#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2205613.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205613_Fobs loop_ _publ_author_name 'Essehli, Rachid' 'Lachkar, Mohammed' 'Svoboda, Ingrid' 'Fuess, Hartmut' 'El Bali, Brahim' _publ_section_title ; (NH~4~)~2~[Co(H~2~P~2~O~7~)~2~(H~2~O)~2~] ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i61 _journal_page_last i63 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 81.23 _cell_angle_beta 70.68 _cell_angle_gamma 88.54 _cell_length_a 7.067 _cell_length_b 7.368 _cell_length_c 7.852 _exptl_crystal_F_000 245.00 _reflns_d_resolution_high 0.8000 _[local]_cod_data_source_file wm6057Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CO0.5NH4H2P2O7.H2O IN SPACE GROUP P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 83.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1181.92 1370.42 182.42 o 3 0 0 133.26 158.91 7.50 o 4 0 0 1460.66 1569.27 70.43 o 5 0 0 350.27 321.73 28.64 o 6 0 0 94.44 79.72 2.76 o 7 0 0 203.84 196.20 6.63 o 8 0 0 115.09 118.89 6.90 o -8 1 0 35.05 32.20 5.36 o -7 1 0 442.79 450.43 8.39 o -6 1 0 522.18 557.43 30.49 o -5 1 0 140.08 143.51 5.59 o -4 1 0 20.57 21.87 2.06 o -3 1 0 147.57 89.75 11.84 o -2 1 0 6481.38 6465.60 663.17 o -1 1 0 666.52 668.60 81.43 o 1 1 0 856.87 861.62 65.58 o 2 1 0 227.40 261.24 13.02 o 3 1 0 125.50 151.84 3.42 o 4 1 0 315.88 324.37 6.40 o 5 1 0 2291.25 2325.37 159.00 o 6 1 0 61.01 49.93 4.15 o 7 1 0 91.27 85.88 9.58 o 8 1 0 2.81 4.66 2.62 o -8 2 0 14.72 18.25 5.17 o -7 2 0 0.40 1.39 1.53 o -6 2 0 348.65 362.19 7.12 o -5 2 0 230.11 203.55 8.12 o -4 2 0 316.14 319.78 25.86 o -3 2 0 935.03 928.45 116.30 o -2 2 0 665.02 786.90 17.66 o -1 2 0 647.75 646.18 29.51 o 0 2 0 3527.01 3223.29 20.26 o 1 2 0 20.98 28.73 2.28 o 2 2 0 64.91 80.04 3.44 o 3 2 0 1213.18 1254.29 56.48 o 4 2 0 678.92 741.45 18.06 o 5 2 0 152.62 162.72 5.64 o 6 2 0 150.97 140.69 13.83 o 7 2 0 16.62 14.36 3.07 o 8 2 0 32.63 30.15 4.41 o -7 3 0 3.32 2.29 1.79 o -6 3 0 66.46 57.87 3.01 o -5 3 0 510.55 519.65 24.39 o -4 3 0 78.88 84.12 3.94 o -3 3 0 326.82 357.84 9.98 o -2 3 0 186.52 212.44 7.89 o -1 3 0 763.35 714.40 13.14 o 0 3 0 289.37 377.94 23.59 o 1 3 0 5.33 2.74 0.91 o 2 3 0 2784.79 2733.65 277.80 o 3 3 0 1067.26 1101.16 58.42 o 4 3 0 59.98 57.42 4.66 o 5 3 0 488.58 486.89 11.12 