#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/55/2205530.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205530_Fobs loop_ _publ_author_name 'Lynch, Daniel E.' 'McClenaghan, Ian' _publ_section_title ; Diethyl 2-aminothiazole-4,5-dicarboxylate hemihydrate ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o824 _journal_page_last o826 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 111.653 _cell_angle_gamma 90.000 _cell_length_a 16.7835 _cell_length_b 8.4580 _cell_length_c 18.0373 _exptl_crystal_F_000 1064.00 _reflns_d_resolution_high 0.7691 _[local]_cod_data_source_file kp6046Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'Diethyl 2-aminothiazole-4,5-dicarboxylate hydrate' _shelx_refln_list_code 4 _shelx_f_calc_maximum 303.39 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 1537.33 1638.05 34.41 o 6 0 0 24.90 47.49 3.46 o 8 0 0 17.44 14.12 3.42 o 10 0 0 5.67 4.55 4.11 o 12 0 0 334.49 357.99 15.84 o 14 0 0 43.05 28.97 8.13 o 16 0 0 1003.19 1247.14 92.84 o 18 0 0 1581.73 1655.24 109.34 o 20 0 0 462.00 382.67 52.70 o 2 1 0 6267.26 6602.45 98.19 o 3 1 0 3908.41 3766.93 54.14 o 4 1 0 8.47 14.76 1.73 o 5 1 0 502.39 455.64 8.90 o 6 1 0 807.73 769.72 11.68 o 7 1 0 1187.01 1194.59 19.76 o 8 1 0 284.88 297.17 6.80 o 9 1 0 977.02 1018.29 17.10 o 10 1 0 559.70 554.08 15.46 o 11 1 0 963.33 1004.79 18.13 o 12 1 0 525.63 445.65 11.45 o 13 1 0 41.25 47.36 5.14 o 14 1 0 3801.16 4035.13 99.77 o 15 1 0 565.72 555.49 20.89 o 16 1 0 174.83 197.72 17.35 o 17 1 0 23.06 17.22 6.67 o 18 1 0 276.66 300.19 18.70 o 19 1 0 72.36 41.85 13.62 o 20 1 0 40.07 70.41 25.07 o 0 2 0 61.79 44.56 4.70 o 1 2 0 20.07 45.56 2.36 o 2 2 0 19431.13 21754.56 295.54 o 3 2 0 603.19 618.45 8.98 o 4 2 0 1210.34 1234.64 16.82 o 5 2 0 229.90 202.81 5.63 o 6 2 0 440.34 411.14 7.61 o 7 2 0 10.95 14.99 2.32 o 8 2 0 12.84 6.88 2.11 o 9 2 0 454.40 437.44 9.85 o 10 2 0 149.91 161.73 7.51 o 11 2 0 3.27 2.13 2.83 o 12 2 0 45.35 37.62 5.06 o 13 2 0 1180.29 1087.04 30.56 o 14 2 0 642.34 535.46 16.22 o 15 2 0 387.52 395.65 20.26 o 16 2 0 1078.94 1073.92 47.89 o 17 2 0 120.51 124.58 12.47 o 18 2 0 654.44 619.79 49.67 o 19 2 0 4.13 17.56 17.22 o 1 3 0 11534.53 11990.80 201.77 o 2 3 0 167.08 147.73 4.60 o 3 3 0 125.53 307.87 19.95 o 4 3 0 13.90 13.95 2.19 o 5 3 0 397.48 409.76 10.06 o 6 3 0 912.54 967.70 18.97 o 7 3 0 80.75 86.06 3.97 o 8 3 0 22.18 13.55 2.81 o 9 3 0 1.47 21.42 3.20 o 10 3 0 9.37 0.62 2.67 o 11 3 0 3.70 6.43 3.48 o 12 3 