#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:11:14 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180977 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/57/2205728.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205728_Fobs loop_ _publ_author_name 'Tian, Li' 'Wang, Da-Xiang' _publ_section_title ; 6-Cyano-3,3-dimethyl-5-methylsulfanyl-1,3-dihydro-2-oxo-1-thia-3b,4,8-triazaindacene 1,1-dioxide ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1286 _journal_page_last o1287 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 98.316 _cell_angle_beta 98.953 _cell_angle_gamma 98.420 _cell_length_a 7.1497 _cell_length_b 8.5729 _cell_length_c 11.1708 _exptl_crystal_F_000 320.00 _reflns_d_resolution_high 0.8400 _cod_data_source_file hg61513sup2.hkl _cod_data_source_block 3 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 50125A in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 144.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4.32 -0.96 0.64 o 2 0 0 20752.83 19725.36 334.89 o 3 0 0 15.66 30.44 0.98 o 4 0 0 3937.68 4794.24 73.47 o 5 0 0 55.90 65.80 1.85 o 6 0 0 210.75 251.16 4.88 o 7 0 0 81.93 100.94 2.91 o 8 0 0 38.34 47.34 3.51 o -8 1 0 3.70 3.18 1.49 o -7 1 0 214.21 203.38 4.38 o -6 1 0 9.00 8.68 1.07 o -5 1 0 310.87 295.13 5.32 o -4 1 0 11.75 10.60 0.76 o -3 1 0 134.74 163.32 2.94 o -2 1 0 1931.35 1875.98 28.82 o -1 1 0 1103.39 1110.66 17.10 o 0 1 0 5700.45 5022.45 112.90 o 1 1 0 3094.00 2969.11 45.44 o 2 1 0 9885.35 8961.57 137.32 o 3 1 0 82.56 92.96 2.00 o 4 1 0 3110.65 3065.52 47.30 o 5 1 0 258.78 257.86 6.87 o 6 1 0 435.48 420.30 7.52 o 7 1 0 15.30 15.25 1.73 o 8 1 0 91.20 77.50 3.09 o -8 2 0 4.22 3.94 1.51 o -7 2 0 22.55 18.32 1.51 o -6 2 0 0.01 0.40 0.92 o -5 2 0 0.29 -0.29 0.69 o -4 2 0 164.26 160.32 3.07 o -3 2 0 515.95 550.58 8.84 o -2 2 0 124.74 137.07 2.76 o -1 2 0 161.76 167.88 2.82 o 0 2 0 251.76 275.69 6.61 o 1 2 0 257.67 245.99 4.14 o 2 2 0 408.31 395.64 6.56 o 3 2 0 657.66 676.25 11.79 o 4 2 0 98.34 92.60 2.30 o 5 2 0 87.46 93.87 3.56 o 6 2 0 5.20 5.97 1.17 o 7 2 0 24.47 18.42 1.75 o -8 3 0 2.63 3.56 1.55 o -7 3 0 70.39 76.16 4.95 o -6 3 0 32.70 34.40 1.52 o -5 3 0 433.81 418.75 7.19 o -4 3 0 159.87 151.32 2.97 o -3 3 0 424.16 425.20 6.98 o -2 3 0 38.81 23.25 0.84 o -1 3 0 203.38 192.44 3.31 o 0 3 0 1500.65 1495.46 33.96 o 1 3 0 1211.05 1311.28 30.07 o 2 3 0 444.60 389.75 6.60 o 3 3 0 147.73 141.06 4.53 o 4 3 0 779.95 773.86 13.76 o 5 3 0 25.39 22.35 1.51 o 6 3 0 130.28 137.83 3.64 o 7 3 0 1.45 1.45 1.67 o -8 4 0 0.85 1.22 2.12 o -7 4 0 170.41 168.59 4.55 