#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/60/2206004.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206004_Fobs loop_ _publ_author_name 'Hempel, Andrew' 'Camerman, Norman' 'Camerman, Arthur' 'Mastropaolo, Donald' _publ_section_title ; Pargyline hydrochloride, a monoamine oxidase inhibitor: an orthorhombic form ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1598 _journal_page_last o1600 _journal_volume 61 _journal_year 2005 _space_group_IT_number 29 _symmetry_space_group_name_Hall 'P 2c -2b' _symmetry_space_group_name_H-M 'P b c 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.9580 _cell_length_b 11.0390 _cell_length_c 33.5960 _exptl_crystal_F_000 832.00 _reflns_d_resolution_high 0.8508 _[local]_cod_data_source_file lh6415Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' * PARGYLINE * Pbc21 Z=8 C11H13N *' _shelx_refln_list_code 4 _shelx_f_calc_maximum 163.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x, -y+1/2, z+1/2' '-x, y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 350.10 329.80 15.51 o 2 0 0 26.19 22.08 3.02 o 3 0 0 55.53 60.36 4.99 o 4 0 0 5460.95 6909.30 318.21 o 5 0 0 11.38 11.83 5.93 o 6 0 0 139.74 131.86 9.38 o 7 0 0 0.40 3.97 3.49 o 1 1 0 2689.44 2754.22 126.43 o 2 1 0 14969.37 19414.09 870.34 o 3 1 0 4.02 2.08 3.44 o 4 1 0 204.12 196.18 11.56 o 5 1 0 291.20 283.99 15.70 o 6 1 0 366.26 329.92 18.16 o 0 2 0 174.18 152.72 7.41 o 1 2 0 3515.23 3734.47 171.73 o 2 2 0 45.39 43.03 3.67 o 3 2 0 585.89 637.87 30.31 o 4 2 0 301.53 267.65 14.87 o 5 2 0 1.05 0.00 10531.56 o 6 2 0 5.18 10.96 5.33 o 1 3 0 3186.96 3315.38 152.66 o 2 3 0 298.84 278.42 13.79 o 3 3 0 992.49 1227.96 57.40 o 4 3 0 20.33 18.17 5.28 o 5 3 0 21.45 24.93 6.15 o 6 3 0 2.52 5.38 5.37 o 0 4 0 12799.86 9610.10 431.44 o 1 4 0 76.03 71.77 4.68 o 2 4 0 13.75 13.69 3.38 o 3 4 0 137.89 150.22 8.99 o 4 4 0 512.16 570.18 28.25 o 5 4 0 19.52 14.63 5.61 o 6 4 0 4.70 2.07 5.76 o 1 5 0 0.62 0.00 6445.66 o 2 5 0 4918.30 6134.28 282.20 o 3 5 0 50.71 51.32 5.85 o 4 5 0 602.95 707.94 34.52 o 5 5 0 2.61 0.00 8573.54 o 6 5 0 198.07 201.07 11.81 o 0 6 0 243.42 178.88 9.52 o 1 6 0 4.91 6.78 3.72 o 2 6 0 137.21 124.44 8.10 o 3 6 0 20.89 24.25 5.47 o 4 6 0 905.44 1044.63 50.12 o 5 6 0 0.90 0.00 8729.43 o 6 6 0 21.33 10.89 4.41 o 1 7 0 10.94 5.23 4.48 o 2 7 0 96.75 91.17 7.94 o 3 7 0 36.26 29.95 6.16 o 4 7 0 18.32 15.15 5.56 o 5 7 0 8.66 7.88 4.75 o 0 8 0 134.23 116.61 7.68 o 1 8 0 221.98 218.98 12.43 