#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:10:58 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180976 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/56/2205614.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205614_Fobs loop_ _publ_author_name 'Essehli, Rachid' 'Lachkar, Mohammed' 'Svoboda, Ingrid' 'Fuess, Hartmut' 'El Bali, Brahim' _publ_section_title ; (NH~4~)~2~[Ni(H~2~P~2~O~7~)~2~(H~2~O)~2~] ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i64 _journal_page_last i66 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 81.53 _cell_angle_beta 70.91 _cell_angle_gamma 88.21 _cell_length_a 7.0344 _cell_length_b 7.3214 _cell_length_c 7.7920 _exptl_crystal_F_000 246.00 _reflns_d_resolution_high 0.8002 _cod_data_source_file wm6058Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' NI0.5NH4H2P2O7.H2O IN SPACE GROUP P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 85.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1041.54 1155.68 8.05 o 3 0 0 102.50 113.78 1.01 o 4 0 0 1647.31 1700.07 48.54 o 5 0 0 345.63 367.43 6.80 o 6 0 0 74.18 60.16 1.42 o 7 0 0 298.47 309.74 4.53 o 8 0 0 169.63 170.89 4.64 o -8 1 0 56.83 57.59 3.75 o -7 1 0 543.56 550.50 6.02 o -6 1 0 672.53 707.37 15.86 o -5 1 0 121.22 136.15 2.24 o -4 1 0 15.02 15.56 0.95 o -3 1 0 167.13 117.57 0.95 o -2 1 0 6590.81 6291.12 35.08 o -1 1 0 752.54 781.73 15.36 o 1 1 0 1019.58 970.36 26.92 o 2 1 0 200.87 207.14 4.15 o 3 1 0 118.32 137.85 1.91 o 4 1 0 360.66 342.50 2.94 o 5 1 0 2577.46 2685.15 35.34 o 6 1 0 85.48 76.54 1.97 o 7 1 0 86.39 74.62 2.39 o 8 1 0 3.74 2.53 1.18 o -8 2 0 24.50 22.49 3.16 o -7 2 0 0.31 1.03 0.84 o -6 2 0 389.20 368.42 18.04 o -5 2 0 300.88 252.87 2.55 o -4 2 0 332.94 336.18 7.60 o -3 2 0 1046.01 1004.99 15.08 o -2 2 0 717.50 726.65 2.63 o -1 2 0 775.25 747.37 5.99 o 0 2 0 3202.48 3128.39 69.03 o 1 2 0 17.84 26.28 0.71 o 2 2 0 92.59 119.13 1.13 o 3 2 0 1185.71 1175.31 13.57 o 4 2 0 792.48 775.81 3.40 o 5 2 0 233.50 238.58 2.75 o 6 2 0 170.71 165.35 2.34 o 7 2 0 24.37 22.21 1.93 o 8 2 0 29.00 25.89 3.37 o -7 3 0 7.23 3.81 1.14 o -6 3 0 65.08 55.93 2.26 o -5 3 0 560.29 586.10 13.50 o -4 3 0 108.17 107.22 1.88 o -3 3 0 383.66 391.01 2.65 o -2 3 0 236.44 253.83 1.95 o -1 3 0 861.17 799.72 4.37 o 0 3 0 276.18 333.43 10.85 o 1 3 0 1.68 2.49 0.41 o 2 3 0 2801.43 2865.07 81.00 