#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:10:58 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180976 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/56/2205654.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205654_Fobs loop_ _publ_author_name 'B\"uy\"ukg\"ung\"or, Orhan' 'Ko\,sar, Ba\,sak' 'Demircan, Ayd\?in' 'Tura\,c, Ersen' _publ_section_title ; 6-Bromo-8-thia-1,4-epoxybicyclo[4.3.0]non-2-ene ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1441 _journal_page_last o1442 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 81.030 _cell_angle_beta 88.572 _cell_angle_gamma 81.179 _cell_length_a 6.6508 _cell_length_b 7.9576 _cell_length_c 8.4012 _exptl_crystal_F_000 232.00 _reflns_d_resolution_high 0.8107 _cod_data_source_file bt66502asup2.hkl _cod_data_source_block 2a #BEGIN Tags that were not found in dictionaries: _shelx_title ' TEST STRUCTURE D:\DATA\ORHAYDEM1T_2DENE\ORHAYDEM1T' _shelx_refln_list_code 4 _shelx_f_calc_maximum 84.05 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 227.37 227.90 8.80 o 2 0 0 2709.05 2678.65 141.84 o 3 0 0 1241.80 1178.12 63.71 o 4 0 0 583.42 556.71 31.89 o 5 0 0 585.40 547.31 41.53 o 6 0 0 0.23 5.83 4.11 o 7 0 0 79.51 79.30 4.06 o 8 0 0 4.40 1.68 4.46 o -7 1 0 26.59 25.24 4.28 o -6 1 0 18.89 18.10 5.81 o -5 1 0 582.82 569.98 35.93 o -4 1 0 77.74 79.85 7.03 o -3 1 0 525.08 515.16 29.11 o -2 1 0 1378.78 1333.03 76.82 o -1 1 0 3902.69 4179.21 131.06 o 0 1 0 1421.48 1516.30 40.62 o 1 1 0 866.38 895.32 11.35 o 2 1 0 674.27 592.39 43.38 o 3 1 0 2012.11 1926.01 107.52 o 4 1 0 80.56 76.09 6.15 o 5 1 0 164.00 171.10 16.68 o 6 1 0 1.98 10.55 3.78 o 7 1 0 62.90 53.85 7.34 o 8 1 0 9.24 14.33 3.72 o -7 2 0 7.97 12.78 4.20 o -6 2 0 23.60 24.76 4.30 o -5 2 0 40.82 39.75 4.44 o -4 2 0 179.87 182.08 10.15 o -3 2 0 86.50 76.48 5.64 o -2 2 0 2084.70 2118.19 116.71 o -1 2 0 300.82 359.01 19.56 o 0 2 0 137.11 149.52 7.23 o 1 2 0 2741.11 2641.25 26.06 o 2 2 0 2679.45 2555.27 104.52 o 3 2 0 769.58 692.01 49.20 o 4 2 0 4.07 7.07 3.49 o 5 2 0 176.08 173.77 13.33 o 6 2 0 73.16 75.07 4.58 o 7 2 0 2.62 5.57 3.43 o 8 2 0 17.81 20.32 6.12 o -7 3 0 45.46 51.52 7.98 o -6 3 0 55.16 57.34 5.69 o -5 3 0 19.17 