#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:10:58 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180976 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/56/2205625.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205625_Fobs loop_ _publ_author_name 'Alagar, M.' 'Krishnakumar, R. V.' 'Mostad, A.' 'Natarajan, S.' _publ_section_title ; \b-DL-Methionine at 105 K ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1165 _journal_page_last o1167 _journal_volume 61 _journal_year 2005 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-I 2ya' _symmetry_space_group_name_H-M 'I 1 2/a 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.250 _cell_angle_gamma 90.000 _cell_length_a 9.8770 _cell_length_b 4.6915 _cell_length_c 32.6030 _exptl_crystal_F_000 640.00 _reflns_d_resolution_high 0.8022 _cod_data_source_file wn6339Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' DL-methionine in I2/a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 229.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2243.54 2678.06 78.13 o 4 0 0 7964.73 9025.44 261.54 o 6 0 0 221.79 261.70 10.33 o 8 0 0 5.23 6.90 3.17 o 10 0 0 1007.77 908.49 19.68 o 1 1 0 16909.94 15824.95 235.31 o 3 1 0 273.78 373.35 11.44 o 5 1 0 370.53 402.39 8.01 o 7 1 0 444.60 436.70 6.63 o 9 1 0 1860.73 1673.31 24.37 o 11 1 0 812.86 742.00 20.52 o 0 2 0 17185.21 18650.03 391.06 o 2 2 0 1597.55 1624.07 46.77 o 4 2 0 5697.44 6080.99 90.43 o 6 2 0 3.27 25.38 3.97 o 8 2 0 49.43 48.04 2.78 o 10 2 0 110.16 101.73 3.50 o 1 3 0 0.83 40.99 2.85 o 3 3 0 284.15 247.79 3.94 o 5 3 0 1.27 5.37 1.47 o 7 3 0 54.14 72.97 3.16 o 9 3 0 178.78 165.73 4.97 o 0 4 0 1646.97 1406.97 56.84 o 2 4 0 857.86 919.48 12.34 o 4 4 0 0.32 39.34 4.28 o 6 4 0 122.55 155.88 3.91 o 8 4 0 6.71 5.29 3.26 o 1 5 0 506.87 504.36 7.83 o 3 5 0 143.55 166.39 7.46 o 5 5 0 373.58 377.36 8.03 o -10 1 1 666.68 660.55 8.83 o -8 1 1 656.80 605.37 7.87 o -6 1 1 1.47 21.87 3.46 o -4 1 1 717.16 746.12 13.43 o -2 1 1 5215.10 5394.64 82.51 o 0 1 1 1436.70 1422.30 31.04 o 2 1 1 1460.26 1564.08 30.23 o 4 1 1 4673.42 5017.35 85.62 o 6 1 1 187.65 234.78 8.78 o 8 1 1 52.85 76.61 2.86 o 10 1 1 17.79 27.13 2.35 o -11 2 1 80.62 97.10 4.06 o -9 2 1 1580.95 1617.13 21.34 o -7 2 1 684.69 691.42 9.05 o -5 2 1 550.29 591.68 9.70 o -3 2 1 1465.75 1549.71 23.50 o -1 2 1 76.11 