#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2205856.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205856_Fobs loop_ _publ_author_name 'Shishkina, Svetlana V.' 'Shishkin, Oleg V.' 'Ukrainets, Igor V.' 'Kolesnik, Elena V.' _publ_section_title ; 1-Allyl-4-hydroxy-2-oxo-1,2,5,6,7,8-hexahydroquinoline-3-carboxylic acid ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1833 _journal_page_last o1835 _journal_volume 61 _journal_year 2005 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 16.8230 _cell_length_b 7.1790 _cell_length_c 19.8470 _exptl_crystal_F_000 1056.00 _reflns_d_resolution_high 0.8392 _[local]_cod_data_source_file bh6001Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' u13 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 223.56 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 49977.60 47486.31 144.04 o 4 0 0 17249.48 16527.37 124.15 o 6 0 0 9057.76 9250.31 116.84 o 8 0 0 6.26 -7.02 11.11 o 12 0 0 0.01 -3.66 48.26 o 14 0 0 483.96 495.58 23.10 o 16 0 0 179.65 210.72 20.03 o 18 0 0 53.84 48.26 67.71 o 2 1 0 320.88 341.01 14.04 o 4 1 0 533.93 616.22 17.26 o 6 1 0 916.87 961.03 23.40 o 8 1 0 8.16 19.60 11.26 o 10 1 0 194.10 183.37 13.89 o 12 1 0 762.58 812.02 24.71 o 14 1 0 93.58 108.50 18.57 o 16 1 0 10.43 -4.39 59.81 o 18 1 0 37.24 46.36 20.18 o 2 2 0 41806.61 38758.48 210.72 o 6 2 0 1369.47 1254.67 25.44 o 10 2 0 10.27 2.49 14.33 o 12 2 0 9.84 -15.65 43.58 o 14 2 0 122.63 95.34 16.38 o 16 2 0 33.80 -31.15 47.67 o 18 2 0 7.80 13.16 62.88 o 2 3 0 2289.31 2254.16 37.44 o 4 3 0 690.81 619.44 20.18 o 6 3 0 474.09 464.72 19.60 o 8 3 0 247.08 268.92 18.72 o 10 3 0 66.28 74.14 18.57 o 12 3 0 108.17 131.32 20.91 o 14 3 0 11.35 0.44 17.84 o 16 3 0 5.26 23.25 70.48 o 0 4 0 8476.71 9218.57 120.79 o 2 4 0 9778.90 10309.17 141.55 o 4 4 0 5042.00 5097.77 74.87 o 6 4 0 39.33 35.24 14.62 o 8 4 0 217.27 219.49 18.13 o 10 4 0 0.94 -23.10 50.89 o 12 4 0 39.43 19.16 57.47 o 14 4 0 10.37 0.73 60.83 o 16 4 0 9.26 -19.16 50.30 o 2 5 0 1128.45 1111.65 28.95 o 4 5 0 48.65 57.32 17.11 o 6 5 0 116.67 133.07 17.84 o 8 5 0 160.53 148.13 19.16 o 10 5 0 125.31 144.77 19.16 o 12 5 0 16.51 44.45 54.84 o 14 5 0 0.05 21.35 52.79 o 16 5 0 19.12 2.19 69.17 o 0 6 0 74.17 56.74 19.45 o 2 6 0 