o 2 8 0 10.08 7.59 5.33 o 3 8 0 40.72 43.46 6.58 o 4 8 0 16.70 23.62 5.47 o 5 8 0 59.35 65.45 5.57 o 1 9 0 0.20 1.29 10.08 o 2 9 0 774.28 795.61 38.78 o 3 9 0 45.66 47.07 6.12 o 4 9 0 27.53 33.35 5.11 o 0 10 0 2340.85 2018.70 94.43 o 1 10 0 1.71 5.63 4.72 o 2 10 0 14.63 15.96 5.34 o 3 10 0 7.36 13.74 4.60 o 4 10 0 354.22 306.16 16.31 o 1 11 0 13.01 20.09 4.47 o 2 11 0 258.60 269.55 15.04 o 3 11 0 8.22 5.49 4.07 o 0 12 0 0.93 0.00 5438.92 o 1 12 0 0.57 3.06 3.91 o 2 12 0 0.01 0.00 6811.90 o 1 1 1 1723.60 1675.81 76.94 o 2 1 1 7654.34 8639.39 389.43 o 3 1 1 9.51 10.88 3.74 o 4 1 1 243.57 220.88 12.49 o 5 1 1 277.78 289.32 15.84 o 6 1 1 225.16 218.63 13.09 o 0 2 1 3148.85 3513.50 142.83 o 1 2 1 4910.27 5669.87 255.94 o 2 2 1 31.76 34.87 3.44 o 3 2 1 288.84 284.31 14.44 o 4 2 1 1636.73 1899.68 88.64 o 5 2 1 208.93 210.70 12.74 o 6 2 1 15.93 20.60 5.39 o 1 3 1 3588.04 4065.24 186.93 o 2 3 1 922.04 869.40 40.71 o 3 3 1 985.79 1130.51 53.02 o 4 3 1 228.67 249.82 13.88 o 5 3 1 186.16 191.33 11.93 o 6 3 1 169.54 188.39 11.53 o 0 4 1 3016.89 3864.44 185.70 o 1 4 1 53.63 69.01 4.52 o 2 4 1 35.53 44.56 4.14 o 3 4 1 151.40 147.85 9.02 o 4 4 1 64.05 67.92 7.04 o 5 4 1 9.43 14.77 5.40 o 6 4 1 2.17 5.63 4.79 o 1 5 1 53.29 53.24 4.25 o 2 5 1 145.61 155.41 9.15 o 3 5 1 97.10 106.97 7.90 o 4 5 1 17.09 17.22 6.02 o 5 5 1 9.11 16.14 5.07 o 6 5 1 18.66 29.50 4.89 o 0 6 1 984.87 692.22 32.88 o 1 6 1 512.96 543.59 26.19 o 2 6 1 77.12 75.10 6.09 o 3 6 1 65.60 64.84 6.82 o 4 6 1 321.37 361.66 19.16 o 5 6 1 63.43 41.79 6.79 o 6 6 1 21.68 20.23 4.32 o 1 7 1 1043.42 1286.72 60.37 o 2 7 1 803.29 911.10 43.59 o 3 7 1 423.31 535.22 26.65 o 4 7 1 4.26 0.00 9405.51 o 5 7 1 110.33 110.13 8.02 o 0 8 1 604.43 440.54 21.98 o 1 8 1 238.08 270.72 14.57 o 2 8 1 2.32 8.16 5.12 o 3 8 1 368.05 448.19 23.10 o 4 8 1 185.01 195.65 11.75 o 5 8 1 22.55 14.72 4.64 o 1 9 1 58.07 70.43 6.60 o 2 9 1 212.58 216.57 13.14 o 3 9 1 55.55 67.04 6.75 o 4 9 1 6.85 6.24 4.76 o 5 9 1 21.14 17.95 3.97 o 0 10 1 11.75 23.95 5.33 o 1 10 1 1.94 1.83 6.20 o 2 10 1 4.54 3.32 4.97 o 3 10 1 3.85 4.41 4.88 o 4 10 1 14.53 15.36 4.27 o 1 11 1 31.06 33.18 5.23 o 2 11 1 243.71 218.26 12.86 o 3 11 1 16.42 21.26 4.18 o 0 12 1 65.18 54.63 5.25 o 1 12 1 162.86 152.68 9.54 o 2 12 1 4.76 6.41 3.60 o 0 0 2 624.10 743.94 27.27 o 1 0 2 7825.47 10534.25 472.87 o 2 0 2 2063.35 2407.78 111.05 o 3 0 2 2656.18 3258.54 150.09 o 4 0 2 944.39 1062.72 50.36 o 5 0 2 369.62 435.17 22.28 o 