#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/55/2205529.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205529_Fobs loop_ _publ_author_name 'Hu, Mao-Lin' 'Cheng, Ya-Qian' 'Wang, Shun' 'Yuan, Ji-Xin' 'Cai, Xiao-Qing' _publ_section_title ; 6,6'-Dioxo-2,2-bi(7-oxatricyclo[3.2.1.1^3,8^]nonane)-4,4'-dicarboxylic acid ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1196 _journal_page_last o1197 _journal_volume 61 _journal_year 2005 _space_group_IT_number 41 _symmetry_space_group_name_Hall 'A 2 -2ab' _symmetry_space_group_name_H-M 'A b a 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.8562 _cell_length_b 13.4978 _cell_length_c 11.8371 _exptl_crystal_F_000 760.00 _reflns_d_resolution_high 0.8333 _[local]_cod_data_source_file kp6045Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' c in Aba2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 166.97 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' 'x+1/2, -y+1, z+1/2' '-x+1/2, y+1, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5948.79 5956.09 134.91 o 4 0 0 1331.50 1405.66 37.20 o 6 0 0 923.45 870.77 27.82 o 8 0 0 2329.00 2151.10 60.02 o 10 0 0 77.65 108.63 12.15 o 0 2 0 1407.39 1250.22 43.56 o 1 2 0 27880.05 26174.01 479.12 o 2 2 0 10150.49 10120.64 160.85 o 3 2 0 380.24 341.02 7.79 o 4 2 0 1735.88 1860.64 30.62 o 5 2 0 389.54 399.87 9.94 o 6 2 0 12.82 8.80 2.24 o 7 2 0 28.12 16.92 3.16 o 8 2 0 96.82 84.57 6.19 o 9 2 0 54.68 45.87 5.27 o 10 2 0 138.97 144.03 8.99 o 11 2 0 80.41 109.65 8.51 o 0 4 0 8933.23 9041.09 292.47 o 1 4 0 1417.47 1253.32 26.41 o 2 4 0 10.47 12.82 2.87 o 3 4 0 682.20 662.57 14.45 o 4 4 0 1032.73 1183.20 23.65 o 5 4 0 1186.63 1252.98 25.62 o 6 4 0 2958.88 2846.45 77.67 o 7 4 0 88.00 83.60 6.58 o 8 4 0 813.37 797.09 20.73 o 9 4 0 115.70 127.88 9.70 o 10 4 0 187.95 191.53 11.31 o 11 4 0 103.87 125.89 10.26 o 0 6 0 4646.84 5050.65 170.16 o 1 6 0 2438.42 2488.47 50.76 o 2 6 0 728.95 782.34 19.61 o 3 6 0 1.76 5.61 2.30 o 4 6 0 4.02 1.72 3.72 o 5 6 0 362.40 393.27 13.61 o 6 6 0 0.81 1.10 2.31 o 7 6 0 21.57 24.51 4.40 o 8 6 0 550.89 527.61 16.54 o 9 6 0 0.16 6.18 3.99 o 10 6 0 30.18 48.09 6.67 o 0 8 0 7469.82 7919.35 183.98 o 1 8 0 733.36 741.25 20.17 o 2 8 0 327.80 354.25 15.05 o 3 8 0 319.48 312.17 11.87 o 4 8 0 13.55 11.35 5.51 o 5 8 0 32.39 29.59 4.85 o 6 8 0 459.39 418.38 15.75 o 7 8 0 537.18 562.85 22.38 o 8 8 0 0.05 6.85 4.60 o 9 8 0 122.89 155.47 15.34 o 10 8 0 33.50 36.24 9.12 o 0 10 0 4.34 1.00 3.32 o 1 10 0 32.15 41.38 5.25 o 2 10 0 17.85 19.72 5.36 o 3 10 0 1158.92 1151.06 29.95 o 4 10 0 1746.86 1659.99 40.09 o 5 10 0 69.67 67.59 10.02 o 6 10 0 14.99 18.04 6.35 o 7 10 0 39.68 62.26 10.37 o 8 10 0 3.11 9.24 6.72 o 9 10 0 44.07 52.70 