72.25 3.05 o 1 2 1 2157.67 2280.59 34.24 o 3 2 1 6372.90 6111.83 90.76 o 5 2 1 34.55 52.61 3.89 o 7 2 1 1417.84 1404.10 18.41 o 9 2 1 191.17 247.92 5.08 o -10 3 1 416.52 446.50 12.04 o -8 3 1 172.47 203.63 5.11 o -6 3 1 481.77 561.12 9.48 o -4 3 1 270.20 301.90 4.74 o -2 3 1 3228.79 3290.56 49.35 o 0 3 1 1351.15 1359.16 24.37 o 2 3 1 1373.00 1475.73 26.43 o 4 3 1 2457.76 2337.69 23.70 o 6 3 1 0.58 14.52 3.18 o 8 3 1 806.45 836.86 13.25 o -7 4 1 36.02 78.17 3.94 o -5 4 1 697.40 732.91 10.35 o -3 4 1 716.22 743.14 9.53 o -1 4 1 430.11 434.62 6.63 o 1 4 1 66.67 114.56 4.44 o 3 4 1 260.05 268.64 4.86 o 5 4 1 368.92 381.83 6.27 o 7 4 1 1357.98 1309.28 30.71 o -4 5 1 240.92 277.20 6.75 o -2 5 1 80.03 100.34 3.45 o 0 5 1 19.53 39.34 2.70 o 2 5 1 416.99 424.09 6.90 o 4 5 1 2.31 17.88 3.58 o -10 0 2 1066.35 986.05 36.59 o -8 0 2 95.13 134.30 5.47 o -6 0 2 10413.36 10625.05 308.02 o -4 0 2 2765.35 3312.31 70.10 o -2 0 2 3185.69 3481.44 73.93 o 2 0 2 1222.30 1644.66 48.24 o 4 0 2 8147.13 8435.45 244.50 o 6 0 2 2150.10 2106.75 62.69 o 8 0 2 98.94 116.45 6.06 o 10 0 2 84.02 72.76 5.38 o -11 1 2 8.72 29.70 6.90 o -9 1 2 0.13 11.10 2.14 o -7 1 2 200.35 189.20 5.08 o -5 1 2 6.45 56.26 5.22 o -1 1 2 3.60 30.00 3.13 o 1 1 2 9.51 66.95 2.91 o 3 1 2 5273.47 5357.96 112.36 o 5 1 2 3540.78 3802.43 108.27 o 7 1 2 1560.39 1504.55 20.42 o 9 1 2 804.57 769.33 9.88 o 11 1 2 102.74 114.22 5.84 o -10 2 2 103.72 106.28 3.46 o -8 2 2 204.42 198.20 4.36 o -6 2 2 1307.98 1361.72 16.44 o -4 2 2 74.57 159.95 5.15 o -2 2 2 2753.37 2635.83 54.79 o 2 2 2 934.45 995.43 25.46 o 4 2 2 114.42 178.20 5.53 o 6 2 2 42.46 36.18 1.98 o 8 2 2 11.87 23.33 2.27 o 10 2 2 6.53 4.68 2.44 o -9 3 2 467.26 441.71 17.49 o -7 3 2 90.96 91.40 3.34 o -5 3 2 38.69 39.92 2.23 o -3 3 2 257.95 298.42 4.45 o -1 3 2 434.71 404.17 13.46 o 1 3 2 767.56 833.73 27.58 o 3 3 2 113.84 105.20 4.12 o 5 3 2 6.40 1.48 1.59 o 7 3 2 12.95 12.36 2.24 o 9 3 2 139.76 143.12 4.74 o -8 4 2 61.62 72.81 4.05 o -6 4 2 169.47 190.01 7.33 o -4 4 2 190.60 196.09 3.82 o -2 4 2 81.67 114.48 4.31 o 0 4 2 173.64 213.47 6.66 o 2 4 2 739.13 807.74 11.02 o 4 4 2 1641.93 1602.92 20.64 o 6 4 2 354.68 335.12 5.84 o 8 4 2 18.06 26.31 4.47 o -5 5 2 372.58 381.67 6.65 o -3 5 2 746.35 716.85 10.35 o -1 5 2 20.77 105.89 10.86 o 1 5 2 292.14 344.80 7.29 o 3 5 2 27.47 44.20 2.82 o 5 5 2 