#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/55/2205545.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205545_Fobs loop_ _publ_author_name 'Ferguson, George' 'O'Leary, Brian J.' 'Spalding, Trevor R.' _publ_section_title ; Tris(triphenylsilyl)phosphate dichloromethane solvate ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o906 _journal_page_last o907 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 91.752 _cell_angle_beta 105.468 _cell_angle_gamma 106.311 _cell_length_a 10.2838 _cell_length_b 13.0553 _cell_length_c 19.0152 _exptl_crystal_F_000 938.68 _reflns_d_resolution_high 0.7830 _[local]_cod_data_source_file lh6381Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' TRS95-08 redone Feb 7 2005' _shelx_refln_list_code 4 _shelx_f_calc_maximum 267.13 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 8863.70 8454.27 69.48 o 2 0 0 22885.10 23132.71 159.33 o 3 0 0 310.71 283.93 21.07 o 4 0 0 1204.09 1285.27 32.65 o 5 0 0 788.66 699.56 31.11 o 6 0 0 138.01 127.10 24.28 o 7 0 0 573.84 671.65 38.09 o 8 0 0 2024.73 1917.86 64.88 o 9 0 0 6.26 73.53 50.23 o 10 0 0 314.79 315.88 50.09 o 11 0 0 192.79 190.73 46.32 o 12 0 0 0.02 16.60 82.18 o -12 1 0 16.13 16.18 74.23 o -11 1 0 3.49 14.23 72.55 o -10 1 0 108.04 110.92 42.97 o -9 1 0 54.99 16.46 65.16 o -8 1 0 230.00 178.17 36.69 o -7 1 0 122.13 173.01 29.58 o -6 1 0 51.16 62.23 44.09 o -5 1 0 0.01 5.30 35.86 o -4 1 0 824.29 901.17 28.46 o -3 1 0 2802.27 2892.69 39.62 o -2 1 0 5954.47 5923.50 58.18 o -1 1 0 9928.23 10289.53 78.27 o 1 1 0 1984.78 1987.48 23.72 o 2 1 0 919.67 962.00 26.09 o 3 1 0 2404.56 2481.38 40.04 o 4 1 0 2261.83 2443.99 43.81 o 5 1 0 321.06 388.71 26.93 o 6 1 0 159.52 116.36 26.37 o 7 1 0 685.22 598.41 39.48 o 8 1 0 1.38 65.44 52.60 o 9 1 0 128.56 160.17 38.51 o 10 1 0 0.57 13.25 65.02 o 11 1 0 129.48 160.73 40.88 o -12 2 0 46.80 40.88 77.16 o -11 2 0 0.00 13.95 57.06 o -10 2 0 49.33 75.20 61.39 o -9 2 0 29.88 80.78 58.18 o -8 2 0 105.07 70.88 31.95 o -7 2 0 232.98 279.60 30.28 o -6 2 0 701.83 844.52 36.41 o -5 2 0 1169.87 1075.29 33.90 o -4 2 0 1373.99 1339.26 31.95 o -3 2 0 37.50 43.39 32.79 o -2 2 0 1130.82 1149.93 25.11 o -1 2 0 3209.85 3204.66 33.07 o 0 2 0 147.33 136.17 13.81 o 1 2 0 7291.19 7545.71 78.41 o 2 2 0 43.30 54.69 19.25 o 3 2 0 36.17 16.04 31.67 o 4 2 0 218.75 40.32 43.53 