10.83 o 0 12 0 479.75 517.85 21.89 o 1 12 0 447.13 434.09 29.17 o 2 12 0 415.66 392.53 20.34 o 3 12 0 215.22 196.77 15.76 o 4 12 0 128.92 155.02 31.11 o 5 12 0 564.33 489.57 35.00 o 6 12 0 159.43 182.23 16.78 o 7 12 0 32.32 29.02 8.30 o 0 14 0 571.36 541.12 36.41 o 1 14 0 106.25 91.50 11.76 o 2 14 0 21.85 34.42 7.26 o 3 14 0 14.20 28.59 7.36 o 4 14 0 27.30 36.46 8.17 o 5 14 0 74.61 96.33 21.08 o 0 16 0 73.35 108.13 19.21 o 1 16 0 30.26 51.48 9.06 o 1 1 1 7645.31 7820.63 81.63 o 2 1 1 11157.62 11428.54 108.48 o 3 1 1 968.45 858.59 10.40 o 4 1 1 4886.83 4929.45 54.12 o 5 1 1 2730.10 2864.40 34.95 o 6 1 1 1897.89 1816.19 26.44 o 7 1 1 429.91 389.33 11.18 o 8 1 1 228.16 217.91 7.59 o 9 1 1 555.00 508.01 10.71 o 10 1 1 121.20 107.58 5.62 o 11 1 1 90.60 81.18 5.57 o 1 3 1 3690.37 3624.79 39.04 o 2 3 1 707.14 694.00 9.69 o 3 3 1 1311.22 1183.60 14.11 o 4 3 1 4924.27 5136.52 53.92 o 5 3 1 390.73 417.43 7.03 o 6 3 1 958.10 921.32 13.40 o 7 3 1 403.00 392.81 8.04 o 8 3 1 209.07 195.25 6.34 o 9 3 1 218.06 217.03 7.10 o 10 3 1 59.57 67.70 4.64 o 11 3 1 194.44 210.74 8.98 o 1 5 1 2559.78 2532.33 35.75 o 2 5 1 673.02 649.09 11.55 o 3 5 1 1.53 1.44 1.36 o 4 5 1 120.07 125.21 5.33 o 5 5 1 1179.27 1198.82 18.99 o 6 5 1 54.10 51.72 3.51 o 7 5 1 41.18 46.49 3.67 o 8 5 1 294.41 292.59 10.01 o 9 5 1 433.96 406.59 10.31 o 10 5 1 137.01 154.62 8.13 o 11 5 1 18.91 27.27 4.50 o 1 7 1 874.03 939.66 16.32 o 2 7 1 2766.21 2861.68 41.52 o 3 7 1 589.82 604.45 12.18 o 4 7 1 464.78 441.12 11.62 o 5 7 1 65.50 68.13 4.60 o 6 7 1 164.75 184.75 6.86 o 7 7 1 68.69 77.80 5.17 o 8 7 1 132.57 117.68 6.51 o 9 7 1 405.14 391.14 12.97 o 10 7 1 72.55 85.95 7.91 o 1 9 1 682.92 668.77 13.64 o 2 9 1 17.80 33.69 3.41 o 3 9 1 661.41 630.64 13.45 o 4 9 1 209.88 178.80 6.93 o 5 9 1 510.20 480.20 13.55 o 6 9 1 220.98 235.46 12.28 o 7 9 1 23.24 22.36 4.44 o 8 9 1 504.15 477.30 14.96 o 9 9 1 23.68 36.61 10.81 o 1 11 1 777.49 800.81 18.59 o 2 11 1 9.17 15.75 3.28 o 3 11 1 1032.49 967.61 21.67 o 4 11 1 1009.19 1004.60 22.71 o 5 11 1 156.90 182.59 11.91 o 6 11 1 43.60 53.32 6.94 o 7 11 1 115.63 101.39 9.28 o 8 11 1 38.82 47.99 8.83 o 1 13 1 51.10 67.09 6.09 o 2 13 1 244.47 255.68 16.42 o 3 13 1 21.05 29.91 5.50 o 4 13 1 314.50 282.79 14.47 o 5 13 1 92.99 102.95 9.17 o 6 13 1 56.33 69.98 15.02 o 1 15 1 35.47 66.29 7.18 o 2 15 1 75.64 115.08 9.31 o 3 15 1 129.44 157.43 11.28 o 4 15 1 126.01 117.07 10.17 o 0 0 2 16410.76 16607.50 370.42 o 2 0 2 16127.29 16369.77 234.45 o 4 0 2 5947.92 6217.00 80.54 o 6 0 2 459.37 454.86 13.93 o 8 0 2 747.64 696.86 16.79 o 10 0 2 88.08 99.90 8.87 o 0 2 2 13076.66 13054.57 182.51 o 1 2 2 941.85 925.18 11.14 o 2 2 2 8240.26 8483.21 89.64 o 3 2 2 6493.32 6908.32 73.30 