142.58 158.01 4.25 o -10 1 3 140.46 144.59 4.05 o -8 1 3 1092.10 1021.75 12.35 o -6 1 3 4008.13 4337.99 95.15 o -4 1 3 2.39 20.61 3.83 o -2 1 3 1377.29 1427.08 32.84 o 0 1 3 903.30 913.39 49.29 o 2 1 3 2073.71 1965.33 29.45 o 4 1 3 4859.65 5533.35 94.34 o 6 1 3 17.68 30.02 2.76 o 8 1 3 1006.86 975.11 11.93 o 10 1 3 345.13 341.64 7.43 o -11 2 3 108.13 117.96 3.76 o -9 2 3 885.23 926.11 12.92 o -7 2 3 144.32 174.59 3.94 o -5 2 3 3545.38 3637.78 54.45 o -3 2 3 3958.37 4001.10 59.68 o -1 2 3 3594.31 3610.72 97.49 o 1 2 3 4659.73 4175.67 72.50 o 3 2 3 2101.33 2226.58 33.46 o 5 2 3 4019.90 4228.83 84.23 o 7 2 3 309.50 306.33 5.39 o 9 2 3 280.59 260.84 5.29 o -10 3 3 1385.10 1396.86 31.46 o -8 3 3 584.98 566.92 9.38 o -6 3 3 2586.45 2320.37 27.54 o -4 3 3 1085.21 1020.59 10.78 o 0 3 3 71.98 53.06 3.83 o 2 3 3 482.89 453.52 9.10 o 4 3 3 4164.03 4258.53 49.70 o 6 3 3 22.30 50.23 3.15 o 8 3 3 1112.35 1114.31 20.86 o -7 4 3 484.13 439.24 9.30 o -5 4 3 337.62 307.82 5.77 o -3 4 3 169.32 174.17 3.90 o -1 4 3 400.31 440.32 6.67 o 1 4 3 2900.96 2714.06 30.64 o 3 4 3 2484.40 2488.07 28.94 o 5 4 3 747.26 782.10 10.92 o 7 4 3 62.22 95.85 10.10 o -6 5 3 64.38 52.29 3.25 o -4 5 3 963.17 992.68 13.70 o -2 5 3 3.77 8.97 2.31 o 0 5 3 242.92 253.98 5.63 o 2 5 3 370.67 386.57 6.48 o 4 5 3 196.51 203.67 5.01 o -10 0 4 264.34 252.40 11.37 o -8 0 4 3992.06 3836.11 79.59 o -6 0 4 3054.96 3434.35 127.22 o -4 0 4 141.73 229.39 5.78 o -2 0 4 28628.72 29606.30 622.95 o 0 0 4 36.90 89.07 2.64 o 2 0 4 141.48 216.50 5.07 o 4 0 4 3434.34 3676.63 107.31 o 6 0 4 535.90 542.03 18.02 o 8 0 4 7910.34 7564.38 105.31 o 10 0 4 210.79 226.43 11.43 o -11 1 4 6.41 6.74 2.50 o -9 1 4 7.17 25.49 3.05 o -7 1 4 12.57 40.40 2.41 o -5 1 4 4693.22 4934.97 84.29 o -3 1 4 9508.48 10607.79 157.25 o -1 1 4 52797.33 51405.36 1869.90 o 1 1 4 16036.63 15356.55 265.14 o 3 1 4 12213.48 13069.05 221.71 o 5 1 4 1366.84 1439.31 25.25 o 7 1 4 501.81 432.70 8.86 o 9 1 4 488.59 461.24 7.39 o 11 1 4 378.85 368.14 8.76 o -10 2 4 0.76 12.12 2.38 o -8 2 4 485.38 443.49 6.96 o -6 2 4 67.18 67.08 2.93 o -4 2 4 6.46 2.99 1.67 o -2 2 4 314.34 380.02 7.23 o 0 2 4 730.41 746.50 13.71 o 2 2 4 629.34 697.66 13.32 o 4 2 4 15.77 21.73 1.60 o 6 2 4 491.99 473.02 11.81 o 8 2 4 476.45 415.22 6.81 o 10 2 4 8.90 15.03 2.60 o -9 3 4 32.87 49.90 3.22 o -7 3 4 372.92 384.96 