 2 578.66 603.83 6.62 o -1 3 2 1033.97 1077.77 9.80 o 0 3 2 341.92 339.19 2.97 o 1 3 2 444.79 440.05 3.33 o 2 3 2 0.44 1.81 0.32 o 3 3 2 365.85 375.03 3.98 o 4 3 2 172.81 160.12 5.14 o 5 3 2 58.04 45.07 0.95 o 6 3 2 27.74 34.76 1.23 o 7 3 2 51.17 54.43 1.34 o 8 3 2 21.60 20.50 0.95 o 9 3 2 94.91 81.25 1.77 o 10 3 2 20.93 17.28 1.17 o 11 3 2 55.09 37.76 1.68 o 12 3 2 10.25 5.32 1.99 o 13 3 2 4.79 7.63 1.77 o 14 3 2 37.47 35.71 3.38 o -15 4 2 13.13 10.42 4.32 o -14 4 2 18.89 13.08 2.48 o -13 4 2 0.02 -0.48 1.03 o -12 4 2 33.03 35.71 1.49 o -11 4 2 0.02 3.89 1.00 o -10 4 2 370.85 360.84 6.39 o -9 4 2 73.01 74.77 1.68 o -8 4 2 24.99 31.39 1.22 o -7 4 2 0.43 4.51 0.51 o -6 4 2 41.12 40.40 1.75 o -5 4 2 392.55 367.26 4.58 o -4 4 2 80.74 64.49 1.22 o -3 4 2 199.47 198.06 2.99 o -2 4 2 62.01 61.23 1.12 o -1 4 2 116.93 112.30 2.90 o 0 4 2 0.29 2.31 0.32 o 1 4 2 163.07 162.31 1.63 o 2 4 2 68.00 62.67 1.09 o 3 4 2 326.93 366.33 3.29 o 4 4 2 66.38 69.68 1.23 o 5 4 2 91.91 112.85 1.79 o 6 4 2 64.35 57.84 1.28 o 7 4 2 4.22 4.45 0.74 o 8 4 2 7.97 12.38 0.91 o 9 4 2 6.12 7.87 0.90 o 10 4 2 31.51 27.41 1.35 o 11 4 2 50.03 50.16 2.17 o 12 4 2 158.45 146.38 5.88 o 13 4 2 48.14 43.01 3.60 o -14 5 2 163.08 158.48 10.78 o -13 5 2 27.02 26.58 3.62 o -12 5 2 49.63 44.45 2.10 o -11 5 2 30.54 31.17 1.43 o -10 5 2 6.27 9.38 0.85 o -9 5 2 75.23 78.28 2.01 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