o 4 2 2 497.55 494.22 7.10 o 5 2 2 525.36 528.61 8.52 o 6 2 2 1337.95 1319.29 16.91 o 7 2 2 170.77 164.30 5.51 o 8 2 2 955.37 892.16 15.65 o 9 2 2 32.87 37.80 3.39 o 10 2 2 47.14 52.94 4.74 o 11 2 2 9.90 18.96 4.12 o 0 4 2 6837.80 6819.15 108.88 o 1 4 2 1577.43 1648.72 19.11 o 2 4 2 7746.10 8084.38 85.62 o 3 4 2 1225.89 1199.00 15.07 o 4 4 2 84.88 88.42 3.22 o 5 4 2 112.24 115.68 3.93 o 6 4 2 467.29 427.73 11.71 o 7 4 2 411.65 396.80 8.61 o 8 4 2 415.84 404.39 10.72 o 9 4 2 54.02 68.60 5.06 o 10 4 2 14.91 14.98 3.39 o 11 4 2 43.61 45.02 4.93 o 0 6 2 841.72 931.75 19.37 o 1 6 2 465.61 466.79 8.05 o 2 6 2 3214.40 3273.77 42.40 o 3 6 2 1591.07 1701.62 22.54 o 4 6 2 2028.96 2031.50 26.64 o 5 6 2 343.35 343.25 11.71 o 6 6 2 98.09 94.78 5.00 o 7 6 2 616.90 556.94 13.83 o 8 6 2 9.77 13.68 2.97 o 9 6 2 85.69 79.58 7.05 o 10 6 2 58.35 71.54 7.94 o 0 8 2 1295.91 1314.90 49.73 o 1 8 2 585.94 599.35 12.17 o 2 8 2 57.52 64.60 4.78 o 3 8 2 1245.46 1160.18 33.27 o 4 8 2 937.06 880.79 19.02 o 5 8 2 280.77 278.80 18.40 o 6 8 2 525.92 477.74 13.64 o 7 8 2 405.49 377.36 12.49 o 8 8 2 189.31 176.76 9.95 o 9 8 2 72.00 99.90 8.29 o 10 8 2 23.00 29.99 5.55 o 0 10 2 12.98 19.72 4.40 o 1 10 2 85.08 81.67 6.02 o 2 10 2 531.45 518.85 13.89 o 3 10 2 361.29 346.55 13.82 o 4 10 2 54.33 52.06 5.25 o 5 10 2 248.32 237.78 10.10 o 6 10 2 95.05 124.36 11.51 o 7 10 2 168.51 160.96 10.87 o 8 10 2 146.20 150.76 13.04 o 9 10 2 23.41 40.53 8.58 o 0 12 2 160.98 148.00 16.28 o 1 12 2 382.48 366.53 12.66 o 2 12 2 334.11 296.87 12.02 o 3 12 2 23.56 37.19 5.01 o 4 12 2 75.57 78.90 6.95 o 5 12 2 381.65 358.23 12.85 o 6 12 2 39.16 46.12 8.63 o 7 12 2 104.64 131.27 13.09 o 0 14 2 6.76 22.18 5.88 o 1 14 2 85.27 107.80 7.87 o 2 14 2 88.74 96.13 7.53 o 3 14 2 94.08 107.91 9.14 o 4 14 2 82.59 99.42 9.26 o 5 14 2 124.04 164.55 18.31 o 0 16 2 113.13 153.07 19.40 o 1 1 3 2862.93 2781.43 34.41 o 2 1 3 12772.89 13184.26 147.01 o 3 1 3 6706.99 6993.50 74.20 o 4 1 3 228.60 212.56 4.22 o 5 1 3 667.98 742.11 9.58 o 6 1 3 326.05 313.96 8.18 o 7 1 3 161.10 149.57 5.18 o 8 1 3 203.91 189.82 7.33 o 9 1 3 221.09 211.33 7.74 o 10 1 3 96.26 107.36 7.42 o 11 1 3 7.65 13.58 4.46 o 1 3 3 3827.69 3864.48 44.47 o 2 3 3 377.32 409.38 5.91 o 3 3 3 909.51 884.17 11.12 o 4 3 3 6423.53 6698.79 69.03 o 5 3 3 1195.92 1188.83 16.78 o 6 3 3 107.30 107.51 4.11 o 7 3 3 554.28 507.58 10.43 o 8 3 3 533.28 513.92 11.43 o 9 3 3 188.11 198.15 7.87 o 10 3 3 123.66 142.48 7.94 o 11 3 3 5.01 11.05 3.71 o 1 5 3 408.68 452.79 8.43 o 2 5 3 1151.04 1150.42 14.62 o 3 5 3 80.86 123.05 5.09 o 4 5 3 486.36 444.99 7.63 o 5 5 3 779.43 762.02 17.21 o 6 5 3 1353.00 1341.35 18.74 o 7 5 3 40.38 43.28 4.01 o 8 5 3 266.08 257.23 9.55 o 9 5 3 164.00 