#------------------------------------------------------------------------------
#$Date: 2016-04-03 00:10:41 +0300 (Sun, 03 Apr 2016) $
#$Revision: 180975 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/55/2205565.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2205565_Fobs
loop_
_publ_author_name
'Senju, Takatoshi'
'Hoki, Tomonori'
'Mizuguchi, Jin'
_publ_section_title
;
 2,9-Dichloro-5,12-dihydroquino[2,3-<i>b</i>]acridine-7,14-dione
;
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              o1061
_journal_page_last               o1063
_journal_volume                  61
_journal_year                    2005
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cod_data_source_file            ob6489Isup2.hkl
_cod_data_source_block           I
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_meas
_refln_F_sigma
_refln_observed_status
0 1 0 4.26 7.26 <
0 0 1 76.83 8.08 o
0 1 1 987.83 18.69 o
0 2 0 260.95 18.19 o
0 0 2 7347.55 178.20 o
0 2 1 141.69 18.51 o
0 1 2 3420.22 52.76 o
0 3 0 7.25 21.58 <
0 2 2 904.06 23.37 o
0 3 1 47.83 23.79 <
0 0 3 0.83 20.14 <
0 1 3 1501.44 28.48 o
0 3 2 1207.71 47.17 o
1 0 0 2265.65 56.43 o
0 2 3 2639.19 39.39 o
0 4 0 422.34 27.20 o
1 1 0 2230.73 43.16 o
1 0 -1 35.92 17.23 <
1 0 1 27.30 18.12 <
0 4 1 1725.65 31.30 o
1 1 -1 332.31 19.24 o
1 1 1 10081.35 161.46 o
1 2 0 7364.00 153.18 o
1 0 -2 645.34 26.96 o
1 2 -1 32786.30 303.91 o
0 3 3 1942.71 46.03 o
1 2 1 1806.15 34.17 o
0 0 4 3139.02 78.67 o
1 1 -2 52.79 22.80 <
0 4 2 32.33 31.04 <
1 0 2 5964.97 180.01 o
0 1 4 4029.39 62.23 o
1 1 2 182.76 22.43 o
1 2 -2 19639.13 168.44 o
1 3 0 281.59 29.26 o
0 5 0 8.01 30.96 <
0 2 4 916.60 33.38 o
1 2 2 842.88 31.24 o
1 3 -1 42.25 25.00 <
1 3 1 232.00 22.84 o
0 5 1 45.52 28.13 <
1 0 -3 83.92 27.85 o
1 1 -3 37.10 23.25 <
0 4 3 26.95 27.94 <
1 0 3 77.73 27.90 <
1 3 -2 476.42 25.96 o
1 1 3 2519.40 67.87 o
0 3 4 370.43 31.50 o
0 5 2 737.60 31.69 o
1 3 2 35.82 13.61 <
1 2 -3 395.83 31.93 o
1 4 0 704.40 35.25 o
1 2 3 260.08 23.50 o
1 4 -1 68.66 29.79 <
0 0 5 45.85 24.84 <
1 4 1 344.86 20.27 o
0 1 5 1374.18 29.12 o
1 0 -4 276.65 34.80 o
1 3 -3 10.98 21.49 <
0 6 0 1535.33 61.56 o
1 4 -2 1193.09 32.50 o
1 1 -4 145.24 30.62 o
0 5 3 1264.10 34.42 o
0 2 5 920.06 30.95 o
0 4 4 1918.40 39.97 o
1 3 3 941.35 28.81 o
1 4 2 111.13 27.52 o
0 6 1 1903.87 35.80 o
1 0 4 1328.56 39.47 o
1 1 4 904.22 40.59 o
1 2 -4 821.01 32.09 o
1 5 0 992.41 46.37 o
0 6 2 2079.84 41.89 o
1 5 -1 22.98 34.23 <
1 2 4 21.81 31.03 <
0 3 5 536.78 31.31 o
1 5 1 147.95 37.11 o
1 4 -3 43.47 15.22 <
1 4 3 1742.21 54.13 o
1 3 -4 159.48 27.58 o
1 5 -2 1416.65 48.65 o
0 5 4 41.50 35.43 <
1 5 2 4531.27 117.68 o
1 3 4 432.00 31.21 o
1 0 -5 1.72 34.15 <
0 0 6 443.78 27.93 o
1 1 -5 1329.29 49.66 o
0 6 3 3172.67 81.27 o
0 1 6 2106.01 54.21 o
0 4 5 112.88 31.07 o
0 7 0 8.97 30.19 <
1 0 5 57.86 50.58 <
0 7 1 219.38 32.18 o