o 3 3 0 1196.90 1168.00 3.67 o 4 3 0 87.75 95.74 1.62 o 5 3 0 480.82 516.39 7.28 o 6 3 0 84.46 85.64 3.38 o 7 3 0 419.13 425.94 5.96 o -7 4 0 497.68 527.43 8.48 o -6 4 0 59.84 58.41 3.73 o -5 4 0 57.10 64.17 3.06 o -4 4 0 2.70 1.40 0.68 o -3 4 0 373.49 368.40 2.78 o -2 4 0 162.07 143.15 2.97 o -1 4 0 0.98 1.93 0.78 o 0 4 0 2700.91 2825.57 50.23 o 1 4 0 2436.43 2356.95 81.28 o 2 4 0 999.85 1019.87 33.68 o 3 4 0 14.70 10.96 0.82 o 4 4 0 135.11 122.24 2.96 o 5 4 0 275.61 280.53 4.46 o 6 4 0 19.33 16.71 2.44 o 7 4 0 139.08 134.14 4.43 o -7 5 0 90.74 87.40 3.29 o -6 5 0 166.96 179.87 6.86 o -5 5 0 2.60 22.51 3.64 o -4 5 0 17.31 16.64 2.07 o -3 5 0 133.94 129.19 3.21 o -2 5 0 1706.49 1760.47 10.90 o -1 5 0 375.90 368.53 3.02 o 0 5 0 24.94 41.72 1.46 o 1 5 0 163.46 188.62 5.69 o 2 5 0 477.74 442.17 12.19 o 3 5 0 133.76 145.76 3.46 o 4 5 0 0.63 1.82 1.24 o 5 5 0 609.39 617.89 6.28 o 6 5 0 319.30 333.04 5.31 o -6 6 0 9.07 4.50 1.86 o -5 6 0 405.65 388.40 5.71 o -4 6 0 677.91 690.69 6.90 o -3 6 0 136.41 135.72 2.98 o -2 6 0 175.15 184.18 3.61 o -1 6 0 426.19 443.11 9.87 o 0 6 0 1.41 1.57 1.04 o 1 6 0 99.08 91.73 8.53 o 2 6 0 13.09 9.75 1.19 o 3 6 0 652.66 715.55 6.52 o 4 6 0 117.67 119.18 3.48 o 5 6 0 0.43 1.18 1.56 o 6 6 0 38.85 38.48 3.46 o -5 7 0 134.39 125.80 4.14 o -4 7 0 699.05 739.40 12.15 o -3 7 0 128.33 130.49 2.67 o -2 7 0 158.28 149.21 4.16 o -1 7 0 0.55 3.95 2.25 o 0 7 0 359.54 384.52 7.34 o 1 7 0 223.34 211.75 2.72 o 2 7 0 7.42 7.62 1.21 o 3 7 0 92.13 111.42 3.37 o 4 7 0 224.84 240.41 4.64 o 5 7 0 16.58 14.75 2.56 o -4 8 0 5.16 2.43 1.14 o -3 8 0 2.44 1.93 1.11 o -2 8 0 2.14 3.83 1.35 o -1 8 0 10.83 5.29 1.14 o 0 8 0 212.51 237.34 3.16 o 1 8 0 507.81 525.28 19.11 o 2 8 0 160.87 163.61 4.00 o 3 8 0 7.78 7.77 1.91 o -1 9 0 176.37 183.34 6.63 o 0 9 0 43.22 46.38 3.73 o -3 -8 1 113.42 129.77 4.28 o -2 -8 1 78.31 85.74 3.23 o -1 -8 1 122.55 114.42 3.81 o 0 -8 1 280.46 281.34 7.34 o 1 -8 1 14.04 11.51 1.63 o 2 -8 1 46.81 41.59 4.18 o 3 -8 1 154.30 155.57 4.51 o -4 -7 1 229.26 237.23 4.60 o -3 -7 1 335.95 357.94 5.04 o -2 -7 1 40.66 38.48 2.45 o -1 -7 1 0.56 0.79 0.97 o 0 -7 1 0.47 2.62 1.01 o 1 -7 1 92.97 87.00 2.55 o 2 -7 1 6.06 10.10 1.35 o 3 -7 1 180.91 160.33 2.87 o 4 -7 1 338.01 333.58 5.30 o 5 -7 1 61.07 59.71 3.26 o -5 -6 1 166.71 167.69 4.08 o -4 -6 1 11.98 9.55 1.71 o -3 -6 1 113.68 