27.72 4.89 o -4 3 0 220.09 238.80 14.39 o -3 3 0 0.64 5.55 5.11 o -2 3 0 452.95 465.81 26.13 o -1 3 0 1645.80 1771.34 18.15 o 0 3 0 371.46 437.40 16.67 o 1 3 0 3045.59 3027.47 54.10 o 2 3 0 185.72 172.04 5.26 o 3 3 0 204.04 159.33 15.78 o 4 3 0 575.59 565.92 44.17 o 5 3 0 373.95 364.03 25.95 o 6 3 0 209.31 214.18 20.30 o 7 3 0 1.78 -7.19 3.59 o 8 3 0 39.95 36.01 6.41 o -6 4 0 16.87 25.88 4.54 o -5 4 0 2.82 3.78 4.69 o -4 4 0 593.53 605.67 71.61 o -3 4 0 272.25 270.43 13.12 o -2 4 0 1278.98 1348.15 56.63 o -1 4 0 1956.64 2060.44 38.90 o 0 4 0 1974.50 2166.80 57.20 o 1 4 0 3269.60 3174.00 63.33 o 2 4 0 120.99 112.80 4.21 o 3 4 0 2471.63 2357.39 182.44 o 4 4 0 233.73 245.51 27.48 o 5 4 0 245.26 248.19 37.31 o 6 4 0 110.66 110.54 5.83 o 7 4 0 3.03 5.97 3.69 o -6 5 0 18.25 42.12 12.21 o -5 5 0 23.66 36.55 11.52 o -4 5 0 240.97 240.78 16.57 o -3 5 0 1.99 11.41 5.18 o -2 5 0 550.72 596.71 29.03 o -1 5 0 87.47 79.99 8.76 o 0 5 0 215.44 221.80 13.05 o 1 5 0 497.84 486.11 13.67 o 2 5 0 15.76 18.69 3.39 o 3 5 0 838.42 835.99 21.44 o 4 5 0 126.51 139.31 8.94 o 5 5 0 5.73 4.72 3.57 o 6 5 0 129.62 136.30 13.66 o 7 5 0 0.11 -2.69 3.31 o -5 6 0 2.56 -11.57 6.00 o -4 6 0 8.10 9.47 5.30 o -3 6 0 93.48 91.23 5.42 o -2 6 0 16.07 18.09 4.75 o -1 6 0 398.46 387.84 20.96 o 0 6 0 75.65 79.65 4.40 o 1 6 0 667.45 658.44 22.99 o 2 6 0 105.51 94.51 4.37 o 3 6 0 107.15 112.35 5.26 o 4 6 0 229.58 214.94 29.13 o 5 6 0 0.02 0.71 4.14 o 6 6 0 83.63 94.98 12.30 o 7 6 0 13.31 19.41 4.69 o -4 7 0 20.36 18.82 5.13 o -3 7 0 110.53 109.63 7.28 o -2 7 0 2.88 5.07 4.42 o -1 7 0 267.55 271.95 13.16 o 0 7 0 100.58 109.78 10.38 o 1 7 0 168.12 155.75 5.54 o 2 7 0 257.92 254.22 5.94 o 3 7 0 2.25 12.97 3.66 o 4 7 0 368.00 373.23 15.22 o 5 7 0 6.78 10.10 4.11 o 6 7 0 62.64 76.21 13.89 o -3 8 0 90.18 94.68 5.00 o -2 8 0 3.88 1.54 4.44 o -1 8 0 318.90 313.77 9.57 o 0 8 0 123.02 111.51 4.80 o 1 8 0 148.82 160.48 4.43 o 2 8 0 457.22 473.83 14.16 o 3 8 0 9.66 16.95 6.18 o 4 8 0 199.02 215.89 10.74 o 5 8 0 6.41 10.09 3.52 o -1 9 0 57.66 61.15 4.33 o 0 9 0 19.11 10.75 4.58 o 1 9 0 39.91 46.28 4.22 o 2 9 0 160.62 155.43 21.07 o 3 9 0 0.69 2.33 3.72 o 4 9 0 43.11 49.32 4.37 o -3 -9 1 85.13 80.16 4.07 o -2 -9 