1 2 -5 11.37 24.74 <
1 1 5 3493.79 75.74 o
1 4 -4 5130.57 123.51 o
1 5 -3 861.02 39.36 o
0 2 6 756.03 36.44 o
1 6 0 19.49 37.91 <
1 6 -1 59.15 37.97 <
1 6 1 599.55 38.48 o
1 5 3 1458.24 40.04 o
1 4 4 480.63 29.27 o
1 2 5 156.47 25.74 o
0 7 2 770.33 37.78 o
1 3 -5 30.72 27.75 <
1 6 -2 55.55 24.75 <
0 3 6 -3.14 30.76 <
0 6 4 769.80 36.43 o
1 6 2 1374.43 64.75 o
0 5 5 84.45 33.18 <
1 3 5 703.46 34.81 o
1 5 -4 2350.18 74.31 o
0 7 3 3754.53 77.18 o
1 0 -6 711.22 55.97 o
2 0 0 530.57 25.51 o
1 1 -6 156.34 39.73 o
1 6 -3 947.75 35.24 o
2 0 -1 12.46 26.87 <
2 1 0 334.60 25.41 o
1 5 4 170.38 34.33 o
1 4 -5 679.78 36.61 o
2 1 -1 272.24 23.66 o
0 4 6 1171.60 39.41 o
2 0 1 31.95 27.32 <
0 8 0 477.63 32.45 o
1 6 3 52.38 35.69 <
1 7 0 458.30 43.10 o
0 0 7 53.29 28.52 <
2 1 1 232.40 26.76 o
1 0 6 359.20 38.47 o
1 2 -6 1036.34 43.73 o
0 8 1 241.86 32.45 o
1 7 -1 155.80 41.34 o
0 1 7 2870.31 50.27 o
1 1 6 3011.43 86.71 o
2 2 0 1265.65 34.64 o
2 0 -2 275.63 44.97 o
1 4 5 105.84 34.14 o
1 7 1 425.71 40.49 o
2 2 -1 103.44 28.11 o
2 1 -2 108.96 31.56 o
2 2 1 874.58 31.30 o
2 0 2 167.54 27.87 o
0 2 7 328.62 32.36 o
1 2 6 40.75 39.81 <
0 6 5 2348.12 56.28 o
1 7 -2 75.02 40.15 <
2 1 2 163.41 33.16 o
0 8 2 13.42 33.56 <
2 2 -2 214.50 30.67 o
1 3 -6 1448.42 46.04 o
0 7 4 1372.40 41.09 o
1 7 2 209.48 42.19 o
2 3 0 3521.80 113.35 o
1 6 -4 202.24 33.43 o
2 3 -1 4250.07 156.81 o
2 0 -3 20.69 33.83 <
1 5 -5 83.75 39.10 <
2 2 2 698.30 33.86 o
0 5 6 103.22 35.81 <
2 3 1 1417.29 63.32 o
2 1 -3 48.74 34.65 <
0 3 7 27.85 35.95 <
1 3 6 514.73 40.40 o
1 6 4 65.95 35.76 <
2 3 -2 66.96 41.26 <
1 5 5 249.88 39.09 o
2 0 3 24.68 35.53 <
1 7 -3 94.41 36.81 <
2 2 -3 402.27 34.31 o
0 8 3 1731.62 43.40 o
2 1 3 795.96 43.37 o
1 4 -6 409.27 46.99 o
2 3 2 125.28 39.50 o
1 7 3 294.42 39.61 o
2 4 0 33.82 32.24 <
1 0 -7 27.11 43.67 <
2 4 -1 3199.82 127.09 o
1 1 -7 40.21 42.80 <
2 2 3 86.16 38.18 <
1 8 0 27.90 44.90 <
2 4 1 54.43 37.47 <
2 0 -4 746.72 50.78 o
1 8 -1 1111.86 47.19 o
0 4 7 161.53 34.36 o
1 4 6 47.08 44.22 <
2 3 -3 693.42 45.62 o
0 9 0 7.93 40.15 <
1 8 1 267.59 46.14 o
2 1 -4 190.12 36.08 o
2 4 -2 5807.85 185.23 o
1 2 -7 564.59 44.97 o
0 7 5 352.21 36.29 o
1 0 7 28.15 41.05 <
0 9 1 19.18 34.18 <
1 6 -5 562.05 42.16 o
1 1 7 12.27 42.75 <
0 6 6 47.75 36.44 <
1 8 -2 180.04 45.89 o
2 4 2 426.00 41.72 o
0 0 8 42.69 30.80 <
1 7 -4 811.79 47.22 o
2 2 -4 31.45 37.16 <
2 3 3 2701.76 148.65 o
0 8 4 19.38 37.02 <
2 0 4 -5.97 30.77 <
0 1 8 409.68 33.96 o
1 8 2 1487.21 53.24 o
1 6 5 680.86 43.54 o
1 5 -6 208.69 44.58 o
1 2 7 292.82 46.87 o
2 1 4 93.01 35.88 <
0 9 2 669.61 39.15 o
2 5 0 58.58 39.39 <
1 7 4 9.46 47.72 <
1 3 -7 1516.57 55.64 o
2 5 -1 165.77 42.36 o
2 4 -3 4172.48 147.78 o
0 2 8 160.48 33.93 o
2 5 1 0.56 40.74 <
2 2 4 -0.80 39.04 <
2 3 -4 989.07 47.78 o
0 5 7 22.97 38.06 <
1 5 6 157.20 47.22 o
1 8 -3 1374.09 52.17 o