1280.71 1242.24 33.34 o 4 6 0 2760.64 2704.55 54.40 o 6 6 0 144.45 157.05 19.30 o 8 6 0 118.58 125.03 19.16 o 10 6 0 25.43 -5.85 60.54 o 12 6 0 4.03 35.39 66.68 o 14 6 0 13.93 15.21 54.69 o 2 7 0 117.36 109.67 20.91 o 4 7 0 51.09 38.61 21.20 o 6 7 0 63.25 108.80 66.83 o 8 7 0 4.72 -4.83 66.39 o 10 7 0 76.09 24.57 66.83 o 0 8 0 9.80 -25.01 90.08 o 2 8 0 156.59 94.76 82.77 o 4 8 0 435.84 423.49 30.71 o 6 8 0 119.26 165.97 26.18 o 1 1 1 297.93 345.84 11.99 o 2 1 1 0.06 5.26 10.09 o 3 1 1 88.69 89.35 11.84 o 4 1 1 1440.63 1328.37 28.08 o 5 1 1 496.17 516.49 16.52 o 6 1 1 1314.46 1319.30 24.57 o 7 1 1 126.21 125.47 11.70 o 8 1 1 70.68 69.17 12.28 o 9 1 1 34.38 30.27 12.72 o 10 1 1 60.04 69.90 13.01 o 11 1 1 250.48 259.56 16.82 o 12 1 1 134.41 122.54 16.38 o 13 1 1 69.37 77.36 16.23 o 14 1 1 7.09 17.11 47.67 o 15 1 1 27.23 41.68 16.82 o 16 1 1 0.11 -41.09 58.05 o 17 1 1 33.33 49.57 65.80 o 18 1 1 0.58 -13.31 39.63 o 19 1 1 0.14 -6.29 58.49 o 0 2 1 2925.32 2608.62 38.17 o 1 2 1 13671.92 12635.13 120.64 o 2 2 1 3402.06 3191.79 48.11 o 3 2 1 19742.69 17922.71 152.08 o 4 2 1 762.39 752.65 19.45 o 5 2 1 807.39 858.23 20.03 o 6 2 1 655.44 624.12 18.72 o 7 2 1 1015.47 924.33 23.40 o 8 2 1 313.92 267.60 15.79 o 9 2 1 606.22 584.34 20.03 o 10 2 1 107.60 72.82 14.77 o 11 2 1 87.68 78.53 15.65 o 12 2 1 134.18 92.56 15.79 o 13 2 1 177.35 144.48 17.69 o 14 2 1 121.74 104.99 16.52 o 15 2 1 2.28 -2.49 15.94 o 16 2 1 1.61 -36.70 52.20 o 17 2 1 0.87 64.34 72.97 o 18 2 1 1.88 -31.59 61.27 o 19 2 1 19.68 81.01 83.50 o 1 3 1 521.93 545.59 17.84 o 2 3 1 6.95 6.43 12.43 o 3 3 1 86.34 67.41 13.16 o 4 3 1 331.05 286.91 17.40 o 5 3 1 385.85 394.82 18.72 o 6 3 1 233.90 182.35 16.23 o 7 3 1 9.70 9.07 15.94 o 8 3 1 135.87 153.10 16.67 o 9 3 1 34.04 34.80 16.96 o 10 3 1 1.42 49.72 55.71 o 11 3 1 393.87 468.96 24.27 o 12 3 1 277.54 279.59 22.52 o 13 3 1 67.01 62.44 18.72 o 14 3 1 44.32 84.81 51.47 o 15 3 1 78.25 63.32 21.06 o 16 3 1 0.33 -4.09 20.91 o 17 3 1 75.53 104.12 21.93 o 18 3 1 0.11 -43.72 60.25 o 0 4 1 247.14 266.14 17.69 o 1 4 1 5349.32 5305.57 72.97 o 2 4 1 462.37 491.78 21.06 o 3 4 1 8586.72 8804.01 118.45 o 4 4 1 628.22 711.85 23.25 o 5 4 1 19.42 17.84 14.18 o 6 4 1 22.61 18.28 14.62 o 7 4 1 145.71 141.55 16.52 o 8 4 1 0.01 