o 5 2 0 224.21 215.28 25.53 o 6 2 0 811.81 803.64 38.93 o 7 2 0 64.90 8.93 64.04 o 8 2 0 0.80 10.46 62.37 o 9 2 0 48.73 79.67 60.27 o 10 2 0 0.00 13.81 81.90 o 11 2 0 4.20 15.77 84.27 o -12 3 0 23.30 72.55 60.97 o -11 3 0 283.34 286.02 43.81 o -10 3 0 90.65 146.50 36.00 o -9 3 0 33.20 10.46 60.27 o -8 3 0 69.70 46.88 28.46 o -7 3 0 134.94 162.54 27.35 o -6 3 0 1369.57 1350.98 41.30 o -5 3 0 4.30 10.46 36.55 o -4 3 0 52.53 68.64 16.60 o -3 3 0 4066.10 3909.24 46.60 o -2 3 0 2748.50 2770.75 37.25 o -1 3 0 28901.90 29733.03 189.61 o 0 3 0 2618.29 2727.50 35.44 o 1 3 0 1332.06 1454.92 31.53 o 2 3 0 2.85 9.35 31.39 o 3 3 0 1035.07 1071.24 32.51 o 4 3 0 1052.91 1034.41 35.72 o 5 3 0 2572.32 2513.05 55.25 o 6 3 0 251.50 196.31 34.46 o 7 3 0 307.12 283.37 42.55 o 8 3 0 243.30 283.37 40.18 o 9 3 0 0.99 12.70 59.02 o 10 3 0 63.53 29.72 67.25 o 11 3 0 9.63 16.46 71.99 o -12 4 0 13.36 61.39 41.72 o -11 4 0 2.69 25.81 33.49 o -10 4 0 0.02 12.00 58.46 o -9 4 0 108.47 127.94 30.42 o -8 4 0 38.26 54.83 48.83 o -7 4 0 472.49 494.18 34.04 o -6 4 0 107.05 6.56 47.16 o -5 4 0 942.70 974.27 33.62 o -4 4 0 1401.06 1444.32 34.74 o -3 4 0 35.01 3.91 36.00 o -2 4 0 2376.97 2362.37 38.23 o -1 4 0 340.39 356.20 22.60 o 0 4 0 1087.25 1146.86 29.02 o 1 4 0 59.40 55.53 18.28 o 2 4 0 243.98 300.95 22.18 o 3 4 0 2228.24 2448.59 48.41 o 4 4 0 744.14 712.11 34.32 o 5 4 0 38.65 22.18 48.00 o 6 4 0 372.83 401.96 36.69 o 7 4 0 478.59 479.95 43.81 o 8 4 0 2.82 11.72 58.88 o 9 4 0 15.36 13.39 76.04 o 10 4 0 7.90 104.22 36.41 o -12 5 0 13.49 55.95 71.02 o -11 5 0 15.78 13.81 65.44 o -10 5 0 49.87 90.83 32.93 o -9 5 0 50.19 70.04 56.23 o -8 5 0 1256.57 1214.53 54.13 o -7 5 0 146.19 167.56 29.02 o -6 5 0 71.50 17.16 45.90 o -5 5 0 3147.24 3115.22 55.95 o -4 5 0 207.64 207.19 21.35 o -3 5 0 2212.04 2334.33 42.27 o -2 5 0 628.47 632.31 26.51 o -1 5 0 2478.23 2682.15 43.53 o 0 5 0 217.06 229.65 21.21 o 1 5 0 20.70 4.60 38.37 o 2 5 0 9.49 36.97 37.25 o 3 5 0 355.42 363.87 27.90 o 4 5 0 40.02 45.62 47.16 o 5 5 0 8.86 8.37 51.20 o 6 5 0 287.36 285.04 40.46 o 7 5 0 23.91 11.02 64.18 o 8 5 0 217.03 236.91 42.97 o 9 5 0 34.38 36.00 74.64 o 10 5 0 13.78 65.99 61.67 o -12 6 0 4.18 15.63 73.95 o -11 6 0 2.69 13.81 65.30 o -10 6 0 9.44 12.28 34.04 o -9 6 0 1116.08 1122.31 56.23 o -8 6 0 130.84 113.01 33.90 o -7 6 0 3171.92 2952.26 