#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/58/2205860.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205860_Fobs loop_ _publ_author_name 'Ko\catena-Poly[[bis(4-aminopyrimidine-\kN^1^)copper(II)]-di-\m-dicyanamido-\k^4^N^1^:N^3^] ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1150 _journal_page_last m1152 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 105.290 _cell_angle_beta 100.190 _cell_angle_gamma 106.270 _cell_length_a 6.2600 _cell_length_b 7.2480 _cell_length_c 9.4510 _exptl_crystal_F_000 195.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file bh6005Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' BH6005 = KOZ84 IN P1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 82.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 233.27 232.35 1.32 o 2 0 0 91.29 76.69 1.35 o 3 0 0 1.24 2.58 0.57 o 4 0 0 32.81 33.13 1.61 o 5 0 0 116.02 115.53 3.21 o 6 0 0 38.63 36.62 1.52 o 7 0 0 74.06 76.42 3.62 o -7 1 0 34.92 34.12 2.58 o -6 1 0 30.55 33.71 1.40 o -5 1 0 412.16 406.46 7.71 o -4 1 0 412.92 406.33 11.79 o -3 1 0 3.30 10.78 0.84 o -2 1 0 1087.13 1020.56 6.80 o -1 1 0 1411.86 1398.57 12.13 o 1 1 0 1.86 3.33 0.43 o 2 1 0 801.67 766.55 17.22 o 3 1 0 981.36 758.31 163.33 o 4 1 0 166.08 169.99 3.01 o 5 1 0 38.26 40.79 3.26 o 6 1 0 16.67 16.35 2.30 o 7 1 0 17.51 19.05 2.58 o -7 2 0 51.26 56.68 1.95 o -6 2 0 160.86 158.03 4.68 o -5 2 0 176.83 162.86 7.04 o -4 2 0 170.86 146.25 1.63 o -3 2 0 397.39 372.27 11.26 o -2 2 0 574.52 534.69 20.16 o -1 2 0 4067.12 3890.68 101.10 o 0 2 0 363.23 402.59 3.29 o 1 2 0 582.94 600.32 10.33 o 2 2 0 231.09 205.97 7.42 o 3 2 0 45.72 45.91 1.73 o 4 2 0 191.14 201.60 3.43 o 5 2 0 237.16 232.63 3.97 o 6 2 0 38.47 39.81 3.00 o -7 3 0 4.01 5.28 1.18 o -6 3 0 176.15 165.33 3.24 o -5 3 0 163.15 170.66 2.09 o -4 3 0 80.01 69.84 1.79 o -3 3 0 1497.72 1504.08 86.62 o -2 3 0 606.94 635.09 22.00 o -1 3 0 937.37 969.32 2.29 o 0 3 0 41.93 31.70 0.52 o 1 3 0 99.76 92.87 0.87 o 2 3 0 7.31 5.67 0.61 o 3 3 0 124.45 130.00 1.98 o 4 3 0 266.84 267.81 4.07 o 5 3 0 35.59 37.12 2.64 o 6 3 0 22.87 20.64 2.44 o -7 4 0 17.59 20.18 2.30 o -6 4 0 175.64 175.54 3.26 o -5 4 0 137.13 139.20 1.87 o -4 4 0 117.95 