0 124.82 114.33 7.74 o 13 3 0 272.79 234.92 8.46 o 14 3 0 36.96 55.20 4.72 o 15 3 0 21.46 6.78 5.64 o 16 3 0 0.67 3.55 6.65 o 17 3 0 553.09 574.37 37.98 o 18 3 0 340.29 298.46 41.20 o 19 3 0 848.08 911.88 55.24 o 0 4 0 4265.86 3811.29 116.28 o 1 4 0 616.58 550.96 16.91 o 2 4 0 192.29 161.89 6.30 o 3 4 0 1984.05 1893.43 35.97 o 4 4 0 34.02 37.59 3.44 o 5 4 0 45.41 43.53 4.23 o 6 4 0 406.71 393.11 11.89 o 7 4 0 86.36 76.06 4.55 o 8 4 0 622.71 635.95 14.77 o 9 4 0 0.51 -0.13 3.47 o 10 4 0 367.22 376.99 12.31 o 11 4 0 123.17 127.64 8.86 o 12 4 0 3.28 -2.52 3.69 o 13 4 0 726.42 725.14 26.48 o 14 4 0 107.27 96.05 21.57 o 15 4 0 190.08 201.63 14.45 o 16 4 0 2.99 5.27 4.95 o 17 4 0 2.40 -12.31 12.31 o 18 4 0 1.40 14.99 13.37 o 1 5 0 2146.80 1961.34 41.46 o 2 5 0 236.62 206.68 8.75 o 3 5 0 280.49 234.51 9.20 o 4 5 0 7.54 5.99 3.50 o 5 5 0 1197.57 1189.08 25.43 o 6 5 0 73.37 68.24 7.03 o 7 5 0 279.24 294.32 11.53 o 8 5 0 160.87 128.55 6.09 o 9 5 0 30.84 33.03 5.79 o 10 5 0 220.02 228.57 11.42 o 11 5 0 0.80 -3.55 3.55 o 12 5 0 11.88 8.09 4.43 o 13 5 0 374.94 372.81 18.69 o 14 5 0 92.87 94.56 12.75 o 15 5 0 77.79 91.41 12.20 o 16 5 0 432.51 452.43 34.39 o 17 5 0 1191.05 1320.53 98.66 o 18 5 0 266.05 304.19 52.87 o 0 6 0 124.66 122.42 13.91 o 1 6 0 314.31 317.17 9.89 o 2 6 0 128.88 125.45 8.66 o 3 6 0 2185.62 2193.23 52.28 o 4 6 0 586.17 537.89 18.58 o 5 6 0 183.67 184.20 9.69 o 6 6 0 289.82 314.03 21.16 o 7 6 0 11.97 9.02 4.43 o 8 6 0 336.17 323.59 13.43 o 9 6 0 473.29 471.72 21.11 o 10 6 0 316.71 305.41 12.37 o 11 6 0 33.68 25.36 7.45 o 12 6 0 294.59 341.16 19.79 o 13 6 0 1126.96 1145.58 61.09 o 14 6 0 1.02 -6.44 11.41 o 15 6 0 348.01 340.54 49.89 o 16 6 0 0.36 -1.85 15.00 o 1 7 0 1148.42 1159.46 41.55 o 2 7 0 97.91 100.65 7.58 o 3 7 0 856.52 826.25 28.99 o 4 7 0 77.68 59.82 7.54 o 5 7 0 1343.91 1330.59 53.86 o 6 7 0 91.41 94.94 11.35 o 7 7 0 129.36 127.16 12.75 o 8 7 0 48.35 57.95 7.31 o 9 7 0 244.67 223.14 14.96 o 10 7 0 36.03 26.47 12.91 o 11 7 0 50.46 48.11 12.16 o 12 7 0 261.64 277.01 29.82 o 13 7 0 31.77 42.86 21.23 o 14 7 0 16.02 27.46 25.56 o 15 7 0 617.80 623.80 55.60 o 0 8 0 1360.21 1337.73 91.99 o 1 8 0 501.46 483.65 29.49 o 2 8 0 379.25 392.55 21.42 o 3 8 0 14.92 10.04 5.93 o 4 8 0 426.04 389.04 25.45 o 5 8 0 0.32 -5.75 8.72 o 6 8 0 72.34 118.01 29.11 o 7 8 0 92.35 90.07 14.33 o 8 8 0 734.43 741.31 46.77 o 9 8 0 364.24 434.38 41.46 o 10 8 0 836.46 926.60 125.95 o 11 8 0 56.50 84.24 23.11 o 12 8 0 12.12 