#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2205986.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205986_Fobs loop_ _publ_author_name 'Ngah, Nurziana' 'Shah, Nabihah M.' 'Kassim, Mohammad B.' 'Yamin, Bohari M.' _publ_section_title ; (2S)-2-(3-Benzoylthioureido)-3-methylbutyric acid ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1767 _journal_page_last o1768 _journal_volume 61 _journal_year 2005 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.2223 _cell_length_b 11.7813 _cell_length_c 22.7383 _exptl_crystal_F_000 592.00 _reflns_d_resolution_high 0.7965 _[local]_cod_data_source_file is6074Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bob313m in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 102.05 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6376.31 6842.36 105.02 o 4 0 0 78.57 69.90 3.40 o 1 1 0 430.05 414.28 5.10 o 2 1 0 1008.55 1071.91 12.71 o 3 1 0 417.91 409.34 7.36 o 4 1 0 85.59 76.65 3.48 o 5 1 0 115.84 111.66 5.00 o 6 1 0 2.37 4.53 2.34 o 0 2 0 855.70 913.85 8.67 o 1 2 0 175.03 208.89 4.61 o 2 2 0 312.29 284.33 5.53 o 3 2 0 698.54 821.41 15.57 o 4 2 0 69.83 74.09 1.98 o 5 2 0 265.81 281.07 7.37 o 6 2 0 1.57 -2.78 1.85 o 1 3 0 714.01 766.65 5.87 o 2 3 0 352.85 378.84 4.31 o 3 3 0 137.38 147.99 2.53 o 4 3 0 29.23 27.50 1.31 o 5 3 0 19.98 20.80 2.71 o 6 3 0 9.22 15.56 3.08 o 0 4 0 1723.59 1972.99 18.38 o 1 4 0 385.54 351.09 3.33 o 2 4 0 401.75 414.78 3.99 o 3 4 0 69.76 63.35 1.62 o 4 4 0 5.84 4.31 1.41 o 5 4 0 8.01 8.49 1.54 o 6 4 0 4.37 4.91 1.54 o 1 5 0 3766.89 4203.81 28.03 o 2 5 0 219.02 224.69 2.57 o 3 5 0 181.33 177.56 2.68 o 4 5 0 4.74 7.30 1.45 o 5 5 0 29.99 26.10 2.31 o 6 5 0 0.00 1.36 1.81 o 0 6 0 13.11 12.16 0.82 o 1 6 0 256.18 281.68 2.63 o 2 6 0 368.87 352.41 3.54 o 3 6 0 53.48 54.29 1.77 o 4 6 0 179.78 174.64 4.88 o 5 6 0 13.20 13.81 2.00 o 1 7 0 541.13 517.22 4.30 o 2 7 0 272.41 277.44 11.20 o 3 7 0 168.71 172.32 4.64 o 4 7 0 158.15 142.70 4.48 o 5 7 0 6.80 6.25 1.57 o 0 8 0 93.45 95.31 3.36 o 1 8 0 331.09 356.61 3.39 o 2 8 0 162.06 165.65 2.72 o 3 8 0 127.49 130.94 4.03 o 4 8 0 17.61 12.04 1.66 o 5 8 0 38.96 41.35 2.79 o 1 9 0 230.30 225.53 3.41 o 2 9 0 4.00 4.73 0.96 o 3 9 0 55.50 57.94 2.79 o 4 9 0 23.22 24.61 2.11 o 5 9 0 10.06 14.11 1.92 o 0 10 0 508.08 543.55 6.95 o 1 10 0 43.23 37.86 1.23 o 2 10 0 9.66 12.59 1.23 o 3 10 0 96.69 81.54 3.37 o 4 10 0 80.35 82.98 3.67 o 1 11 0 63.93 67.23 2.26 o 2 11 0 53.00 46.68 2.03 o 3 11 0 11.30 13.93 2.35 o 4 11 0 5.40 2.49 1.30 o 0 12 0 0.90 5.58 3.07 o 1 12 0 79.51 85.77 2.64 o 2 12 0 8.75 9.50 1.23 o 3 12 0 2.50 3.91 1.31 o 1 13 0 174.55 183.70 5.02 o 2 13 0 15.51 20.67 1.58 o 3 13 0 2.75 4.41 1.41 o 1 14 0 10.41 16.63 2.54 o 2 14 0 0.03 1.92 1.35 o 1 0 1 3066.56 3257.18 35.68 o 2 0 1 244.74 255.47 6.34 o 3 0 1 782.48 872.66 21.50 o 4 0 1 16.65 20.59 1.96 o 5 0 1 12.84 9.96 1.50 o 0 1 1 1359.36 1485.59 13.84 o 1 1 1 1540.65 1599.30 11.20 o 2 1 1 488.55 541.25 6.52 o 3 1 1 156.50 174.40 2.54 o 4 1 1 223.37 209.23 9.22 o 5 1 1 62.98 67.67 2.19 o 6 1 1 137.04 133.83 4.24 o 0 2 1 479.72 484.32 3.39 o 1 2 1 10414.67 11143.28 61.16 o 2 2 1 1273.56 1340.07 11.48 o 3 2 1 94.65 109.27 1.65 o 4 2 1 154.36 155.16 2.51 o 5 2 1 145.35 148.99 3.97 o 