#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/56/2205628.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205628_Fobs loop_ _publ_author_name 'Nie, Qiang' 'Wang, Jing-Kang' 'Wang, Shi' 'Zhang, Mei-Jing' _publ_section_title ; 16\a,17-Epoxy-11\a-(p-tolylsulfonyloxy)pregn-4-ene-3,20-dione ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o912 _journal_page_last o913 _journal_volume 61 _journal_year 2005 _space_group_IT_number 5 _symmetry_space_group_name_Hall 'C 2y' _symmetry_space_group_name_H-M 'C 1 2 1' _cell_angle_alpha 90.000 _cell_angle_beta 108.666 _cell_angle_gamma 90.000 _cell_length_a 19.5080 _cell_length_b 10.7314 _cell_length_c 25.9196 _exptl_crystal_F_000 2128.00 _reflns_d_resolution_high 0.7565 _[local]_cod_data_source_file ww6358Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 41215A in C2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 540.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 10 -12 0 125.07 152.85 79.37 o 7 -11 0 302.22 206.55 59.35 o 9 -11 0 93.42 77.96 59.35 o 11 -11 0 42.55 81.25 69.71 o 6 -10 0 165.85 172.40 52.99 o 8 -10 0 74.40 11.30 52.76 o 10 -10 0 32.72 61.71 57.70 o 12 -10 0 318.25 275.08 63.12 o 5 -9 0 237.88 150.50 42.16 o 7 -9 0 690.06 629.39 44.29 o 9 -9 0 316.02 305.99 38.30 o 11 -9 0 29.12 29.20 50.87 o 13 -9 0 56.42 113.75 52.28 o 4 -8 0 1458.10 1413.33 64.27 o 6 -8 0 11.04 10.21 24.27 o 8 -8 0 161.67 240.86 29.95 o 10 -8 0 21.98 71.32 29.39 o 12 -8 0 463.03 540.66 39.92 o 14 -8 0 174.76 277.91 51.58 o 3 -7 0 486.46 502.18 30.54 o 5 -7 0 402.31 411.02 29.12 o 7 -7 0 303.87 295.10 31.68 o 9 -7 0 71.08 75.82 31.09 o 11 -7 0 922.01 908.32 49.03 o 13 -7 0 809.93 936.27 69.95 o 15 -7 0 72.54 142.94 44.51 o 2 -6 0 677.96 683.23 48.05 o 4 -6 0 409.01 381.08 24.96 o 6 -6 0 1620.49 1570.12 64.42 o 8 -6 0 384.85 378.66 27.20 o 10 -6 0 39.13 33.60 22.98 o 12 -6 0 1193.60 1223.84 118.11 o 14 -6 0 1781.85 1684.55 73.88 o 16 -6 0 418.81 438.56 41.78 o 1 -5 0 4164.98 3926.30 193.83 o 3 -5 0 2520.33 2723.29 98.45 o 5 -5 0 2077.79 2107.47 90.79 o 7 -5 0 180.60 220.78 20.37 o 9 -5 0 223.75 199.97 22.73 o 11 -5 0 836.88 719.16 40.96 o 13 -5 0 2353.01 2476.39 96.26 o 15 -5 0 170.98 235.96 34.09 o 17 -5 0 70.36 139.83 39.57 o 19 -5 0 78.04 247.76 67.36 o 2 -4 0 2051.72 1997.88 72.98 o 4 -4 0 5537.51 5397.00 187.09 o 6 -4 0 