2 5 -2 44.85 43.23 <
1 3 7 1161.87 50.69 o
2 4 3 251.74 47.77 o
2 0 -5 68.96 39.31 <
1 8 3 2361.12 73.15 o
2 1 -5 97.14 40.48 <
0 9 3 69.50 38.47 <
2 5 2 712.76 47.11 o
0 3 8 48.17 38.06 <
1 4 -7 469.19 49.57 o
2 3 4 1399.18 54.38 o
2 2 -5 743.07 44.91 o
1 7 -5 201.50 42.83 o
2 4 -4 1750.79 81.11 o
0 7 6 24.22 40.80 <
1 9 0 541.71 57.05 o
2 5 -3 97.31 48.38 <
0 8 5 201.49 40.99 o
1 6 -6 193.21 40.28 o
1 0 -8 842.62 60.79 o
1 9 -1 129.65 49.68 <
2 0 5 33.97 33.16 <
2 6 0 38.17 40.75 <
1 9 1 305.52 48.62 o
1 4 7 235.95 48.62 o
1 1 -8 10.74 45.49 <
2 6 -1 81.90 49.42 <
2 1 5 1002.49 75.93 o
1 7 5 102.52 43.10 <
1 8 -4 86.04 46.96 <
2 6 1 227.97 50.13 o
0 10 0 351.78 38.09 o
0 4 8 135.20 42.31 o
2 5 3 48.29 52.45 <
0 6 7 1099.09 49.31 o
2 3 -5 419.69 49.50 o
1 6 6 66.06 41.92 <
1 9 -2 60.85 50.17 <
2 4 4 96.18 53.44 <
1 2 -8 231.15 47.46 o
0 10 1 197.82 42.31 o
2 2 5 45.91 45.43 <
1 8 4 264.87 48.48 o
2 6 -2 98.31 47.52 <
0 9 4 430.85 46.93 o
1 0 8 284.34 47.39 o
1 9 2 89.43 51.71 <
1 5 -7 121.92 51.69 <
1 1 8 80.97 46.85 <
2 6 2 67.41 54.63 <
0 10 2 233.52 41.66 o
2 5 -4 16.14 49.77 <
2 0 -6 1066.67 66.98 o
1 2 8 512.93 57.51 o
1 3 -8 630.47 54.38 o
2 1 -6 5.17 48.35 <
2 3 5 198.35 45.34 o
0 0 9 15.44 48.60 <
1 5 7 527.74 49.78 o
1 9 -3 98.20 47.32 <
2 4 -5 804.86 52.43 o
0 1 9 480.54 61.12 o
2 6 -3 334.10 67.50 o
1 9 3 40.26 45.97 <
0 5 8 146.21 43.91 o
2 2 -6 860.80 66.03 o
1 7 -6 219.41 46.31 o
2 5 4 901.73 58.20 o
0 2 9 65.78 39.36 <
2 7 0 64.33 52.42 <
1 8 -5 241.59 51.97 o
1 3 8 30.07 47.42 <
2 6 3 13.45 61.27 <
2 7 -1 38.88 52.87 <
0 8 6 126.68 41.50 o
0 10 3 91.29 42.09 <
2 7 1 76.28 53.06 <
2 0 6 843.78 55.15 o
1 4 -8 581.92 50.90 o
0 7 7 56.70 45.51 <
2 4 5 5.42 53.15 <
1 7 6 503.35 59.46 o
2 1 6 80.69 44.76 <
1 6 -7 991.30 50.37 o
1 8 5 16.14 47.48 <
0 9 5 25.36 45.54 <
2 3 -6 686.89 49.07 o
2 7 -2 515.61 84.98 o
1 10 0 175.91 56.03 o
0 3 9 115.58 40.49 <
1 9 -4 59.71 49.98 <
2 6 -4 101.09 52.85 <
1 10 -1 911.15 54.06 o
2 5 -5 24.66 51.17 <
2 2 6 1146.47 72.23 o
1 10 1 288.19 50.72 o
2 7 2 105.78 56.60 <
1 6 7 382.38 49.97 o
1 4 8 1049.36 54.73 o
1 9 4 167.67 60.20 <
1 0 -9 40.72 49.85 <
1 10 -2 29.83 59.26 <
0 6 8 415.63 52.51 o
1 1 -9 19.98 53.11 <
2 7 -3 296.13 62.78 o
0 11 0 19.37 48.63 <
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1 10 2 367.96 72.99 o
2 4 -6 64.19 53.23 <
2 3 6 261.50 50.21 o
2 0 -7 19.97 50.61 <
1 5 -8 12.20 49.88 <
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2 1 -7 258.52 53.69 o
1 2 -9 38.49 53.07 <
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1 0 9 49.44 53.33 <
1 8 -6 0.02 54.33 <
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2 8 1 492.25 128.01 o
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1 10 3 236.44 60.23 o
1 3 -9 64.46 49.95 <
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1 2 9 61.86 51.43 <