6 2 1 2.26 0.51 2.21 o 0 3 1 455.43 503.93 3.63 o 1 3 1 4133.51 4495.79 28.98 o 2 3 1 226.98 216.76 1.97 o 3 3 1 262.33 254.39 2.52 o 4 3 1 11.31 12.82 0.74 o 5 3 1 16.65 20.26 1.30 o 6 3 1 1.82 2.91 1.37 o 0 4 1 2422.08 2606.68 16.97 o 1 4 1 222.14 225.38 1.50 o 2 4 1 768.68 913.35 6.94 o 3 4 1 704.49 758.98 5.44 o 4 4 1 196.43 194.20 3.76 o 5 4 1 71.24 77.31 2.66 o 6 4 1 1.70 1.93 1.12 o 0 5 1 232.50 238.64 2.20 o 1 5 1 533.13 587.21 3.36 o 2 5 1 762.62 772.93 4.85 o 3 5 1 7.15 6.87 0.58 o 4 5 1 274.54 279.71 3.73 o 5 5 1 6.88 6.91 1.06 o 6 5 1 31.20 33.49 1.81 o 0 6 1 1014.88 1013.81 7.27 o 1 6 1 148.04 137.97 1.17 o 2 6 1 516.91 493.35 3.21 o 3 6 1 32.90 30.39 1.13 o 4 6 1 51.16 44.94 1.79 o 5 6 1 134.04 129.89 3.19 o 0 7 1 63.95 74.27 1.22 o 1 7 1 283.94 252.62 1.81 o 2 7 1 22.72 27.29 1.37 o 3 7 1 131.36 118.26 2.19 o 4 7 1 60.61 50.87 1.95 o 5 7 1 7.77 6.28 1.10 o 0 8 1 468.28 478.11 4.17 o 1 8 1 44.72 38.32 0.69 o 2 8 1 186.47 177.79 2.37 o 3 8 1 37.55 33.93 1.34 o 4 8 1 23.56 20.52 1.38 o 5 8 1 6.80 6.35 1.42 o 0 9 1 2.31 2.12 0.58 o 1 9 1 33.84 32.47 0.74 o 2 9 1 39.66 39.34 1.09 o 3 9 1 93.44 78.16 2.00 o 4 9 1 10.73 12.29 1.21 o 5 9 1 4.05 4.31 1.08 o 0 10 1 65.80 67.92 2.51 o 1 10 1 25.48 24.17 0.84 o 2 10 1 21.68 21.72 1.03 o 3 10 1 12.90 16.34 1.11 o 4 10 1 3.78 2.79 0.97 o 0 11 1 482.02 529.15 6.18 o 1 11 1 78.36 73.99 1.52 o 2 11 1 15.99 16.11 0.96 o 3 11 1 6.44 4.64 0.83 o 4 11 1 11.28 11.30 1.22 o 0 12 1 328.57 357.12 5.79 o 1 12 1 158.99 160.28 2.83 o 2 12 1 37.32 42.85 1.42 o 3 12 1 39.85 38.07 1.58 o 1 13 1 98.23 109.72 2.71 o 2 13 1 17.68 17.86 1.08 o 3 13 1 27.68 30.57 1.85 o 1 14 1 36.14 40.28 2.42 o 2 14 1 3.73 7.62 1.10 o 0 0 2 5398.01 5694.03 64.63 o 1 0 2 6347.76 6639.92 60.65 o 2 0 2 340.20 333.69 4.79 o 3 0 2 0.33 -0.48 0.84 o 4 0 2 91.15 83.99 3.61 o 5 0 2 39.80 40.89 2.28 o 6 0 2 0.15 1.01 1.76 o 0 1 2 4231.83 4345.76 39.81 o 1 1 2 1798.96 2042.89 13.16 o 2 1 2 141.11 163.78 2.03 o 3 1 2 126.86 121.64 2.48 o 4 1 2 112.77 102.40 3.33 o 5 1 2 31.69 34.99 1.74 o 6 1 2 26.05 32.12 2.11 o 0 2 2 9.80 10.87 0.53 o 1 2 2 2844.43 3026.43 24.26 o 2 2 2 31.22 37.75 0.75 o 3 2 2 253.69 252.35 2.78 o 4 2 2 8.10 6.76 0.72 o 5 2 2 306.68 305.06 4.38 o 6 2 2 17.24 17.06 1.95 o 0 3 2 3720.84 4136.79 26.51 o 1 3 2 1466.81 1564.31 9.53 o 2 3 2 2569.73 2900.94 17.44 o 3 3 2 374.87 372.93 3.11 o 4 3 2 305.49 310.81 3.65 o 5 3 2 15.08 14.63 1.16 o 6 3 2 23.52 25.05 2.68 o 0 4 2 713.31 674.87 4.86 o 1 4 2 719.89 767.24 4.21 o 2 4 2 181.56 196.06 2.35 o 3 4 2 105.14 106.31 1.40 o 4 4 2 33.11 35.09 1.21 o 5 4 2 6.47 6.74 1.20 o 6 4 2 1.23 1.97 1.01 o 0 5 2 57.86 45.58 0.82 o 1 5 2 1978.92 2168.49 10.52 o 2 5 2 28.09 27.59 0.64 o 3 5 2 35.67 33.02 0.94 o 4 5 2 62.70 61.21 1.86 o 5 5 2 5.03 2.68 0.92 o 6 5 2 2.46 4.18 1.07 o 0 6 2 118.76 99.24 1.34 o 1 6 2 1079.09 1209.51 6.06 o 2 6 2 298.99 282.68 2.45 o 3 6 2 76.73 70.76 2.32 o 4 6 2 194.76 183.46 3.53 o 5 6 2 20.40 20.15 1.45 o 0 7 2 19.21 21.39 0.71 o 1 7 2 276.93 263.70 2.11 o 2 7 2 70.60 67.75 1.29 o 3 7 2 94.64 87.71 1.72 o 4 7 2 63.18 64.47 2.15 o 5 7 2 1.67 0.10 0.91 o 0 8 2 146.16 152.80 1.96 o 1 8 2 126.43 123.95 1.30 o 2 8 2 69.20 65.18 1.31 o 3 8 2 94.01 82.09 1.97 o 4 8 2 51.30 