169.94 9.02 o 10 5 3 68.82 98.92 7.99 o 1 7 3 272.53 270.26 6.03 o 2 7 3 188.48 215.30 5.22 o 3 7 3 518.86 502.08 11.18 o 4 7 3 774.66 705.19 13.11 o 5 7 3 623.64 570.32 11.73 o 6 7 3 419.43 411.00 10.88 o 7 7 3 90.80 99.83 7.26 o 8 7 3 321.30 286.09 12.08 o 9 7 3 6.78 15.56 4.59 o 10 7 3 137.15 164.99 10.74 o 1 9 3 184.31 185.59 8.03 o 2 9 3 297.51 273.47 9.23 o 3 9 3 105.52 106.38 6.56 o 4 9 3 507.61 489.48 21.83 o 5 9 3 419.46 410.13 13.76 o 6 9 3 741.06 702.02 20.47 o 7 9 3 55.09 64.06 7.16 o 8 9 3 17.34 17.79 4.41 o 9 9 3 96.94 110.70 9.00 o 1 11 3 258.95 235.00 9.12 o 2 11 3 333.65 311.41 10.94 o 3 11 3 394.19 382.52 12.34 o 4 11 3 514.30 511.78 14.89 o 5 11 3 250.15 258.71 13.03 o 6 11 3 212.11 257.95 13.53 o 7 11 3 87.69 89.79 8.98 o 8 11 3 117.30 116.40 10.49 o 1 13 3 215.32 211.37 9.36 o 2 13 3 412.35 387.86 12.00 o 3 13 3 133.67 152.24 9.27 o 4 13 3 75.48 96.27 9.05 o 5 13 3 0.18 11.33 5.74 o 6 13 3 45.76 58.42 8.92 o 1 15 3 48.14 71.17 6.67 o 2 15 3 12.12 33.73 7.09 o 3 15 3 0.22 10.27 4.95 o 0 0 4 16940.65 17473.35 389.87 o 2 0 4 2998.08 3056.20 58.92 o 4 0 4 6876.72 7312.42 103.77 o 6 0 4 2837.07 2993.75 43.29 o 8 0 4 31.75 30.12 5.33 o 10 0 4 88.78 69.85 11.62 o 0 2 4 2200.50 2285.70 31.59 o 1 2 4 1900.12 1866.91 21.20 o 2 2 4 775.74 850.51 12.71 o 3 2 4 1035.77 1137.16 15.15 o 4 2 4 278.94 301.46 5.49 o 5 2 4 1106.64 1142.94 15.13 o 6 2 4 172.26 189.05 7.77 o 7 2 4 218.80 191.57 9.19 o 8 2 4 409.10 372.68 10.64 o 9 2 4 585.72 541.44 15.62 o 10 2 4 91.55 115.10 7.95 o 11 2 4 54.48 47.90 6.49 o 0 4 4 4915.37 5040.82 81.30 o 1 4 4 563.38 618.08 9.39 o 2 4 4 220.83 225.21 4.99 o 3 4 4 1140.70 1187.65 14.57 o 4 4 4 705.89 705.49 9.97 o 5 4 4 207.70 187.10 4.60 o 6 4 4 1292.08 1246.94 18.94 o 7 4 4 50.46 51.95 4.11 o 8 4 4 99.02 97.52 6.54 o 9 4 4 135.21 119.52 8.58 o 10 4 4 685.17 722.74 20.59 o 0 6 4 6265.08 6378.80 104.61 o 1 6 4 2040.12 2167.73 29.68 o 2 6 4 1372.01 1362.95 18.76 o 3 6 4 17.27 19.55 2.92 o 4 6 4 426.55 413.53 9.70 o 5 6 4 301.81 308.46 7.86 o 6 6 4 336.99 336.46 11.18 o 7 6 4 95.39 97.37 7.05 o 8 6 4 12.11 11.91 4.19 o 9 6 4 302.06 277.68 12.59 o 10 6 4 8.86 15.51 4.96 o 0 8 4 2947.04 2766.85 50.39 o 1 8 4 1072.25 1085.37 25.22 o 2 8 4 76.05 74.28 5.19 o 3 8 4 26.53 34.09 3.83 o 4 8 4 115.16 121.27 6.56 o 5 8 4 307.71 320.01 9.61 o 6 8 4 773.28 782.99 17.07 o 7 8 4 181.43 185.85 9.90 o 8 8 4 141.04 160.04 9.75 o 9 8 4 134.34 163.70 10.12 o 0 10 4 899.65 842.24 24.78 o 1 10 4 98.17 104.84 5.79 o 2 10 4 161.34 154.71 7.35 o 3 10 4 135.35 127.68 6.79 o 4 10 4 59.05 52.99 6.29 o 5 10 4 22.78 24.34 4.98 o 6 10 4 46.26 47.44 6.49 o 7 10 4 14.92 23.39 5.35 o 8 10 4 20.85 25.99 5.43 o 0 12 4 239.17 235.62 13.08 o 1 