o 6 3 0 77.51 75.01 4.64 o 7 3 0 379.02 392.87 24.00 o -7 4 0 388.38 440.87 7.58 o -6 4 0 30.95 34.39 3.05 o -5 4 0 44.81 35.37 2.56 o -4 4 0 1.51 2.33 1.30 o -3 4 0 299.07 294.94 5.42 o -2 4 0 108.62 88.26 2.05 o -1 4 0 0.60 1.41 0.64 o 0 4 0 2907.47 3046.17 186.63 o 1 4 0 2291.21 2249.83 82.46 o 2 4 0 841.37 884.26 52.12 o 3 4 0 35.57 34.01 1.75 o 4 4 0 113.55 115.11 3.97 o 5 4 0 267.65 276.34 8.02 o 6 4 0 17.16 15.31 3.73 o 7 4 0 99.74 100.28 7.68 o -7 5 0 66.24 76.10 5.14 o -6 5 0 118.97 132.14 8.01 o -5 5 0 0.31 1.90 1.88 o -4 5 0 23.55 20.49 2.22 o -3 5 0 101.26 86.39 3.07 o -2 5 0 1645.07 1706.21 39.84 o -1 5 0 353.14 339.25 8.30 o 0 5 0 17.46 18.19 1.33 o 1 5 0 100.98 109.26 6.50 o 2 5 0 382.77 376.19 19.13 o 3 5 0 129.75 129.05 3.28 o 4 5 0 0.44 0.76 1.10 o 5 5 0 522.01 546.13 23.65 o 6 5 0 232.74 241.64 7.11 o -6 6 0 6.97 6.02 3.00 o -5 6 0 319.74 332.71 9.12 o -4 6 0 589.42 636.51 14.11 o -3 6 0 107.18 95.20 2.95 o -2 6 0 134.09 149.11 7.87 o -1 6 0 356.94 361.58 8.89 o 0 6 0 6.47 7.32 1.45 o 1 6 0 101.96 97.41 3.97 o 2 6 0 7.71 9.03 2.10 o 3 6 0 626.54 639.84 23.55 o 4 6 0 100.07 110.73 3.52 o 5 6 0 1.65 1.23 1.51 o -5 7 0 111.59 113.35 7.17 o -4 7 0 562.17 648.93 9.22 o -3 7 0 102.55 93.60 4.57 o -2 7 0 166.37 164.91 4.78 o -1 7 0 0.58 1.79 1.34 o 0 7 0 311.04 324.39 6.59 o 1 7 0 221.49 210.79 5.70 o 2 7 0 6.67 10.71 3.80 o 3 7 0 68.78 72.39 4.79 o 4 7 0 181.43 182.66 6.17 o 5 7 0 17.59 16.29 5.20 o -4 8 0 7.66 5.32 3.99 o -3 8 0 4.18 4.14 3.13 o -2 8 0 2.45 2.83 2.43 o -1 8 0 6.20 5.08 2.33 o 0 8 0 195.80 210.94 6.15 o 1 8 0 479.41 528.28 8.97 o 2 8 0 146.30 151.64 6.90 o 3 8 0 18.68 20.20 5.00 o -1 9 0 146.16 154.65 7.40 o 0 9 0 31.78 33.73 5.92 o 1 9 0 17.81 18.10 5.45 o -3 -8 1 81.87 77.31 5.93 o -2 -8 1 64.88 67.52 6.03 o -1 -8 1 130.16 137.92 7.02 o 0 -8 1 267.36 298.17 7.78 o 1 -8 1 10.70 9.00 4.10 o 2 -8 1 50.24 46.86 4.99 o 3 -8 1 103.00 103.33 6.54 o 4 -8 1 292.14 326.30 8.34 o -4 -7 1 225.35 260.39 7.42 o -3 -7 1 340.06 364.13 7.71 o -2 -7 1 39.00 47.18 5.05 o -1 -7 1 0.24 2.16 2.45 o 0 -7 1 0.85 1.01 1.95 o 1 -7 1 67.09 61.20 4.64 o 2 -7 1 1.01 1.78 1.43 o 3 -7 1 131.64 120.71 3.58 o 4 -7 1 307.59 333.74 9.97 o 5 -7 1 54.96 46.03 4.17 o -5 -6 1 173.96 173.44 9.51 o -4 -6 1 5.47 5.71 2.31 o -3 -6 1 95.92 89.46 3.23 o -2 -6 1 313.00 