119.75 3.49 o -3 4 0 519.78 500.39 15.90 o -2 4 0 428.81 415.55 4.26 o -1 4 0 97.13 91.47 1.60 o 0 4 0 225.25 224.53 1.97 o 1 4 0 120.08 108.34 1.16 o 2 4 0 185.51 201.36 2.25 o 3 4 0 142.07 151.93 2.20 o 4 4 0 120.58 122.42 3.46 o 5 4 0 1.54 1.25 1.52 o -7 5 0 301.88 304.53 4.46 o -6 5 0 109.60 115.95 2.89 o -5 5 0 0.87 2.48 1.32 o -4 5 0 81.64 87.65 2.31 o -3 5 0 133.84 125.83 4.05 o -2 5 0 197.45 202.59 4.42 o -1 5 0 362.96 353.08 3.95 o 0 5 0 248.97 248.01 1.80 o 1 5 0 88.65 91.38 2.03 o 2 5 0 131.99 135.34 5.26 o 3 5 0 34.72 35.23 1.58 o 4 5 0 24.57 23.41 2.15 o -7 6 0 84.41 81.94 3.48 o -6 6 0 58.66 58.72 2.88 o -5 6 0 233.53 235.44 3.88 o -4 6 0 393.32 412.11 4.63 o -3 6 0 31.56 30.52 1.55 o -2 6 0 11.40 12.16 0.98 o -1 6 0 38.16 37.18 1.21 o 0 6 0 33.06 33.00 1.10 o 1 6 0 145.52 142.26 2.70 o 2 6 0 124.54 129.99 3.74 o 3 6 0 137.02 138.99 4.30 o -6 7 0 22.73 22.18 2.81 o -5 7 0 42.83 44.54 2.76 o -4 7 0 56.64 58.55 2.54 o -3 7 0 86.41 85.78 2.86 o -2 7 0 421.16 419.00 4.76 o -1 7 0 64.69 59.41 1.64 o 0 7 0 4.88 5.61 1.54 o 1 7 0 51.43 45.15 2.50 o 2 7 0 9.30 8.33 1.55 o -5 8 0 6.81 9.80 2.69 o -4 8 0 69.92 75.72 3.37 o -3 8 0 143.74 138.82 3.28 o -2 8 0 78.32 73.23 3.14 o -1 8 0 3.15 5.33 1.35 o 0 8 0 69.95 66.93 3.27 o 1 8 0 52.89 49.30 3.96 o -3 9 0 31.35 30.66 3.33 o -2 9 0 0.64 2.31 2.20 o 1 -9 1 49.17 48.69 3.63 o 2 -9 1 32.45 28.84 2.93 o 3 -9 1 13.20 11.99 2.54 o 4 -9 1 33.98 29.14 2.76 o -1 -8 1 44.70 41.78 3.14 o 0 -8 1 65.45 63.50 3.05 o 1 -8 1 23.18 24.87 1.76 o 2 -8 1 39.78 35.95 2.48 o 3 -8 1 92.98 93.99 3.26 o 4 -8 1 53.14 50.60 3.02 o 5 -8 1 13.47 12.43 2.31 o 6 -8 1 31.87 31.95 3.36 o -2 -7 1 41.78 38.46 2.68 o -1 -7 1 11.20 13.87 2.28 o 0 -7 1 0.84 1.17 1.09 o 1 -7 1 13.12 11.68 1.29 o 2 -7 1 318.58 331.66 3.54 o 3 -7 1 195.86 194.92 3.70 o 4 -7 1 103.98 112.05 3.02 o 5 -7 1 64.05 66.07 2.76 o 6 -7 1 43.76 40.92 2.53 o -4 -6 1 49.78 46.40 3.18 o -3 -6 1 32.60 35.21 3.22 o -2 -6 1 126.73 129.19 4.64 o -1 -6 1 101.38 97.60 1.70 o 0 -6 1 69.56 73.73 1.70 o 1 -6 1 88.32 91.34 3.70 o 2 -6 1 33.71 39.36 1.40 o 3 -6 1 5.76 8.51 0.91 o 4 -6 1 160.98 172.97 3.30 o 5 -6 1 275.94 286.74 4.13 o 6 -6 1 191.30 191.90 3.57 o 7 -6 1 74.38 