52.20 2.00 o 5 8 2 27.19 28.43 1.67 o 0 9 2 28.49 24.72 0.88 o 1 9 2 588.69 576.50 3.71 o 2 9 2 124.50 122.37 1.88 o 3 9 2 113.84 104.98 2.32 o 4 9 2 45.49 42.12 1.87 o 5 9 2 5.35 7.59 1.20 o 0 10 2 523.99 508.23 10.03 o 1 10 2 28.41 32.53 0.94 o 2 10 2 187.50 179.95 2.67 o 3 10 2 13.05 12.45 1.02 o 4 10 2 57.70 59.41 2.23 o 0 11 2 213.12 219.84 3.72 o 1 11 2 116.55 112.38 2.14 o 2 11 2 16.45 16.29 0.97 o 3 11 2 26.25 25.60 1.29 o 4 11 2 3.91 4.41 1.02 o 0 12 2 125.21 135.16 8.73 o 1 12 2 17.43 20.09 1.18 o 2 12 2 20.39 19.72 1.07 o 3 12 2 5.22 6.92 0.94 o 0 13 2 78.85 93.94 4.03 o 1 13 2 92.69 95.77 3.00 o 2 13 2 4.53 7.28 0.94 o 3 13 2 1.34 2.56 0.89 o 1 14 2 3.60 6.37 1.41 o 2 14 2 10.96 15.03 1.33 o 1 0 3 823.89 940.30 9.38 o 2 0 3 9.46 9.16 0.78 o 3 0 3 769.30 759.85 20.55 o 4 0 3 20.26 20.56 1.50 o 5 0 3 129.11 131.80 3.76 o 0 1 3 1274.62 1290.80 10.38 o 1 1 3 7287.30 7753.06 42.99 o 2 1 3 368.70 378.17 6.55 o 3 1 3 74.14 62.16 1.27 o 4 1 3 160.19 168.69 4.90 o 5 1 3 126.12 132.93 2.69 o 6 1 3 29.47 27.73 2.01 o 0 2 3 4949.43 5414.89 47.38 o 1 2 3 3242.71 3472.13 20.52 o 2 2 3 682.03 673.59 5.04 o 3 2 3 22.50 23.96 0.94 o 4 2 3 45.24 43.97 1.15 o 5 2 3 9.51 14.77 1.65 o 6 2 3 11.34 8.97 1.64 o 0 3 3 3172.16 3515.10 24.52 o 1 3 3 4781.78 5256.74 44.44 o 2 3 3 728.73 770.47 4.84 o 3 3 3 1118.37 1169.78 7.78 o 4 3 3 264.66 258.19 3.31 o 5 3 3 41.74 40.76 1.65 o 6 3 3 1.51 1.59 1.96 o 0 4 3 3472.40 3731.84 27.74 o 1 4 3 341.38 365.98 3.52 o 2 4 3 1730.93 1802.10 10.44 o 3 4 3 48.36 43.15 1.14 o 4 4 3 24.84 25.47 1.11 o 5 4 3 39.14 42.61 1.72 o 6 4 3 2.00 1.42 1.53 o 0 5 3 759.31 802.25 5.81 o 1 5 3 119.69 135.90 1.11 o 2 5 3 626.19 643.35 5.31 o 3 5 3 17.07 18.43 0.79 o 4 5 3 203.94 197.62 3.40 o 5 5 3 53.93 57.13 2.40 o 6 5 3 38.66 40.47 1.92 o 0 6 3 148.63 153.62 1.75 o 1 6 3 754.30 826.49 4.35 o 2 6 3 381.80 393.88 4.42 o 3 6 3 95.80 95.52 2.01 o 4 6 3 99.94 94.82 2.13 o 5 6 3 52.80 51.25 2.02 o 0 7 3 4.85 5.61 0.60 o 1 7 3 704.20 710.50 3.92 o 2 7 3 108.24 115.51 1.65 o 3 7 3 46.81 43.94 1.25 o 4 7 3 13.25 10.82 1.12 o 5 7 3 12.18 12.02 1.23 o 0 8 3 885.62 932.40 7.09 o 1 8 3 77.06 79.10 1.44 o 2 8 3 38.33 37.43 1.00 o 3 8 3 15.54 14.98 0.89 o 4 8 3 25.02 25.46 1.51 o 5 8 3 4.37 5.14 1.07 o 0 9 3 4.85 3.07 0.65 o 1 9 3 35.52 37.45 0.91 o 2 9 3 7.30 7.04 0.75 o 3 9 3 187.61 167.02 2.96 o 4 9 3 13.66 11.04 1.17 o 5 9 3 8.39 7.60 1.18 o 0 10 3 35.49 40.09 1.51 o 1 10 3 41.22 39.08 1.03 o 2 10 3 25.60 25.83 1.29 o 3 10 3 37.24 37.33 1.49 o 4 10 3 23.58 26.20 1.60 o 0 11 3 237.14 251.20 9.49 o 1 11 3 101.39 97.30 1.69 o 2 11 3 55.88 58.03 1.73 o 3 11 3 20.53 19.70 1.21 o 4 11 3 48.76 53.48 2.18 o 0 12 3 42.71 43.70 2.42 o 1 12 3 5.38 9.46 0.83 o 2 12 3 56.82 55.87 1.78 o 3 12 3 36.44 37.08 1.56 o 0 13 3 15.48 16.23 2.47 o 1 13 3 42.39 52.34 1.94 o 2 13 3 1.75 1.83 0.88 o 3 13 3 24.75 25.77 1.42 o 1 14 3 0.63 0.17 1.19 o 2 14 3 43.45 49.24 2.06 o 0 0 4 8553.20 8607.14 94.05 o 1 0 4 243.81 202.52 4.67 o 2 0 4 2631.34 2768.97 25.81 o 3 0 4 389.64 347.26 4.56 o 4 0 4 54.42 56.15 1.79 o 5 0 4 205.20 203.32 5.49 o 6 0 4 69.55 71.12 2.98 o 0 1 4 652.52 644.49 5.34 o 1 1 4 5450.97 5809.56 36.92 o 2 1 4 137.52 141.00 1.97 o 3 1 4 291.36 287.90 3.52 o 4 1 4 