108.33 3.28 o -2 -6 1 329.83 345.08 4.50 o -1 -6 1 2.83 4.10 1.02 o 0 -6 1 110.33 111.89 3.14 o 1 -6 1 324.77 326.11 7.63 o 2 -6 1 1081.19 1173.47 13.34 o 3 -6 1 0.60 3.04 1.58 o 4 -6 1 104.26 99.24 2.00 o 5 -6 1 0.99 10.11 2.60 o 6 -6 1 262.46 267.26 5.39 o -6 -5 1 5.66 5.50 2.19 o -5 -5 1 28.14 25.73 2.44 o -4 -5 1 3.22 2.68 1.29 o -3 -5 1 46.02 50.78 3.09 o -2 -5 1 120.28 121.01 2.90 o -1 -5 1 980.90 1018.76 4.22 o 0 -5 1 847.94 953.96 4.17 o 1 -5 1 6.80 5.37 1.03 o 2 -5 1 322.77 304.23 8.45 o 3 -5 1 323.63 318.63 4.62 o 4 -5 1 28.40 26.87 2.37 o 5 -5 1 1.58 13.99 2.59 o 6 -5 1 206.12 212.49 4.36 o 7 -5 1 514.70 561.40 7.04 o -6 -4 1 15.04 12.70 2.35 o -5 -4 1 190.60 192.55 4.14 o -4 -4 1 99.20 109.12 3.02 o -3 -4 1 1094.44 1145.77 17.15 o -2 -4 1 548.54 520.40 4.77 o -1 -4 1 9.45 6.00 0.65 o 0 -4 1 217.71 202.55 4.27 o 1 -4 1 952.95 956.27 28.93 o 2 -4 1 363.78 376.85 7.40 o 3 -4 1 367.56 373.24 4.38 o 4 -4 1 622.97 595.72 5.35 o 5 -4 1 881.68 880.14 6.96 o 6 -4 1 39.44 34.88 2.69 o 7 -4 1 5.72 7.15 2.14 o -7 -3 1 1.23 1.87 1.95 o -6 -3 1 60.36 51.38 3.08 o -5 -3 1 465.38 477.55 6.17 o -4 -3 1 716.42 761.18 20.66 o -3 -3 1 1564.58 1596.34 17.48 o -2 -3 1 562.82 511.00 18.03 o -1 -3 1 3.28 3.93 0.47 o 0 -3 1 24.11 45.00 1.19 o 1 -3 1 807.94 759.72 2.82 o 2 -3 1 924.94 849.41 7.53 o 3 -3 1 311.24 295.13 1.72 o 4 -3 1 84.37 90.57 1.78 o 5 -3 1 276.49 250.69 8.52 o 6 -3 1 95.23 83.91 6.75 o 7 -3 1 27.33 21.04 2.98 o 8 -3 1 50.48 45.66 3.43 o -7 -2 1 66.09 57.04 2.30 o -6 -2 1 179.21 180.98 3.55 o -5 -2 1 2478.57 2636.61 7.48 o -4 -2 1 1332.87 1331.45 22.64 o -3 -2 1 193.96 180.54 1.83 o -2 -2 1 2.85 1.29 0.51 o -1 -2 1 1634.77 1479.85 22.40 o 0 -2 1 1973.12 2216.21 36.29 o 1 -2 1 63.03 63.22 1.46 o 2 -2 1 181.98 166.63 2.08 o 3 -2 1 208.87 186.52 1.45 o 4 -2 1 68.28 66.15 2.14 o 5 -2 1 333.45 346.10 10.52 o 6 -2 1 169.15 164.98 8.59 o 7 -2 1 457.73 489.23 20.83 o 8 -2 1 146.30 141.48 8.14 o -7 -1 1 191.01 195.40 3.00 o -6 -1 1 146.72 149.04 3.16 o -5 -1 1 39.60 47.41 3.57 o -4 -1 1 242.35 231.49 1.59 o -3 -1 1 619.52 662.84 3.80 o -2 -1 1 405.95 392.07 12.49 o -1 -1 1 2827.65 2602.01 123.42 o 0 -1 1 7070.73 7320.57 25.99 o 1 -1 1 976.80 912.41 14.40 o 2 -1 1 465.08 474.59 7.50 o 3 -1 1 141.21 146.43 2.32 o 4 -1 1 870.92 846.02 30.45 o 5 -1 1 157.25 175.00 4.93 o 6 -1 1 43.79 41.62 1.60 