70.16 3.53 o -5 -5 1 36.53 32.07 3.29 o -4 -5 1 61.65 57.01 2.22 o -3 -5 1 29.58 28.93 1.61 o -2 -5 1 45.65 43.64 1.46 o -1 -5 1 44.04 45.57 1.27 o 0 -5 1 62.85 58.61 1.56 o 1 -5 1 756.91 782.57 5.28 o 2 -5 1 148.76 151.05 3.68 o 3 -5 1 690.75 708.32 34.51 o 4 -5 1 52.49 48.47 3.01 o 5 -5 1 1.84 3.79 1.82 o 6 -5 1 114.21 113.97 2.80 o 7 -5 1 60.72 68.24 3.19 o -5 -4 1 27.08 24.06 2.59 o -4 -4 1 16.07 17.55 2.45 o -3 -4 1 88.91 94.12 1.75 o -2 -4 1 53.39 53.83 1.90 o -1 -4 1 153.81 156.43 1.84 o 0 -4 1 137.39 134.85 1.75 o 1 -4 1 1953.62 2011.46 5.10 o 2 -4 1 327.38 312.87 10.28 o 3 -4 1 405.94 364.32 7.03 o 4 -4 1 22.05 19.55 0.71 o 5 -4 1 113.79 119.32 2.51 o 6 -4 1 204.15 201.21 3.22 o 7 -4 1 11.93 15.51 2.02 o -6 -3 1 20.74 17.81 3.19 o -5 -3 1 17.25 19.30 2.07 o -4 -3 1 167.30 175.44 6.35 o -3 -3 1 181.87 186.38 2.11 o -2 -3 1 2.04 3.27 0.76 o -1 -3 1 103.45 89.19 1.69 o 0 -3 1 1606.92 1612.32 8.65 o 1 -3 1 425.31 406.68 8.06 o 2 -3 1 1400.10 1345.14 71.59 o 3 -3 1 57.20 48.26 1.33 o 4 -3 1 284.08 288.93 2.08 o 5 -3 1 480.42 494.25 2.97 o 6 -3 1 12.08 14.46 1.27 o -6 -2 1 2.00 3.21 1.33 o -5 -2 1 277.18 277.72 4.15 o -4 -2 1 279.13 286.43 3.81 o -3 -2 1 0.96 1.09 0.53 o -2 -2 1 358.48 350.76 8.98 o -1 -2 1 163.62 164.35 6.03 o 0 -2 1 6742.90 6491.47 37.76 o 1 -2 1 50.04 55.56 2.34 o 2 -2 1 809.70 771.30 17.50 o 3 -2 1 83.32 69.30 1.80 o 4 -2 1 284.66 289.18 2.05 o 5 -2 1 252.68 249.54 2.25 o 6 -2 1 20.85 19.47 1.22 o 7 -2 1 85.27 91.20 3.35 o -7 -1 1 17.87 20.16 3.31 o -6 -1 1 1.12 2.54 0.96 o -5 -1 1 106.70 105.93 1.83 o -4 -1 1 9.81 7.49 1.49 o -3 -1 1 94.94 88.07 2.76 o -2 -1 1 5729.89 6032.38 206.17 o -1 -1 1 2367.24 2405.33 27.75 o 0 -1 1 712.49 337.71 184.09 o 1 -1 1 14.03 11.95 0.89 o 2 -1 1 111.59 161.52 5.07 o 3 -1 1 112.82 101.75 1.15 o 4 -1 1 465.82 483.05 14.23 o 5 -1 1 244.13 255.10 5.35 o 6 -1 1 145.21 151.50 3.17 o 7 -1 1 82.97 94.61 3.64 o -7 0 1 46.62 52.02 2.20 o -6 0 1 225.60 221.14 3.38 o -5 0 1 95.55 92.62 1.77 o -4 0 1 23.23 16.78 0.89 o -3 0 1 393.36 391.37 2.18 o -2 0 1 7.94 8.79 0.71 o 1 0 1 2994.29 2990.57 63.57 o 2 0 1 257.64 248.86 5.10 o 3 0 1 220.84 213.22 3.95 o 4 0 1 90.84 87.61 1.82 o 5 0 1 60.36 61.90 1.95 o 6 