12 4 1434.72 1314.33 25.16 o 2 12 4 83.68 103.30 6.87 o 3 12 4 309.96 277.18 13.48 o 4 12 4 34.84 49.11 6.55 o 5 12 4 7.26 26.74 5.46 o 6 12 4 174.45 169.32 11.82 o 7 12 4 51.04 69.69 8.40 o 0 14 4 281.33 279.94 15.74 o 1 14 4 26.83 46.26 5.01 o 2 14 4 6.42 16.92 4.41 o 3 14 4 5.95 17.82 4.87 o 4 14 4 16.93 29.35 6.08 o 1 1 5 1329.76 1374.27 16.44 o 2 1 5 6753.25 7267.11 87.78 o 3 1 5 3491.28 3876.08 48.80 o 4 1 5 525.06 549.10 8.88 o 5 1 5 1542.17 1592.75 22.87 o 6 1 5 832.79 868.03 18.15 o 7 1 5 146.92 132.39 10.32 o 8 1 5 127.79 131.18 9.19 o 9 1 5 141.81 154.35 9.06 o 10 1 5 64.32 65.34 9.73 o 11 1 5 44.99 51.25 7.24 o 1 3 5 771.94 805.52 10.11 o 2 3 5 391.12 380.94 7.06 o 3 3 5 219.49 227.94 6.47 o 4 3 5 497.30 473.51 9.32 o 5 3 5 85.09 96.13 4.45 o 6 3 5 5.03 9.23 2.06 o 7 3 5 983.25 881.14 21.87 o 8 3 5 780.46 762.79 19.57 o 9 3 5 169.90 178.83 10.36 o 10 3 5 78.06 87.83 7.91 o 1 5 5 741.70 704.72 10.92 o 2 5 5 756.95 750.68 11.61 o 3 5 5 1107.07 1124.33 17.64 o 4 5 5 2450.43 2367.43 31.10 o 5 5 5 449.94 459.97 9.39 o 6 5 5 21.94 30.10 3.29 o 7 5 5 671.23 644.78 15.48 o 8 5 5 347.31 348.08 12.69 o 9 5 5 212.10 229.27 11.67 o 10 5 5 55.59 63.48 6.53 o 1 7 5 393.87 333.72 17.40 o 2 7 5 773.83 768.89 19.84 o 3 7 5 1200.79 1161.60 18.74 o 4 7 5 384.95 352.49 10.24 o 5 7 5 409.55 381.93 9.49 o 6 7 5 837.40 793.73 17.00 o 7 7 5 49.28 49.87 5.52 o 8 7 5 5.84 15.81 4.17 o 9 7 5 18.46 43.57 6.30 o 1 9 5 7.76 5.24 2.03 o 2 9 5 980.15 946.49 18.61 o 3 9 5 142.76 122.82 7.18 o 4 9 5 112.54 113.70 7.43 o 5 9 5 399.94 391.26 12.88 o 6 9 5 605.26 594.29 14.90 o 7 9 5 30.05 36.81 5.26 o 8 9 5 14.76 19.48 4.46 o 1 11 5 136.39 125.47 6.59 o 2 11 5 270.91 250.71 10.66 o 3 11 5 308.53 291.46 11.70 o 4 11 5 174.63 170.03 10.82 o 5 11 5 10.30 14.81 4.69 o 6 11 5 14.29 23.58 6.97 o 7 11 5 175.85 181.41 12.51 o 1 13 5 37.87 52.42 6.02 o 2 13 5 396.22 386.03 13.82 o 3 13 5 101.28 110.76 10.61 o 4 13 5 30.59 45.06 7.48 o 5 13 5 2.48 6.28 4.89 o 1 15 5 125.72 140.61 9.94 o 0 0 6 1441.62 1487.92 38.02 o 2 0 6 65.67 55.61 3.27 o 4 0 6 2185.37 2095.31 38.02 o 6 0 6 3029.28 3002.95 62.73 o 8 0 6 495.33 462.55 22.60 o 10 0 6 49.05 64.20 15.89 o 0 2 6 54.76 50.14 3.02 o 1 2 6 589.02 625.55 8.46 o 2 2 6 5198.12 5575.09 64.17 o 3 2 6 637.59 616.76 10.84 o 4 2 6 310.86 320.63 7.34 o 5 2 6 60.42 60.31 4.14 o 6 2 6 960.38 913.04 19.63 o 7 2 6 1159.72 1091.31 26.73 o 8 2 6 48.60 52.56 6.39 o 9 2 6 148.79 167.54 19.93 o 10 2 6 5.35 20.95 5.38 o 0 4 6 1432.34 1441.61 23.86 o 1 4 6 154.77 170.60 4.18 o 2 4 6 1092.82 1115.82 16.25 o 3 4 6 541.36 569.34 10.18 o 4 4 6 18.43 14.43 2.11 o 5 4 6 68.35 63.20 5.64 o 6 4 6 94.52 90.33 5.83 o 7 4 6 534.25 532.17 15.53 o 8 4 6 232.35 