o 7 -1 1 574.97 581.80 17.95 o 8 -1 1 165.50 156.63 4.15 o -7 0 1 454.41 451.67 5.57 o -6 0 1 173.46 166.19 3.60 o -5 0 1 274.08 285.24 5.17 o -4 0 1 74.98 66.95 1.11 o -3 0 1 1032.36 959.82 11.35 o -2 0 1 15.05 13.07 0.48 o -1 0 1 732.32 683.46 12.74 o 2 0 1 57.92 75.62 0.60 o 3 0 1 159.22 163.59 2.30 o 4 0 1 3643.73 3728.96 65.72 o 5 0 1 3156.18 3143.08 33.48 o 6 0 1 161.69 154.29 3.46 o 7 0 1 33.67 24.92 1.84 o 8 0 1 14.31 13.13 2.80 o -7 1 1 15.49 14.78 2.40 o -6 1 1 181.99 167.47 3.55 o -5 1 1 367.44 339.59 2.72 o -4 1 1 28.16 25.70 1.10 o -3 1 1 3061.93 3080.00 43.33 o -2 1 1 7298.64 7014.49 313.60 o -1 1 1 283.45 272.41 7.23 o 1 1 1 8.14 5.82 0.86 o 2 1 1 6996.07 6694.99 171.96 o 3 1 1 771.26 649.12 4.13 o 4 1 1 25.94 27.69 0.75 o 5 1 1 321.74 314.70 7.38 o 6 1 1 541.68 520.63 12.25 o 7 1 1 20.07 14.84 1.41 o 8 1 1 21.54 15.51 1.73 o -7 2 1 24.60 25.82 2.72 o -6 2 1 1.09 0.97 0.80 o -5 2 1 602.93 608.17 8.94 o -4 2 1 2008.52 2051.23 5.71 o -3 2 1 396.68 412.97 8.30 o -2 2 1 500.35 512.49 15.47 o -1 2 1 52.28 44.33 3.20 o 0 2 1 4430.17 4593.54 63.60 o 1 2 1 612.73 647.87 14.13 o 2 2 1 410.65 389.14 3.84 o 3 2 1 441.53 402.30 1.93 o 4 2 1 18.31 11.99 0.70 o 5 2 1 164.46 203.41 6.57 o 6 2 1 42.97 35.53 1.47 o 7 2 1 251.97 247.71 4.49 o 8 2 1 178.99 166.05 4.50 o -7 3 1 380.00 379.95 5.81 o -6 3 1 387.57 413.00 4.40 o -5 3 1 22.36 27.38 1.71 o -4 3 1 38.05 33.77 1.43 o -3 3 1 0.85 1.85 0.59 o -2 3 1 377.17 407.99 13.18 o -1 3 1 194.59 201.83 2.35 o 0 3 1 219.00 188.59 4.93 o 1 3 1 1804.84 1766.70 64.29 o 2 3 1 205.00 205.39 7.03 o 3 3 1 152.99 154.67 1.76 o 4 3 1 3.74 3.65 0.62 o 5 3 1 192.69 196.39 3.45 o 6 3 1 100.19 98.67 2.89 o 7 3 1 189.14 183.75 3.90 o 8 3 1 157.67 156.41 5.04 o -7 4 1 66.31 57.06 3.41 o -6 4 1 188.74 181.76 4.40 o -5 4 1 1.32 22.60 4.77 o -4 4 1 24.87 20.62 1.63 o -3 4 1 349.44 351.96 6.17 o -2 4 1 139.92 125.71 1.77 o -1 4 1 435.24 424.04 2.41 o 0 4 1 28.38 30.04 1.93 o 1 4 1 373.61 321.23 3.32 o 2 4 1 1.30 2.15 2.21 o 3 4 1 46.37 40.53 1.91 o 4 4 1 764.63 772.53 5.89 o 5 4 1 1073.31 1093.68 7.47 o 6 4 1 500.39 499.69 5.88 o 7 4 1 0.48 0.65 1.34 o -6 5 1 10.14 9.52 1.88 o -5 5 1 686.35 700.09 4.79 o -4 5 1 141.44 132.16 2.90 o -3 5 1 144.54 135.42 2.10 o -2 5 1 642.86 639.58 5.76 o -1 5 1 1397.95 1357.25 5.25 o 0 5 1 56.90 54.77 1.75 o 1 5 1 597.40 606.83 12.71 