66.83 o -6 6 0 2365.10 2229.54 54.83 o -5 6 0 140.44 177.89 23.02 o -4 6 0 272.52 266.62 26.09 o -3 6 0 1225.52 1252.90 35.58 o -2 6 0 1099.12 1032.73 32.37 o -1 6 0 155.95 226.16 22.74 o 0 6 0 1777.11 1954.41 43.11 o 1 6 0 950.39 919.30 34.46 o 2 6 0 0.30 71.99 19.95 o 3 6 0 459.17 479.81 33.21 o 4 6 0 546.39 502.41 38.23 o 5 6 0 12.16 9.21 52.60 o 6 6 0 251.97 284.06 37.53 o 7 6 0 48.15 77.43 56.79 o 8 6 0 111.25 47.58 62.64 o 9 6 0 0.55 23.02 69.06 o -12 7 0 0.33 24.42 54.41 o -11 7 0 31.50 21.63 54.55 o -10 7 0 147.27 134.36 38.23 o -9 7 0 45.30 84.83 57.90 o -8 7 0 657.79 624.64 48.69 o -7 7 0 1244.99 1321.26 50.79 o -6 7 0 16.00 70.60 24.28 o -5 7 0 551.70 581.38 34.04 o -4 7 0 90.63 52.04 23.16 o -3 7 0 322.00 358.15 26.37 o -2 7 0 18.08 25.39 36.28 o -1 7 0 231.41 219.19 26.93 o 0 7 0 260.37 220.16 26.09 o 1 7 0 266.61 337.36 28.04 o 2 7 0 443.34 467.26 34.60 o 3 7 0 239.20 296.76 32.37 o 4 7 0 182.41 213.19 33.21 o 5 7 0 439.67 458.47 43.67 o 6 7 0 0.00 11.30 57.34 o 7 7 0 43.80 12.84 69.34 o 8 7 0 1.25 14.37 83.99 o 9 7 0 0.40 16.18 82.18 o -12 8 0 3.71 49.53 63.90 o -11 8 0 163.01 258.81 45.34 o -10 8 0 40.88 65.85 52.74 o -9 8 0 0.68 11.58 56.51 o -8 8 0 3.25 36.28 51.06 o -7 8 0 936.21 914.84 50.51 o -6 8 0 64.06 62.37 49.39 o -5 8 0 0.01 7.53 43.67 o -4 8 0 368.47 422.47 29.86 o -3 8 0 428.99 378.38 30.69 o -2 8 0 96.09 122.64 26.23 o -1 8 0 70.35 59.58 51.34 o 0 8 0 0.35 6.84 52.60 o 1 8 0 43.92 7.39 50.79 o 2 8 0 11.37 8.09 54.27 o 3 8 0 104.05 144.13 31.53 o 4 8 0 25.31 9.91 62.64 o 5 8 0 233.61 263.83 40.46 o 6 8 0 66.93 74.50 64.60 o 7 8 0 47.34 55.67 68.92 o 8 8 0 38.37 70.46 75.48 o -12 9 0 83.65 143.57 42.83 o -11 9 0 37.23 15.21 62.78 o -10 9 0 193.72 165.89 45.34 o -9 9 0 680.11 659.79 52.88 o -8 9 0 49.80 54.69 51.34 o -7 9 0 596.48 660.49 46.18 o -6 9 0 623.14 633.43 39.76 o -5 9 0 911.03 916.93 44.09 o -4 9 0 834.13 786.76 40.32 o -3 9 0 922.89 912.05 44.09 o -2 9 0 2088.74 2097.98 55.95 o -1 9 0 871.31 839.50 43.67 o 0 9 0 113.90 149.57 30.00 o 1 9 0 13.38 72.13 26.93 o 2 9 0 156.91 141.47 33.07 o 3 9 0 13.71 9.91 70.18 o 4 9 0 63.38 16.04 50.09 o 5 9 0 299.03 245.98 43.67 o 6 9 0 129.92 153.47 42.55 o 7 9 0 0.02 14.93 64.32 o 8 9 0 10.66 92.50 73.81 o -11 10 0 302.11 330.66 47.72 o -10 10 0 331.04 338.62 48.41 o -9 10 0 0.43 12.70 50.37 o -8 10 0 