112.39 113.41 1.98 o 5 1 4 202.80 213.98 4.60 o 6 1 4 29.86 36.65 5.20 o 0 2 4 11.23 9.26 0.45 o 1 2 4 1387.06 1377.18 16.16 o 2 2 4 246.95 219.74 2.29 o 3 2 4 1572.38 1693.41 11.76 o 4 2 4 0.73 0.92 0.64 o 5 2 4 94.53 94.28 2.06 o 6 2 4 15.33 14.93 1.92 o 0 3 4 3996.94 4166.16 32.63 o 1 3 4 736.94 765.28 5.50 o 2 3 4 659.96 712.88 4.53 o 3 3 4 36.83 33.10 1.19 o 4 3 4 499.77 502.85 5.19 o 5 3 4 9.14 9.28 1.22 o 6 3 4 47.37 46.11 2.78 o 0 4 4 1001.82 1020.96 7.08 o 1 4 4 265.23 258.02 2.17 o 2 4 4 214.86 231.76 2.14 o 3 4 4 144.74 134.49 4.65 o 4 4 4 54.30 55.24 1.66 o 5 4 4 36.14 34.50 1.57 o 6 4 4 3.45 0.91 1.37 o 0 5 4 733.74 805.74 5.86 o 1 5 4 28.76 34.59 0.73 o 2 5 4 114.23 125.30 1.49 o 3 5 4 143.69 142.47 2.21 o 4 5 4 91.61 89.74 1.97 o 5 5 4 56.94 54.16 3.23 o 6 5 4 6.35 9.56 1.39 o 0 6 4 1667.89 1684.89 11.53 o 1 6 4 275.74 307.42 2.12 o 2 6 4 244.59 223.31 2.65 o 3 6 4 41.04 37.67 1.08 o 4 6 4 29.25 30.64 1.46 o 5 6 4 26.06 29.05 2.27 o 0 7 4 946.88 1016.21 7.49 o 1 7 4 443.54 446.00 2.89 o 2 7 4 253.02 235.47 3.01 o 3 7 4 42.08 35.33 1.38 o 4 7 4 93.37 99.37 2.61 o 5 7 4 1.63 1.44 1.14 o 0 8 4 13.05 14.04 0.73 o 1 8 4 73.38 74.85 1.15 o 2 8 4 43.89 49.80 1.15 o 3 8 4 211.33 194.00 2.77 o 4 8 4 1.37 -0.69 0.82 o 5 8 4 59.81 63.35 2.36 o 0 9 4 20.59 20.28 0.93 o 1 9 4 180.62 172.34 1.91 o 2 9 4 218.55 204.42 2.76 o 3 9 4 42.70 38.58 1.48 o 4 9 4 157.15 139.10 3.60 o 5 9 4 5.03 4.46 1.13 o 0 10 4 34.21 31.14 1.17 o 1 10 4 66.03 62.81 1.18 o 2 10 4 216.13 207.04 2.88 o 3 10 4 24.63 23.32 1.25 o 4 10 4 7.99 8.00 1.13 o 0 11 4 609.19 611.77 15.99 o 1 11 4 80.59 82.44 1.62 o 2 11 4 46.62 38.38 1.46 o 3 11 4 34.59 35.35 1.93 o 4 11 4 1.22 1.08 0.94 o 0 12 4 84.91 85.15 3.25 o 1 12 4 7.62 7.85 1.32 o 2 12 4 1.60 4.49 0.96 o 3 12 4 31.10 32.45 1.49 o 0 13 4 1.28 1.20 2.63 o 1 13 4 51.87 53.30 3.38 o 2 13 4 12.59 13.79 1.22 o 0 14 4 3.41 8.02 3.29 o 1 14 4 3.80 4.39 1.41 o 1 0 5 510.32 508.71 7.74 o 2 0 5 1837.17 2029.42 19.25 o 3 0 5 1.96 2.79 0.69 o 4 0 5 136.04 133.99 2.76 o 5 0 5 76.23 78.47 4.16 o 6 0 5 0.10 2.32 1.31 o 0 1 5 3175.57 3449.92 26.45 o 1 1 5 1715.35 1752.11 14.64 o 2 1 5 286.25 276.73 3.81 o 3 1 5 413.58 403.65 4.00 o 4 1 5 216.32 215.27 2.60 o 5 1 5 24.85 24.69 1.54 o 6 1 5 0.10 -0.04 0.93 o 0 2 5 1075.03 1152.63 10.76 o 1 2 5 2353.22 2543.13 20.32 o 2 2 5 352.16 344.80 3.93 o 3 2 5 856.86 864.04 9.01 o 4 2 5 76.33 70.72 2.25 o 5 2 5 14.01 13.69 1.52 o 6 2 5 5.80 6.55 1.91 o 0 3 5 1212.42 1276.94 10.58 o 1 3 5 1510.17 1533.12 15.80 o 2 3 5 333.33 368.31 3.59 o 3 3 5 261.22 264.67 3.80 o 4 3 5 361.51 361.74 4.17 o 5 3 5 8.59 9.65 1.24 o 6 3 5 16.37 15.94 1.85 o 0 4 5 1837.22 2022.97 19.21 o 1 4 5 677.84 723.19 4.56 o 2 4 5 1995.02 2100.31 12.99 o 3 4 5 30.75 26.61 0.91 o 4 4 5 8.83 10.46 0.88 o 5 4 5 28.70 27.08 1.44 o 6 4 5 7.33 6.57 2.06 o 0 5 5 39.19 31.92 0.71 o 1 5 5 251.90 270.80 3.41 o 2 5 5 18.46 16.11 0.74 o 3 5 5 179.69 178.41 2.41 o 4 5 5 109.73 110.84 2.17 o 5 5 5 67.22 64.57 2.10 o 6 5 5 25.52 27.84 2.32 o 0 6 5 554.50 545.89 4.37 o 1 6 5 635.10 653.10 4.97 o 2 6 5 327.93 304.04 3.37 o 3 6 5 308.46 290.16 7.14 o 4 6 5 71.48 72.78 2.10 o 5 6 5 20.93 22.78 1.89 o 0 7 5 1580.49 1665.65 11.59 o 1 7 5 379.33 353.98 2.70 o 