238.00 11.40 o 9 4 6 51.28 74.70 8.82 o 10 4 6 14.48 31.08 5.31 o 0 6 6 1299.30 1264.63 45.43 o 1 6 6 739.00 746.05 13.10 o 2 6 6 464.23 429.03 11.84 o 3 6 6 137.74 122.02 5.19 o 4 6 6 821.49 766.03 14.13 o 5 6 6 45.27 45.91 3.78 o 6 6 6 802.18 751.42 16.34 o 7 6 6 86.84 82.29 6.96 o 8 6 6 32.68 34.13 8.01 o 9 6 6 111.07 122.38 10.79 o 0 8 6 91.53 81.68 7.64 o 1 8 6 333.47 328.78 8.70 o 2 8 6 194.68 172.36 7.34 o 3 8 6 1059.91 961.07 18.66 o 4 8 6 286.04 263.22 9.00 o 5 8 6 69.68 63.48 5.28 o 6 8 6 232.99 205.49 9.96 o 7 8 6 39.71 43.36 5.36 o 8 8 6 33.49 52.31 6.82 o 0 10 6 56.97 70.93 7.98 o 1 10 6 737.35 665.05 14.27 o 2 10 6 1140.42 1011.71 18.94 o 3 10 6 385.07 391.34 11.31 o 4 10 6 18.59 15.58 3.47 o 5 10 6 78.32 79.44 6.96 o 6 10 6 190.61 208.27 10.97 o 7 10 6 246.88 297.40 15.24 o 0 12 6 244.26 226.34 14.26 o 1 12 6 97.71 99.04 7.09 o 2 12 6 167.78 182.16 9.42 o 3 12 6 51.32 79.66 7.22 o 4 12 6 4.49 8.87 4.73 o 5 12 6 85.18 90.31 8.99 o 6 12 6 25.56 53.35 7.70 o 0 14 6 27.91 29.22 8.75 o 1 14 6 30.10 31.39 6.35 o 2 14 6 48.38 70.74 8.75 o 3 14 6 90.73 116.60 9.32 o 1 1 7 1375.68 1369.55 16.28 o 2 1 7 985.80 940.26 12.98 o 3 1 7 103.34 75.20 4.39 o 4 1 7 1064.37 1016.50 20.80 o 5 1 7 378.16 345.30 8.27 o 6 1 7 612.98 610.74 13.81 o 7 1 7 290.60 270.47 12.61 o 8 1 7 26.39 44.65 5.97 o 9 1 7 17.89 26.03 5.14 o 10 1 7 141.59 178.08 19.58 o 1 3 7 528.61 521.91 7.99 o 2 3 7 84.05 80.87 3.61 o 3 3 7 231.98 247.35 6.89 o 4 3 7 402.21 394.06 9.82 o 5 3 7 673.79 684.30 14.35 o 6 3 7 194.71 210.47 10.26 o 7 3 7 196.28 196.99 11.16 o 8 3 7 4.04 6.94 4.15 o 9 3 7 26.55 37.58 5.29 o 10 3 7 84.03 106.04 8.86 o 1 5 7 121.45 120.31 4.98 o 2 5 7 63.28 59.74 4.11 o 3 5 7 421.65 443.73 10.88 o 4 5 7 848.28 826.85 14.14 o 5 5 7 27.02 35.99 3.98 o 6 5 7 83.79 82.20 5.84 o 7 5 7 505.62 446.56 14.37 o 8 5 7 15.53 22.37 4.48 o 9 5 7 0.29 12.54 4.07 o 1 7 7 76.68 62.66 4.29 o 2 7 7 880.75 863.23 15.85 o 3 7 7 62.26 60.20 4.63 o 4 7 7 671.95 637.60 14.32 o 5 7 7 107.09 88.70 5.87 o 6 7 7 293.35 277.54 12.85 o 7 7 7 24.62 20.71 7.72 o 8 7 7 12.37 17.90 5.40 o 1 9 7 28.15 29.51 3.78 o 2 9 7 217.06 218.66 8.12 o 3 9 7 560.37 525.65 21.00 o 4 9 7 419.48 404.71 11.55 o 5 9 7 260.22 247.71 9.70 o 6 9 7 92.62 112.51 11.97 o 7 9 7 8.69 14.36 5.88 o 1 11 7 136.88 130.82 7.95 o 2 11 7 9.86 18.13 3.81 o 3 11 7 46.39 53.38 4.79 o 4 11 7 110.58 116.39 10.59 o 5 11 7 110.22 101.10 8.19 o 6 11 7 45.30 52.34 6.64 o 1 13 7 170.78 188.92 11.22 o 2 13 7 1.96 4.84 4.74 o 3 13 7 80.18 115.57 9.40 o 0 0 8 8651.82 8934.30 204.36 o 2 0 8 293.24 308.96 8.81 o 4 0 8 337.31 293.53 18.64 o 6 0 8 55.18 64.29 7.21 o 8 0 8 67.53 62.00 10.19 o 0 2 8 998.71 998.95 20.94 o 1 2 8 1320.92 1281.55 