153.75 119.47 21.67 o 8 -4 0 755.36 830.40 38.62 o 10 -4 0 519.87 551.21 30.20 o 12 -4 0 356.20 279.69 53.11 o 14 -4 0 756.83 820.57 46.27 o 16 -4 0 1195.01 1239.20 60.27 o 18 -4 0 22.66 90.71 38.79 o 20 -4 0 38.34 87.14 68.54 o 22 -4 0 52.96 115.17 81.49 o 1 -3 0 11078.53 10526.24 361.91 o 3 -3 0 805.62 895.75 34.19 o 5 -3 0 244.65 263.14 16.56 o 7 -3 0 5575.84 6118.49 208.04 o 9 -3 0 2229.15 2283.38 84.59 o 11 -3 0 4032.23 3950.59 141.19 o 13 -3 0 1095.84 1045.89 51.20 o 15 -3 0 641.75 612.82 105.04 o 17 -3 0 286.29 293.16 38.58 o 19 -3 0 61.83 74.28 39.38 o 21 -3 0 77.68 110.69 74.66 o 23 -3 0 93.19 44.04 87.61 o 0 -2 0 99898.25 91744.92 4140.15 o 2 -2 0 11433.34 11412.86 385.32 o 4 -2 0 50254.41 46265.04 1578.71 o 6 -2 0 2800.91 2678.52 94.79 o 8 -2 0 2721.04 2655.90 96.64 o 10 -2 0 1659.42 1682.49 65.94 o 12 -2 0 1236.77 1230.57 54.05 o 14 -2 0 1255.51 1300.73 59.51 o 16 -2 0 345.44 371.99 35.82 o 18 -2 0 334.28 231.87 40.05 o 20 -2 0 122.53 111.59 67.83 o 22 -2 0 20.10 29.68 77.49 o 24 -2 0 29.89 -22.37 91.38 o 1 -1 0 4342.79 4264.44 140.65 o 3 -1 0 18232.02 17689.89 600.79 o 5 -1 0 13051.79 13267.97 450.18 o 7 -1 0 1981.26 2030.86 115.64 o 9 -1 0 762.73 792.75 54.40 o 11 -1 0 4327.75 4412.65 235.52 o 13 -1 0 217.48 179.70 45.69 o 15 -1 0 5.27 57.70 49.93 o 17 -1 0 423.31 362.35 51.81 o 19 -1 0 19.90 15.52 45.81 o 21 -1 0 143.83 105.87 45.69 o 23 -1 0 0.18 14.84 85.96 o 2 0 0 27043.46 26955.15 1362.23 o 4 0 0 20291.46 19944.28 1008.95 o 6 0 0 696.32 761.19 47.57 o 8 0 0 2259.06 2267.56 124.59 o 10 0 0 14163.15 13576.84 694.54 o 12 0 0 242.58 203.49 36.98 o 14 0 0 755.64 708.43 65.47 o 16 0 0 599.16 619.65 69.71 o 18 0 0 286.36 352.33 69.01 o 20 0 0 176.21 130.71 72.77 o 22 0 0 0.69 -6.45 44.73 o 24 0 0 203.28 63.83 97.03 o 1 1 0 4181.38 4046.31 126.65 o 3 1 0 18153.90 18100.44 583.63 o 5 1 0 13060.85 13472.66 436.80 o 7 1 0 1990.71 2160.98 86.67 o 9 1 0 759.60 762.66 30.70 o 11 1 0 4339.33 4362.72 234.34 o 13 1 0 222.47 222.80 37.92 o 15 1 0 4.75 -0.94 38.62 o 17 1 0 428.62 391.90 59.11 o 19 1 0 21.98 -4.47 60.76 o 21 1 0 144.56 60.06 77.01 o 23 1 0 0.20 -48.05 87.38 o 0 2 0 99762.36 93310.40 3937.37 o 2 2 0 11459.59 11475.10 346.73 o 4 2 0 50281.86 47827.73 1218.77 o 6 2 0 2833.10 2699.88 72.25 o 8 2 0 2699.40 2702.12 72.67 o 10 2 0 1652.42 1691.47 61.34 o 12 2 0 1262.88 