2 7 5 0.91 1.48 0.50 o 3 7 5 92.04 81.23 1.62 o 4 7 5 15.86 14.63 1.16 o 5 7 5 16.58 18.80 2.19 o 0 8 5 117.90 112.62 1.66 o 1 8 5 41.81 41.34 0.89 o 2 8 5 63.77 57.72 1.26 o 3 8 5 57.54 49.85 1.42 o 4 8 5 60.98 60.81 2.17 o 5 8 5 0.77 2.16 1.01 o 0 9 5 1.75 2.27 0.72 o 1 9 5 946.29 942.57 7.65 o 2 9 5 0.15 -0.14 0.58 o 3 9 5 54.64 59.17 1.57 o 4 9 5 16.95 20.08 1.45 o 5 9 5 11.52 12.82 1.39 o 0 10 5 35.92 31.94 1.47 o 1 10 5 3.78 4.31 0.57 o 2 10 5 9.49 9.09 0.83 o 3 10 5 43.72 43.02 1.59 o 4 10 5 4.02 2.76 0.96 o 0 11 5 67.41 62.04 2.25 o 1 11 5 21.68 25.28 1.01 o 2 11 5 26.68 20.83 1.05 o 3 11 5 27.80 32.08 1.44 o 4 11 5 17.69 15.45 1.39 o 0 12 5 0.09 -0.09 0.95 o 1 12 5 74.02 79.16 2.37 o 2 12 5 90.64 92.30 2.58 o 3 12 5 7.56 9.08 1.01 o 0 13 5 74.30 75.28 3.64 o 1 13 5 125.78 126.07 4.49 o 2 13 5 23.70 28.36 1.59 o 0 14 5 26.90 36.46 2.53 o 1 14 5 5.01 8.70 3.84 o 0 0 6 302.02 354.35 4.59 o 1 0 6 2154.18 2368.95 16.74 o 2 0 6 2570.62 2723.31 21.75 o 3 0 6 645.99 682.24 14.98 o 4 0 6 0.98 0.54 0.97 o 5 0 6 7.69 10.77 1.39 o 6 0 6 1.32 3.31 1.20 o 0 1 6 1669.37 1822.19 14.26 o 1 1 6 387.58 381.81 3.74 o 2 1 6 1275.46 1270.72 7.59 o 3 1 6 216.17 210.61 4.94 o 4 1 6 119.01 116.18 2.03 o 5 1 6 167.22 163.09 3.22 o 6 1 6 5.90 9.68 1.14 o 0 2 6 1028.86 1163.79 10.99 o 1 2 6 1487.69 1601.34 13.03 o 2 2 6 172.51 177.93 2.13 o 3 2 6 114.23 115.78 1.66 o 4 2 6 143.82 144.86 2.75 o 5 2 6 7.24 6.95 0.93 o 6 2 6 12.33 16.16 1.78 o 0 3 6 2104.19 2267.34 20.63 o 1 3 6 96.12 94.92 1.74 o 2 3 6 468.58 476.93 5.24 o 3 3 6 71.01 64.57 2.21 o 4 3 6 304.95 295.08 3.68 o 5 3 6 19.88 19.84 1.11 o 6 3 6 16.17 17.24 1.76 o 0 4 6 406.41 432.64 7.50 o 1 4 6 218.78 221.41 1.98 o 2 4 6 1306.01 1274.90 12.73 o 3 4 6 120.64 116.13 2.90 o 4 4 6 72.68 74.28 1.76 o 5 4 6 52.29 51.56 1.85 o 6 4 6 6.85 8.58 1.64 o 0 5 6 29.46 36.24 1.27 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9 4.51 4.67 0.94 o 0 3 9 22.23 14.80 0.61 o 1 3 9 337.75 343.15 3.28 o 2 3 9 910.73 890.86 6.77 o 3 3 9 59.58 61.29 1.32 o 4 3 9 1.07 2.02 0.74 o 5 3 9 3.60 4.30 0.89 o 6 3 9 22.11 22.88 2.04 o 0 4 9 1089.02 1256.75 10.87 o 1 4 9 560.29 564.51 4.62 o 2 4 9 168.13 165.64 2.39 o 3 4 9 248.65 239.30 5.23 o 4 4 9 66.27 66.74 1.72 o 5 4 9 32.28 31.52 1.70 o 0 5 9 47.72 52.71 1.25 o 1 5 9 83.93 80.57 1.18 o 2 5 9 56.31 53.43 1.22 o 3 5 9 1254.05 1232.07 16.50 o 4 5 9 99.05 94.96 1.87 o 5 5 9 18.13 20.29 1.32 o 0 6 9 0.00 0.26 0.87 o 1 6 9 511.33 485.16 4.33 o 2 6 9 13.42 14.14 0.82 o 3 6 9 464.53 480.44 6.11 o 4 6 9 19.18 17.42 1.00 o 5 6 9 11.07 13.57 1.21 o 0 7 9 17.07 13.77 0.93 o 1 7 9 304.75 289.61 4.24 o 2 7 9 666.67 665.04 6.41 o 3 7 9 70.32 70.44 1.75 o 4 7 9 113.75 97.40 2.25 o 5 7 9 8.02 9.04 1.50 o 0 8 9 16.17 16.05 1.00 o 1 8 9 69.31 67.80 1.74 o 2 8 9 423.46 410.77 4.77 o 3 8 9 13.13 13.78 0.88 o 4 8 9 44.37 39.69 1.55 o 5 8 9 1.53 2.46 1.19 o 0 9 9 24.70 26.61 1.53 o 1 9 9 163.26 158.27 3.24 o 2 9 9 35.76 33.65 1.10 o 3 9 9 79.04 71.21 1.77 o 4 9 9 10.30 11.00 0.93 o 0 10 9 1.45 1.65 1.01 o 1 10 9 12.55 14.29 0.93 o 2 10 9 35.34 33.88 1.12 o 3 10 9 54.31 49.63 1.56 o 4 10 9 52.40 58.08 2.09 o 0 11 9 3.69 3.71 0.99 o 1 11 9 3.26 2.45 0.78 o 2 11 9 70.98 71.71 2.26 o 3 11 9 11.18 11.71 0.95 