1 1.55 1.09 3.77 o -1 -9 1 141.86 117.31 5.12 o 0 -9 1 14.98 26.62 4.32 o 1 -9 1 46.37 34.63 4.35 o -5 -8 1 6.98 10.35 5.56 o -4 -8 1 14.92 15.49 3.58 o -3 -8 1 215.94 222.28 15.86 o -2 -8 1 18.08 22.46 3.91 o -1 -8 1 208.05 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21.33 4.89 o 2 -5 1 148.95 142.60 10.76 o 3 -5 1 159.12 160.47 13.60 o 4 -5 1 0.84 -1.49 6.37 o 5 -5 1 15.36 6.23 6.06 o 6 -5 1 3.70 12.56 5.85 o -7 -4 1 28.51 26.79 3.77 o -6 -4 1 7.26 14.70 3.86 o -5 -4 1 51.61 44.82 6.59 o -4 -4 1 160.54 161.04 8.91 o -3 -4 1 735.74 736.78 65.33 o -2 -4 1 1102.99 1053.27 27.39 o -1 -4 1 162.32 164.63 8.31 o 0 -4 1 645.42 630.55 22.45 o 1 -4 1 857.88 898.29 29.38 o 2 -4 1 384.80 413.25 24.32 o 3 -4 1 496.01 473.58 31.60 o 4 -4 1 11.15 26.43 8.84 o 5 -4 1 53.28 67.76 18.35 o 6 -4 1 22.74 25.52 5.36 o -8 -3 1 2.60 7.23 5.00 o -7 -3 1 74.54 84.36 5.78 o -6 -3 1 117.18 117.98 9.53 o -5 -3 1 88.70 89.16 8.85 o -4 -3 1 499.65 459.22 47.88 o -3 -3 1 143.76 142.78 10.70 o -2 -3 1 657.38 592.21 35.55 o -1 -3 1 755.18 708.97 31.39 o 0 -3 1 3374.47 3488.87 186.07 o 1 -3 1 1870.67 1876.24 62.31 o 2 -3 1 37.73 40.04 6.33 o 3 -3 1 612.01 634.52 90.52 o 4 -3 1 60.10 55.34 6.98 o 5 -3 1 258.68 279.37 62.11 o 6 -3 1 142.16 152.18 26.05 o 7 -3 1 7.51 9.58 12.23 o -8 -2 1 0.01 1.75 4.62 o -7 -2 1 58.73 70.25 6.88 o -6 -2 1 86.24 94.08 8.45 o -5 -2 1 264.03 266.80 22.66 o -4 -2 1 1218.83 1131.90 86.27 o -3 -2 1 375.69 396.82 34.03 o -2 -2 1 4244.77 3817.99 318.82 o -1 -2 1 308.60 306.63 15.15 o 0 -2 1 6816.37 6808.07 423.76 o 1 -2 1 2694.14 2673.42 90.44 o 2 -2 1 586.91 585.94 51.62 o 3 -2 1 2293.68 2342.40 114.98 o 4 -2 1 0.85 10.63 5.40 o 5 -2 1 442.34 453.60 25.68 o 6 -2 1 6.40 6.99 4.58 o 7 -2 1 35.09 42.15 4.37 o -8 -1 1 0.88 -4.31 4.29 o -7 -1 1 32.98 46.72 4.76 o -6 -1 1 117.50 114.61 12.51 o -5 -1 1 228.42 222.95 26.24 o -4 -1 1 1030.18 960.24 73.91 o -3 -1 1 86.80 83.24 8.13 o -2 -1 1 3829.97 3459.59 245.40 o -1 -1 1 15.31 17.47 6.74 o 0 -1 1 336.23 321.32 25.28 o 1 -1 1 161.48 174.77 11.01 o 2 -1 1 189.39 195.95 14.31 o 3 -1 1 302.90 289.20 19.47 o 4 -1 1 45.13 43.47 4.61 o 5 -1 1 12.01 15.63 4.33 o 6 -1 1 13.60 13.29 4.22 o 7 -1 1 0.06 5.21 5.50 o -8 