6 0 2 181.01 175.55 11.13 o 1 1 2 693.11 673.63 31.24 o 2 1 2 5026.24 5695.99 261.77 o 3 1 2 745.25 710.19 33.65 o 4 1 2 124.49 126.95 8.69 o 5 1 2 349.01 344.29 18.41 o 6 1 2 204.16 200.71 12.22 o 0 2 2 11231.29 8340.41 373.79 o 1 2 2 3715.69 3975.47 182.48 o 2 2 2 526.68 561.97 26.49 o 3 2 2 1250.48 1338.53 62.32 o 4 2 2 171.41 183.26 11.27 o 5 2 2 36.48 43.20 6.46 o 6 2 2 4.93 0.00 9339.39 o 1 3 2 3018.37 3112.07 143.15 o 2 3 2 983.30 1097.69 51.08 o 3 3 2 238.58 267.41 13.87 o 4 3 2 81.96 92.16 7.55 o 5 3 2 233.71 198.74 12.59 o 6 3 2 120.60 129.07 9.19 o 0 4 2 123.23 128.12 6.85 o 1 4 2 728.69 737.91 34.56 o 2 4 2 198.90 216.20 11.13 o 3 4 2 1978.72 2129.24 98.75 o 4 4 2 34.63 36.03 6.31 o 5 4 2 98.91 90.44 7.98 o 6 4 2 52.81 57.62 6.31 o 1 5 2 469.21 484.24 23.22 o 2 5 2 10.05 23.00 4.06 o 3 5 2 935.59 1066.48 50.44 o 4 5 2 148.94 150.01 10.19 o 5 5 2 164.53 187.53 11.50 o 6 5 2 10.60 12.57 4.61 o 0 6 2 598.00 486.58 23.46 o 1 6 2 1709.77 1739.86 80.86 o 2 6 2 192.13 182.83 10.44 o 3 6 2 82.92 92.45 7.56 o 4 6 2 96.53 98.52 8.63 o 5 6 2 121.71 101.89 8.40 o 6 6 2 35.27 32.06 4.75 o 1 7 2 191.77 238.73 12.98 o 2 7 2 225.18 214.66 12.31 o 3 7 2 78.98 87.85 7.87 o 4 7 2 4.82 2.17 6.20 o 5 7 2 14.57 9.07 5.35 o 0 8 2 39.92 34.95 4.96 o 1 8 2 165.77 175.13 10.61 o 2 8 2 183.59 203.02 12.08 o 3 8 2 202.59 210.24 12.62 o 4 8 2 36.80 38.52 5.82 o 5 8 2 20.50 22.35 4.47 o 1 9 2 361.51 448.50 22.78 o 2 9 2 65.25 69.49 7.31 o 3 9 2 217.23 236.05 13.60 o 4 9 2 32.44 12.52 5.13 o 5 9 2 72.52 57.25 5.38 o 0 10 2 206.45 176.80 10.67 o 1 10 2 29.73 43.90 8.16 o 2 10 2 64.42 58.09 6.57 o 3 10 2 126.68 157.48 10.16 o 4 10 2 39.20 38.38 4.96 o 1 11 2 93.06 98.14 7.64 o 2 11 2 85.64 86.73 7.47 o 3 11 2 31.59 29.79 4.70 o 0 12 2 57.58 49.82 4.75 o 1 12 2 40.64 36.44 5.02 o 2 12 2 1.18 8.47 3.63 o 1 1 3 3874.35 3995.70 183.67 o 2 1 3 15.35 24.07 3.15 o 3 1 3 1078.93 1020.85 47.78 o 4 1 3 302.22 334.04 17.30 o 5 1 3 134.95 129.86 9.48 o 6 1 3 86.08 81.18 7.49 o 0 2 3 1729.63 1225.64 53.66 o 1 2 3 26891.25 26107.33 1204.99 o 2 2 3 453.94 517.25 24.53 o 3 2 3 3056.13 3506.76 161.97 o 4 2 3 115.73 123.04 8.81 o 5 2 3 112.39 144.80 9.83 o 6 2 3 17.86 20.53 5.34 o 1 3 3 15995.46 21542.94 964.27 o 2 3 3 1276.31 1459.97 67.85 o 3 3 3 399.79 407.54 20.05 o 4 3 3 111.40 122.70 8.80 o 5 3 3 1343.32 1523.68 72.01 o 6 3 3 45.64 34.73 6.06 o 0 4 3 3538.69 2499.51 115.08 o 1 4 3 576.14 563.85 26.54 o 2 4 3 82.22 83.20 5.66 