20.74 21.63 o 13 8 0 207.19 150.00 29.57 o 1 9 0 9.68 33.38 15.49 o 2 9 0 157.91 186.27 63.16 o 3 9 0 48.27 74.49 24.57 o 4 9 0 80.21 68.58 18.97 o 5 9 0 278.28 305.01 73.92 o 6 9 0 3.37 15.98 16.03 o 7 9 0 184.01 176.31 40.16 o 8 9 0 34.23 72.02 23.00 o 9 9 0 142.89 161.95 31.84 o 10 9 0 158.86 151.29 28.80 o 11 9 0 35.02 71.50 24.52 o 0 10 0 211.33 310.05 50.10 o 1 10 0 19.05 27.59 27.27 o 2 10 0 102.62 149.77 27.21 o 3 10 0 277.26 279.55 41.66 o 4 10 0 188.81 171.44 31.00 o 5 10 0 29.90 47.85 28.63 o 6 10 0 29.54 39.27 20.91 o 7 10 0 2.52 9.89 20.16 o 8 10 0 155.88 150.80 55.99 o -19 0 1 4.32 1.74 12.20 o -17 0 1 218.77 205.53 21.12 o -15 0 1 978.81 1023.88 39.71 o -13 0 1 1062.23 984.98 34.62 o -11 0 1 492.39 457.67 18.03 o -9 0 1 34866.64 43365.79 794.64 o -7 0 1 37.27 44.90 4.51 o -5 0 1 3972.50 3487.12 71.87 o -3 0 1 1200.85 1189.00 27.42 o 3 0 1 7221.83 7415.95 144.64 o 5 0 1 994.02 1025.73 23.40 o 7 0 1 33354.41 42360.48 872.84 o 9 0 1 305.44 299.77 12.07 o 11 0 1 4946.85 4739.33 121.40 o 13 0 1 972.94 1027.54 35.24 o 15 0 1 1433.16 1387.48 80.04 o 17 0 1 120.87 111.92 14.02 o 19 0 1 30.53 8.03 25.09 o -20 1 1 3.15 13.77 11.42 o -19 1 1 801.47 800.23 34.03 o -18 1 1 12.51 38.36 9.98 o -17 1 1 1.68 17.17 7.96 o -16 1 1 56.77 64.72 6.96 o -15 1 1 1217.72 1282.18 40.47 o -14 1 1 716.71 744.88 19.52 o -13 1 1 893.99 894.00 17.87 o -12 1 1 821.97 808.69 18.34 o -11 1 1 760.50 788.97 15.30 o -10 1 1 299.41 320.08 9.85 o -9 1 1 681.63 746.29 14.66 o -8 1 1 671.86 609.34 11.51 o -7 1 1 1740.90 2074.40 31.53 o -6 1 1 2246.64 2470.81 36.25 o -5 1 1 2744.37 2741.47 39.05 o -4 1 1 13590.74 15269.57 222.05 o -3 1 1 240.26 203.12 5.38 o -2 1 1 2261.34 2178.47 33.46 o 1 1 1 0.42 -1.42 1.42 o 2 1 1 22.35 21.95 1.59 o 3 1 1 1313.99 1186.89 16.54 o 4 1 1 1643.42 1564.13 22.73 o 5 1 1 1212.91 1142.36 17.72 o 6 1 1 2240.89 2349.46 32.71 o 7 1 1 186.25 174.96 4.66 o 8 1 1 1501.98 1637.10 25.96 o 9 1 1 3976.27 4085.56 71.39 o 10 1 1 275.72 303.06 9.96 o 11 1 1 476.76 482.55 12.30 o 12 1 1 147.91 120.00 5.76 o 13 1 1 397.34 362.07 11.40 o 14 1 1 516.32 513.54 15.61 o 15 1 1 6.08 4.83 3.73 o 16 1 1 355.29 353.92 22.88 o 17 1 1 0.19 10.63 6.21 o 18 1 1 0.62 0.48 11.03 o 19 1 1 125.10 133.01 17.08 o -20 2 1 66.10 34.29 27.23 o -19 2 1 13.55 8.63 13.54 o -18 2 1 61.42 72.90 16.85 o -17 2 1 15.77 8.73 9.99 o -16 2 1 12.44 10.16 5.17 o -15 2 1 48.24 41.21 5.13 o -14 2 1 341.53 326.28 12.78 o -13 2 1 66.30 64.17 4.99 o -12 2 1 