15.35 15.94 o 9 4 1 24.67 38.75 16.82 o 10 4 1 10.83 16.96 16.52 o 11 4 1 121.68 128.68 19.74 o 12 4 1 61.48 64.20 52.64 o 13 4 1 125.67 146.52 20.03 o 14 4 1 53.79 45.19 19.16 o 15 4 1 0.39 -3.07 57.18 o 16 4 1 21.56 23.10 21.20 o 17 4 1 1.73 27.20 49.72 o 1 5 1 40.10 19.01 16.09 o 2 5 1 4.17 -22.08 46.94 o 3 5 1 198.78 216.13 18.57 o 4 5 1 23.75 44.02 16.52 o 5 5 1 14.67 9.80 17.40 o 6 5 1 22.63 6.14 17.26 o 8 5 1 10.20 16.09 16.09 o 9 5 1 0.13 8.92 49.57 o 10 5 1 166.28 197.27 20.33 o 11 5 1 43.20 53.08 60.83 o 12 5 1 67.35 51.47 18.13 o 13 5 1 0.14 22.52 54.54 o 14 5 1 17.18 45.77 56.30 o 15 5 1 10.48 37.87 60.10 o 16 5 1 0.12 -34.36 58.35 o 0 6 1 18.19 -16.82 54.11 o 1 6 1 531.55 597.50 24.57 o 2 6 1 47.44 21.93 19.74 o 3 6 1 1303.85 1242.82 35.10 o 4 6 1 207.04 225.78 22.52 o 5 6 1 430.98 448.05 23.69 o 6 6 1 9.33 6.58 62.00 o 7 6 1 26.09 -23.54 50.16 o 8 6 1 8.69 -30.85 58.49 o 9 6 1 91.51 108.65 22.67 o 10 6 1 1.72 -14.04 56.01 o 11 6 1 120.01 119.62 20.76 o 12 6 1 1.44 -6.29 56.15 o 13 6 1 15.74 17.55 60.98 o 14 6 1 12.46 52.06 67.71 o 1 7 1 0.00 -43.28 62.44 o 2 7 1 15.47 -32.61 68.14 o 3 7 1 115.56 88.47 19.89 o 4 7 1 9.61 11.26 65.22 o 5 7 1 10.10 70.92 64.93 o 6 7 1 17.51 -47.09 75.02 o 7 7 1 2.24 -21.64 57.76 o 8 7 1 6.42 40.51 69.61 o 9 7 1 11.78 60.69 65.51 o 10 7 1 114.22 124.00 80.13 o 11 7 1 0.12 -63.46 71.65 o 0 8 1 2.11 7.46 21.06 o 1 8 1 13.94 -53.23 71.65 o 2 8 1 9.44 -21.20 78.09 o 3 8 1 154.16 114.50 25.15 o 4 8 1 26.67 16.96 74.58 o 5 8 1 263.07 256.93 27.35 o 6 8 1 5.19 -33.05 63.32 o 7 8 1 33.59 64.93 68.44 o 0 0 2 28709.70 27537.42 100.90 o 1 0 2 855.75 847.56 15.21 o 2 0 2 11878.06 11819.74 38.17 o 3 0 2 1117.57 1136.51 22.81 o 4 0 2 4026.38 3729.49 58.05 o 5 0 2 469.65 453.46 15.06 o 6 0 2 1875.49 1649.34 28.66 o 7 0 2 703.19 864.08 22.08 o 9 0 2 403.02 431.97 18.13 o 10 0 2 1894.30 1959.06 38.75 o 11 0 2 333.80 366.89 17.69 o 12 0 2 256.31 299.04 18.57 o 13 0 2 1104.21 1134.90 30.85 o 14 0 2 1344.60 1419.32 35.68 o 15 0 2 300.90 327.56 21.50 o 16 0 2 3.01 9.07 52.50 o 17 0 2 17.45 -30.71 62.15 o 18 0 2 1.01 -10.67 54.40 o 19 0 2 29.63 -0.73 54.40 o 1 1 2 3872.59 3455.74 46.65 o 2 1 2 456.03 473.79 15.79 o 3 1 2 12108.06 11809.79 105.29 o 4 1 2 1226.72 1084.45 23.69 