17.44 o 2 2 8 585.87 583.69 11.28 o 3 2 8 28.47 31.60 3.34 o 4 2 8 133.88 125.98 6.09 o 5 2 8 91.24 93.22 7.16 o 6 2 8 113.39 103.29 7.10 o 7 2 8 82.42 64.27 6.09 o 8 2 8 45.57 46.27 6.30 o 9 2 8 2.72 10.79 4.26 o 0 4 8 274.70 296.51 25.98 o 1 4 8 837.00 800.05 15.43 o 2 4 8 194.33 178.07 5.57 o 3 4 8 277.84 272.72 7.48 o 4 4 8 576.10 507.23 11.19 o 5 4 8 307.19 304.16 8.53 o 6 4 8 251.99 229.18 9.25 o 7 4 8 16.29 21.36 3.91 o 8 4 8 69.70 85.70 7.67 o 9 4 8 207.13 196.46 11.71 o 0 6 8 2442.89 2327.32 51.33 o 1 6 8 692.97 644.50 14.09 o 2 6 8 258.76 277.21 7.80 o 3 6 8 80.54 81.73 5.17 o 4 6 8 212.56 223.84 10.03 o 5 6 8 105.54 119.50 7.29 o 6 6 8 88.89 88.41 7.05 o 7 6 8 16.77 20.69 3.87 o 8 6 8 26.16 42.21 6.01 o 0 8 8 2148.32 2087.76 68.59 o 1 8 8 189.53 159.15 8.07 o 2 8 8 115.93 130.80 8.72 o 3 8 8 91.41 91.98 6.12 o 4 8 8 1.92 0.14 2.86 o 5 8 8 96.40 95.28 7.16 o 6 8 8 32.21 48.94 6.50 o 7 8 8 164.71 165.50 13.90 o 0 10 8 186.22 160.01 11.86 o 1 10 8 269.63 272.98 10.57 o 2 10 8 16.55 23.16 3.92 o 3 10 8 238.38 223.26 10.93 o 4 10 8 158.55 138.97 8.02 o 5 10 8 50.27 49.46 6.71 o 6 10 8 14.43 29.86 5.63 o 0 12 8 99.21 105.08 13.08 o 1 12 8 49.14 36.38 5.87 o 2 12 8 87.80 101.26 7.54 o 3 12 8 14.81 31.37 4.87 o 4 12 8 1.91 12.02 4.56 o 1 1 9 538.06 514.73 13.43 o 2 1 9 72.20 74.87 4.90 o 3 1 9 894.20 816.26 15.94 o 4 1 9 243.09 232.52 7.44 o 5 1 9 840.46 827.37 14.57 o 6 1 9 169.78 155.43 8.76 o 7 1 9 149.23 167.84 8.42 o 8 1 9 133.72 132.78 11.71 o 9 1 9 237.56 293.43 15.46 o 1 3 9 708.67 651.19 15.07 o 2 3 9 77.44 74.21 5.42 o 3 3 9 252.07 240.07 7.17 o 4 3 9 349.77 331.16 10.34 o 5 3 9 8.84 15.07 3.16 o 6 3 9 173.88 205.79 9.95 o 7 3 9 121.20 117.93 9.65 o 8 3 9 215.30 213.45 11.86 o 1 5 9 1059.50 1001.90 19.09 o 2 5 9 441.82 447.61 14.85 o 3 5 9 685.47 633.86 14.37 o 4 5 9 79.17 70.60 5.31 o 5 5 9 117.30 129.05 7.19 o 6 5 9 134.96 160.24 9.29 o 7 5 9 58.45 52.99 5.99 o 8 5 9 44.64 79.50 8.05 o 1 7 9 423.54 390.41 12.93 o 2 7 9 1151.58 1084.47 23.49 o 3 7 9 246.52 239.13 10.46 o 4 7 9 187.81 195.94 10.90 o 5 7 9 33.34 37.54 5.62 o 6 7 9 105.61 118.23 9.79 o 7 7 9 2.11 22.57 4.87 o 1 9 9 114.30 125.60 7.39 o 2 9 9 132.73 131.31 7.73 o 3 9 9 44.74 48.33 5.42 o 4 9 9 33.75 35.63 5.49 o 5 9 9 22.82 38.95 6.39 o 6 9 9 7.54 22.54 6.04 o 1 11 9 17.07 21.58 3.94 o 2 11 9 0.37 8.72 3.44 o 3 11 9 38.95 54.45 5.66 o 4 11 9 285.34 326.09 13.97 o 0 0 10 49.25 68.60 7.93 o 2 0 10 289.70 275.85 12.20 o 4 0 10 69.38 95.82 10.50 o 6 0 10 265.18 306.15 15.60 o 8 0 10 46.01 47.39 11.46 o 0 2 10 398.60 355.66 16.99 o 1 2 10 55.39 65.69 7.49 o 2 2 10 67.77 67.66 5.25 o 3 2 10 1476.63 1391.45 26.92 o 4 2 10 398.74 351.45 11.06 o 5 2 10 133.33 149.88 7.53 o 