5.89 o -5 3 4 331.63 360.58 4.56 o -3 3 4 43.84 75.72 2.19 o -1 3 4 1159.30 1351.90 28.90 o 1 3 4 146.44 211.26 7.63 o 3 3 4 522.90 506.43 8.86 o 5 3 4 199.96 189.12 3.54 o 7 3 4 51.19 92.77 3.83 o 9 3 4 0.07 3.49 2.83 o -8 4 4 216.94 215.52 5.93 o -6 4 4 928.45 877.15 14.99 o -4 4 4 4.97 24.25 2.49 o -2 4 4 919.62 827.33 11.26 o 0 4 4 101.40 121.03 2.98 o 2 4 4 71.82 75.55 3.80 o 4 4 4 6.18 13.02 3.77 o 6 4 4 646.01 641.07 11.01 o 8 4 4 453.90 460.11 18.85 o -5 5 4 176.76 222.26 6.71 o -3 5 4 0.43 23.06 2.76 o -1 5 4 2181.65 2116.77 27.02 o 1 5 4 905.69 910.46 12.59 o 3 5 4 0.63 15.51 2.71 o 5 5 4 206.05 241.15 6.48 o -10 1 5 88.82 93.93 3.52 o -8 1 5 1.97 13.44 2.10 o -6 1 5 1045.80 1209.55 31.51 o -4 1 5 3610.42 3980.21 59.27 o -2 1 5 13225.46 12904.31 242.32 o 0 1 5 1506.91 1504.81 31.49 o 2 1 5 471.68 444.82 7.05 o 4 1 5 246.89 275.56 5.74 o 6 1 5 920.67 946.88 19.08 o 8 1 5 354.72 339.85 5.85 o 10 1 5 42.19 45.45 3.24 o -11 2 5 271.60 339.88 10.34 o -9 2 5 281.19 296.94 5.51 o -7 2 5 32.52 89.02 7.51 o -5 2 5 817.46 891.89 14.72 o -3 2 5 71.95 69.54 4.02 o -1 2 5 11466.83 11046.51 244.73 o 1 2 5 405.21 426.41 8.23 o 3 2 5 2684.88 2805.15 44.16 o 5 2 5 15.37 14.66 2.29 o 7 2 5 295.03 314.67 5.53 o 9 2 5 344.75 343.73 7.46 o -10 3 5 740.13 787.48 13.33 o -8 3 5 165.62 192.59 5.40 o -6 3 5 87.69 120.45 4.48 o -4 3 5 512.12 610.91 6.85 o -2 3 5 3479.83 3341.03 74.76 o 0 3 5 30.20 28.98 2.39 o 2 3 5 2031.84 2068.20 36.62 o 4 3 5 51.49 44.79 4.83 o 6 3 5 777.84 677.82 9.84 o 8 3 5 510.02 486.26 11.44 o -7 4 5 128.77 225.97 18.60 o -5 4 5 229.49 267.15 5.02 o -3 4 5 315.51 286.71 4.66 o -1 4 5 1501.08 1519.01 19.52 o 1 4 5 343.23 374.25 12.92 o 3 4 5 2323.71 2415.27 26.16 o 5 4 5 0.29 9.37 2.26 o 7 4 5 14.52 33.34 4.07 o -6 5 5 11.51 16.41 2.67 o -4 5 5 498.77 509.70 13.17 o -2 5 5 93.71 128.86 5.63 o 0 5 5 367.31 409.69 6.70 o 2 5 5 209.76 242.29 4.89 o 4 5 5 38.54 58.28 3.56 o -12 0 6 145.72 171.43 7.31 o -10 0 6 180.53 175.84 8.87 o -8 0 6 191.37 256.12 16.95 o -6 0 6 628.08 715.85 16.18 o -4 0 6 1928.26 1729.76 36.88 o -2 0 6 3436.90 3714.13 102.88 o 0 0 6 450.97 453.87 29.09 o 2 0 6 4965.75 5428.68 114.31 o 4 0 6 2103.97 2021.69 59.67 o 6 0 6 2330.58 2296.20 68.24 o 8 0 6 177.49 189.28 5.73 o 10 0 6 1815.37 1580.71 49.34 o -11 1 6 157.31 159.74 4.36 o -9 1 6 1091.82 1020.78 