o 5 1 2 2973.96 2810.57 43.43 o 6 1 2 141.79 142.14 11.70 o 7 1 2 1783.82 1711.79 30.85 o 8 1 2 1889.89 2063.33 35.39 o 9 1 2 6116.22 6136.46 86.13 o 10 1 2 752.92 769.76 22.52 o 11 1 2 255.34 256.78 17.11 o 12 1 2 16.88 43.14 49.28 o 14 1 2 185.93 178.26 20.33 o 15 1 2 1.25 34.51 55.86 o 16 1 2 144.84 139.07 19.16 o 17 1 2 83.00 103.39 20.03 o 18 1 2 25.39 -51.62 66.54 o 19 1 2 68.36 113.48 69.31 o 0 2 2 20144.85 17774.87 142.28 o 1 2 2 3097.71 2726.63 41.82 o 2 2 2 3704.98 3528.27 50.30 o 3 2 2 744.55 780.73 20.47 o 4 2 2 731.92 632.16 17.55 o 5 2 2 66.94 60.10 11.11 o 6 2 2 1065.59 1081.09 23.69 o 7 2 2 771.18 758.94 22.08 o 8 2 2 485.69 581.85 19.89 o 9 2 2 167.17 172.11 14.48 o 10 2 2 220.86 251.52 17.55 o 11 2 2 391.96 440.01 20.47 o 12 2 2 114.94 96.37 15.79 o 13 2 2 738.77 617.97 24.27 o 14 2 2 413.28 344.08 20.33 o 15 2 2 100.20 7.46 51.33 o 16 2 2 17.78 12.58 16.52 o 17 2 2 0.02 66.24 61.42 o 18 2 2 0.31 0.58 63.03 o 19 2 2 5.50 -2.78 62.44 o 1 3 2 249.97 228.71 14.62 o 2 3 2 30.35 15.50 12.72 o 3 3 2 54.11 51.62 13.60 o 4 3 2 12.03 4.09 13.16 o 5 3 2 128.56 113.77 15.65 o 6 3 2 595.18 663.45 22.96 o 7 3 2 708.20 862.47 25.88 o 8 3 2 320.39 332.68 20.18 o 9 3 2 1292.47 1468.60 35.68 o 10 3 2 114.75 130.58 19.01 o 11 3 2 44.74 37.00 19.16 o 12 3 2 328.06 369.38 23.98 o 13 3 2 90.53 94.90 20.91 o 14 3 2 26.28 -3.36 19.60 o 15 3 2 3.64 -32.61 68.29 o 16 3 2 2.67 8.04 19.16 o 17 3 2 0.03 -9.80 56.88 o 18 3 2 4.84 1.75 69.46 o 0 4 2 1461.89 1508.08 31.88 o 1 4 2 1671.96 1774.81 33.63 o 2 4 2 800.05 870.52 24.86 o 3 4 2 792.35 820.21 23.10 o 4 4 2 136.04 122.40 14.77 o 5 4 2 36.58 45.33 14.18 o 6 4 2 199.82 190.39 16.52 o 7 4 2 486.96 492.36 22.23 o 8 4 2 273.07 291.15 20.76 o 9 4 2 62.13 69.75 16.67 o 10 4 2 64.33 65.51 18.86 o 11 4 2 364.15 367.48 23.25 o 12 4 2 17.82 8.04 18.13 o 13 4 2 257.29 231.92 22.23 o 14 4 2 6.66 13.45 55.86 o 15 4 2 0.19 2.34 53.23 o 16 4 2 59.24 105.43 79.40 o 17 4 2 29.73 80.72 69.90 o 1 5 2 106.87 121.37 16.82 o 2 5 2 96.98 89.20 17.69 o 4 5 2 5.05 21.64 16.09 o 5 5 2 5.18 10.53 15.79 o 6 5 2 122.25 143.45 17.69 o 7 5 2 120.90 106.75 17.69 o 8 5 2 55.94 52.64 17.11 o 9 5 2 41.67 42.41 18.86 o 10 5 2 113.37 120.79 19.74 o 11 5 2 39.18 -16.23 61.12 o 12 5 2 292.31 