o 2 5 1 1330.76 1350.65 7.37 o 3 5 1 1769.87 1856.69 9.25 o 4 5 1 274.23 265.62 4.11 o 5 5 1 69.84 68.61 3.16 o 6 5 1 142.38 147.64 4.04 o 7 5 1 175.94 184.89 4.76 o -6 6 1 27.33 25.34 2.24 o -5 6 1 162.82 165.64 9.43 o -4 6 1 1022.75 1101.31 8.57 o -3 6 1 230.13 239.04 4.58 o -2 6 1 38.24 36.82 1.81 o -1 6 1 12.43 21.76 9.01 o 0 6 1 1747.07 1904.93 80.37 o 1 6 1 644.58 631.67 7.48 o 2 6 1 186.88 187.28 6.51 o 3 6 1 172.22 204.79 4.13 o 4 6 1 178.56 176.56 3.73 o 5 6 1 8.75 7.21 1.62 o 6 6 1 144.56 129.25 3.76 o -5 7 1 5.29 6.19 2.44 o -4 7 1 16.41 15.02 2.41 o -3 7 1 10.27 9.83 1.52 o -2 7 1 42.56 41.19 5.34 o -1 7 1 0.90 1.70 0.96 o 0 7 1 333.46 379.66 14.97 o 1 7 1 923.78 996.35 30.88 o 2 7 1 64.93 64.77 2.03 o 3 7 1 19.43 17.30 1.97 o 4 7 1 32.53 32.22 2.72 o 5 7 1 156.20 145.18 4.20 o -3 8 1 16.29 16.86 2.01 o -2 8 1 161.10 155.16 2.83 o -1 8 1 188.31 190.38 5.07 o 0 8 1 0.50 0.94 0.75 o 1 8 1 53.48 53.36 3.27 o 2 8 1 1.13 1.53 0.92 o 3 8 1 10.79 10.43 2.37 o 4 8 1 9.73 6.30 2.19 o -1 9 1 173.51 168.21 4.22 o 0 9 1 23.26 21.40 1.90 o 1 9 1 33.17 30.68 3.20 o -2 -8 2 32.67 31.30 3.11 o -1 -8 2 80.39 80.79 3.43 o 0 -8 2 9.08 8.34 2.07 o 1 -8 2 169.93 186.53 3.94 o 2 -8 2 163.45 171.24 4.41 o 3 -8 2 25.59 19.34 2.54 o -3 -7 2 9.16 7.72 1.96 o -2 -7 2 275.54 281.49 4.57 o -1 -7 2 48.91 48.27 2.57 o 0 -7 2 72.61 73.90 2.47 o 1 -7 2 256.51 260.99 2.80 o 2 -7 2 549.11 585.31 6.13 o 3 -7 2 35.07 30.36 2.81 o 4 -7 2 106.86 102.38 3.56 o 5 -7 2 6.53 23.28 3.46 o -5 -6 2 4.39 6.42 2.85 o -4 -6 2 29.57 25.28 2.56 o -3 -6 2 1.86 12.35 2.19 o -2 -6 2 247.32 240.41 3.95 o -1 -6 2 429.50 465.45 4.98 o 0 -6 2 170.57 198.32 7.71 o 1 -6 2 235.96 212.05 2.41 o 2 -6 2 39.50 38.14 2.09 o 3 -6 2 72.64 65.98 2.75 o 4 -6 2 34.16 30.47 2.56 o 5 -6 2 29.97 27.50 2.67 o 6 -6 2 224.53 235.65 5.23 o -5 -5 2 0.40 1.41 1.35 o -4 -5 2 262.30 272.78 4.38 o -3 -5 2 282.49 300.02 4.41 o -2 -5 2 11.31 10.35 1.58 o -1 -5 2 278.29 248.19 19.39 o 0 -5 2 102.79 99.56 1.98 o 1 -5 2 0.74 3.00 2.25 o 2 -5 2 198.54 183.36 2.17 o 3 -5 2 318.60 299.97 2.79 o 4 -5 2 1302.72 1460.72 8.73 o 5 -5 2 179.74 173.08 3.79 o 6 -5 2 17.15 14.74 2.68 o 7 -5 2 7.67 6.12 2.25 o -6 -4 2 73.35 75.16 3.54 o -5 -4 2 145.38 154.61 3.81 o -4 -4 2 24.14 23.53 1.28 o -3 -4 2 983.75 1007.96 4.62 o -2 -4 2 410.94 373.00 7.20 o -1 -4 2 169.93 150.21 4.43 