6 2 10 22.33 20.45 3.81 o 7 2 10 155.54 143.38 9.52 o 8 2 10 21.01 46.67 6.66 o 0 4 10 398.69 380.56 18.40 o 1 4 10 53.64 51.16 4.85 o 2 4 10 1278.53 1180.43 24.14 o 3 4 10 152.23 148.00 8.11 o 4 4 10 338.10 288.77 12.18 o 5 4 10 77.29 61.85 6.04 o 6 4 10 136.93 115.71 8.29 o 7 4 10 7.35 23.53 4.49 o 0 6 10 462.60 432.47 20.63 o 1 6 10 81.89 92.55 6.65 o 2 6 10 605.61 600.10 17.48 o 3 6 10 37.37 41.26 4.94 o 4 6 10 456.53 409.38 13.05 o 5 6 10 303.09 306.92 16.37 o 6 6 10 151.96 194.64 11.91 o 7 6 10 26.74 36.12 5.34 o 0 8 10 599.51 577.46 20.56 o 1 8 10 98.62 103.06 7.39 o 2 8 10 7.85 9.97 3.50 o 3 8 10 14.45 20.23 3.99 o 4 8 10 11.81 22.35 4.29 o 5 8 10 121.04 151.85 12.95 o 6 8 10 49.53 58.56 13.63 o 0 10 10 158.62 197.81 15.57 o 1 10 10 90.52 98.81 7.07 o 2 10 10 88.95 104.31 8.14 o 3 10 10 34.26 52.87 5.98 o 4 10 10 9.99 19.15 4.48 o 1 1 11 119.35 131.02 7.89 o 2 1 11 137.62 137.34 7.85 o 3 1 11 622.35 584.58 15.35 o 4 1 11 105.95 114.31 6.32 o 5 1 11 317.56 321.61 10.86 o 6 1 11 93.70 92.93 7.18 o 7 1 11 55.64 75.48 6.51 o 1 3 11 684.94 692.39 19.07 o 2 3 11 110.52 107.20 7.95 o 3 3 11 103.11 113.17 7.44 o 4 3 11 247.18 256.86 14.89 o 5 3 11 13.00 13.89 5.15 o 6 3 11 12.34 27.84 4.27 o 7 3 11 75.09 138.33 10.16 o 1 5 11 340.08 362.31 13.69 o 2 5 11 7.38 10.81 4.56 o 3 5 11 371.80 373.78 12.66 o 4 5 11 160.36 125.46 9.59 o 5 5 11 46.58 69.15 13.95 o 6 5 11 12.32 31.64 6.96 o 1 7 11 52.43 63.28 6.82 o 2 7 11 561.20 611.86 17.14 o 3 7 11 64.62 75.42 7.54 o 4 7 11 327.80 329.64 13.31 o 5 7 11 48.79 49.47 6.53 o 1 9 11 190.20 226.23 12.46 o 2 9 11 1.57 13.74 4.10 o 3 9 11 125.50 127.36 9.43 o 0 0 12 438.78 430.37 29.72 o 2 0 12 258.04 284.14 18.27 o 4 0 12 60.73 80.22 11.23 o 6 0 12 123.28 118.77 18.38 o 0 2 12 50.83 44.89 10.16 o 1 2 12 53.95 53.08 9.34 o 2 2 12 1.23 8.11 3.72 o 3 2 12 0.53 9.27 3.14 o 4 2 12 143.69 132.60 8.38 o 5 2 12 72.01 87.21 10.06 o 6 2 12 66.70 83.46 8.42 o 0 4 12 45.14 38.92 9.92 o 1 4 12 409.00 448.48 15.44 o 2 4 12 70.75 74.45 7.25 o 3 4 12 16.79 35.12 5.10 o 4 4 12 80.06 96.48 8.27 o 5 4 12 44.73 47.11 7.76 o 0 6 12 767.68 690.39 29.44 o 1 6 12 71.36 61.10 8.17 o 2 6 12 1.70 11.71 4.13 o 3 6 12 198.56 220.89 12.52 o 4 6 12 32.27 48.38 5.79 o 0 8 12 601.77 654.53 29.68 o 1 8 12 19.65 36.06 6.03 o 2 8 12 3.64 19.05 5.08 o 1 1 13 121.30 124.31 9.56 o 2 1 13 37.93 57.83 6.86 o 3 1 13 41.24 61.72 6.93 o 4 1 13 129.45 145.00 10.34 o 1 3 13 6.14 22.10 4.81 o 2 3 13 6.11 14.43 7.37 o 3 3 13 49.74 46.04 7.00 o 4 3 13 13.00 30.23 5.46 o 1 5 13 43.11 57.73 9.40 o 2 5 13 3.60 24.58 5.00 o 3 5 13 144.31 193.90 16.03 o 0 0 14 26.50 28.24 9.74 o 2 0 14 161.14 169.96 16.21 o 0 2 14 47.63 71.30 10.97 o 1 2 14 48.93 65.11 7.20 o