o -6 4 0 43.62 47.41 1.89 o -5 4 0 301.22 304.03 5.49 o -4 4 0 303.63 315.85 5.51 o -3 4 0 1393.20 1412.46 22.08 o -2 4 0 215.21 227.12 4.10 o -1 4 0 788.96 849.09 13.42 o 0 4 0 22.83 22.54 1.42 o 1 4 0 70.56 84.58 3.11 o 2 4 0 13.94 15.80 1.64 o 3 4 0 33.64 36.54 2.83 o 4 4 0 148.95 151.88 3.48 o 5 4 0 86.84 81.26 5.85 o 6 4 0 26.19 27.03 1.94 o 7 4 0 5.35 4.71 1.94 o -7 5 0 0.69 0.18 1.33 o -6 5 0 111.09 106.84 2.82 o -5 5 0 5.20 4.18 0.93 o -4 5 0 4.29 5.15 0.82 o -3 5 0 10.70 13.87 1.06 o -2 5 0 226.44 230.46 4.13 o -1 5 0 9.92 8.86 0.72 o 0 5 0 86.82 83.70 3.00 o 1 5 0 1.84 1.20 1.16 o 2 5 0 56.06 48.00 2.64 o 3 5 0 38.56 35.29 1.64 o 4 5 0 133.02 128.51 3.67 o 5 5 0 3.88 3.37 1.28 o 6 5 0 18.64 16.89 1.96 o -6 6 0 206.38 214.92 4.49 o -5 6 0 366.78 355.72 6.45 o -4 6 0 335.38 336.47 6.02 o -3 6 0 490.36 463.80 7.86 o -2 6 0 95.57 101.80 2.37 o -1 6 0 1186.83 1144.28 18.21 o 0 6 0 15.47 14.82 1.66 o 1 6 0 228.04 203.77 6.15 o 2 6 0 29.36 23.26 2.20 o 3 6 0 146.27 142.83 5.41 o 4 6 0 56.38 48.52 3.31 o 5 6 0 4.52 4.35 1.55 o -5 7 0 237.37 277.03 5.42 o -4 7 0 104.08 106.27 2.72 o -3 7 0 561.95 639.56 10.68 o -2 7 0 13.50 11.36 1.96 o -1 7 0 379.48 430.77 7.53 o 0 7 0 0.42 2.86 1.44 o 1 7 0 511.99 589.36 14.98 o 2 7 0 0.27 20.57 2.46 o 3 7 0 173.19 212.91 7.21 o 4 7 0 2.73 25.74 2.98 o -5 8 0 19.37 22.36 2.58 o -4 8 0 43.97 45.81 1.99 o -3 8 0 55.62 59.50 2.09 o -2 8 0 9.55 9.51 1.51 o -1 8 0 21.89 22.51 1.45 o 0 8 0 30.42 37.00 2.86 o 1 8 0 42.87 45.59 3.25 o 2 8 0 54.96 44.49 3.27 o 3 8 0 16.61 12.18 2.76 o -4 9 0 2.50 4.87 2.18 o -3 9 0 48.14 52.97 2.26 o -2 9 0 0.01 0.11 1.23 o -1 9 0 102.85 109.46 3.13 o 0 9 0 6.12 6.31 2.16 o 1 9 0 29.65 40.61 3.51 o 2 9 0 1.55 0.58 2.48 o -2 10 0 4.48 7.23 2.62 o -1 10 0 10.03 13.59 3.60 o 0 -10 1 20.79 27.02 3.15 o 1 -10 1 66.80 70.64 4.33 o 2 -10 1 50.83 53.67 3.75 o -2 -9 1 5.34 3.17 2.30 o -1 -9 1 0.01 -0.56 2.00 o 0 -9 1 6.20 4.83 2.06 o 1 -9 1 2.81 2.27 1.27 o 2 -9 1 12.65 15.53 2.38 o 3 -9 1 0.55 -0.12 1.90 o 4 -9 1 4.57 3.53 2.22 o 5 -9 1 4.74 5.63 2.44 o -4 -8 1 4.82 6.55 2.58 o -3 -8 1 0.35 1.06 2.30 o -2 -8 1 6.28 3.27 2.18 o -1 -8 1 26.00 32.21 2.72 o 0 -8 1 1.40 1.40 1.66 o 1 -8 1 3.58 4.14 0.99 o 2 -8 1 0.42 0.84 1.02 o 3 -8 1 95.87 99.12 4.15 o 4 -8 1 0.42 2.18 1.86 o 5 -8 1 41.25 45.81 3.17 o 6 -8 1 11.05 14.38 2.68 o -5 -7 1 5.30 5.45 2.82 o -4 -7 1 57.20 69.15 4.11 o -3 -7 1 0.44 0.98 1.84 o -2 -7 1 61.54 61.46 3.57 o -1 -7 1 8.01 9.30 1.94 o 0 -7 1 33.67 33.11 2.46 o 1 -7 1 34.49 31.33 1.40 o 2 -7 1 5.84 2.93 0.99 o 3 -7 1 4.14 3.84 0.94 o 4 -7 1 53.53 