256.17 270.95 40.32 o -7 10 0 32.90 10.60 58.60 o -6 10 0 57.64 9.77 61.95 o -5 10 0 4.66 18.14 54.13 o -4 10 0 267.69 188.21 37.25 o -3 10 0 545.80 543.16 38.93 o -2 10 0 63.70 80.36 32.65 o -1 10 0 99.84 126.41 35.44 o 0 10 0 341.54 388.57 36.41 o 1 10 0 8.31 9.49 65.71 o 2 10 0 47.80 79.95 34.04 o 3 10 0 1.15 22.04 62.92 o 4 10 0 44.68 29.72 59.58 o 5 10 0 64.66 71.71 63.62 o 6 10 0 35.06 22.04 73.39 o 7 10 0 25.20 65.02 40.46 o -11 11 0 26.56 15.91 81.06 o -10 11 0 0.43 14.51 59.58 o -9 11 0 128.13 140.64 38.65 o -8 11 0 0.01 12.28 48.27 o -7 11 0 3.24 68.78 52.60 o -6 11 0 88.31 148.73 34.46 o -5 11 0 0.36 10.05 55.25 o -4 11 0 412.60 397.63 42.97 o -3 11 0 157.75 180.68 37.67 o -2 11 0 61.04 115.24 35.72 o -1 11 0 479.96 421.07 45.90 o 0 11 0 177.24 195.05 37.39 o 1 11 0 100.34 154.73 35.30 o 2 11 0 377.55 339.59 43.81 o 3 11 0 0.04 36.69 58.18 o 4 11 0 7.26 13.39 64.32 o 5 11 0 11.15 14.65 73.11 o 6 11 0 13.74 15.91 79.39 o -11 12 0 92.82 116.92 42.97 o -10 12 0 3.55 15.35 69.06 o -9 12 0 73.26 26.51 39.90 o -8 12 0 0.90 66.13 52.88 o -7 12 0 16.97 61.95 53.99 o -6 12 0 0.75 46.32 49.67 o -5 12 0 349.89 330.66 43.11 o -4 12 0 5.41 37.11 55.39 o -3 12 0 146.91 145.38 35.58 o -2 12 0 19.63 10.74 65.85 o -1 12 0 37.84 82.32 37.39 o 0 12 0 28.49 45.20 62.51 o 1 12 0 39.21 11.86 63.34 o 2 12 0 7.98 12.70 66.97 o 3 12 0 23.63 67.67 63.48 o 4 12 0 0.12 14.65 68.92 o 5 12 0 33.57 54.55 71.85 o -10 13 0 0.01 52.32 39.34 o -9 13 0 1.36 69.06 57.90 o -8 13 0 14.37 14.09 64.18 o -7 13 0 72.34 87.06 69.90 o -6 13 0 10.50 18.84 58.74 o -5 13 0 202.21 256.30 42.27 o -4 13 0 33.04 19.53 39.21 o -3 13 0 11.85 93.34 36.97 o -2 13 0 38.30 79.81 37.11 o -1 13 0 164.10 193.93 40.88 o 0 13 0 112.53 125.99 39.21 o 1 13 0 1.52 26.51 47.72 o 2 13 0 0.35 13.95 73.67 o 3 13 0 90.80 126.82 43.67 o 4 13 0 8.75 16.04 43.39 o -9 14 0 224.45 49.11 94.04 o -8 14 0 61.39 91.39 67.25 o -7 14 0 139.88 50.65 75.62 o -6 14 0 24.22 27.49 64.32 o -5 14 0 15.13 13.39 59.02 o -4 14 0 124.16 127.38 39.90 o -3 14 0 24.28 32.23 60.83 o -2 14 0 40.29 13.25 76.88 o -1 14 0 164.74 160.87 45.34 o 0 14 0 34.94 81.48 41.44 o 1 14 0 49.96 109.66 40.74 o 2 14 0 4.28 23.16 61.11 o 3 14 0 60.77 171.89 43.11 o -8 15 0 54.85 16.18 82.60 o -7 15 0 0.12 31.25 73.39 o -6 15 0 46.06 69.62 40.74 o -5 15 0 0.36 29.16 70.46 o -4 15 