0 1 1.12 -0.64 6.62 o -7 0 1 44.28 35.97 4.60 o -6 0 1 55.23 56.21 7.09 o -5 0 1 0.53 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94.07 8.16 o 6 7 1 9.88 16.33 3.78 o -3 8 1 4.23 3.61 4.30 o -2 8 1 105.01 101.28 8.96 o -1 8 1 30.63 27.10 3.92 o 0 8 1 264.56 265.32 8.68 o 1 8 1 239.58 207.11 7.95 o 2 8 1 3.79 6.33 6.04 o 3 8 1 299.57 271.74 14.71 o 4 8 1 0.00 4.89 3.62 o 5 8 1 120.42 122.68 4.48 o -2 9 1 46.46 48.63 7.55 o -1 9 1 0.29 3.12 4.11 o 0 9 1 87.32 86.44 6.51 o 1 9 1 117.84 116.68 7.02 o 2 9 1 25.47 29.85 4.04 o 3 9 1 175.21 168.70 5.11 o 4 9 1 3.95 14.40 4.77 o -2 -9 2 120.90 129.49 4.27 o -1 -9 2 0.68 1.55 5.37 o 0 -9 2 146.24 140.64 7.41 o -4 -8 2 103.00 98.10 5.89 o -3 -8 2 15.58 20.73 4.79 o -2 -8 2 267.81 276.63 14.02 o -1 -8 2 8.03 11.59 4.12 o 0 -8 2 288.34 252.11 17.52 o 1 -8 2 54.10 55.86 4.35 o 2 -8 2 21.80 12.61 4.87 o -6 -7 2 14.41 9.77 4.17 o -5 -7 2 47.02 50.00 3.59 o -4 -7 2 188.01 182.08 13.01 o -3 -7 2 66.17 60.79 4.78 o -2 -7 2 484.82 479.95 25.63 o -1 -7 2 19.46 26.95 5.39 o 0 -7 2 121.86 110.29 8.57 o 1 -7 2 69.93 73.13 4.99 o 2 -7 2 9.16 9.98 4.88 o 3 -7 2 129.07 129.40 10.26 o 4 -7 2 4.40 -7.67 5.94 o -6 -6 2 57.00 72.06 15.12 o -5 -6 2 4.54 9.26 4.22 o -4 -6 2 63.83 73.28 6.00 o -3 -6 2 4.12 10.27 3.76 o -2 -6 2 154.00 149.95 11.72 o -1 -6 2 345.85 346.67 12.84 o 0 -6 2 25.93 32.84 6.10 o 1 -6 2 589.34 583.80 23.03 o 2 -6 2 2.49 2.42 4.88 o 3 -6 2 129.56 121.72 7.40 o 4 -6 2 21.69 22.49 5.87 o 5 -6 2 20.80 37.42 7.77 o -7 -5 2 18.84 32.22 3.59 o -6 -5 2 178.32 199.95 41.21 o -5 -5 2 11.96 7.44 4.37 o -4 -5 2 572.45 559.82 74.67 o -3 -5 2 733.50 708.33 36.05 o -2 -5 2 450.01 424.14 23.57 o -1 -5 2 950.31 896.44 45.90 o 0 -5 2 110.77 116.61 5.35 o 1 -5 2 983.17 966.07 38.57 o 2 -5 2 60.51 65.58 6.21 o 3 -5 2 84.19 83.05 7.08 o 4 -5 2 138.93 140.27 15.00 o 5 -5 2 30.42 39.32 5.71 o -7 -4 2 18.49 31.09 9.09 o -6 -4 2 130.39 134.05 11.08 o -5 -4 2 5.65 8.75 13.53 o -4 -4 2 1075.33 1015.41 128.15 o -3 -4 2 403.47 415.90 33.42 o -2 -4 2 781.15 744.29 29.22 o -1 -4 2 1701.57 1592.59 70.50 o 0 -4 2 4.49 -0.18 4.29 o 1 -4 2 1340.70 1309.86 50.61 o 2 -4 2 193.95 200.86 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