58.05 2.97 o 5 -7 1 12.51 15.73 2.18 o 6 -7 1 11.96 12.82 2.50 o -5 -6 1 7.58 9.21 1.63 o -4 -6 1 69.57 64.72 2.57 o -3 -6 1 1.27 1.76 1.58 o -2 -6 1 91.53 89.45 3.93 o -1 -6 1 29.69 28.47 2.08 o 0 -6 1 119.21 117.85 4.13 o 1 -6 1 1.64 2.03 0.66 o 2 -6 1 0.95 2.20 0.67 o 3 -6 1 203.47 200.66 6.55 o 4 -6 1 18.77 24.25 1.29 o 5 -6 1 142.98 145.91 3.31 o 6 -6 1 15.44 13.68 2.20 o 7 -6 1 89.47 87.64 4.35 o -6 -5 1 1.45 0.23 1.52 o -5 -5 1 93.06 94.14 3.00 o -4 -5 1 2.73 3.10 1.10 o -3 -5 1 242.61 237.29 4.74 o -2 -5 1 260.39 252.65 7.19 o -1 -5 1 43.33 35.98 2.12 o 0 -5 1 257.46 265.93 7.11 o 1 -5 1 19.66 18.65 1.01 o 2 -5 1 1098.40 1093.40 17.24 o 3 -5 1 2.34 3.27 0.69 o 4 -5 1 95.82 100.84 3.33 o 5 -5 1 22.19 24.55 1.35 o 6 -5 1 82.17 88.08 2.57 o 7 -5 1 119.35 118.61 4.79 o -7 -4 1 64.03 62.52 2.86 o -6 -4 1 1.02 2.47 1.37 o -5 -4 1 286.71 300.73 5.96 o -4 -4 1 35.61 44.13 1.82 o -3 -4 1 328.21 374.72 11.07 o -2 -4 1 24.74 31.50 1.25 o -1 -4 1 127.21 127.65 4.01 o 0 -4 1 294.74 252.01 6.53 o 1 -4 1 93.90 91.36 1.88 o 2 -4 1 1074.17 1028.07 16.14 o 3 -4 1 70.39 80.22 1.84 o 4 -4 1 875.12 836.89 17.88 o 5 -4 1 20.45 20.98 1.22 o 6 -4 1 110.95 138.29 12.77 o 7 -4 1 6.24 7.50 2.50 o 8 -4 1 0.12 8.65 2.56 o -7 -3 1 12.27 11.10 2.81 o -6 -3 1 9.90 13.12 1.55 o -5 -3 1 235.72 227.36 4.69 o -4 -3 1 93.13 96.65 2.49 o -3 -3 1 193.65 186.06 3.65 o -2 -3 1 1.27 0.57 0.53 o -1 -3 1 348.72 341.42 5.70 o 0 -3 1 3.69 7.29 0.80 o 1 -3 1 1706.16 1757.64 27.07 o 2 -3 1 158.96 194.83 3.39 o 3 -3 1 92.95 96.24 2.01 o 4 -3 1 1.87 7.14 1.18 o 5 -3 1 97.18 96.97 4.07 o 6 -3 1 1.58 0.87 0.97 o 7 -3 1 0.28 -0.56 1.18 o 8 -3 1 4.70 3.27 1.57 o -7 -2 1 0.54 0.57 1.35 o -6 -2 1 12.69 9.81 1.26 o -5 -2 1 14.71 20.40 1.57 o -4 -2 1 28.05 21.65 1.11 o -3 -2 1 141.19 149.20 2.97 o -2 -2 1 213.83 228.72 3.22 o -1 -2 1 4.18 7.27 0.59 o 0 -2 1 0.09 -0.38 0.25 o 1 -2 1 1.92 2.09 0.25 o 2 -2 1 606.57 644.01 10.14 o 3 -2 1 7.42 4.20 1.15 o 4 -2 1 129.92 129.97 2.61 o 5 -2 1 54.38 45.72 1.52 o 6 -2 1 365.50 354.73 6.44 o 7 -2 1 0.12 0.15 1.18 o 8 -2 1 49.20 50.04 2.30 o -8 -1 1 29.47 34.38 2.26 o -7 -1 1 3.82 8.02 1.78 o -6 -1 1 58.18 77.08 2.29 o -5 -1 1 76.48 70.68 1.98 o -4 -1 1 53.45 60.80 1.66 o -1 -1 1 2111.83 2228.73 36.83 o 0 -1 1 525.19 525.13 10.44 o 1 -1 1 1671.48 1751.57 58.19 o 2 -1 1 311.61 278.74 3.70 o 3 -1 1 42.86 39.68 1.13 o 4 -1 1 57.49 63.82 1.63 o 6 -1 1 100.52 110.29 3.05 o 7 -1 1 19.94 18.98 1.52 o 8 -1 1 33.02 39.07 2.48 o -8 0 1 35.25 31.39 1.97 o -7 0 1 3.52 3.95 1.17 o -6 0 1 279.41 248.15 5.83 o -5 0 1 4.14 6.01 0.93 o -4 