o 3 4 3 1554.65 1566.50 73.24 o 4 4 3 155.00 164.35 10.48 o 5 4 3 195.68 210.22 12.62 o 6 4 3 19.34 15.01 4.92 o 1 5 3 574.95 712.41 33.66 o 2 5 3 318.71 406.57 20.17 o 3 5 3 152.35 173.61 10.57 o 4 5 3 8.57 7.63 5.89 o 5 5 3 26.67 29.01 5.54 o 6 5 3 22.56 29.13 4.98 o 0 6 3 142.69 107.07 6.58 o 1 6 3 667.84 617.41 29.64 o 2 6 3 174.28 182.37 10.42 o 3 6 3 550.04 561.67 27.69 o 4 6 3 136.80 130.90 9.35 o 5 6 3 81.51 83.58 7.33 o 6 6 3 6.28 2.78 4.03 o 1 7 3 1166.16 1247.63 58.69 o 2 7 3 95.37 98.90 7.67 o 3 7 3 73.51 87.77 7.93 o 4 7 3 89.04 98.51 7.96 o 5 7 3 330.96 324.33 17.46 o 0 8 3 67.84 57.80 5.86 o 1 8 3 855.83 1038.45 49.48 o 2 8 3 43.06 47.12 6.28 o 3 8 3 841.78 994.01 47.68 o 4 8 3 3.91 0.00 9257.83 o 5 8 3 37.68 36.90 5.01 o 1 9 3 104.96 107.90 8.41 o 2 9 3 84.64 104.14 8.10 o 3 9 3 192.83 217.85 12.73 o 4 9 3 13.23 21.08 4.75 o 5 9 3 21.74 8.21 4.05 o 0 10 3 42.26 44.61 5.86 o 1 10 3 2.52 14.34 4.84 o 2 10 3 43.26 64.46 6.37 o 3 10 3 21.95 18.56 5.24 o 4 10 3 16.09 6.24 4.27 o 1 11 3 87.22 86.09 7.02 o 2 11 3 16.73 10.30 5.04 o 3 11 3 33.17 29.46 4.76 o 0 12 3 33.03 42.61 4.24 o 1 12 3 309.30 322.95 16.88 o 2 12 3 12.99 12.46 3.87 o 0 0 4 17294.51 16339.58 731.62 o 1 0 4 348.65 375.58 17.55 o 2 0 4 1580.68 1738.02 80.26 o 3 0 4 606.44 814.47 38.38 o 4 0 4 176.33 191.25 11.41 o 5 0 4 394.58 461.29 23.43 o 6 0 4 6.04 2.12 6.04 o 1 1 4 4083.23 4143.11 190.03 o 2 1 4 1420.19 1459.34 67.51 o 3 1 4 1315.04 1338.58 62.36 o 4 1 4 205.34 199.58 11.66 o 5 1 4 42.17 45.32 6.57 o 6 1 4 76.27 72.62 7.41 o 0 2 4 3240.15 2254.01 103.71 o 1 2 4 1864.96 1832.01 84.48 o 2 2 4 759.16 819.95 38.19 o 3 2 4 149.90 149.17 8.69 o 4 2 4 86.63 71.55 7.16 o 5 2 4 19.48 23.88 6.02 o 6 2 4 15.97 23.55 5.10 o 1 3 4 4082.43 4449.00 204.61 o 2 3 4 881.17 912.37 42.60 o 3 3 4 21.87 25.34 4.34 o 4 3 4 41.75 40.86 6.14 o 5 3 4 405.49 451.79 23.35 o 6 3 4 33.73 22.22 5.59 o 0 4 4 11103.91 8900.62 399.49 o 1 4 4 791.21 791.88 37.10 o 2 4 4 25.67 30.87 3.95 o 3 4 4 1101.67 1197.55 56.17 o 4 4 4 792.32 788.22 38.18 o 5 4 4 148.92 152.61 10.28 o 6 4 4 17.15 25.99 5.01 o 1 5 4 831.18 945.72 44.26 o 2 5 4 4540.59 5608.54 258.41 o 3 5 4 1772.22 2006.75 93.59 o 4 5 4 54.03 65.08 6.77 o 5 5 4 32.11 27.25 5.76 o 6 5 4 273.43 246.56 13.67 o 0 6 4 1684.75 1284.36 59.87 o 1 6 4 225.64 197.48 10.75 o 2 6 4 256.07 267.77 14.13 o 3 6 4 338.99 354.08 18.53 o 4 6 4 757.35 811.16 39.37 o 5 6 4 37.24 47.90 6.07 o 6 6 4 12.06 11.49 4.13 o 