0 1 37.38 35.32 2.10 o 7 0 1 52.62 49.47 3.20 o -7 1 1 5.71 6.14 1.26 o -6 1 1 272.47 249.09 3.85 o -5 1 1 116.03 126.25 1.87 o -4 1 1 159.97 145.57 1.87 o -3 1 1 1635.61 1657.40 4.02 o -2 1 1 10.93 8.16 0.75 o -1 1 1 1619.03 1602.60 36.19 o 0 1 1 1.86 2.62 0.19 o 1 1 1 98.48 118.24 0.92 o 2 1 1 515.19 519.35 23.90 o 3 1 1 1009.48 1033.57 48.47 o 4 1 1 390.80 426.08 4.41 o 5 1 1 75.98 82.96 2.73 o 6 1 1 40.16 43.76 2.88 o -8 2 1 49.54 54.92 3.81 o -7 2 1 92.17 90.06 2.89 o -6 2 1 152.42 151.50 2.10 o -5 2 1 177.66 173.34 2.11 o -4 2 1 448.93 448.29 5.27 o -3 2 1 516.53 539.55 3.57 o -2 2 1 638.53 604.37 6.22 o -1 2 1 82.08 67.26 0.60 o 0 2 1 23.83 35.65 0.48 o 1 2 1 350.58 331.02 3.68 o 2 2 1 752.31 748.66 21.89 o 3 2 1 102.71 92.53 2.17 o 4 2 1 352.36 375.87 4.38 o 5 2 1 21.34 21.00 2.18 o 6 2 1 63.70 65.64 2.95 o -8 3 1 50.94 51.61 2.31 o -7 3 1 137.09 129.16 2.36 o -6 3 1 31.64 33.24 1.45 o -5 3 1 114.94 114.09 3.63 o -4 3 1 337.49 344.93 17.92 o -3 3 1 194.28 179.48 9.29 o -2 3 1 713.03 724.98 4.07 o -1 3 1 653.49 652.45 9.96 o 0 3 1 271.52 273.45 1.69 o 1 3 1 327.58 327.11 6.10 o 2 3 1 162.92 163.66 1.98 o 3 3 1 62.98 62.57 2.11 o 4 3 1 162.79 168.12 3.51 o 5 3 1 6.66 8.86 2.30 o -8 4 1 45.87 43.51 3.24 o -7 4 1 26.51 26.19 2.58 o -6 4 1 37.28 39.35 1.35 o -5 4 1 88.61 89.63 3.66 o -4 4 1 107.78 113.09 2.43 o -3 4 1 354.74 294.22 39.06 o -2 4 1 634.30 619.99 4.11 o -1 4 1 212.30 204.50 1.19 o 0 4 1 222.26 215.05 1.86 o 1 4 1 189.37 183.85 2.52 o 2 4 1 112.70 116.36 1.92 o 3 4 1 384.35 412.38 4.71 o 4 4 1 3.21 1.72 1.22 o 5 4 1 8.50 8.12 2.30 o -7 5 1 163.18 166.10 3.43 o -6 5 1 204.88 209.66 3.75 o -5 5 1 5.57 7.30 1.66 o -4 5 1 35.40 34.35 1.59 o -3 5 1 61.45 65.29 1.93 o -2 5 1 279.05 298.05 2.72 o -1 5 1 115.40 114.88 1.13 o 0 5 1 341.39 347.86 3.16 o 1 5 1 453.94 450.68 9.88 o 2 5 1 65.58 67.24 1.88 o 3 5 1 38.60 32.92 2.47 o 4 5 1 23.66 15.94 2.73 o -7 6 1 19.52 17.18 2.64 o -6 6 1 9.44 9.25 2.22 o -5 6 1 76.17 76.38 2.88 o -4 6 1 698.17 721.16 6.12 o -3 6 1 248.47 247.64 3.70 o -2 6 1 45.07 46.49 1.28 o -1 6 1 8.27 8.88 0.79 o 0 6 1 42.16 42.31 1.04 o 1 6 1 63.95 64.60 4.22 o 2 6 1 85.70 86.77 2.17 o 3 6 1 9.71 11.48 2.59 o -6 7 1 5.01 