0 1 68.57 68.55 2.61 o -3 0 1 637.09 752.88 9.75 o -2 0 1 534.42 596.02 9.39 o -1 0 1 1342.65 1295.58 19.96 o 1 0 1 1568.94 1592.38 24.45 o 2 0 1 3274.91 3274.91 52.47 o 3 0 1 20.40 23.36 0.91 o 4 0 1 435.33 484.08 36.40 o 5 0 1 99.26 102.17 4.30 o 6 0 1 195.09 172.48 5.32 o 7 0 1 32.58 30.34 2.82 o 8 0 1 22.81 18.87 2.17 o -8 1 1 9.60 9.90 1.52 o -7 1 1 4.30 2.90 1.13 o -6 1 1 95.30 92.08 2.46 o -5 1 1 50.67 50.28 1.63 o -4 1 1 3.15 1.35 0.56 o -3 1 1 2069.37 2059.03 31.71 o -2 1 1 0.22 0.61 0.27 o -1 1 1 2760.30 2660.69 40.91 o 0 1 1 1394.50 1402.89 31.55 o 1 1 1 6517.78 5841.62 89.48 o 2 1 1 1667.02 1737.30 26.84 o 3 1 1 1136.04 1120.23 17.63 o 4 1 1 1459.02 1421.34 22.37 o 5 1 1 745.63 711.99 11.79 o 6 1 1 918.92 867.56 17.14 o 7 1 1 77.19 64.95 5.02 o -8 2 1 113.05 114.98 3.28 o -7 2 1 10.00 14.61 1.37 o -6 2 1 433.68 439.53 7.66 o -5 2 1 483.54 468.33 7.91 o -4 2 1 957.66 985.27 15.58 o -3 2 1 130.93 107.41 2.11 o -2 2 1 2008.99 2033.44 31.29 o -1 2 1 3511.38 3349.34 51.23 o 0 2 1 483.16 477.06 11.16 o 1 2 1 786.70 724.48 11.48 o 2 2 1 707.69 715.00 11.45 o 3 2 1 745.11 674.92 9.06 o 4 2 1 721.92 717.84 12.53 o 5 2 1 140.92 141.19 3.23 o 6 2 1 488.03 457.72 8.35 o 7 2 1 34.36 36.48 2.09 o -8 3 1 51.70 43.11 3.09 o -7 3 1 13.93 14.23 1.50 o -6 3 1 248.49 252.15 4.83 o -5 3 1 324.32 318.94 5.66 o -4 3 1 245.49 240.68 4.30 o -3 3 1 1210.69 1297.91 20.23 o -2 3 1 2210.12 2296.41 35.36 o -1 3 1 1295.20 1327.32 20.57 o 0 3 1 176.23 181.90 4.79 o 1 3 1 39.28 33.39 1.68 o 2 3 1 478.51 490.00 8.16 o 3 3 1 99.29 103.69 2.46 o 4 3 1 53.36 61.54 3.02 o 6 3 1 11.93 13.73 1.51 o 7 3 1 0.22 1.07 1.59 o -8 4 1 0.75 0.72 1.92 o -7 4 1 1.01 2.14 1.76 o -6 4 1 50.83 50.62 1.91 o -5 4 1 17.06 13.67 1.02 o -4 4 1 11.01 7.98 0.79 o -3 4 1 17.84 16.53 0.83 o -2 4 1 23.51 28.10 1.04 o -1 4 1 31.08 26.07 1.08 o 0 4 1 330.57 359.25 8.93 o 1 4 1 244.98 223.40 6.17 o 2 4 1 61.48 67.19 2.84 o 3 4 1 91.69 84.39 2.37 o 4 4 1 13.12 11.79 1.80 o 5 4 1 66.39 62.72 2.45 o 6 4 1 33.34 34.05 2.10 o -7 5 1 1.85 1.82 1.82 o -6 5 1 226.17 223.34 4.52 o -5 5 1 71.82 81.93 3.81 o -4 5 1 248.07 236.74 4.42 o -3 5 1 59.64 54.02 1.58 o -2 5 1 820.62 779.84 12.51 o -1 5 1 772.99 734.03 11.85 o 0 5 1 86.16 84.40 3.04 o 1 5 1 675.42 637.86 15.59 o 2 5 1 6.35 6.87 1.64 o 3 5 1 464.51 436.81 11.60 o 4 5 1 6.78 7.81 2.00 o 5 5 1 70.77 75.01 2.83 o 6 5 1 5.88 4.09 1.79 o -7 6 1 0.19 1.52 2.02 o -6 6 1 9.21 12.12 1.90 o -5 6 1 50.11 68.43 2.19 o -4 6 1 19.61 21.39 1.23 o -3 6 1 52.99 60.26 1.81 o -2 6 1 0.03 1.38 0.68 o -1 6 1 285.31 298.41 5.38 o 0 6 1 18.62 