o 0 -4 2 286.50 306.68 9.76 o 1 -4 2 206.98 204.74 6.62 o 2 -4 2 2097.37 2165.56 45.09 o 3 -4 2 47.05 48.54 1.36 o 4 -4 2 247.86 224.36 3.82 o 5 -4 2 191.36 194.27 3.90 o 6 -4 2 128.49 122.83 3.23 o 7 -4 2 0.68 2.02 1.50 o -6 -3 2 86.67 82.77 2.43 o -5 -3 2 1223.24 1331.02 16.54 o -4 -3 2 349.66 330.31 3.03 o -3 -3 2 303.68 321.09 6.68 o -2 -3 2 54.61 54.92 4.92 o -1 -3 2 1247.51 1287.13 20.16 o 0 -3 2 3337.82 3777.00 25.08 o 1 -3 2 73.22 62.54 1.15 o 2 -3 2 1707.79 1538.79 39.73 o 3 -3 2 1235.92 1277.55 30.47 o 4 -3 2 9.16 9.22 0.99 o 5 -3 2 183.48 180.56 3.61 o 6 -3 2 24.04 24.08 1.77 o 7 -3 2 777.02 885.07 7.76 o 8 -3 2 57.75 61.66 3.81 o -7 -2 2 221.15 231.35 3.31 o -6 -2 2 125.15 132.11 2.50 o -5 -2 2 21.94 27.68 4.18 o -4 -2 2 150.33 161.23 3.13 o -3 -2 2 22.02 28.54 1.83 o -2 -2 2 222.93 243.69 9.58 o -1 -2 2 1681.74 1534.68 51.70 o 0 -2 2 3889.07 3954.86 18.12 o 1 -2 2 2657.44 2661.75 18.96 o 2 -2 2 0.80 2.10 0.70 o 3 -2 2 397.21 403.20 2.76 o 4 -2 2 1.35 1.72 0.67 o 5 -2 2 204.55 196.55 5.75 o 6 -2 2 140.76 160.36 3.64 o 7 -2 2 419.02 439.38 5.44 o 8 -2 2 40.32 33.27 2.96 o -7 -1 2 542.72 594.81 6.68 o -6 -1 2 67.47 65.13 2.16 o -5 -1 2 110.71 138.20 7.99 o -4 -1 2 209.92 209.42 3.85 o -3 -1 2 1900.79 1947.17 8.65 o -2 -1 2 78.32 56.69 1.90 o -1 -1 2 120.49 116.71 3.40 o 0 -1 2 122.11 184.76 3.74 o 1 -1 2 1590.25 1528.76 15.70 o 2 -1 2 2598.17 2682.22 58.45 o 3 -1 2 201.23 220.94 1.64 o 4 -1 2 2216.27 2427.71 5.33 o 5 -1 2 2367.56 2352.94 85.34 o 6 -1 2 276.99 248.69 4.13 o 7 -1 2 172.00 169.41 9.71 o 8 -1 2 57.37 53.51 3.58 o -7 0 2 0.61 2.64 1.76 o -6 0 2 129.96 120.78 3.09 o -5 0 2 216.77 209.25 3.78 o -4 0 2 63.73 48.21 1.67 o -3 0 2 1525.13 1642.32 12.74 o -2 0 2 1712.02 1651.85 37.66 o -1 0 2 4.07 10.16 0.73 o 0 0 2 2221.16 2197.34 102.33 o 1 0 2 2.03 1.65 0.34 o 2 0 2 2449.48 2443.03 72.76 o 3 0 2 14.41 28.53 0.69 o 4 0 2 379.49 355.35 5.44 o 5 0 2 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688.43 751.39 7.46 o 2 -4 8 13.29 13.66 2.06 o 3 -4 8 1.25 1.63 1.20 o 0 -3 8 41.03 36.22 4.68 o 1 -3 8 13.56 10.81 1.78 o 2 -3 8 0.68 1.04 1.10 o 3 -3 8 17.84 15.17 2.00 o 4 -3 8 543.26 584.58 6.90 o 5 -3 8 139.11 138.66 5.60 o -1 -2 8 27.11 23.84 4.08 o 0 -2 8 3.19 2.61 1.18 o 1 -2 8 107.36 109.04 17.00 o 2 -2 8 986.63 1032.29 96.43 o 3 -2 8 219.04 209.24 23.23 o 4 -2 8 