5.77 2.15 o -5 7 1 194.35 192.50 4.13 o -4 7 1 83.52 86.52 2.85 o -3 7 1 86.32 79.90 2.60 o -2 7 1 87.97 92.16 2.83 o -1 7 1 126.74 132.36 2.28 o 0 7 1 73.03 67.74 2.73 o 1 7 1 2.91 4.44 1.21 o 2 7 1 16.70 14.47 2.50 o -5 8 1 106.08 97.61 3.52 o -4 8 1 5.93 4.99 1.91 o -3 8 1 118.13 116.36 3.46 o -2 8 1 48.66 52.29 3.34 o -1 8 1 24.10 19.12 2.45 o 0 8 1 36.85 41.43 3.42 o 1 -9 2 45.83 38.06 3.34 o 2 -9 2 47.88 50.30 3.57 o 3 -9 2 17.72 15.39 2.81 o 4 -9 2 44.17 44.14 4.03 o -1 -8 2 1.56 1.75 2.00 o 0 -8 2 70.46 75.08 3.34 o 1 -8 2 69.28 71.74 2.40 o 2 -8 2 55.00 51.13 2.16 o 3 -8 2 114.99 121.37 3.41 o 4 -8 2 48.06 50.79 3.28 o 5 -8 2 9.93 11.01 2.36 o -3 -7 2 32.45 29.88 3.86 o -2 -7 2 25.30 24.38 2.64 o -1 -7 2 35.14 35.29 2.63 o 0 -7 2 4.06 2.11 1.40 o 1 -7 2 27.46 28.82 4.07 o 2 -7 2 115.27 108.90 1.91 o 3 -7 2 432.17 446.82 26.32 o 4 -7 2 59.18 68.76 2.78 o 5 -7 2 113.57 123.27 3.20 o 6 -7 2 124.96 129.72 3.45 o -4 -6 2 10.61 8.72 1.66 o -3 -6 2 18.29 15.88 1.59 o -2 -6 2 26.17 28.10 1.37 o -1 -6 2 140.36 147.16 3.27 o 0 -6 2 77.35 83.03 1.75 o 1 -6 2 768.89 765.73 11.25 o 2 -6 2 95.94 95.99 3.02 o 3 -6 2 2.55 1.44 0.58 o 4 -6 2 3.86 5.58 0.89 o 5 -6 2 243.04 263.29 3.89 o 6 -6 2 152.10 149.58 3.29 o 7 -6 2 58.01 65.37 3.26 o -5 -5 2 24.51 22.99 3.14 o -4 -5 2 50.62 49.15 4.37 o -3 -5 2 22.71 23.22 3.09 o -2 -5 2 36.57 35.26 1.30 o -1 -5 2 80.20 77.61 1.41 o 0 -5 2 676.64 679.70 6.23 o 1 -5 2 376.63 376.63 7.43 o 2 -5 2 230.15 232.19 7.59 o 3 -5 2 34.31 34.40 1.07 o 4 -5 2 305.83 284.85 23.31 o 5 -5 2 97.47 98.78 2.41 o 6 -5 2 0.75 1.33 1.04 o -5 -4 2 71.29 69.03 3.04 o -4 -4 2 8.47 8.57 1.18 o -3 -4 2 5.02 6.41 0.99 o -2 -4 2 240.70 253.43 5.35 o -1 -4 2 43.13 44.77 1.40 o 0 -4 2 2575.11 2586.25 14.98 o 1 -4 2 41.06 43.48 3.26 o 2 -4 2 380.30 387.25 13.32 o 3 -4 2 280.00 261.78 9.89 o 4 -4 2 135.01 134.18 4.39 o 5 -4 2 75.39 76.96 1.51 o 6 -4 2 82.74 83.85 2.48 o -6 -3 2 22.64 20.52 2.65 o -5 -3 2 64.15 66.51 2.68 o -4 -3 2 51.52 51.30 1.60 o -3 -3 2 82.10 83.88 2.95 o -2 -3 2 497.42 516.15 19.70 o -1 -3 2 457.52 467.30 9.60 o 0 -3 2 679.27 704.34 5.62 o 1 -3 2 16.56 8.31 0.96 o 2 -3 2 94.80 76.09 1.49 o 3 -3 2 407.14 392.41 4.02 o 4 -3 2 