21.78 1.76 o 1 6 1 49.32 54.33 2.84 o 2 6 1 14.10 12.80 1.90 o 3 6 1 98.58 105.05 4.47 o 4 6 1 0.81 3.75 2.06 o 5 6 1 5.94 6.17 2.70 o -6 7 1 50.84 47.38 2.92 o -5 7 1 8.57 7.97 1.76 o -4 7 1 274.07 251.57 4.92 o -3 7 1 5.62 6.39 1.04 o -2 7 1 514.48 477.09 8.21 o -1 7 1 0.72 2.28 0.95 o 0 7 1 557.86 540.14 13.70 o 1 7 1 30.71 27.99 2.38 o 2 7 1 237.05 219.52 7.01 o 3 7 1 0.02 -0.60 2.14 o 4 7 1 63.81 65.31 4.27 o -5 8 1 0.26 0.34 1.76 o -4 8 1 123.66 114.03 4.15 o -3 8 1 30.04 27.18 1.58 o -2 8 1 784.10 752.62 12.56 o -1 8 1 153.41 159.10 6.67 o 0 8 1 617.35 609.29 15.59 o 1 8 1 114.53 118.67 5.01 o 2 8 1 399.31 375.75 10.86 o 3 8 1 58.91 59.72 4.11 o -4 9 1 46.40 44.55 2.92 o -3 9 1 5.66 5.95 1.44 o -2 9 1 61.27 60.22 2.80 o -1 9 1 29.17 27.76 2.47 o 0 9 1 83.28 81.63 2.77 o 1 9 1 28.88 31.85 3.31 o 2 9 1 94.58 91.31 5.07 o 0 -10 2 2.25 3.95 2.66 o 1 -10 2 1.78 0.82 2.44 o 2 -10 2 2.81 4.45 2.30 o -2 -9 2 2.23 4.13 2.36 o -1 -9 2 179.55 196.80 7.09 o 0 -9 2 10.58 12.18 2.36 o 1 -9 2 80.22 74.14 4.03 o 2 -9 2 78.27 90.45 4.19 o 3 -9 2 8.84 6.13 2.02 o 4 -9 2 61.40 59.78 3.77 o -4 -8 2 0.34 -0.60 2.22 o -3 -8 2 365.48 352.21 10.42 o -2 -8 2 37.86 36.18 3.00 o -1 -8 2 328.81 330.70 9.58 o 0 -8 2 15.81 16.43 2.18 o 1 -8 2 533.48 523.20 9.05 o 2 -8 2 25.69 28.93 2.50 o 3 -8 2 57.65 49.12 3.02 o 4 -8 2 42.84 45.97 3.06 o 5 -8 2 16.81 18.55 2.58 o 6 -8 2 23.76 23.56 2.96 o -5 -7 2 10.01 11.64 3.12 o -4 -7 2 1.80 -0.16 1.92 o -3 -7 2 81.87 71.56 3.79 o -2 -7 2 10.19 8.83 2.04 o -1 -7 2 380.95 371.91 10.24 o 0 -7 2 26.63 23.94 2.12 o 1 -7 2 405.49 386.52 6.80 o 2 -7 2 84.03 81.99 2.21 o 3 -7 2 191.65 177.27 5.57 o 4 -7 2 12.20 12.38 1.94 o 5 -7 2 60.38 51.38 3.23 o 6 -7 2 1.15 1.96 2.24 o -6 -6 2 20.96 18.40 2.29 o -5 -6 2 61.65 57.41 2.58 o -4 -6 2 0.14 1.36 1.72 o -3 -6 2 283.21 268.29 6.23 o -2 -6 2 38.97 39.32 2.64 o -1 -6 2 277.80 278.81 7.87 o 0 -6 2 36.88 36.02 2.22 o 1 -6 2 256.45 245.78 4.49 o 2 -6 2 145.27 144.15 2.96 o 3 -6 2 53.33 52.89 2.01 o 4 -6 2 0.38 0.12 1.26 o 5 -6 2 0.10 0.04 1.44 o 6 -6 2 3.81 4.17 2.06 o 7 -6 2 3.12 4.25 2.38 o -6 -5 2 0.18 2.83 1.60 o -5 -5 2 119.23 124.75 6.27 o -4 -5 2 0.40 60.36 3.55 o -3 -5 2 301.83 322.38 5.98 o -2 -5 2 210.05 287.09 7.05 o 0 -5 2 134.92 265.11 7.09 o 1 -5 2 661.44 671.88 10.80 o 2 -5 2 712.00 728.16 11.68 o 3 -5 2 387.74 418.24 7.74 o 4 -5 2 112.81 178.64 6.73 o 5 -5 2 314.61 321.18 8.79 o 6 -5 2 16.48 45.87 2.82 o 7 -5 2 16.83 18.09 2.42 o -7 -4 2 0.02 0.08 1.59 o -6 -4 2 3.00 1.82 1.40 o -5 -4 2 9.64 11.64 1.36 o -4 -4 2 8.05 9.87 2.78 o -3 -4 2 0.72 0.72 