o 0 12 9 60.31 59.90 2.30 o 1 12 9 19.18 20.41 1.36 o 2 12 9 16.12 17.90 1.20 o 3 12 9 13.19 17.31 1.38 o 0 13 9 20.98 28.74 2.10 o 1 13 9 29.33 32.15 1.99 o 2 13 9 47.09 48.41 3.10 o 0 14 9 27.74 31.92 2.31 o 0 0 10 76.70 86.99 2.03 o 1 0 10 1789.92 1829.75 14.72 o 2 0 10 10.35 7.93 0.57 o 3 0 10 397.28 374.39 5.60 o 4 0 10 78.93 77.68 2.86 o 5 0 10 25.15 28.37 2.00 o 6 0 10 10.95 11.42 1.58 o 0 1 10 935.99 936.43 15.34 o 1 1 10 500.63 505.20 3.21 o 2 1 10 560.96 573.76 3.48 o 3 1 10 214.96 212.27 3.32 o 4 1 10 131.39 127.90 2.89 o 5 1 10 1.53 0.82 0.77 o 6 1 10 2.67 3.97 0.88 o 0 2 10 1637.56 1698.14 13.72 o 1 2 10 820.69 895.52 5.59 o 2 2 10 261.25 242.57 2.27 o 3 2 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11.23 0.82 o 4 8 10 60.07 63.38 1.91 o 5 8 10 7.18 10.16 1.65 o 0 9 10 285.15 266.24 4.67 o 1 9 10 175.46 169.18 2.55 o 2 9 10 85.73 77.18 1.59 o 3 9 10 17.11 17.25 1.08 o 4 9 10 12.30 12.21 1.08 o 0 10 10 61.70 56.47 2.16 o 1 10 10 103.90 103.36 2.03 o 2 10 10 22.51 20.43 1.33 o 3 10 10 34.67 35.47 1.49 o 4 10 10 8.85 11.46 1.13 o 0 11 10 44.87 46.24 3.56 o 1 11 10 66.99 69.11 1.89 o 2 11 10 88.75 86.97 2.23 o 3 11 10 23.46 23.09 1.18 o 0 12 10 29.18 25.19 1.64 o 1 12 10 45.64 45.51 1.61 o 2 12 10 32.56 35.32 1.52 o 3 12 10 16.99 22.34 1.93 o 0 13 10 5.85 6.77 1.17 o 1 13 10 2.33 2.59 0.94 o 2 13 10 7.17 5.44 1.06 o 1 0 11 3.01 6.29 0.64 o 2 0 11 491.51 485.65 4.37 o 3 0 11 49.60 46.59 1.61 o 4 0 11 184.07 187.89 7.37 o 5 0 11 93.79 92.69 3.42 o 6 0 11 34.68 40.77 2.47 o 0 1 11 126.69 125.13 1.80 o 1 1 11 167.06 160.29 1.50 o 2 1 11 280.31 290.60 2.23 o 3 1 11 101.01 99.00 1.49 o 4 1 11 106.41 99.58 2.92 o 5 1 11 55.54 50.70 3.19 o 6 1 11 10.18 12.66 1.43 o 0 2 11 480.30 411.43 4.11 o 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8 11 34.10 32.27 1.20 o 4 8 11 105.11 93.70 2.31 o 0 9 11 6.43 5.97 1.27 o 1 9 11 367.77 360.21 4.04 o 2 9 11 18.56 19.57 0.99 o 3 9 11 85.31 82.78 1.88 o 4 9 11 9.54 13.85 1.12 o 0 10 11 99.17 98.51 2.83 o 1 10 11 86.56 81.37 2.01 o 2 10 11 51.72 48.41 1.47 o 3 10 11 32.96 34.16 1.35 o 4 10 11 47.23 53.78 1.75 o 0 11 11 5.52 4.80 1.01 o 1 11 11 50.42 48.59 1.64 o 2 11 11 7.46 5.94 0.91 o 3 11 11 14.25 17.45 1.10 o 0 12 11 1.58 2.87 0.99 o 1 12 11 29.76 29.74 2.10 o 2 12 11 11.18 13.22 1.22 o 0 13 11 81.11 82.80 4.07 o 1 13 11 1.14 1.68 0.93 o 0 0 12 875.94 950.00 11.73 o 1 0 12 1985.04 2040.10 16.49 o 2 0 12 182.08 198.57 2.34 o 3 0 12 118.96 118.76 2.97 o 4 0 12 30.81 28.64 1.95 o 5 0 12 3.88 3.61 1.21 o 0 1 12 365.71 361.68 3.78 o 1 1 12 282.71 291.82 3.58 o 2 1 12 288.06 294.49 2.29 o 3 1 12 107.68 107.00 1.57 o 4 1 12 96.21 89.68 2.23 o 5 1 12 3.35 2.33 0.83 o 0 2 12 14.06 18.91 0.78 o 1 2 12 153.11 148.29 1.47 o 2 2 12 61.80 56.77 0.98 o 3 2 12 12.77 13.43 0.70 o 4 2 12 98.05 96.30 2.06 o 5 2 12 43.03 42.22 1.70 o 0 3 12 124.99 120.19 2.14 o 1 3 12 118.42 121.00 1.39 o 2 3 12 286.78 266.12 4.63 o 3 3 12 52.84 51.47 1.28 o 4 3 12 221.20 222.17 3.20 o 5 3 12 13.86 12.91 1.36 o 0 4 12 2444.22 2765.27 21.99 o 1 4 12 256.69 252.85 2.74 o 2 4 12 20.28 24.27 0.93 o 3 4 12 115.90 112.27 1.93 o 4 4 12 52.00 51.74 1.44 o 5 4 12 22.21 22.02 1.37 o 0 5 12 507.94 441.54 4.54 o 1 5 12 167.66 138.77 2.76 o 