1277.44 81.72 o 14 2 0 1268.43 1369.06 90.20 o 16 2 0 332.75 238.81 50.17 o 18 2 0 333.43 382.72 62.65 o 20 2 0 116.72 33.21 67.83 o 22 2 0 18.81 29.68 75.37 o 24 2 0 30.76 -96.56 96.56 o 1 3 0 11159.24 10983.72 325.99 o 3 3 0 846.29 835.21 31.23 o 5 3 0 243.03 234.61 12.11 o 7 3 0 5545.34 6047.90 159.98 o 9 3 0 2240.84 2307.94 87.18 o 11 3 0 4071.72 3982.50 135.57 o 13 3 0 1118.55 1190.54 77.72 o 15 3 0 645.74 548.28 59.82 o 17 3 0 295.15 211.97 52.76 o 19 3 0 63.51 -45.45 57.00 o 21 3 0 78.29 152.61 74.19 o 23 3 0 90.43 -77.25 83.37 o 0 4 0 161.66 176.64 19.55 o 2 4 0 2116.56 2069.02 82.08 o 4 4 0 5586.03 5490.19 145.07 o 6 4 0 140.26 135.18 19.09 o 8 4 0 776.27 912.68 39.12 o 10 4 0 485.90 467.33 21.30 o 12 4 0 348.54 264.01 38.39 o 14 4 0 755.01 761.90 67.12 o 16 4 0 1178.29 1095.15 89.73 o 18 4 0 22.04 -15.54 51.58 o 20 4 0 38.58 -50.64 68.30 o 22 4 0 50.84 28.97 86.20 o 1 5 0 4176.09 4248.73 130.90 o 3 5 0 2440.12 2774.89 95.27 o 5 5 0 2077.77 2149.57 61.78 o 7 5 0 196.13 255.10 16.60 o 9 5 0 214.68 183.25 24.82 o 11 5 0 855.11 895.73 65.94 o 13 5 0 2354.51 2484.94 146.49 o 15 5 0 174.33 222.56 47.10 o 17 5 0 69.05 26.85 52.05 o 19 5 0 79.79 -1.88 60.06 o 21 5 0 1.98 -32.27 73.48 o 0 6 0 2164.05 2164.17 104.33 o 2 6 0 696.60 767.27 33.64 o 4 6 0 399.15 353.36 23.81 o 6 6 0 1665.49 1647.42 50.47 o 8 6 0 370.52 340.76 21.27 o 10 6 0 36.39 36.47 17.63 o 12 6 0 1154.75 1119.60 54.14 o 14 6 0 1744.71 1715.98 113.52 o 16 6 0 421.28 375.89 61.23 o 18 6 0 190.13 209.37 68.06 o 20 6 0 34.86 29.20 76.07 o 22 6 0 20.79 -15.78 92.56 o 1 7 0 21.21 76.88 18.64 o 3 7 0 442.77 420.70 27.71 o 5 7 0 398.61 375.41 36.86 o 7 7 0 328.24 284.58 21.72 o 9 7 0 71.00 70.71 19.00 o 11 7 0 942.27 1002.55 50.41 o 13 7 0 815.17 913.33 78.43 o 15 7 0 72.70 7.07 53.70 o 17 7 0 246.78 177.58 67.59 o 19 7 0 2.30 -38.39 65.71 o 21 7 0 0.59 -73.25 78.90 o 0 8 0 191.20 133.07 31.56 o 2 8 0 2808.31 2620.83 130.48 o 4 8 0 1494.11 1569.48 107.51 o 6 8 0 13.64 -1.27 17.72 o 8 8 0 166.72 199.42 30.30 o 10 8 0 22.92 1.75 21.72 o 12 8 0 453.84 308.49 37.64 o 14 8 0 169.06 106.22 53.23 o 16 8 0 61.24 16.72 57.94 o 18 8 0 8.35 -15.78 65.24 o 20 8 0 12.60 -56.76 79.13 o 1 9 0 564.76 571.04 36.54 o 3 9 0 572.14 428.98 53.93 o 5 9 0 235.43 222.59 24.70 o 7 9 0 705.41 679.50 34.43 o 9 9 0 312.72 291.17 29.46 o 11 9 0 28.29 