0.69 o -2 -4 2 0.03 -0.06 0.41 o -1 -4 2 89.25 96.54 1.71 o 0 -4 2 667.10 664.43 11.00 o 1 -4 2 401.49 417.72 5.62 o 2 -4 2 874.83 931.92 14.67 o 3 -4 2 477.69 504.79 8.28 o 4 -4 2 245.67 254.64 4.61 o 5 -4 2 1.32 1.52 0.89 o 6 -4 2 31.88 32.18 1.65 o 7 -4 2 0.24 -0.14 1.90 o -7 -3 2 13.33 15.08 1.86 o -6 -3 2 0.03 0.19 1.14 o -5 -3 2 0.20 7.91 6.31 o -4 -3 2 82.58 81.37 2.25 o -3 -3 2 519.49 528.61 7.16 o -2 -3 2 76.74 69.93 1.35 o -1 -3 2 527.55 526.88 6.97 o 0 -3 2 89.11 77.93 2.41 o 1 -3 2 2976.54 2952.35 37.24 o 2 -3 2 29.33 29.20 0.73 o 3 -3 2 477.88 453.84 7.43 o 4 -3 2 5.99 6.48 0.72 o 5 -3 2 505.88 502.05 8.49 o 6 -3 2 0.10 0.19 0.96 o 7 -3 2 85.45 91.34 2.78 o 8 -3 2 5.02 5.97 2.60 o -8 -2 2 19.73 30.07 2.25 o -7 -2 2 3.41 2.92 1.38 o -6 -2 2 35.66 44.49 1.94 o -5 -2 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0.08 0.16 1.02 o -4 1 9 5.36 6.17 1.99 o -3 1 9 86.20 90.73 3.39 o -2 1 9 125.50 116.09 3.69 o -1 1 9 253.45 234.92 6.03 o 0 1 9 15.49 15.12 1.52 o 1 1 9 523.65 521.87 12.90 o 2 1 9 61.26 69.06 4.92 o 3 1 9 162.78 167.23 5.71 o 4 1 9 20.03 19.41 2.46 o -6 2 9 107.07 107.94 4.25 o -5 2 9 11.82 12.20 2.02 o -4 2 9 137.98 145.02 4.79 o -3 2 9 18.54 16.99 1.82 o -2 2 9 68.80 68.33 2.96 o -1 2 9 101.23 106.11 3.63 o 0 2 9 0.41 -0.22 1.20 o 1 2 9 59.38 61.02 2.76 o 2 2 9 20.32 22.82 2.16 o 3 2 9 35.93 35.32 2.74 o 4 2 9 25.82 30.13 3.00 o -6 3 9 20.02 29.73 2.80 o -5 3 9 0.86 1.28 1.84 o -4 3 9 15.25 24.22 2.14 o -3 3 9 6.63 6.09 1.54 o -2 3 9 37.81 38.10 2.38 o -1 3 9 13.83 17.35 1.88 o 0 3 9 5.29 3.47 1.48 o 1 3 9 67.78 70.94 3.25 o 3 3 9 58.86 64.14 4.01 o -6 4 9 35.76 36.60 3.15 o -5 4 9 0.19 -1.26 1.90 o -4 4 9 67.22 59.96 3.39 o -3 4 9 21.03 16.95 2.16 o -2 4 9 91.92 88.30 3.81 o -1 4 9 11.07 7.17 1.82 o 0 4 9 11.84 8.39 1.90 o 1 4 9 184.42 192.11 5.89 o -5 5 9 0.67 -0.78 1.96 o -4 5 9 258.70 283.10 8.13 o -3 5 9 1.94 1.38 1.92 o -2 5 9 207.42 206.04 6.39 o -1 5 9 56.44 54.53 3.15 o 0 5 9 41.06 43.27 3.00 o 1 5 9 36.43 38.96 2.96 o -3 6 9 0.63 1.06 1.96 o -2 6 9 96.69 100.74 4.59 o -1 6 9 10.86 7.55 2.10 o 0 6 9 22.22 22.84 2.64 o -2 -7 10 18.61 18.76 1.93 o -1 -7 10 7.41 4.74 1.59 o 0 -7 10 0.10 -0.45 1.34 o 1 -7 10 2.04 1.51 1.59 o 2 -7 10 1.69 0.90 1.55 o -3 -6 10 116.01 122.36 4.87 o -2 -6 10 5.53 8.93 1.47 o -1 -6 10 170.69 169.57 4.14 o 0 -6 10 15.65 17.10 1.64 o 1 -6 10 112.15 107.89 5.12 o 2 -6 10 0.45 0.29 1.37 o 3 -6 10 107.06 117.32 3.55 o -4 -5 10 198.59 207.18 6.57 o -3 -5 10 314.46 293.88 8.37 o -2 -5 10 172.91 185.82 5.87 o -1 -5 10 189.11 189.93 4.28 o 0 -5 10 41.39 50.46 2.12 