0 25.78 14.51 74.64 o -3 15 0 6.17 14.51 66.41 o -2 15 0 25.29 36.69 42.97 o -1 15 0 125.50 120.13 85.67 o 0 15 0 12.34 15.49 71.99 o 1 15 0 15.97 16.18 74.64 o -6 16 0 6.35 89.15 78.97 o -5 16 0 4.48 16.04 68.78 o -4 16 0 2.42 85.81 62.92 o -3 16 0 6.86 85.94 68.64 o -2 16 0 2.46 16.04 88.46 o -1 16 0 149.39 140.36 96.69 o 1 -16 1 119.47 82.18 93.76 o 2 -16 1 6.13 34.88 47.02 o 3 -16 1 66.62 62.51 81.90 o 4 -16 1 6.70 54.69 69.34 o 5 -16 1 0.82 16.04 83.43 o 6 -16 1 21.83 16.32 84.13 o 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98.63 112.45 39.07 o 8 -13 1 115.70 107.43 79.39 o 9 -13 1 0.60 15.21 69.34 o 10 -13 1 63.60 61.25 43.39 o -5 -12 1 73.23 92.36 79.95 o -4 -12 1 144.04 156.12 44.93 o -3 -12 1 22.00 13.39 72.83 o -2 -12 1 290.31 264.95 46.60 o -1 -12 1 36.22 11.86 59.30 o 0 -12 1 0.01 11.30 61.53 o 1 -12 1 161.46 143.99 40.74 o 2 -12 1 21.23 10.74 68.09 o 3 -12 1 539.53 567.99 46.46 o 4 -12 1 116.19 124.31 37.81 o 5 -12 1 82.09 11.16 63.48 o 6 -12 1 357.08 337.92 47.16 o 7 -12 1 359.09 393.73 43.81 o 8 -12 1 156.81 100.32 68.50 o 9 -12 1 162.54 189.89 41.30 o 10 -12 1 143.61 97.66 46.74 o -6 -11 1 0.02 15.77 71.99 o -5 -11 1 0.01 14.37 75.62 o -4 -11 1 17.31 77.43 52.46 o -3 -11 1 131.66 224.07 39.07 o -2 -11 1 62.47 11.30 56.92 o -1 -11 1 86.06 158.64 34.88 o 0 -11 1 57.69 45.07 59.58 o 1 -11 1 0.31 58.46 64.32 o 2 -11 1 6.95 38.37 57.90 o 3 -11 1 400.59 341.41 43.95 o 4 -11 1 36.15 49.67 34.04 o 5 -11 1 10.73 10.19 57.76 o 6 -11 1 9.69 10.74 59.71 o 7 -11 1 282.27 309.32 38.37 o 8 -11 1 0.06 12.42 60.13 o 9 -11 1 0.27 20.65 54.69 o 10 -11 1 12.17 97.94 69.48 o 11 -11 1 0.92 22.18 39.07 o -7 -10 1 2.44 15.91 75.62 o -6 -10 1 39.05 58.18 67.39 o -5 -10 1 24.33 77.16 65.02 o -4 -10 1 40.84 12.00 72.41 o -3 -10 1 9.13 10.88 54.27 o -2 -10 1 9.41 35.30 55.53 o -1 -10 1 0.65 9.35 36.00 o 0 -10 1 218.40 26.65 65.30 o 1 -10 1 496.07 549.43 42.83 o 2 -10 1 457.81 492.65 39.90 o 3 -10 1 28.43 46.46 55.53 o 4 -10 1 530.07 494.04 39.90 o 5 -10 1 552.12 599.24 44.93 o 6 -10 1 296.66 281.27 37.53 o 7 -10 1 55.99 37.81 34.60 o 8 -10 1 193.29 208.03 37.81 o 9 -10 1 202.20 200.49 39.76 o 10 -10 1 77.54 40.88 41.16 o 11 -10 1 2.98 31.95 63.90 o -8 -9 1 58.62 58.04 76.32 o -7 -9 1 56.88 14.79 72.55 o -6 -9 1 26.02 46.74 63.62 o -5 -9 1 183.42 191.56 42.41 o -4 -9 1 227.03 