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2 5 -6 20.62 55.46 <
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2 1 7 22.39 58.45 <
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2 8 2 46.89 62.21 <
0 1 10 28.24 54.05 <
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1 6 -8 38.34 54.65 <
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2 6 5 41.85 62.67 <
1 3 9 9.31 52.49 <
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2 2 7 27.69 55.75 <
1 10 -4 117.26 55.02 <
1 4 -9 1996.64 108.35 o
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2 8 -3 86.94 77.76 <
1 11 0 1213.10 61.09 o
1 11 -1 1092.90 65.98 o
1 10 4 73.63 57.67 <
2 5 6 23.74 62.21 <
2 4 -7 103.09 58.15 <
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1 6 8 1023.82 66.86 o
2 8 3 71.65 59.89 <
2 3 7 102.48 54.15 <
2 7 -5 6.57 58.68 <
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2 0 -8 41.51 57.64 <
1 11 -2 408.13 61.45 o
2 6 -6 198.93 57.73 o
1 8 -7 183.27 59.05 o
1 9 -6 1076.55 62.96 o
2 1 -8 39.04 56.31 <
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1 11 2 196.75 55.87 o
0 6 9 2849.95 76.29 o
2 9 0 435.28 80.11 o
3 2 0 20.22 192.71 <
3 2 -1 2.91 192.01 <
2 9 -1 148.54 64.64 <
0 12 0 999.02 58.55 o
1 0 -10 491.50 56.91 o
2 8 -4 35.45 66.05 <
1 5 -9 196.28 54.18 o
2 9 1 67.61 60.73 <
3 2 1 293.43 50.10 o
1 1 -10 2.80 58.68 <
2 2 -8 77.20 57.76 <
0 12 1 793.94 64.52 o
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1 9 6 1108.83 66.92 o
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3 2 -2 215.06 70.76 o
1 7 -8 28.83 59.20 <
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1 10 -5 34.76 54.43 <
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2 3 -8 39.81 56.66 <
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3 3 -2 22.49 43.93 <
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1 3 -10 216.54 54.52 o
3 0 3 57.11 47.00 <
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1 11 4 7.63 57.47 <
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1 4 -10 1207.29 61.26 o
3 2 -4 27.58 49.94 <
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1 12 -1 594.10 59.81 o
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1 10 -6 14.29 64.07 <
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2 10 -1 669.57 88.88 o
2 0 -9 31.89 60.04 <
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3 6 -2 54.14 284.85 <
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1 12 -4 47.02 64.26 <
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2 5 13 104.28 35.63 <
3 3 11 80.22 38.04 <
1 1 15 23.46 40.37 <
1 17 3 129.65 37.85 o
3 0 -12 3323.61 56.73 o
3 8 9 175.67 42.80 o
2 16 0 78.12 33.09 <
2 12 9 1.31 38.15 <
3 11 -7 -0.23 37.31 <
2 14 -7 5.46 39.76 <
3 9 -9 -5.35 47.39 <
1 7 -14 12.50 38.16 <
3 1 -12 402.49 239.35 <
2 16 -1 10.65 31.39 <
1 13 10 77.00 33.99 <
2 16 1 23.58 30.24 <