319.33 10.24 o -1 -6 1 1.26 1.77 1.31 o 0 -6 1 124.68 106.80 6.10 o 1 -6 1 249.83 245.22 11.30 o 2 -6 1 954.15 1054.05 11.62 o 3 -6 1 2.22 2.02 1.04 o 4 -6 1 96.14 89.33 3.22 o 5 -6 1 2.86 2.63 1.91 o 6 -6 1 173.91 195.80 5.68 o -6 -5 1 12.23 7.64 3.64 o -5 -5 1 28.73 25.38 2.93 o -4 -5 1 1.11 3.28 1.55 o -3 -5 1 66.62 66.73 2.80 o -2 -5 1 78.48 75.36 2.64 o -1 -5 1 868.10 890.26 28.23 o 0 -5 1 739.53 828.89 17.49 o 1 -5 1 9.70 8.30 1.00 o 2 -5 1 262.08 271.47 4.76 o 3 -5 1 289.84 287.46 4.50 o 4 -5 1 19.06 18.12 2.18 o 5 -5 1 2.91 2.07 1.36 o 6 -5 1 146.54 149.21 6.39 o 7 -5 1 394.17 437.97 8.61 o -6 -4 1 14.12 17.12 4.77 o -5 -4 1 221.85 211.56 7.95 o -4 -4 1 43.67 44.31 5.30 o -3 -4 1 934.95 975.78 60.03 o -2 -4 1 499.93 536.59 42.66 o -1 -4 1 9.97 18.98 7.46 o 0 -4 1 157.90 140.35 5.39 o 1 -4 1 866.32 896.74 45.32 o 2 -4 1 346.70 366.35 5.50 o 3 -4 1 272.53 267.51 5.94 o 4 -4 1 504.79 468.43 9.34 o 5 -4 1 713.61 724.76 16.82 o 6 -4 1 38.51 40.43 4.89 o 7 -4 1 1.92 3.63 2.44 o -7 -3 1 0.70 1.52 1.89 o -6 -3 1 26.61 25.30 3.26 o -5 -3 1 312.21 328.35 6.80 o -4 -3 1 604.61 624.26 10.90 o -3 -3 1 1612.21 1707.81 136.05 o -2 -3 1 597.28 623.90 64.83 o -1 -3 1 12.59 12.11 1.34 o 0 -3 1 39.54 42.18 1.50 o 1 -3 1 740.45 685.33 28.42 o 2 -3 1 982.16 887.50 18.36 o 3 -3 1 215.20 190.84 15.24 o 4 -3 1 43.60 45.30 2.48 o 5 -3 1 220.24 210.01 6.40 o 6 -3 1 96.40 91.83 3.52 o 7 -3 1 24.97 19.73 2.72 o 8 -3 1 24.23 24.68 3.99 o -7 -2 1 80.66 77.85 5.22 o -6 -2 1 133.69 125.69 10.57 o -5 -2 1 2297.68 2304.29 226.65 o -4 -2 1 1326.56 1432.72 42.18 o -3 -2 1 163.16 152.25 7.23 o -2 -2 1 2.60 5.13 2.86 o -1 -2 1 1511.08 1547.68 150.70 o 0 -2 1 1994.96 2284.74 55.08 o 1 -2 1 53.39 49.63 1.55 o 2 -2 1 125.83 109.00 3.67 o 3 -2 1 178.15 149.36 15.26 o 4 -2 1 60.66 59.67 3.78 o 5 -2 1 283.35 275.21 8.02 o 6 -2 1 121.86 127.90 3.38 o 7 -2 1 374.69 426.32 5.43 o 8 -2 1 104.86 115.36 7.98 o -7 -1 1 139.32 135.26 12.54 o -6 -1 1 130.98 130.01 9.24 o -5 -1 1 50.67 55.49 7.25 o -4 -1 1 269.67 254.95 7.79 o -3 -1 1 646.02 707.56 11.89 o -2 -1 1 485.12 515.79 33.88 o -1 -1 1 2732.99 2885.88 296.75 o 0 -1 1 6888.73 7692.66 678.46 o 1 -1 1 927.30 900.16 33.73 o 2 -1 1 553.16 563.55 58.43 o 3 -1 1 125.12 140.91 10.68 o 4 -1 1 850.24 810.09 16.98 o 5 -1 1 170.45 176.60 13.07 o 6 -1 1 