306.21 22.08 o 13 5 2 8.91 -6.73 51.77 o 14 5 2 7.86 -1.90 72.97 o 15 5 2 3.08 -44.16 70.78 o 16 5 2 7.13 -8.19 71.80 o 0 6 2 0.55 10.53 17.69 o 1 6 2 226.02 215.69 21.35 o 2 6 2 176.59 164.51 20.47 o 3 6 2 296.84 283.84 22.23 o 4 6 2 198.25 183.37 20.62 o 5 6 2 165.03 186.45 21.20 o 6 6 2 24.33 11.70 49.86 o 7 6 2 289.73 243.62 20.76 o 8 6 2 3.58 19.30 18.43 o 9 6 2 65.55 58.20 69.46 o 10 6 2 49.30 62.15 20.47 o 11 6 2 94.91 40.36 62.44 o 12 6 2 0.51 43.43 57.76 o 13 6 2 46.42 51.77 71.95 o 14 6 2 0.02 51.18 68.14 o 1 7 2 15.46 -10.53 61.42 o 2 7 2 39.55 77.80 69.90 o 3 7 2 0.20 9.80 62.44 o 4 7 2 18.56 -20.18 70.78 o 5 7 2 0.25 34.66 62.88 o 6 7 2 5.02 12.58 59.81 o 7 7 2 2.76 42.85 64.93 o 8 7 2 59.73 79.26 75.89 o 9 7 2 32.54 50.01 71.07 o 10 7 2 68.61 -3.95 75.75 o 11 7 2 9.29 -43.58 62.59 o 0 8 2 10.56 14.18 75.46 o 1 8 2 14.74 -23.84 71.21 o 2 8 2 15.87 1.61 75.89 o 3 8 2 58.55 82.91 88.62 o 4 8 2 52.00 34.80 70.34 o 5 8 2 135.01 74.72 24.42 o 6 8 2 17.05 -18.86 93.44 o 1 1 3 351.47 406.08 15.06 o 2 1 3 96.81 91.39 12.28 o 3 1 3 1439.02 1445.06 27.05 o 4 1 3 423.76 398.48 14.62 o 5 1 3 1325.16 1345.48 25.88 o 6 1 3 931.80 903.13 20.76 o 7 1 3 39.86 55.28 12.14 o 8 1 3 257.04 256.34 14.92 o 9 1 3 290.37 310.74 16.38 o 10 1 3 501.99 425.83 19.30 o 11 1 3 57.51 50.45 14.18 o 12 1 3 112.93 136.43 16.09 o 13 1 3 95.62 112.45 18.13 o 14 1 3 2.96 23.54 49.86 o 15 1 3 2.17 3.51 17.26 o 16 1 3 2.31 -3.66 56.15 o 17 1 3 21.64 -12.87 64.49 o 18 1 3 1.38 -27.49 52.94 o 19 1 3 1.42 -37.73 59.66 o 0 2 3 2975.32 2631.43 42.85 o 1 2 3 2816.13 2778.25 39.77 o 2 2 3 603.86 578.78 16.67 o 4 2 3 446.46 477.45 15.21 o 5 2 3 314.65 320.39 14.92 o 6 2 3 380.72 384.30 15.50 o 7 2 3 3072.26 2918.93 47.67 o 8 2 3 160.16 145.21 14.62 o 9 2 3 107.79 99.29 14.92 o 10 2 3 41.35 33.49 14.92 o 11 2 3 1081.15 1038.24 29.68 o 12 2 3 317.24 275.21 18.57 o 13 2 3 4.61 82.91 49.13 o 14 2 3 0.30 -52.64 52.64 o 15 2 3 147.22 114.21 18.43 o 16 2 3 207.97 172.11 18.43 o 17 2 3 11.74 -25.01 45.04 o 18 2 3 11.50 -0.15 56.74 o 19 2 3 12.42 77.80 75.31 o 1 3 3 273.31 244.50 16.38 o 2 3 3 160.82 118.30 13.60 o 3 3 3 692.43 716.10 20.76 o 4 3 3 7.48 17.84 12.72 o 5 3 3 1621.07 1673.91 33.63 o 6 3 3 1208.29 1240.04 29.83 o 8 3 3 203.08 236.16 