12.45 o -7 1 6 58.38 150.43 3.84 o -5 1 6 6554.54 6928.81 102.99 o -3 1 6 5945.06 6297.37 93.44 o -1 1 6 8402.53 8051.34 206.92 o 1 1 6 3.08 11.33 2.31 o 3 1 6 5.33 -2.03 2.25 o 5 1 6 1261.75 1252.30 24.15 o 7 1 6 54.84 47.19 3.06 o 9 1 6 40.29 51.81 3.44 o -10 2 6 3.74 3.74 2.29 o -8 2 6 28.19 31.04 2.15 o -6 2 6 759.02 766.56 9.69 o -4 2 6 54.28 54.79 2.34 o -2 2 6 145.48 168.15 6.43 o 0 2 6 825.22 816.89 58.16 o 2 2 6 137.70 124.05 3.64 o 4 2 6 90.19 112.76 3.73 o 6 2 6 1737.94 1723.82 20.64 o 8 2 6 11.79 20.55 2.31 o 10 2 6 58.20 54.99 3.85 o -9 3 6 2.48 4.58 2.34 o -7 3 6 17.26 41.61 2.25 o -5 3 6 693.18 709.65 7.87 o -3 3 6 121.76 117.56 2.64 o -1 3 6 953.63 946.53 17.45 o 1 3 6 827.51 811.57 24.52 o 3 3 6 196.44 227.29 6.45 o 5 3 6 22.85 30.66 1.98 o 7 3 6 33.84 44.07 3.03 o 9 3 6 138.34 119.71 4.67 o -8 4 6 59.76 66.34 4.05 o -6 4 6 130.05 151.50 4.72 o -4 4 6 1179.92 1142.39 14.02 o -2 4 6 422.63 457.09 6.92 o 0 4 6 396.99 390.41 5.57 o 2 4 6 411.74 442.52 6.13 o 4 4 6 1.03 2.39 1.91 o 6 4 6 10.87 27.52 2.67 o -5 5 6 560.18 552.62 12.13 o -3 5 6 36.43 60.99 4.73 o -1 5 6 259.58 333.12 7.92 o 1 5 6 2.07 35.20 9.77 o 3 5 6 660.95 655.30 10.55 o 5 5 6 603.83 579.49 10.30 o -10 1 7 191.26 183.99 4.35 o -8 1 7 740.87 753.15 10.44 o -6 1 7 58.30 63.84 3.10 o -4 1 7 69.62 74.11 2.66 o -2 1 7 319.32 285.00 8.56 o 0 1 7 5741.25 5398.83 154.38 o 2 1 7 23577.77 23403.62 346.67 o 4 1 7 266.20 216.69 4.84 o 6 1 7 53.15 39.62 2.65 o 8 1 7 243.56 240.03 5.47 o 10 1 7 49.13 47.40 3.72 o -11 2 7 1433.53 1355.56 18.90 o -9 2 7 258.08 287.26 5.38 o -7 2 7 2513.47 2441.18 28.78 o -5 2 7 27.45 26.82 2.35 o -3 2 7 159.86 115.67 2.83 o -1 2 7 274.15 268.14 11.85 o 1 2 7 15.19 39.75 2.34 o 3 2 7 8783.92 8987.32 148.84 o 5 2 7 1035.16 983.01 15.11 o 7 2 7 717.25 784.89 11.05 o 9 2 7 438.73 432.78 7.29 o -10 3 7 130.18 170.55 4.67 o -8 3 7 871.27 882.34 12.10 o -6 3 7 322.84 382.09 5.70 o -4 3 7 1127.53 1004.65 11.37 o -2 3 7 3837.23 3745.90 65.39 o 0 3 7 828.15 815.52 15.26 o 2 3 7 12747.35 12043.47 256.54 o 4 3 7 531.81 499.97 7.54 o 6 3 7 1105.08 1178.39 16.01 o 8 3 7 288.66 277.59 6.19 o -7 4 7 1987.06 1834.68 43.90 o -5 4 7 2.79 13.30 2.00 o -3 4 7 0.18 18.52 2.05 o -1 4 7 68.81 72.15 5.51 o 1 4 7 651.49 617.76 7.72 o 3 4 7 1618.35 1506.05 17.20 o 5 4 7 19.19 32.92 2.72 o 7 4 7 524.23 552.70 12.57 