222.43 193.91 6.58 o -11 2 1 4537.15 4587.83 77.36 o -10 2 1 854.44 946.35 18.85 o -9 2 1 781.85 749.13 13.64 o -8 2 1 796.86 867.11 15.35 o -7 2 1 12413.46 13666.55 185.79 o -6 2 1 39.14 77.24 4.21 o -5 2 1 12615.54 13481.86 180.37 o -4 2 1 1389.00 1397.97 19.95 o -3 2 1 437.04 486.51 10.49 o -2 2 1 755.10 704.88 12.66 o -1 2 1 1219.02 1237.73 19.54 o 0 2 1 437.91 451.67 9.05 o 1 2 1 11249.12 11458.99 162.89 o 2 2 1 4990.56 4856.39 63.53 o 3 2 1 11168.21 11319.68 157.65 o 4 2 1 1.06 -0.73 1.68 o 5 2 1 3493.98 3248.11 55.37 o 6 2 1 66.31 50.49 3.28 o 7 2 1 0.49 0.60 1.79 o 8 2 1 118.03 152.84 5.43 o 9 2 1 8231.70 8812.50 132.15 o 10 2 1 2676.44 2839.10 48.49 o 11 2 1 665.67 651.47 16.44 o 12 2 1 4.80 3.83 2.63 o 13 2 1 147.27 147.36 5.66 o 14 2 1 106.47 92.30 5.26 o 15 2 1 332.89 359.11 15.99 o 16 2 1 294.97 267.87 31.43 o 17 2 1 259.66 250.18 24.24 o 18 2 1 132.47 112.35 15.78 o 19 2 1 145.48 148.48 19.89 o -19 3 1 566.71 620.96 44.60 o -18 3 1 117.48 129.35 23.85 o -17 3 1 30.75 26.20 7.08 o -16 3 1 21.45 15.72 6.27 o -15 3 1 2.32 -4.91 4.91 o -14 3 1 23.29 29.98 6.38 o -13 3 1 64.00 51.13 5.77 o -12 3 1 884.47 831.93 19.63 o -11 3 1 569.13 530.31 13.55 o -10 3 1 2322.16 2438.49 43.66 o -9 3 1 247.41 218.27 6.09 o -8 3 1 7432.99 8184.88 127.46 o -7 3 1 203.75 215.63 6.01 o -6 3 1 1312.03 1216.28 17.81 o -5 3 1 1335.07 1447.12 19.91 o -4 3 1 2573.79 2470.34 34.67 o -3 3 1 165.62 123.80 5.04 o -2 3 1 439.20 359.73 10.69 o -1 3 1 8.68 9.59 2.04 o 0 3 1 2117.96 2117.23 35.76 o 1 3 1 1006.48 1103.99 17.81 o 2 3 1 1536.73 1349.59 21.70 o 3 3 1 526.81 452.05 8.13 o 4 3 1 3883.18 3863.43 55.18 o 5 3 1 1941.55 1986.09 29.14 o 6 3 1 1676.44 1745.11 29.72 o 7 3 1 953.21 1077.66 20.56 o 8 3 1 1840.11 1788.66 30.34 o 9 3 1 2142.44 2255.07 37.48 o 10 3 1 1353.92 1336.34 24.50 o 11 3 1 405.51 463.03 16.13 o 12 3 1 1080.82 1137.23 28.74 o 13 3 1 26.90 27.55 2.94 o 14 3 1 1089.43 1171.61 33.39 o 15 3 1 799.52 690.08 32.86 o 16 3 1 556.37 622.63 42.64 o 17 3 1 210.31 203.72 22.06 o 18 3 1 4.37 -1.03 15.21 o 19 3 1 76.41 58.69 16.54 o -19 4 1 400.90 357.03 50.89 o -18 4 1 528.09 640.81 52.86 o -17 4 1 6.39 8.16 8.83 o -16 4 1 0.76 -9.42 9.42 o -15 4 1 35.25 39.06 11.01 o -14 4 1 183.59 161.50 10.98 o -13 4 1 205.89 187.41 8.78 o -12 4 1 261.39 278.31 9.55 o -11 4 1 17.91 14.70 4.10 o -10 4 1 354.63 320.83 8.83 o -9 4 1 546.47 485.75 11.53 o -8 4 1 271.10 257.73 7.41 o -7 4 1 125.45 101.61 4.54 o -6 4 1 0.29 4.08 3.01 o -5 