2 5 12 581.23 565.13 5.06 o 3 5 12 55.07 50.50 1.40 o 4 5 12 10.71 11.01 1.45 o 5 5 12 21.06 22.30 2.04 o 0 6 12 25.00 21.20 1.53 o 1 6 12 251.41 249.38 2.87 o 2 6 12 90.48 84.09 1.67 o 3 6 12 538.29 539.59 9.63 o 4 6 12 7.73 9.93 0.85 o 5 6 12 4.79 3.65 1.22 o 0 7 12 36.08 39.00 2.14 o 1 7 12 47.51 41.29 1.17 o 2 7 12 536.56 514.25 6.53 o 3 7 12 101.43 99.06 1.96 o 4 7 12 81.56 78.84 1.85 o 5 7 12 13.30 16.52 1.56 o 0 8 12 113.43 110.61 2.86 o 1 8 12 21.11 18.10 1.15 o 2 8 12 3.78 5.44 0.79 o 3 8 12 3.15 4.79 0.79 o 4 8 12 34.18 34.70 1.48 o 0 9 12 250.98 238.22 4.50 o 1 9 12 3.48 6.46 0.80 o 2 9 12 63.60 60.40 1.85 o 3 9 12 52.04 54.42 1.73 o 4 9 12 2.47 3.92 0.89 o 0 10 12 4.01 4.37 1.08 o 1 10 12 304.29 285.69 4.83 o 2 10 12 0.35 0.80 0.66 o 3 10 12 66.40 68.88 1.84 o 0 11 12 4.58 6.05 1.08 o 1 11 12 9.02 12.30 1.02 o 2 11 12 55.67 57.77 1.66 o 3 11 12 8.39 8.20 1.04 o 0 12 12 25.77 24.93 1.73 o 1 12 12 16.90 19.28 1.19 o 2 12 12 2.13 2.54 0.94 o 0 13 12 8.73 10.52 1.63 o 1 13 12 11.82 11.51 1.62 o 1 0 13 42.68 47.67 1.20 o 2 0 13 65.02 51.99 1.91 o 3 0 13 138.57 130.39 2.77 o 4 0 13 104.76 106.91 3.49 o 5 0 13 2.16 2.43 1.19 o 0 1 13 580.96 568.07 6.61 o 1 1 13 199.54 203.64 2.02 o 2 1 13 276.56 256.01 4.06 o 3 1 13 173.43 165.92 2.52 o 4 1 13 18.63 17.21 1.18 o 5 1 13 84.36 78.47 3.82 o 0 2 13 368.89 384.59 4.08 o 1 2 13 384.24 419.03 4.15 o 2 2 13 128.12 115.40 1.61 o 3 2 13 104.77 96.84 1.57 o 4 2 13 50.39 53.75 1.59 o 5 2 13 28.73 31.89 1.93 o 0 3 13 1693.52 1725.25 14.25 o 1 3 13 149.76 147.41 1.61 o 2 3 13 341.13 318.66 3.62 o 3 3 13 0.05 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o 1 2 21 790.45 805.31 6.75 o 2 2 21 0.07 0.56 0.65 o 3 2 21 59.54 65.04 2.06 o 4 2 21 26.32 25.32 1.87 o 0 3 21 65.91 60.11 3.23 o 1 3 21 10.09 10.02 0.87 o 2 3 21 58.99 58.86 1.66 o 3 3 21 41.77 39.51 1.64 o 4 3 21 9.23 6.16 0.98 o 0 4 21 50.81 50.25 2.83 o 1 4 21 6.28 6.78 0.82 o 2 4 21 10.40 11.08 0.83 o 3 4 21 5.92 8.65 1.49 o 4 4 21 9.12 12.77 1.17 o 0 5 21 125.64 121.79 5.40 o 1 5 21 7.86 7.61 0.96 o 2 5 21 10.02 12.35 1.01 o 3 5 21 56.37 55.55 1.76 o 0 6 21 27.50 29.59 4.61 o 1 6 21 11.95 13.55 1.09 o 2 6 21 38.74 41.56 1.72 o 3 6 21 0.83 1.41 0.89 o 0 7 21 232.24 238.21 5.95 o 1 7 21 13.19 15.38 1.76 o 2 7 21 85.36 85.35 2.46 o 3 7 21 38.17 40.58 1.46 o 0 8 21 8.47 12.46 1.66 o 1 8 21 33.22 31.63 1.57 o 2 8 21 11.17 12.91 1.44 o 0 9 21 0.05 2.09 1.16 o 1 9 21 7.80 7.87 1.04 o 0 10 21 30.31 33.16 2.83 o 0 0 22 13.09 11.96 2.06 o 1 0 22 17.21 17.75 1.33 o 2 0 22 14.86 14.14 1.53 o 3 0 22 31.43 30.14 2.12 o 4 0 22 5.58 6.22 1.43 o 0 1 22 36.27 38.04 1.77 o 1 1 22 87.71 89.35 1.95 o 2 1 22 12.64 13.08 1.08 o 3 1 22 6.35 7.04 0.96 o 4 1 22 0.58 0.14 0.82 o 0 2 22 62.31 62.01 2.07 o 1 2 22 10.72 13.28 1.59 o 2 2 22 28.80 28.42 1.23 o 3 2 22 11.43 10.66 1.07 o 4 2 22 39.76 42.90 1.85 o 0 3 22 7.27 10.07 1.41 o 1 3 22 12.61 12.86 0.95 o 2 3 22 55.18 56.81 1.66 o 3 3 22 85.41 93.09 2.49 o 0 4 22 43.51 40.31 2.31 o 1 4 22 139.21 136.93 5.04 o 2 4 22 48.63 45.92 1.76 o 3 4 22 23.15 25.06 1.27 o 0 5 22 83.80 89.74 3.37 o 1 5 22 21.38 20.65 1.26 o 2 5 22 108.83 110.17 2.37 o 3 5 22 23.23 26.39 1.49 o 0 6 22 4.60 6.78 1.35 o 1 6 22 17.05 20.82 1.30 o 2 6 