o -6 5 7 18.16 27.46 3.00 o -4 5 7 25.14 48.60 3.87 o -2 5 7 1548.84 1501.68 19.70 o 0 5 7 388.80 429.47 6.96 o 2 5 7 950.46 899.06 12.47 o 4 5 7 795.20 768.81 14.36 o -12 0 8 21.19 28.56 4.56 o -10 0 8 306.01 285.92 13.52 o -8 0 8 2724.07 2799.98 54.83 o -6 0 8 165.93 202.38 10.19 o -4 0 8 421.00 578.63 12.99 o -2 0 8 14904.92 15169.84 345.57 o 0 0 8 43795.95 40533.55 1374.83 o 2 0 8 1446.43 1369.19 29.19 o 4 0 8 9176.93 8723.96 252.86 o 6 0 8 5187.05 5003.54 146.21 o 8 0 8 38.58 54.26 4.21 o 10 0 8 371.97 325.33 14.18 o -11 1 8 422.38 441.69 9.39 o -9 1 8 927.73 881.22 12.14 o -7 1 8 6457.39 6337.17 81.55 o -5 1 8 76.94 116.16 5.81 o -3 1 8 237.62 272.49 5.78 o -1 1 8 16.05 7.16 1.01 o 1 1 8 146.67 164.71 4.10 o 3 1 8 1469.46 1411.40 21.39 o 5 1 8 1041.21 1087.30 19.40 o 7 1 8 1526.61 1471.27 19.31 o 9 1 8 616.80 580.03 15.10 o -10 2 8 11.09 10.83 2.31 o -8 2 8 102.12 118.51 3.24 o -6 2 8 402.23 382.74 6.17 o -4 2 8 1239.95 1290.01 19.81 o -2 2 8 9.87 12.92 1.55 o 0 2 8 3667.02 3514.20 76.21 o 2 2 8 42.65 95.97 7.19 o 4 2 8 1416.86 1460.93 23.43 o 6 2 8 43.77 20.49 2.07 o 8 2 8 239.78 235.59 4.95 o -9 3 8 11.44 21.64 2.46 o -7 3 8 173.24 187.17 3.86 o -5 3 8 1180.30 1210.17 13.59 o -3 3 8 95.57 104.59 2.57 o -1 3 8 11.06 26.64 5.27 o 1 3 8 956.62 996.60 38.12 o 3 3 8 521.15 466.14 6.51 o 5 3 8 16.35 19.79 2.20 o 7 3 8 0.17 2.85 2.60 o -8 4 8 162.26 151.66 6.49 o -6 4 8 22.10 38.18 4.41 o -4 4 8 9.70 31.41 2.65 o -2 4 8 596.21 580.09 7.69 o 0 4 8 794.80 784.20 9.08 o 2 4 8 434.87 429.47 6.04 o 4 4 8 29.43 37.77 3.02 o 6 4 8 727.07 783.26 17.74 o -5 5 8 67.09 102.20 4.73 o -3 5 8 890.54 832.12 11.77 o -1 5 8 425.91 427.24 6.95 o 1 5 8 49.24 51.75 2.70 o 3 5 8 45.79 74.91 11.29 o -12 1 9 67.61 80.88 9.23 o -10 1 9 222.66 237.40 4.85 o -8 1 9 170.80 186.09 3.92 o -6 1 9 95.31 85.73 3.00 o -4 1 9 3747.49 3963.79 59.11 o -2 1 9 103.17 108.62 2.40 o 0 1 9 17.09 18.91 1.34 o 2 1 9 4934.89 5281.83 78.52 o 4 1 9 1891.03 1776.07 30.86 o 6 1 9 554.09 598.07 9.85 o 8 1 9 81.57 87.33 3.94 o 10 1 9 14.81 16.70 2.96 o -11 2 9 194.36 245.37 8.39 o -9 2 9 755.81 758.46 10.84 o -7 2 9 140.15 162.54 4.65 o -5 2 9 63.17 95.76 3.09 o -3 2 9 2254.51 2142.10 32.29 o -1 2 9 873.37 827.16 15.10 o 1 2 9 2061.09 2028.30 39.20 o 3 2 9 581.92 438.79 7.40 o 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