o 1 -5 10 324.43 325.24 6.40 o 2 -5 10 4.44 3.70 1.20 o 3 -5 10 72.06 73.32 2.67 o -5 -4 10 65.92 66.67 3.63 o -4 -4 10 4.39 4.99 1.88 o -3 -4 10 190.60 188.47 5.97 o -2 -4 10 1.22 2.38 1.58 o -1 -4 10 105.95 99.79 2.75 o 0 -4 10 59.91 59.59 2.22 o 1 -4 10 11.21 11.81 1.30 o 2 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56.21 2.22 o -4 0 10 158.05 148.54 4.81 o -3 0 10 53.93 51.86 1.96 o -2 0 10 422.30 396.61 12.79 o -1 0 10 2.30 2.60 1.30 o 0 0 10 716.73 685.26 16.67 o 1 0 10 33.90 32.13 2.26 o 2 0 10 464.11 476.01 8.62 o 3 0 10 7.94 8.59 2.26 o 4 0 10 104.99 113.91 5.19 o -6 1 10 14.59 12.02 2.44 o -5 1 10 126.41 131.77 4.66 o -4 1 10 177.74 164.34 3.72 o -3 1 10 60.52 62.62 2.29 o -2 1 10 194.01 180.85 4.53 o -1 1 10 0.58 0.66 0.88 o 0 1 10 510.05 483.15 12.24 o 1 1 10 11.37 13.06 1.86 o 2 1 10 143.49 146.40 5.05 o 3 1 10 2.74 1.88 2.12 o -6 2 10 16.10 15.11 1.74 o -5 2 10 4.81 5.05 2.04 o -4 2 10 0.52 0.52 1.66 o -3 2 10 0.33 1.66 1.56 o -2 2 10 9.13 5.53 1.54 o -1 2 10 7.45 4.63 1.54 o 0 2 10 1.01 -0.08 1.40 o 2 2 10 3.04 2.48 1.80 o -5 3 10 87.35 78.67 3.87 o -4 3 10 21.07 22.74 2.44 o -3 3 10 40.18 34.64 2.56 o -2 3 10 0.28 0.22 1.66 o -1 3 10 54.90 53.13 3.04 o 0 3 10 19.69 20.21 1.94 o 1 3 10 0.21 -0.20 1.68 o -5 4 10 159.06 187.41 6.41 o -4 4 10 45.94 40.57 2.88 o -3 4 10 158.52 158.80 5.43 o -2 4 10 30.40 33.84 2.70 o -1 4 10 102.09 98.90 4.01 o 0 4 10 7.57 9.22 1.86 o 1 4 10 0.95 0.08 1.90 o -4 5 10 78.34 80.79 4.29 o -3 5 10 15.20 15.61 2.58 o -2 5 10 31.16 30.33 2.90 o -1 5 10 8.36 10.86 2.40 o 0 5 10 1.70 1.72 2.14 o -2 -6 11 87.99 85.34 4.03 o -1 -6 11 0.08 0.69 1.43 o 0 -6 11 103.27 105.55 3.30 o 1 -6 11 19.46 20.25 1.89 o 2 -6 11 47.38 47.29 2.35 o -4 -5 11 12.17 11.24 2.38 o -3 -5 11 1.51 2.56 1.96 o -2 -5 11 0.77 -0.34 1.78 o -1 -5 11 34.50 31.43 2.60 o 0 -5 11 12.20 15.69 1.53 o 1 -5 11 10.57 7.11 1.35 o 2 -5 11 49.36 46.84 2.30 o -4 -4 11 77.46 88.24 4.17 o -3 -4 11 104.84 98.82 4.25 o -2 -4 11 224.05 231.38 6.97 o -1 -4 11 15.79 17.01 2.00 o 0 -4 11 97.12 101.49 4.21 o 1 -4 11 12.99 13.58 2.20 o 2 -4 11 230.67 235.64 5.13 o 3 -4 11 38.58 35.57 2.10 o -5 -3 11 138.10 143.13 5.37 o -4 -3 11 69.59 72.58 3.59 o -3 -3 11 116.51 104.79 4.33 o -2 -3 11 45.50 52.43 2.94 o -1 -3 11 55.66 55.25 2.98 o 0 -3 11 199.18 209.24 6.45 o 1 -3 11 3.47 3.65 1.26 o 2 -3 11 75.05 76.57 2.67 o 3 -3 11 18.70 18.80 1.76 o -5 -2 11 173.45 168.72 5.85 o -4 -2 11 10.34 11.22 2.10 o -3 -2 11 23.05 25.12 2.18 o -2 -2 11 1.18 0.30 1.54 o -1 -2 11 9.48 7.61 1.62 o 0 -2 11 0.79 -0.60 1.32 o 1 -2 11 26.91 33.94 