215.28 41.58 o -3 -9 1 8.28 9.77 60.69 o -2 -9 1 3.38 8.93 63.20 o -1 -9 1 1401.40 1420.88 51.06 o 0 -9 1 2293.10 2345.49 59.99 o 1 -9 1 902.99 883.45 43.81 o 2 -9 1 368.98 377.68 34.88 o 3 -9 1 783.99 722.44 39.21 o 4 -9 1 511.43 451.77 35.44 o 5 -9 1 35.27 101.29 27.21 o 6 -9 1 364.85 342.38 36.83 o 7 -9 1 623.63 613.06 47.30 o 8 -9 1 24.69 61.11 55.81 o 9 -9 1 7.24 37.39 52.88 o 10 -9 1 164.69 180.12 42.69 o 11 -9 1 112.78 30.97 74.92 o 12 -9 1 0.17 68.64 79.53 o -8 -8 1 0.57 15.35 73.95 o -7 -8 1 38.53 13.67 72.13 o -6 -8 1 266.17 299.55 41.58 o -5 -8 1 22.08 10.88 36.69 o -4 -8 1 510.61 531.44 44.23 o -3 -8 1 45.01 65.99 32.79 o -2 -8 1 24.95 63.48 50.23 o -1 -8 1 86.38 106.45 26.23 o 0 -8 1 164.07 186.54 25.95 o 1 -8 1 203.73 197.28 28.32 o 2 -8 1 1388.91 1472.78 44.09 o 3 -8 1 1.13 6.70 48.27 o 4 -8 1 284.77 290.48 27.90 o 5 -8 1 290.71 291.04 31.25 o 6 -8 1 78.96 120.69 29.16 o 7 -8 1 12.25 9.35 59.30 o 8 -8 1 304.85 325.64 40.18 o 9 -8 1 1.39 11.72 55.39 o 10 -8 1 2.65 26.79 60.69 o 11 -8 1 78.74 112.73 81.34 o 12 -8 1 11.54 81.20 42.69 o -9 -7 1 6.97 15.91 84.69 o -8 -7 1 49.69 28.60 40.60 o -7 -7 1 129.75 147.61 36.00 o -6 -7 1 2.04 11.16 54.55 o -5 -7 1 50.02 82.32 55.53 o -4 -7 1 379.33 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66.55 o -5 -10 2 328.44 360.66 42.27 o -4 -10 2 3.92 11.86 64.60 o -3 -10 2 60.66 91.94 37.11 o -2 -10 2 19.06 10.05 61.53 o -1 -10 2 142.01 93.90 70.18 o 0 -10 2 28.73 62.09 59.85 o 1 -10 2 2.45 47.72 62.64 o 2 -10 2 32.59 8.51 58.60 o 3 -10 2 1041.95 1033.99 46.74 o 4 -10 2 343.93 338.34 36.83 o 5 -10 2 169.80 179.84 37.53 o 6 -10 2 9.73 10.05 52.88 o 7 -10 2 18.59 32.93 58.60 o 8 -10 2 92.95 36.00 67.25 o 9 -10 2 27.98 19.95 57.62 o 10 -10 2 5.23 14.37 62.23 o 11 -10 2 65.71 86.78 42.69 o -8 -9 2 5.42 16.18 83.43 o -7 -9 2 144.48 151.24 46.04 o -6 -9 2 446.82 452.33 48.55 o -5 -9 2 11.91 42.55 35.30 o -4 -9 2 172.77 220.02 38.23 o -3 -9 2 44.03 9.77 66.83 o -2 -9 2 632.84 508.55 44.37 o -1 -9 2 612.91 636.77 40.74 o 0 -9 2 832.98 826.10 42.69 o 1 -9 2 725.74 701.79 42.27 o 2 -9 2 1207.01 1152.02 45.76 o 3 -9 2 48.53 55.39 30.56 o 4 -9 2 430.00 503.81 35.86 o 5 -9 2 147.96 170.91 30.28 o 6 -9 2 7.17 9.35 55.25 o 7 -9 2 17.15 39.34 29.02 o 8 -9 2 8.62 11.30 59.16 o 9 -9 2 227.10 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