22 36.35 37.08 1.66 o 3 6 22 22.62 24.78 1.48 o 0 7 22 17.23 20.09 2.76 o 1 7 22 4.11 5.20 0.91 o 2 7 22 10.57 15.50 1.24 o 0 8 22 0.33 2.58 1.25 o 1 8 22 1.91 1.42 0.96 o 2 8 22 2.31 4.69 0.93 o 0 9 22 10.29 7.99 1.51 o 1 9 22 3.88 5.65 0.96 o 1 0 23 177.65 178.23 4.53 o 2 0 23 9.38 12.06 1.67 o 3 0 23 10.57 15.69 2.59 o 0 1 23 0.05 0.90 1.10 o 1 1 23 124.87 130.44 2.72 o 2 1 23 66.16 74.04 2.13 o 3 1 23 77.30 81.79 2.38 o 0 2 23 48.97 43.90 2.94 o 1 2 23 172.89 168.01 3.16 o 2 2 23 1.10 1.18 0.68 o 3 2 23 15.01 16.60 1.22 o 0 3 23 10.48 9.62 1.78 o 1 3 23 3.27 3.25 0.82 o 2 3 23 77.77 74.44 2.18 o 3 3 23 18.62 21.76 1.34 o 0 4 23 98.95 101.21 5.65 o 1 4 23 2.23 3.71 0.88 o 2 4 23 28.30 27.03 1.44 o 3 4 23 4.59 6.58 1.27 o 0 5 23 7.54 10.78 1.98 o 1 5 23 20.34 21.32 1.32 o 2 5 23 17.65 18.44 1.54 o 3 5 23 29.48 32.58 1.66 o 0 6 23 0.62 2.92 1.26 o 1 6 23 2.94 2.95 0.91 o 2 6 23 8.25 11.33 2.43 o 0 7 23 64.82 65.02 3.08 o 1 7 23 17.07 18.17 1.26 o 2 7 23 35.21 42.99 1.85 o 0 8 23 40.25 43.57 2.68 o 1 8 23 45.11 48.74 1.97 o 0 0 24 42.31 36.12 3.09 o 1 0 24 60.48 60.87 2.71 o 2 0 24 23.76 29.70 3.05 o 3 0 24 10.70 7.54 1.41 o 0 1 24 0.10 1.98 1.69 o 1 1 24 124.91 124.90 2.72 o 2 1 24 97.25 104.97 2.59 o 3 1 24 18.44 18.31 1.30 o 0 2 24 58.19 61.06 3.16 o 1 2 24 24.74 31.05 2.61 o 2 2 24 49.06 54.19 1.89 o 3 2 24 21.14 22.87 1.39 o 0 3 24 7.86 7.21 1.35 o 1 3 24 20.57 20.31 2.01 o 2 3 24 1.22 1.77 0.83 o 3 3 24 82.00 88.18 2.53 o 0 4 24 36.75 41.58 2.41 o 1 4 24 39.40 39.87 1.66 o 2 4 24 25.71 26.17 1.43 o 3 4 24 12.24 14.01 1.45 o 0 5 24 90.79 99.67 3.66 o 1 5 24 13.36 16.88 1.20 o 2 5 24 32.03 36.87 1.98 o 0 6 24 18.14 25.12 2.06 o 1 6 24 35.41 36.17 1.67 o 2 6 24 30.36 31.20 1.88 o 0 7 24 1.78 5.58 1.78 o 1 7 24 12.79 14.12 1.22 o 0 8 24 0.50 2.06 1.32 o 1 0 25 0.07 1.49 1.57 o 2 0 25 18.86 23.64 1.96 o 3 0 25 8.52 12.20 3.50 o 0 1 25 217.46 213.51 7.34 o 1 1 25 45.80 47.49 2.95 o 2 1 25 29.49 34.91 1.60 o 3 1 25 15.82 18.27 1.29 o 0 2 25 0.00 -0.25 1.50 o 1 2 25 15.50 19.27 1.26 o 2 2 25 19.42 24.48 1.66 o 3 2 25 18.92 22.91 1.39 o 0 3 25 40.30 39.50 2.30 o 1 3 25 7.68 9.71 1.82 o 2 3 25 76.84 81.43 2.36 o 0 4 25 33.63 38.13 2.64 o 1 4 25 85.05 87.36 3.54 o 2 4 25 45.53 44.04 2.10 o 0 5 25 0.78 5.16 1.36 o 1 5 25 0.31 0.80 0.84 o 2 5 25 16.47 20.04 1.59 o 0 6 25 14.29 16.75 1.84 o 1 6 25 2.35 2.58 0.90 o 0 7 25 1.78 5.17 1.44 o 0 0 26 33.73 38.38 3.17 o 1 0 26 0.82 0.96 1.72 o 2 0 26 76.85 79.13 3.29 o 0 1 26 4.03 7.33 2.08 o 1 1 26 0.43 4.20 1.78 o 2 1 26 32.04 34.96 1.90 o 0 2 26 26.33 28.48 2.87 o 1 2 26 42.49 47.91 2.10 o 2 2 26 33.45 35.13 1.94 o 0 3 26 1.11 1.21 1.61 o 1 3 26 1.61 3.15 1.04 o 2 3 26 27.07 26.64 1.73 o 0 4 26 54.78 57.82 2.88 o 1 4 26 0.90 2.40 1.09 o 2 4 26 39.16 46.72 2.87 o 0 5 26 20.43 22.48 2.62 o 1 5 26 31.12 35.13 2.54 o 0 6 26 1.04 5.00 1.38 o 1 0 27 37.40 42.79 3.51 o 2 0 27 0.14 1.77 1.71 o 0 1 27 67.59 79.75 4.62 o 1 1 27 49.12 53.87 2.71 o 2 1 27 1.22 2.80 1.08 o 0 2 27 39.85 46.49 3.60 o 1 2 27 35.97 45.37 2.61 o 0 3 27 10.20 9.72 2.18 o 1 3 27 54.65 65.84 2.55 o 0 4 27 14.24 16.72 1.85 o 1 4 27 1.64 2.79 1.08 o 1 0 28 24.67 34.95 3.26 o 0 1 28 49.83 66.80 4.28 o 1 1 28 26.43 34.79 3.35 o 0 2 28 10.16 21.92 2.76 o