26.45 23.24 2.14 o 7 -1 1 406.89 411.01 20.54 o 8 -1 1 116.88 115.45 6.93 o -7 0 1 384.76 424.78 29.78 o -6 0 1 154.24 163.30 6.58 o -5 0 1 291.29 265.55 8.65 o -4 0 1 89.26 76.19 6.97 o -3 0 1 869.45 781.44 56.37 o -2 0 1 3.30 3.43 1.98 o -1 0 1 641.78 597.72 51.69 o 2 0 1 65.76 82.68 1.65 o 3 0 1 140.11 140.79 6.48 o 4 0 1 3424.67 3703.91 66.45 o 5 0 1 2754.02 2725.45 182.76 o 6 0 1 106.46 110.08 3.15 o 7 0 1 53.25 47.47 4.53 o 8 0 1 7.92 9.28 3.95 o -7 1 1 10.48 4.68 2.63 o -6 1 1 134.00 138.60 3.17 o -5 1 1 271.96 239.95 9.38 o -4 1 1 48.60 45.85 1.86 o -3 1 1 2857.22 2935.35 305.82 o -2 1 1 6879.87 7145.37 770.81 o -1 1 1 224.01 220.61 1.73 o 1 1 1 17.03 15.20 1.35 o 2 1 1 6926.51 6582.21 262.01 o 3 1 1 742.80 619.45 12.19 o 4 1 1 7.15 7.32 1.12 o 5 1 1 189.79 163.12 11.68 o 6 1 1 406.68 368.69 7.10 o 7 1 1 13.88 11.87 3.33 o 8 1 1 13.47 17.12 5.44 o -7 2 1 9.16 9.58 2.56 o -6 2 1 3.06 2.65 1.53 o -5 2 1 597.71 597.90 15.86 o -4 2 1 1788.96 1833.51 92.04 o -3 2 1 339.21 374.67 32.67 o -2 2 1 441.83 487.99 34.10 o -1 2 1 60.85 57.85 8.02 o 0 2 1 4407.16 5039.90 340.45 o 1 2 1 550.37 559.94 54.36 o 2 2 1 334.37 314.66 13.48 o 3 2 1 345.91 304.12 17.52 o 4 2 1 4.70 2.73 0.91 o 5 2 1 171.51 154.69 3.23 o 6 2 1 41.38 36.00 3.72 o 7 2 1 239.33 253.54 27.54 o 8 2 1 162.40 184.93 11.21 o -7 3 1 294.29 314.08 18.31 o -6 3 1 325.30 360.90 12.78 o -5 3 1 15.77 13.43 2.19 o -4 3 1 31.58 28.85 3.79 o -3 3 1 2.33 4.15 0.78 o -2 3 1 360.37 427.20 26.57 o -1 3 1 224.30 248.55 24.16 o 0 3 1 210.92 177.26 8.55 o 1 3 1 1528.36 1436.35 126.13 o 2 3 1 151.94 160.88 10.63 o 3 3 1 141.61 135.94 5.66 o 4 3 1 2.52 2.76 0.86 o 5 3 1 193.80 200.84 5.63 o 6 3 1 103.40 108.63 4.71 o 7 3 1 152.57 142.51 6.54 o 8 3 1 111.30 117.20 9.74 o -7 4 1 57.14 62.26 7.42 o -6 4 1 170.34 172.02 4.30 o -5 4 1 4.78 4.99 1.58 o -4 4 1 28.05 26.46 2.40 o -3 4 1 282.17 279.04 13.95 o -2 4 1 127.79 132.84 4.67 o -1 4 1 386.20 390.19 39.89 o 0 4 1 44.76 48.90 3.16 o 1 4 1 289.89 231.18 8.22 o 2 4 1 0.79 2.37 1.13 o 3 4 1 77.76 59.93 4.74 o 4 4 1 740.36 774.36 15.51 o 5 4 1 915.82 949.50 29.12 o 6 4 1 420.66 418.65 7.56 o 7 4 1 1.06 1.89 3.31 o -6 5 1 6.95 7.70 4.25 o -5 5 1 535.96 583.74 8.92 o -4 5 1 100.45 91.54 4.34 o -3 5 1 128.86 123.04 4.02 o -2 5 1 584.86 594.97 14.96 o -1 5 1 1172.90 1147.83 