4 1 1561.36 1562.08 23.53 o -4 4 1 1409.72 1337.87 28.02 o -3 4 1 238.96 264.82 10.00 o -2 4 1 10.49 12.80 3.81 o -1 4 1 135.44 176.96 7.09 o 0 4 1 2871.17 2710.09 46.00 o 1 4 1 22.58 22.49 2.51 o 2 4 1 951.20 949.12 15.69 o 3 4 1 2608.12 2567.96 42.47 o 4 4 1 4050.04 4024.51 64.33 o 5 4 1 97.13 135.60 4.70 o 6 4 1 1816.24 1680.65 30.17 o 7 4 1 118.89 111.85 4.62 o 8 4 1 523.70 574.44 12.36 o 9 4 1 239.47 207.97 8.69 o 10 4 1 2.09 -0.50 2.52 o 11 4 1 1437.87 1556.94 33.44 o 12 4 1 4.06 5.51 3.05 o 13 4 1 199.54 194.27 8.28 o 14 4 1 2.24 19.26 7.99 o 15 4 1 172.97 181.36 21.79 o 16 4 1 96.71 97.18 14.48 o 17 4 1 19.19 8.85 11.75 o 18 4 1 0.55 -13.68 16.46 o -18 5 1 18.35 31.43 17.90 o -17 5 1 33.39 54.86 13.21 o -16 5 1 0.01 6.28 12.98 o -15 5 1 40.18 40.22 11.99 o -14 5 1 256.89 208.28 15.15 o -13 5 1 18.53 17.07 7.14 o -12 5 1 1692.61 1733.05 50.88 o -11 5 1 364.01 396.31 15.79 o -10 5 1 3426.55 3246.55 82.72 o -9 5 1 753.37 823.19 20.25 o -8 5 1 118.88 127.43 6.40 o -7 5 1 65.39 63.17 5.06 o -6 5 1 4235.99 4369.58 80.54 o -5 5 1 71.11 50.35 3.85 o -4 5 1 4017.72 3997.43 80.28 o -3 5 1 138.65 149.11 7.20 o -2 5 1 164.64 141.67 6.81 o -1 5 1 8.31 5.68 4.60 o 0 5 1 461.92 491.69 12.50 o 1 5 1 921.75 913.61 16.49 o 2 5 1 2545.49 2472.04 44.09 o 3 5 1 16.08 21.05 3.26 o 4 5 1 225.68 191.35 7.40 o 5 5 1 509.78 510.84 16.08 o 6 5 1 59.65 46.36 4.54 o 7 5 1 351.79 353.74 12.22 o 8 5 1 1751.44 1723.88 32.49 o 9 5 1 975.53 1079.41 24.05 o 10 5 1 376.08 376.93 12.49 o 11 5 1 95.27 71.36 7.62 o 12 5 1 1429.90 1444.10 40.98 o 13 5 1 17.67 7.56 8.76 o 14 5 1 238.74 229.10 19.77 o 15 5 1 4.93 3.42 9.94 o 16 5 1 322.09 316.90 25.16 o 17 5 1 32.23 13.29 21.34 o -17 6 1 28.52 27.86 30.00 o -16 6 1 2.38 -16.39 16.39 o -15 6 1 230.69 219.18 27.30 o -14 6 1 17.03 1.67 10.86 o -13 6 1 42.13 16.39 10.43 o -12 6 1 678.99 741.30 41.78 o -11 6 1 64.69 56.60 8.48 o -10 6 1 6.42 12.56 4.98 o -9 6 1 75.56 78.82 7.87 o -8 6 1 5.81 7.53 4.82 o -7 6 1 52.72 53.94 6.70 o -6 6 1 1336.69 1380.43 31.74 o -5 6 1 282.74 218.54 12.18 o -4 6 1 1.04 1.43 3.75 o -3 6 1 1739.39 1662.90 45.48 o -2 6 1 45.90 50.41 5.51 o -1 6 1 207.65 198.20 12.29 o 0 6 1 776.65 788.28 24.89 o 1 6 1 91.73 79.13 6.47 o 2 6 1 138.15 139.16 11.01 o 3 6 1 37.66 40.85 4.96 o 4 6 1 687.04 596.66 20.03 o 5 6 1 20.76 15.57 4.14 o 6 6 1 49.53 31.31 6.89 o 7 6 1 82.51 78.19 6.57 o 8 6 1 2233.09 2265.85 78.69 o 9 6 1 411.52 455.30 15.59 o 10 6 1 82.46 71.82 6.69 o 11 6 1 