19.45 o 9 3 3 626.92 703.81 24.42 o 10 3 3 1145.77 1233.17 34.80 o 11 3 3 131.50 155.30 20.91 o 12 3 3 505.67 577.76 27.35 o 13 3 3 326.58 340.57 23.69 o 14 3 3 10.14 85.69 66.24 o 15 3 3 16.31 4.53 62.59 o 16 3 3 14.43 -4.39 64.05 o 17 3 3 76.47 30.85 71.51 o 18 3 3 0.09 -4.09 67.12 o 0 4 3 190.73 177.96 16.38 o 1 4 3 359.68 401.99 18.86 o 2 4 3 711.79 796.38 22.23 o 3 4 3 303.95 307.82 17.55 o 4 4 3 1.79 -7.31 14.62 o 5 4 3 2.00 18.86 14.77 o 6 4 3 411.34 431.97 20.03 o 7 4 3 389.35 351.83 21.20 o 8 4 3 95.47 85.25 16.96 o 9 4 3 42.41 71.80 17.26 o 10 4 3 0.17 -16.38 54.69 o 11 4 3 717.21 709.95 27.64 o 12 4 3 272.12 266.87 22.08 o 13 4 3 0.35 -3.07 56.74 o 14 4 3 22.70 20.91 20.33 o 15 4 3 141.04 150.76 20.91 o 16 4 3 142.26 114.21 21.64 o 17 4 3 13.16 15.06 76.48 o 1 5 3 13.11 19.45 17.11 o 2 5 3 55.69 71.51 15.65 o 3 5 3 0.04 -3.66 16.23 o 4 5 3 61.77 59.66 16.38 o 5 5 3 135.13 117.86 19.01 o 6 5 3 275.94 242.89 20.47 o 7 5 3 44.81 57.03 19.01 o 8 5 3 0.33 -2.92 16.67 o 9 5 3 5.53 -14.92 46.94 o 10 5 3 545.78 507.72 25.01 o 11 5 3 46.96 51.03 19.60 o 12 5 3 325.75 351.39 23.98 o 13 5 3 57.49 59.81 63.90 o 14 5 3 13.53 1.02 65.66 o 15 5 3 11.64 -40.65 64.20 o 16 5 3 5.98 33.63 63.61 o 0 6 3 30.47 45.04 17.69 o 1 6 3 16.36 -17.69 59.95 o 2 6 3 103.10 122.69 20.18 o 3 6 3 263.66 209.55 20.18 o 4 6 3 87.59 60.10 18.43 o 6 6 3 27.78 16.38 62.59 o 7 6 3 1.07 -48.11 48.11 o 8 6 3 0.95 -35.53 52.35 o 9 6 3 24.74 40.36 20.03 o 10 6 3 15.25 25.01 48.26 o 11 6 3 60.93 52.94 78.09 o 12 6 3 24.90 2.49 56.30 o 13 6 3 3.51 51.77 51.91 o 14 6 3 26.33 0.88 68.14 o 1 7 3 9.82 43.14 52.64 o 2 7 3 1.29 10.38 52.94 o 3 7 3 1.72 52.20 59.37 o 4 7 3 7.53 24.71 63.61 o 5 7 3 14.18 42.70 19.60 o 6 7 3 14.80 -24.27 49.72 o 7 7 3 10.60 4.39 21.64 o 8 7 3 22.66 26.91 50.30 o 9 7 3 27.43 47.23 55.57 o 10 7 3 186.38 158.81 23.25 o 11 7 3 16.52 8.19 59.37 o 0 8 3 31.13 58.93 83.64 o 1 8 3 11.30 -40.07 67.27 o 2 8 3 0.19 5.12 61.86 o 3 8 3 107.02 126.64 77.06 o 4 8 3 38.59 62.88 82.77 o 5 8 3 80.40 50.30 79.55 o 6 8 3 15.18 53.08 97.83 o 0 0 4 17814.86 15960.72 112.31 o 1 0 4 18.63 27.49 9.65 o 2 0 4 1375.42 1365.80 25.59 o 3 0 4 6287.61 5618.36 82.04 o 4 0 4 1158.84 1295.17 24.57 o 5 0 4 506.20 453.17 14.18 o 6 0 4 2831.63 