35.46 41.60 3.05 o 5 -2 8 112.38 116.44 2.97 o 6 -2 8 17.27 16.01 1.87 o -1 -1 8 123.34 127.42 5.72 o 0 -1 8 365.73 421.88 33.83 o 1 -1 8 59.38 53.56 6.99 o 2 -1 8 48.52 45.96 5.14 o 3 -1 8 470.91 435.20 34.20 o 4 -1 8 0.41 1.38 1.60 o 5 -1 8 24.92 24.28 2.70 o 6 -1 8 8.54 8.31 1.59 o -2 0 8 2.50 2.42 1.27 o -1 0 8 241.45 254.31 13.29 o 0 0 8 420.12 488.07 24.79 o 1 0 8 297.63 309.31 19.78 o 2 0 8 224.03 209.50 17.21 o 3 0 8 33.28 28.26 4.09 o 4 0 8 45.11 39.41 3.31 o 5 0 8 73.95 71.73 3.35 o 6 0 8 96.64 87.64 3.67 o 7 0 8 126.56 112.48 4.42 o -2 1 8 215.21 230.53 4.76 o -1 1 8 32.80 32.41 2.00 o 0 1 8 1.65 1.19 0.96 o 1 1 8 125.03 126.20 2.53 o 2 1 8 82.93 77.65 3.55 o 3 1 8 55.48 43.21 4.24 o 4 1 8 270.17 259.79 28.92 o 5 1 8 511.98 547.36 6.27 o 6 1 8 250.80 244.32 4.59 o 7 1 8 117.37 113.47 4.87 o -2 2 8 103.55 108.83 4.63 o -1 2 8 2.07 4.43 2.10 o 0 2 8 22.93 19.50 2.38 o 1 2 8 3.76 3.01 2.00 o 2 2 8 952.48 985.08 93.37 o 3 2 8 493.95 518.21 6.00 o 4 2 8 115.57 130.29 3.32 o 5 2 8 104.06 116.00 3.56 o 6 2 8 145.52 145.41 4.31 o 7 2 8 23.49 17.94 2.74 o -2 3 8 0.80 2.56 2.23 o -1 3 8 32.19 29.18 3.17 o 0 3 8 269.21 284.07 4.40 o 1 3 8 120.81 116.41 3.18 o 2 3 8 103.34 103.19 3.15 o 3 3 8 346.98 361.04 4.89 o 4 3 8 12.81 12.37 2.22 o 5 3 8 5.95 5.41 1.61 o 6 3 8 5.18 2.19 1.69 o 2 4 8 53.23 50.11 2.85 o 3 4 8 23.25 20.31 2.29 o 4 4 8 57.18 49.85 2.91 o 5 4 8 150.02 147.35 3.59 o 6 4 8 12.47 9.36 2.24 o 3 5 8 96.36 101.24 3.38 o 4 5 8 54.55 56.32 3.12 o 5 5 8 55.94 48.85 3.25 o 2 -2 9 196.72 183.64 13.76 o 3 -2 9 95.20 84.75 5.73 o 1 -1 9 116.36 117.25 9.36 o 2 -1 9 32.11 25.80 2.44 o 3 -1 9 2.51 1.78 1.20 o 4 -1 9 178.26 171.26 14.44 o 5 -1 9 73.73 80.51 4.26 o 0 0 9 30.36 30.90 4.46 o 1 0 9 223.74 229.99 8.47 o 2 0 9 132.94 129.93 2.95 o 3 0 9 19.67 14.03 1.82 o 4 0 9 72.90 69.87 5.75 o 5 0 9 765.73 827.60 8.39 o 0 1 9 12.73 10.53 3.12 o 1 1 9 6.13 3.37 1.20 o 2 1 9 122.75 127.88 4.65 o 3 1 9 308.06 303.39 37.81 o 4 1 9 39.02 39.02 2.59 o 5 1 9 73.85 76.79 3.74 o 0 2 9 36.82 42.66 2.32 o 1 2 9 22.54 20.09 2.13 o 2 2 9 13.15 10.76 2.14 o 3 2 9 159.49 159.47 3.84 o 4 2 9 11.70 9.13 2.11 o 5 2 9 51.54 50.92 3.54 o 1 3 9 108.33 112.97 3.69 o 2 3 9 0.38 0.27 1.03 o 3 3 9 13.72 13.81 2.30 o 4 3 9 259.10 269.33 4.77 o 5 3 9 78.57 82.55 3.74 o 3 4 9 172.79 172.97 4.24 o 4 4 9 76.46 69.90 3.46 o