290.70 300.99 2.00 o 5 -3 2 329.80 350.43 2.53 o -7 -2 2 1.75 3.48 1.48 o -6 -2 2 24.07 21.33 2.21 o -5 -2 2 96.41 100.57 2.95 o -4 -2 2 329.43 334.97 9.08 o -3 -2 2 492.92 535.42 8.88 o -2 -2 2 120.88 126.75 1.39 o -1 -2 2 2267.90 2341.82 22.51 o 0 -2 2 491.19 552.48 5.80 o 1 -2 2 32.82 29.02 2.81 o 2 -2 2 537.90 549.43 8.62 o 3 -2 2 489.72 504.14 3.35 o 4 -2 2 430.84 452.61 8.64 o 5 -2 2 320.93 320.79 4.06 o 6 -2 2 21.96 20.01 1.89 o 7 -2 2 39.76 37.47 2.62 o -7 -1 2 9.04 8.37 1.61 o -6 -1 2 141.42 130.31 2.41 o -5 -1 2 24.91 24.91 1.77 o -4 -1 2 13.84 15.38 0.92 o -3 -1 2 591.58 634.49 10.71 o -2 -1 2 1474.26 1554.05 51.98 o -1 -1 2 3216.36 3262.36 17.54 o 0 -1 2 99.69 83.17 1.66 o 1 -1 2 255.93 267.20 2.63 o 2 -1 2 30.35 22.93 0.54 o 3 -1 2 48.24 45.36 2.55 o 4 -1 2 361.83 357.13 12.54 o 5 -1 2 164.94 156.86 2.74 o 6 -1 2 175.43 183.58 3.40 o 7 -1 2 16.98 13.99 2.88 o -7 0 2 71.47 65.26 2.09 o -6 0 2 168.39 168.20 4.33 o -5 0 2 135.83 141.82 2.86 o -4 0 2 159.40 163.37 1.87 o -3 0 2 488.90 503.69 10.89 o -2 0 2 58.16 56.23 1.23 o -1 0 2 484.39 523.96 6.47 o 0 0 2 733.19 756.89 13.23 o 1 0 2 3137.26 3019.48 82.02 o 2 0 2 1047.97 1034.41 19.02 o 3 0 2 430.37 417.05 5.77 o 4 0 2 584.42 574.78 36.47 o 5 0 2 42.20 34.88 1.99 o 6 0 2 25.68 30.63 2.54 o 7 0 2 1.93 4.20 2.84 o -7 1 2 100.30 94.52 4.70 o -6 1 2 60.26 66.70 1.77 o -5 1 2 100.88 97.24 2.15 o -4 1 2 434.56 443.34 6.69 o -3 1 2 228.36 228.97 5.83 o -2 1 2 38.98 28.54 0.66 o -1 1 2 1428.49 1353.34 46.39 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8 238.40 250.40 3.88 o 0 2 8 60.04 56.91 2.49 o 1 2 8 85.44 87.75 2.53 o 2 2 8 15.94 17.17 1.55 o -6 3 8 84.14 83.74 3.64 o -5 3 8 80.02 76.19 2.14 o -4 3 8 2.20 3.44 1.42 o -3 3 8 21.03 25.54 2.15 o -2 3 8 0.66 1.20 1.35 o -1 3 8 193.53 205.41 3.73 o 0 3 8 217.40 238.31 4.24 o 1 3 8 87.96 94.70 2.89 o -5 4 8 53.32 50.58 2.32 o -4 4 8 65.63 72.69 3.18 o -3 4 8 63.14 72.21 3.41 o -2 4 8 93.60 91.24 2.91 o -1 4 8 41.76 40.42 2.89 o 0 4 8 5.06 5.82 1.96 o -4 5 8 90.59 95.34 4.03 o -3 5 8 63.75 59.14 3.01 o -2 5 8 41.80 42.59 3.46 o -2 -7 9 34.68 32.90 3.18 o -1 -7 9 28.72 26.70 2.75 o 0 -7 9 28.53 28.34 3.23 o 1 -7 9 33.25 33.45 2.18 o 2 -7 9 