9.30 33.72 o 13 9 0 64.75 16.72 55.82 o 15 9 0 98.72 183.47 68.06 o 17 9 0 49.33 47.81 74.19 o 0 10 0 682.61 672.64 64.06 o 2 10 0 77.36 62.68 40.74 o 4 10 0 485.79 575.08 82.90 o 6 10 0 162.18 156.45 26.69 o 8 10 0 73.72 29.15 26.11 o 10 10 0 34.51 60.33 35.76 o 12 10 0 322.30 314.22 46.21 o 14 10 0 236.30 252.71 68.54 o 16 10 0 28.93 0.24 67.59 o 1 11 0 365.04 405.43 50.87 o 3 11 0 258.51 336.72 40.86 o 5 11 0 41.79 55.84 29.73 o 7 11 0 312.62 365.30 35.14 o 9 11 0 94.46 75.06 31.67 o 11 11 0 40.87 14.71 40.05 o 13 11 0 187.85 101.04 66.18 o 15 11 0 33.60 2.83 71.36 o 0 12 0 334.53 446.07 64.30 o 2 12 0 20.81 5.55 39.55 o 4 12 0 28.50 42.90 31.34 o 6 12 0 8.66 20.71 32.29 o 8 12 0 64.48 73.94 35.34 o 10 12 0 127.56 137.81 45.71 o 12 12 0 12.10 -10.60 49.16 o 1 13 0 255.58 364.27 71.83 o 3 13 0 228.29 266.55 52.95 o 5 13 0 8.68 0.78 45.63 o 7 13 0 285.47 250.76 42.21 o 9 13 0 211.36 241.03 56.70 o 0 14 0 388.11 480.93 84.79 o 2 14 0 35.12 67.99 53.21 o 8 -12 1 59.37 71.13 73.25 o 10 -12 1 123.89 119.88 73.72 o -11 -11 1 179.81 280.97 74.42 o -9 -11 1 122.42 170.99 66.42 o 7 -11 1 153.39 236.46 65.94 o 9 -11 1 52.19 92.79 60.76 o 11 -11 1 125.90 166.98 73.01 o -12 -10 1 141.04 261.42 60.29 o -10 -10 1 226.64 291.33 57.47 o -8 -10 1 524.39 450.54 63.59 o -6 -10 1 173.57 131.89 52.28 o 6 -10 1 265.01 216.44 51.58 o 8 -10 1 299.37 296.04 60.29 o 10 -10 1 589.81 764.25 76.07 o 12 -10 1 3.71 12.48 61.71 o 14 -10 1 11.95 26.85 62.88 o -13 -9 1 159.39 230.34 59.11 o -11 -9 1 825.85 871.67 101.04 o -9 -9 1 378.18 368.61 38.38 o -7 -9 1 76.70 50.63 31.04 o -5 -9 1 920.38 950.76 60.88 o 5 -9 1 369.80 389.07 49.93 o 7 -9 1 957.69 967.40 50.69 o 9 -9 1 336.74 423.69 53.46 o 11 -9 1 579.54 641.31 68.30 o 13 -9 1 100.30 124.82 58.64 o 15 -9 1 137.69 293.45 69.95 o -14 -8 1 130.86 113.44 69.95 o -12 -8 1 95.01 116.30 32.37 o -10 -8 1 1240.06 1423.30 144.25 o -8 -8 1 503.30 449.09 35.52 o -6 -8 1 375.57 385.75 33.22 o -4 -8 1 457.19 582.37 36.14 o 2 -8 1 1455.57 1431.71 82.67 o 4 -8 1 3791.46 3568.32 183.94 o 6 -8 1 4254.47 4307.75 154.64 o 8 -8 1 305.39 270.83 31.44 o 10 -8 1 258.43 290.33 37.45 o 12 -8 1 212.74 290.39 52.76 o 14 -8 1 60.37 93.97 53.46 o 16 -8 1 585.50 790.16 78.43 o -15 -7 1 23.91 62.34 34.47 o -13 -7 1 156.03 124.83 32.05 o -11 -7 1 612.50 769.83 96.09 o -9 -7 1 195.96 161.01 