2734.38 44.02 o 7 0 4 4634.65 4787.62 69.46 o 8 0 4 594.31 628.06 18.57 o 10 0 4 1179.32 1202.90 27.78 o 11 0 4 102.80 95.78 16.09 o 12 0 4 267.26 253.71 17.40 o 13 0 4 1109.54 1094.98 30.85 o 14 0 4 1634.21 1810.05 41.82 o 15 0 4 1031.76 1009.73 30.42 o 16 0 4 40.37 62.44 65.51 o 17 0 4 110.44 98.85 19.45 o 18 0 4 81.01 91.54 21.64 o 19 0 4 0.26 22.08 57.76 o 1 1 4 2964.52 2596.63 40.94 o 2 1 4 1683.50 1487.76 28.95 o 3 1 4 3880.72 3725.39 54.40 o 4 1 4 3714.59 3624.64 52.06 o 5 1 4 0.12 10.82 10.24 o 6 1 4 1798.09 1798.65 32.32 o 7 1 4 2119.11 2310.75 41.53 o 8 1 4 2769.96 3028.01 49.57 o 9 1 4 1377.14 1504.87 31.15 o 10 1 4 86.02 97.54 14.18 o 11 1 4 202.26 213.50 17.11 o 12 1 4 122.19 120.20 16.67 o 13 1 4 2503.68 2439.29 46.79 o 14 1 4 2239.06 2091.40 45.04 o 15 1 4 156.78 170.36 20.33 o 16 1 4 942.36 843.76 30.71 o 17 1 4 61.27 110.70 53.37 o 18 1 4 0.42 44.75 49.28 o 19 1 4 13.26 -11.99 52.64 o 0 2 4 8553.92 7514.39 102.22 o 1 2 4 403.31 366.16 13.45 o 2 2 4 621.29 585.95 16.38 o 3 2 4 363.79 330.78 13.45 o 4 2 4 972.97 1002.56 22.37 o 5 2 4 10.42 17.26 11.11 o 6 2 4 2228.22 2209.85 39.48 o 7 2 4 470.79 504.64 19.01 o 8 2 4 230.73 204.58 15.79 o 9 2 4 85.91 70.48 13.45 o 10 2 4 406.46 405.65 20.18 o 11 2 4 0.86 24.13 44.75 o 12 2 4 69.65 57.76 44.60 o 14 2 4 839.51 726.62 26.32 o 15 2 4 776.52 681.73 26.47 o 16 2 4 0.31 -11.55 62.88 o 17 2 4 60.75 52.79 21.35 o 18 2 4 15.06 59.08 66.97 o 19 2 4 3.52 11.11 45.77 o 1 3 4 45.48 31.44 13.01 o 2 3 4 205.73 141.26 14.92 o 3 3 4 17.15 31.59 45.19 o 4 3 4 181.89 188.35 15.50 o 5 3 4 101.02 114.06 15.65 o 6 3 4 125.90 141.55 16.67 o 7 3 4 498.26 634.06 25.15 o 8 3 4 200.24 251.52 19.16 o 10 3 4 129.03 141.26 19.45 o 11 3 4 313.77 361.92 24.27 o 12 3 4 453.94 444.98 26.61 o 13 3 4 314.11 352.13 23.54 o 14 3 4 485.65 530.67 25.30 o 15 3 4 83.81 69.61 20.91 o 17 3 4 0.06 12.72 56.74 o 18 3 4 74.57 50.45 71.65 o 0 4 4 1402.15 1666.01 33.19 o 1 4 4 28.88 33.19 13.45 o 2 4 4 131.40 130.58 15.35 o 3 4 4 175.03 183.67 16.67 o 4 4 4 191.30 199.90 16.82 o 5 4 4 151.64 146.82 16.09 o 6 4 4 1089.05 1069.10 29.39 o 7 4 4 93.16 82.77 16.82 o 8 4 4 21.70 34.36 16.38 o 9 4 4 73.15 85.11 17.69 o 10 4 4 0.47 -6.87 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