231.90 220.52 14.17 o 12 6 1 120.34 94.11 14.78 o 13 6 1 16.05 15.03 11.15 o 14 6 1 225.29 249.99 41.28 o 15 6 1 6.50 4.97 16.22 o 16 6 1 1.36 -14.09 26.49 o -15 7 1 46.95 56.55 49.79 o -14 7 1 11.66 3.29 18.97 o -13 7 1 2.08 -2.50 52.88 o -12 7 1 1174.80 1233.69 77.94 o -11 7 1 0.75 4.78 8.21 o -10 7 1 0.66 1.73 7.92 o -9 7 1 469.65 511.21 26.42 o -8 7 1 1777.06 1718.98 59.83 o -7 7 1 625.86 667.01 30.38 o -6 7 1 660.02 605.16 26.57 o -5 7 1 140.89 146.17 14.83 o -4 7 1 249.96 244.26 14.38 o -3 7 1 213.39 218.10 12.63 o -2 7 1 479.38 457.84 25.46 o -1 7 1 0.02 0.38 3.86 o 0 7 1 262.05 248.51 12.45 o 1 7 1 162.62 156.46 15.52 o 2 7 1 144.96 136.16 9.05 o 3 7 1 925.27 863.82 34.28 o 4 7 1 356.00 347.64 15.37 o 5 7 1 0.59 10.05 5.34 o 6 7 1 1902.97 1995.56 78.56 o 7 7 1 136.82 133.55 10.11 o 8 7 1 455.53 447.10 25.41 o 9 7 1 0.65 7.56 7.69 o 10 7 1 253.97 226.70 35.97 o 11 7 1 413.51 429.37 61.03 o 12 7 1 1411.98 1657.37 75.62 o 13 7 1 172.50 154.52 26.97 o 14 7 1 97.13 84.18 36.44 o 15 7 1 60.87 19.90 21.78 o -14 8 1 83.48 78.35 27.81 o -13 8 1 145.68 125.17 26.74 o -12 8 1 81.31 88.24 29.53 o -11 8 1 45.54 44.86 19.10 o -10 8 1 482.87 524.08 44.31 o -9 8 1 701.06 790.91 87.89 o -8 8 1 108.93 118.75 17.59 o -7 8 1 580.43 593.86 33.35 o -6 8 1 79.08 82.69 10.18 o -5 8 1 66.21 65.77 8.51 o -4 8 1 4.63 -0.53 7.43 o -3 8 1 401.48 377.24 26.03 o -2 8 1 418.03 388.91 30.99 o -1 8 1 432.07 443.83 30.42 o 0 8 1 0.58 -6.60 7.14 o 1 8 1 650.35 656.61 31.53 o 2 8 1 55.07 42.50 9.66 o 3 8 1 507.67 481.35 32.40 o 4 8 1 17.40 30.58 6.48 o 5 8 1 611.61 615.14 33.17 o 6 8 1 1687.25 1957.94 102.43 o 7 8 1 375.46 374.57 38.60 o 8 8 1 119.79 95.80 22.37 o 9 8 1 4.27 14.29 16.26 o 10 8 1 33.36 11.47 16.82 o 11 8 1 8.23 45.63 20.99 o 12 8 1 198.21 212.08 34.05 o 13 8 1 5.70 -7.51 22.88 o -11 9 1 1.07 5.99 19.24 o -10 9 1 80.76 153.75 25.28 o -9 9 1 21.53 17.30 18.55 o -8 9 1 47.31 42.50 20.07 o -7 9 1 58.44 52.78 16.66 o -6 9 1 55.10 47.98 28.83 o -5 9 1 168.28 167.47 18.92 o -4 9 1 15.94 4.09 11.10 o -3 9 1 7.02 -0.45 23.34 o -2 9 1 526.73 494.21 45.83 o -1 9 1 0.09 8.23 14.52 o 0 9 1 49.61 57.96 17.91 o 1 9 1 0.51 -12.59 16.56 o 2 9 1 266.32 340.16 35.03 o 3 9 1 2.82 7.79 15.07 o 4 9 1 52.16 46.95 21.92 o 5 9 1 902.95 935.06 78.13 o 6 9 1 453.87 538.63 69.37 o 7 9 1 171.99 146.83 29.86 o 8 9 1 159.69 178.74 79.34 o 9 9 1 227.70 151.02 33.08 o 10 9 1 46.00 51.43 28.15 o 11 9 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