26.92 o -7 -7 1 371.66 326.76 27.96 o -5 -7 1 628.68 546.24 33.65 o -3 -7 1 669.09 694.82 110.69 o 3 -7 1 382.64 395.90 42.86 o 5 -7 1 938.16 1016.15 47.07 o 7 -7 1 467.45 513.76 72.54 o 9 -7 1 34.68 16.99 22.96 o 11 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6905.59 319.13 o 3 -5 1 20121.74 19638.03 676.14 o 5 -5 1 539.64 513.18 35.45 o 7 -5 1 1363.90 1372.56 53.80 o 9 -5 1 776.34 787.33 37.42 o 11 -5 1 1742.82 1756.63 71.95 o 13 -5 1 514.50 549.21 38.34 o 15 -5 1 451.79 476.68 38.88 o 17 -5 1 176.79 206.01 41.22 o 19 -5 1 41.26 49.93 59.82 o -22 -4 1 22.85 15.78 76.54 o -20 -4 1 184.99 198.54 69.01 o -18 -4 1 148.36 162.50 38.18 o -16 -4 1 189.68 179.39 36.62 o -14 -4 1 1843.19 1928.51 79.25 o -12 -4 1 1139.47 1181.56 52.21 o -10 -4 1 4884.92 4796.09 170.70 o -8 -4 1 664.03 801.30 35.35 o -6 -4 1 7203.96 7178.42 236.65 o -4 -4 1 3084.22 3259.42 112.76 o -2 -4 1 4362.20 4486.10 166.39 o 0 -4 1 2312.49 2242.36 113.05 o 2 -4 1 8537.95 8444.74 284.18 o 4 -4 1 4269.22 4843.59 163.63 o 6 -4 1 16092.58 17138.33 568.55 o 8 -4 1 2948.88 3107.24 108.28 o 10 -4 1 2082.57 1879.15 75.36 o 12 -4 1 673.12 758.67 92.20 o 14 -4 1 622.87 661.81 76.43 o 16 -4 1 511.55 556.96 42.62 o 18 -4 1 20.92 19.82 45.93 o 20 -4 1 75.60 100.50 46.55 o -23 -3 1 28.37 70.66 84.55 o -21 -3 1 13.43 104.57 72.77 o -19 -3 1 32.70 3.88 35.42 o -17 -3 1 66.69 126.77 34.51 o -15 -3 1 148.03 121.18 30.56 o -13 -3 1 6.20 -23.36 23.36 o -11 -3 1 19.34 42.10 19.07 o -9 -3 1 1679.76 1718.47 66.36 o -7 -3 1 17010.10 17438.79 583.39 o -5 -3 1 2193.76 2228.66 77.25 o -3 -3 1 33255.20 31838.66 1062.46 o -1 -3 1 28378.09 27592.14 1071.96 o 1 -3 1 18485.01 17896.00 607.25 o 3 -3 1 29939.65 29310.31 990.73 o 5 -3 1 5057.02 5327.66 181.22 o 7 -3 1 12218.97 12573.55 425.45 o 9 -3 1 171.22 171.14 45.69 o 11 -3 1 1728.61 1810.41 69.20 o 13 -3 1 345.33 386.96 71.01 o 15 -3 1 646.02 678.65 92.32 o 17 -3 1 339.50 239.94 46.63 o 19 -3 1 135.75 27.57 38.39 o 21 -3 1 14.47 17.15 50.28 o 23 -3 1 40.00 147.90 89.73 o -24 -2 1 53.48 -28.73 89.97 o -22 -2 1 177.24 86.20 72.54 o -20 -2 1 236.02 195.99 43.15 o -18 -2 1 174.42 196.67 35.93 o -16 -2 1 253.22 207.82 40.74 o -14 -2 1 806.70 818.36 44.37 o -12 -2 1 19.80 37.57 33.56 o -10 -2 1 1688.54 1679.54 71.01 o -8 -2 1 14066.63 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