2.38 o 2 -2 11 1.55 3.01 1.24 o -5 -1 11 5.59 10.36 2.22 o -4 -1 11 11.76 11.46 2.08 o -3 -1 11 1.28 -0.34 1.40 o -2 -1 11 14.85 12.30 1.74 o -1 -1 11 4.60 1.70 1.42 o 0 -1 11 16.87 17.61 2.06 o 1 -1 11 0.81 1.72 1.66 o 2 -1 11 24.96 25.00 2.34 o 3 -1 11 0.59 0.42 2.22 o -5 0 11 187.32 209.57 7.06 o -4 0 11 9.16 10.27 1.35 o -2 0 11 6.94 7.67 1.74 o 0 0 11 4.12 6.93 1.78 o 1 0 11 5.72 8.43 1.86 o 2 0 11 0.44 0.48 1.80 o -5 1 11 2.87 4.24 1.49 o -4 1 11 45.23 48.06 4.26 o -3 1 11 0.03 -0.40 1.11 o -2 1 11 3.82 2.36 1.60 o -1 1 11 0.12 0.22 1.42 o 0 1 11 3.50 5.49 1.78 o 1 1 11 0.34 0.80 1.58 o 2 1 11 40.18 38.42 2.84 o -5 2 11 86.03 89.84 3.00 o -4 2 11 10.56 9.80 2.14 o -3 2 11 204.10 207.50 6.17 o -2 2 11 60.54 56.85 3.09 o 1 2 11 84.03 96.54 4.31 o 2 2 11 1.03 2.36 2.22 o -4 3 11 5.29 6.75 2.26 o -3 3 11 73.82 78.67 3.85 o -2 3 11 16.73 14.16 2.18 o -1 3 11 161.49 167.13 5.43 o -3 4 11 3.06 2.04 2.12 o -2 4 11 0.95 1.78 1.94 o -1 4 11 0.52 0.16 2.08 o -2 -5 12 0.86 0.60 1.82 o -1 -5 12 130.08 121.70 4.81 o 0 -5 12 20.87 15.83 2.44 o 1 -5 12 71.50 72.05 3.14 o -3 -4 12 131.36 138.19 5.19 o -2 -4 12 9.85 9.74 2.02 o -1 -4 12 112.77 116.41 4.75 o 0 -4 12 22.05 21.23 2.36 o 1 -4 12 70.52 64.06 3.73 o 2 -4 12 3.80 3.57 1.60 o -4 -3 12 5.72 6.25 2.30 o -3 -3 12 19.42 16.63 2.46 o -2 -3 12 2.92 2.56 1.72 o -1 -3 12 40.14 35.72 2.80 o 0 -3 12 29.14 31.39 2.68 o 1 -3 12 29.90 33.45 2.66 o 2 -3 12 0.10 -0.60 2.04 o -4 -2 12 38.43 42.07 3.15 o -3 -2 12 256.85 255.92 7.71 o -2 -2 12 8.42 8.91 1.88 o -1 -2 12 251.17 247.12 7.47 o 0 -2 12 6.94 6.59 2.02 o 1 -2 12 306.86 325.13 9.22 o 2 -2 12 3.67 2.06 2.08 o -4 -1 12 82.69 80.49 4.05 o -3 -1 12 36.58 34.08 2.80 o -2 -1 12 5.14 4.87 1.92 o -1 -1 12 195.19 181.48 5.95 o 0 -1 12 13.01 9.52 2.10 o 1 -1 12 214.39 223.80 7.01 o 2 -1 12 0.39 0.26 2.02 o -4 0 12 0.04 0.10 1.74 o -3 0 12 0.00 1.10 1.84 o -2 0 12 0.31 0.90 1.78 o -1 0 12 2.15 0.14 1.56 o 0 0 12 31.96 38.14 2.84 o 1 0 12 2.46 2.90 1.82 o 2 0 12 0.98 1.72 2.14 o -4 1 12 155.60 163.31 5.67 o -3 1 12 4.42 5.03 1.98 o -2 1 12 81.69 98.54 4.29 o -1 1 12 9.63 11.86 2.16 o 0 1 12 61.42 65.89 3.57 o -3 2 12 5.49 7.67 2.08 o -2 2 12 148.67 148.22 5.39 o -1 2 12 6.30 8.91 2.18 o 0 2 12 30.08 31.17 2.84 o -2 -3 13 254.07 272.56 8.27 o -1 -3 13 0.06 0.12 2.12 o 0 -3 13 229.44 247.18 7.81 o -2 -2 13 72.12 76.52 3.91 o -1 -2 13 0.02 -0.38 2.06 o 0 -2 13 111.59 114.79 4.79 o -3 -1 13 18.93 16.77 2.60 o -2 -1 13 31.04 29.03 2.86 o -1 -1 13 53.93 56.01 3.39 o 0 -1 13 1.53 1.60 2.20 o -2 0 13 167.50 199.55 6.71 o -1 0 13 49.97 80.41 4.23 o