28.77 o 0 5 1 84.30 94.56 4.16 o 1 5 1 524.33 542.29 41.54 o 2 5 1 1343.71 1447.46 121.83 o 3 5 1 1674.39 1748.08 86.46 o 4 5 1 206.66 196.79 8.01 o 5 5 1 100.44 99.69 6.14 o 6 5 1 93.28 92.13 6.28 o 7 5 1 148.14 147.79 6.98 o -6 6 1 35.83 32.45 5.01 o -5 6 1 128.70 131.91 6.63 o -4 6 1 897.82 1024.47 10.73 o -3 6 1 208.79 212.68 5.65 o -2 6 1 61.49 61.19 5.43 o -1 6 1 20.99 15.50 1.69 o 0 6 1 1755.63 1848.35 114.04 o 1 6 1 700.16 723.34 9.01 o 2 6 1 144.14 144.43 4.79 o 3 6 1 83.47 95.03 5.44 o 4 6 1 112.90 123.46 5.31 o 5 6 1 8.51 8.79 3.56 o 6 6 1 116.46 121.05 5.93 o -5 7 1 1.43 3.65 3.95 o -4 7 1 9.87 12.01 3.63 o -3 7 1 9.90 6.54 2.52 o -2 7 1 41.74 42.12 2.85 o -1 7 1 0.57 1.21 1.23 o 0 7 1 312.59 341.85 11.56 o 1 7 1 833.36 940.27 10.38 o 2 7 1 36.49 40.51 4.18 o 3 7 1 45.03 38.00 4.38 o 4 7 1 30.32 25.25 4.10 o 5 7 1 183.28 183.15 6.56 o -4 8 1 5.66 6.73 4.55 o -3 8 1 13.27 12.76 4.00 o -2 8 1 143.83 151.14 5.91 o -1 8 1 162.00 166.70 8.69 o 0 8 1 0.92 2.91 2.80 o 1 8 1 30.10 24.65 4.07 o 2 8 1 0.37 1.57 2.65 o 3 8 1 5.06 7.97 3.73 o 4 8 1 19.98 17.64 5.24 o -1 9 1 152.97 151.33 6.43 o 0 9 1 11.64 14.48 4.69 o 1 9 1 39.54 33.56 5.81 o -2 -8 2 34.64 35.46 5.86 o -1 -8 2 74.01 72.76 6.61 o 0 -8 2 3.50 4.03 3.55 o 1 -8 2 116.41 137.84 7.21 o 2 -8 2 132.29 152.78 8.03 o 3 -8 2 23.48 22.06 4.97 o -3 -7 2 8.83 6.01 2.32 o -2 -7 2 246.53 251.28 6.54 o -1 -7 2 34.51 33.90 3.86 o 0 -7 2 51.88 53.73 7.27 o 1 -7 2 210.77 220.12 12.42 o 2 -7 2 499.71 544.59 5.55 o 3 -7 2 45.04 37.42 2.13 o 4 -7 2 91.68 85.44 5.65 o 5 -7 2 0.68 1.88 3.49 o -5 -6 2 4.45 5.42 3.48 o -4 -6 2 22.31 14.62 2.47 o -3 -6 2 0.77 1.16 1.39 o -2 -6 2 225.75 233.31 8.18 o -1 -6 2 380.25 384.82 18.57 o 0 -6 2 135.74 133.52 3.86 o 1 -6 2 238.36 219.91 3.57 o 2 -6 2 51.52 49.15 1.82 o 3 -6 2 57.20 51.73 1.90 o 4 -6 2 49.96 44.41 3.11 o 5 -6 2 15.04 14.22 4.11 o 6 -6 2 196.82 215.13 7.11 o -5 -5 2 2.02 2.51 2.21 o -4 -5 2 232.76 256.60 4.42 o -3 -5 2 282.12 297.70 14.63 o -2 -5 2 15.07 13.66 1.87 o -1 -5 2 220.54 205.05 12.28 o 0 -5 2 113.01 100.71 5.33 o 1 -5 2 1.94 1.93 1.03 o 2 -5 2 222.13 201.14 2.72 o 3 -5 2 185.45 175.43 2.23 o 4 -5 2 1083.73 1176.67 24.52 o 5 -5 2 180.10 167.37 3.92 o 6 -5 2 19.43 12.00 3.53 o 7 -5 2 2.03 1.56 3.06 o -6 -4 2 51.22 48.24 6.36 o -5 -4 2 113.87 107.70 