36.19 38.54 2.50 o 3 -7 9 7.76 8.04 1.92 o -3 -6 9 19.65 17.07 2.38 o -2 -6 9 34.55 28.36 2.71 o -1 -6 9 25.30 24.46 2.41 o 0 -6 9 59.41 59.43 2.07 o 1 -6 9 32.60 35.10 1.94 o 2 -6 9 17.32 18.12 2.13 o 3 -6 9 64.79 64.82 3.05 o -3 -5 9 9.12 5.69 1.66 o -2 -5 9 24.41 27.43 2.24 o -1 -5 9 132.29 141.45 3.13 o 0 -5 9 22.12 21.66 1.43 o 1 -5 9 39.54 40.03 1.63 o 2 -5 9 10.38 10.34 1.48 o 3 -5 9 137.09 134.03 2.53 o 4 -5 9 19.63 20.86 1.96 o -3 -4 9 132.24 130.93 3.09 o -2 -4 9 104.22 110.73 2.69 o -1 -4 9 47.75 52.42 1.63 o 0 -4 9 73.80 64.58 1.78 o 1 -4 9 42.71 46.07 1.60 o 2 -4 9 126.03 125.10 2.15 o 3 -4 9 131.10 123.19 2.45 o 4 -4 9 41.33 33.87 2.07 o -5 -3 9 1.75 3.54 2.03 o -4 -3 9 24.60 23.52 2.42 o -3 -3 9 73.56 70.31 2.65 o -2 -3 9 105.73 102.84 4.61 o -1 -3 9 25.30 23.22 1.18 o 0 -3 9 164.24 166.14 2.25 o 1 -3 9 84.39 86.85 5.13 o 2 -3 9 69.23 72.40 2.04 o 3 -3 9 0.66 1.07 0.95 o 4 -3 9 14.10 13.61 1.91 o -6 -2 9 5.44 6.01 1.59 o -5 -2 9 62.04 52.74 2.12 o -4 -2 9 68.79 69.16 2.87 o -2 -2 9 63.46 61.07 1.42 o -1 -2 9 26.35 21.82 1.20 o 0 -2 9 314.81 330.21 4.39 o 1 -2 9 96.13 94.83 2.74 o 2 -2 9 171.51 163.67 5.80 o 3 -2 9 97.27 101.71 3.04 o 4 -2 9 17.89 19.05 2.38 o -6 -1 9 6.81 5.90 1.80 o -5 -1 9 55.61 47.50 1.96 o -4 -1 9 75.83 78.13 3.08 o -3 -1 9 22.29 23.77 1.23 o -2 -1 9 19.58 16.84 1.31 o -1 -1 9 20.92 20.49 1.27 o 0 -1 9 142.22 142.24 5.65 o 1 -1 9 166.15 169.87 3.43 o 2 -1 9 100.45 95.46 3.08 o 3 -1 9 45.46 49.37 3.02 o -6 0 9 11.58 11.08 1.78 o -5 0 9 41.71 42.83 2.82 o -4 0 9 39.29 40.54 2.41 o -3 0 9 90.78 91.76 2.29 o -2 0 9 4.94 6.07 1.48 o -1 0 9 351.91 377.66 4.58 o 0 0 9 76.76 80.84 2.52 o 1 0 9 50.45 54.85 2.59 o 2 0 9 19.95 24.11 1.61 o 3 0 9 15.44 16.27 1.87 o -6 1 9 35.28 32.19 3.38 o -5 1 9 109.74 100.95 3.29 o -4 1 9 20.73 23.73 1.32 o -3 1 9 81.21 92.77 3.19 o -2 1 9 54.38 53.84 2.54 o -1 1 9 152.95 159.93 3.26 o 0 1 9 49.69 52.66 2.48 o 1 1 9 66.12 66.16 2.81 o 2 1 9 42.39 37.78 2.57 o -6 2 9 26.16 24.54 2.71 o -5 2 9 0.99 1.44 0.95 o -4 2 9 6.00 6.86 1.60 o -3 2 9 101.80 105.49 3.16 o -2 2 9 233.25 243.05 4.09 o -1 2 9 105.70 111.79 3.02 o 0 2 9 62.31 62.28 2.93 o 1 2 9 32.15 30.91 3.00 o -5 3 9 50.07 52.28 2.94 o -4 3 9 103.03 100.14 3.14 o -3 3 9 21.13 24.11 2.49 o -2 3 9 0.86 0.67 1.00 o -1 3 9 26.62 28.34 2.52 o 0 3 9 90.60 86.82 3.24 o -4 4 9 50.59 45.67 3.20 o -3 4 9 13.53 14.01 2.52 o -2 4 9 44.12 41.45 2.70 o -1 -7 10 35.00 28.37 3.16 o 0 -7 10 0.23 1.31 2.36 o 1 -7 10 32.47 33.80 2.28 o -2 -6 10 27.35 26.47 3.07 o -1 -6 10 11.56 12.85 2.38 o 0 -6 10 0.51 1.82 1.16 o 1 -6 10 57.51 58.13 4.30 o 2 -6 10 24.69 24.39 1.94 o -3 -5 10 16.92 14.29 2.21 o -2 -5 10 1.65 2.29 1.78 o -1 -5 10 1.56 0.72 1.31 o 0 -5 10 69.77 71.64 2.25 o 1 -5 10 42.93 43.23 3.05 o 2 -5 10 108.09 102.30 3.96 o 3 -5 10 46.05 42.31 2.44 o -2 -4 10 96.91 101.40 2.89 o -1 -4 10 0.37 1.10 0.92 o 0 -4 10 65.15 68.25 1.93 o 1 -4 10 1.43 2.65 1.19 o 2 -4 10 72.69 71.89 2.24 o 3 -4 10 42.21 48.09 2.18 o -5 -3 10 14.78 14.58 2.96 o -4 -3 10 15.81 15.53 2.52 o -2 -3 10 16.83 16.66 1.45 o -1 -3 10 66.28 61.59 1.77 o 0 -3 10 195.54 198.67 4.04 o 1 -3 10 199.59 195.88 3.44 o 2 -3 10 37.10 38.69 1.80 o 3 -3 10 0.46 1.04 1.16 o -5 -2 10 52.74 45.31 2.23 o -4 -2 10 9.64 8.53 2.22 o -2 -2 10 2.47 3.23 1.15 o -1 -2 10 186.72 196.07 2.34 o 0 -2 10 70.26 70.81 1.94 o 1 -2 10 84.26 80.78 4.53 o 2 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54.11 53.29 2.28 o 1 -5 11 51.65 49.29 2.24 o -1 -4 11 184.72 187.77 3.08 o 0 -4 11 24.88 25.36 1.95 o 1 -4 11 3.95 4.83 1.34 o 2 -4 11 2.76 6.13 1.98 o -2 -3 11 20.40 18.10 2.19 o -1 -3 11 55.31 50.66 1.88 o 0 -3 11 47.89 46.54 2.05 o 1 -3 11 92.24 90.97 4.37 o 2 -3 11 33.59 30.26 2.18 o -2 -2 11 14.48 14.91 1.91 o -1 -2 11 32.46 36.63 2.58 o 0 -2 11 50.95 50.84 1.98 o 1 -2 11 34.28 29.75 2.24 o -3 -1 11 27.71 30.56 2.96 o -2 -1 11 30.65 30.03 2.86 o -1 -1 11 59.29 62.47 2.68 o 0 -1 11 11.74 13.00 2.50 o 1 -1 11 0.39 1.07 1.32 o -3 0 11 9.27 7.25 1.87 o -2 0 11 35.14 36.24 2.64 o -1 0 11 30.97 32.92 2.94 o 0 0 11 28.30 23.74 2.51 o -4 1 11 37.68 33.73 3.36 o -3 1 11 16.27 19.94 3.13 o -2 1 11 133.92 139.07 3.72 o -1 1 11 35.03 32.53 3.31 o -1 -4 12 75.20 71.18 2.35 o -1 -3 12 37.52 39.14 3.59 o 0 -3 12 13.22 11.24 1.84 o -2 -2 12 22.46 25.49 2.92 o -1 -2 12 10.58 12.35 2.44 o 0 -2 12 9.99 8.85 2.22 o -2 -1 12 103.70 110.60 4.35 o -1 -1 12 24.86 23.39 2.44 o