6.58 o -4 -4 2 17.06 20.77 2.33 o -3 -4 2 925.49 984.79 24.88 o -2 -4 2 404.99 392.17 4.25 o -1 -4 2 186.18 180.50 3.59 o 0 -4 2 337.31 330.72 13.62 o 1 -4 2 160.22 149.36 2.41 o 2 -4 2 1910.43 2108.91 61.71 o 3 -4 2 30.33 28.38 1.61 o 4 -4 2 172.24 160.67 3.06 o 5 -4 2 168.78 160.29 3.75 o 6 -4 2 105.82 109.57 3.55 o 7 -4 2 0.24 0.85 2.40 o -6 -3 2 58.56 56.53 4.11 o -5 -3 2 1109.93 1148.40 11.68 o -4 -3 2 322.36 324.33 6.02 o -3 -3 2 324.73 337.84 7.96 o -2 -3 2 28.29 23.92 1.49 o -1 -3 2 1110.81 1224.14 119.99 o 0 -3 2 3191.27 3696.85 120.26 o 1 -3 2 57.92 50.36 1.13 o 2 -3 2 1405.19 1344.38 43.40 o 3 -3 2 1101.66 1132.53 41.29 o 4 -3 2 6.42 6.62 1.69 o 5 -3 2 158.04 135.64 3.03 o 6 -3 2 7.54 6.69 1.62 o 7 -3 2 574.60 643.13 31.54 o 8 -3 2 39.83 42.55 5.36 o -7 -2 2 151.41 163.11 26.54 o -6 -2 2 99.84 107.09 4.43 o -5 -2 2 21.55 22.87 2.77 o -4 -2 2 128.88 159.44 6.61 o -3 -2 2 53.83 66.76 2.25 o -2 -2 2 179.86 207.49 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411.41 445.09 8.62 o 1 4 8 393.63 402.09 9.36 o 2 4 8 67.67 63.52 5.86 o 3 4 8 28.32 27.23 4.23 o 4 4 8 45.52 37.80 3.45 o 5 4 8 140.18 141.21 5.13 o 6 4 8 11.73 12.02 3.07 o 0 5 8 29.94 34.29 6.12 o 1 5 8 15.15 16.46 4.89 o 2 5 8 149.16 155.62 9.46 o 3 5 8 129.39 129.89 4.75 o 4 5 8 44.09 41.98 3.83 o 5 5 8 26.79 27.15 6.33 o 1 6 8 29.20 23.06 5.46 o 2 6 8 78.33 69.86 7.24 o 3 6 8 473.78 491.60 14.65 o 4 6 8 321.40 323.34 6.47 o 2 -2 9 184.61 204.96 8.43 o 3 -2 9 96.60 96.65 6.19 o 4 -2 9 33.63 34.56 5.07 o 1 -1 9 126.28 138.18 6.67 o 2 -1 9 53.16 43.63 5.13 o 3 -1 9 13.99 13.42 4.79 o 4 -1 9 200.75 182.48 12.91 o 5 -1 9 94.27 88.61 4.60 o 2 0 9 146.11 140.83 6.93 o 3 0 9 15.36 15.18 4.88 o 4 0 9 62.92 66.21 5.98 o 5 0 9 694.15 746.15 10.96 o 1 1 9 4.38 1.49 2.16 o 2 1 9 122.92 139.50 7.39 o 3 1 9 354.23 345.04 8.29 o 4 1 9 40.24 34.54 5.36 o 5 1 9 53.85 51.12 6.24 o 6 1 9 7.97 9.59 3.20 o 0 2 9 29.37 39.80 5.40 o 1 2 9 14.92 16.22 4.45 o 2 2 9 8.62 10.76 5.12 o 3 2 9 181.64 196.90 5.23 o 4 2 9 12.07 10.56 3.11 o 5 2 9 71.13 66.94 4.18 o 0 3 9 299.63 312.85 7.09 o 1 3 9 111.60 116.16 5.66 o 2 3 9 0.41 3.07 2.35 o 3 3 9 21.72 10.75 3.13 o 4 3 9 229.57 237.08 8.29 o 5 3 9 71.44 67.45 7.88 o 1 4 9 3.51 3.85 2.69 o 2 4 9 361.02 385.95 8.17 o 3 4 9 187.47 184.66 5.71 o 4 4 9 59.02 45.81 7.54 o