1 7 4 24.22 30.74 4.90 o 2 7 4 56.90 56.08 6.74 o 3 7 4 13.92 25.91 5.77 o 4 7 4 59.40 75.40 6.96 o 5 7 4 19.02 16.23 5.21 o 0 8 4 199.00 182.81 10.74 o 1 8 4 95.22 107.11 8.06 o 2 8 4 3.81 3.56 5.34 o 3 8 4 18.42 16.48 5.80 o 4 8 4 32.68 37.72 5.94 o 5 8 4 8.42 6.72 4.19 o 1 9 4 172.36 199.44 11.86 o 2 9 4 317.08 408.11 21.27 o 3 9 4 164.81 181.98 11.33 o 4 9 4 0.28 0.00 7730.15 o 0 10 4 789.60 759.52 36.85 o 1 10 4 159.09 175.49 10.62 o 2 10 4 4.42 0.00 8914.55 o 3 10 4 34.11 27.33 5.53 o 4 10 4 160.31 162.57 9.74 o 1 11 4 38.02 23.44 5.56 o 2 11 4 183.10 155.43 10.09 o 3 11 4 19.01 16.78 4.24 o 0 12 4 26.03 24.85 4.18 o 1 12 4 5.20 5.45 3.94 o 2 12 4 12.62 12.94 3.75 o 1 1 5 7199.69 7399.91 333.80 o 2 1 5 1023.93 1026.99 47.78 o 3 1 5 1419.58 1550.71 71.99 o 4 1 5 169.13 190.91 11.29 o 5 1 5 78.61 93.53 7.97 o 6 1 5 94.36 104.69 7.97 o 0 2 5 248.00 221.64 8.25 o 1 2 5 48.49 45.16 3.46 o 2 2 5 414.05 451.18 21.45 o 3 2 5 1021.92 1232.74 57.54 o 4 2 5 1272.91 1477.22 69.46 o 5 2 5 158.39 176.39 11.35 o 6 2 5 21.90 13.89 5.44 o 1 3 5 1353.71 1396.50 64.59 o 2 3 5 2945.93 3160.16 145.43 o 3 3 5 191.84 206.40 11.20 o 4 3 5 18.67 20.43 5.57 o 5 3 5 277.45 332.12 17.80 o 6 3 5 325.64 328.00 17.70 o 0 4 5 3857.58 2862.59 131.76 o 1 4 5 2169.75 2242.41 103.52 o 2 4 5 449.56 428.48 20.73 o 3 4 5 67.92 78.14 6.22 o 4 4 5 484.37 503.05 25.34 o 5 4 5 44.23 51.74 6.69 o 6 4 5 1.93 0.00 7561.17 o 1 5 5 1458.05 1748.92 81.00 o 2 5 5 176.20 209.19 11.49 o 3 5 5 116.83 141.75 9.10 o 4 5 5 11.52 13.80 5.92 o 5 5 5 6.74 2.56 5.18 o 6 5 5 17.93 12.84 4.82 o 0 6 5 3111.31 2388.46 110.55 o 1 6 5 167.16 203.18 11.00 o 2 6 5 220.15 238.37 12.97 o 3 6 5 76.46 87.85 7.65 o 4 6 5 611.46 650.18 32.12 o 5 6 5 6.51 19.92 5.03 o 6 6 5 27.01 21.33 4.26 o 1 7 5 4.79 6.53 4.48 o 2 7 5 1884.73 2184.98 101.63 o 3 7 5 298.29 305.20 16.67 o 4 7 5 64.69 53.62 6.64 o 5 7 5 34.04 26.42 5.60 o 0 8 5 1497.07 1365.35 64.32 o 1 8 5 9.21 0.00 10391.71 o 2 8 5 73.47 69.24 6.86 o 3 8 5 0.79 2.22 6.31 o 4 8 5 416.74 455.76 23.46 o 5 8 5 18.71 10.59 4.40 o 1 9 5 8.89 0.61 22.57 o 2 9 5 203.38 208.38 12.56 o 3 9 5 42.69 48.58 6.43 o 4 9 5 9.12 2.03 5.53 o 0 10 5 73.31 79.95 7.23 o 1 10 5 6.80 11.67 4.65 o 2 10 5 48.57 67.41 6.39 o 3 10 5 48.22 43.31 5.67 o 4 10 5 4.08 4.77 4.03 o 1 11 5 13.87 18.63 4.47 o 2 11 5 253.31 267.55 14.74 o 3 11 5 23.45 16.60 4.28 o 0 12 5 104.27 106.51 7.18 o 1 12 5 7.75 8.51 3.59 o 2 12 5 12.77 1.81 4.17 o 0 0 6 1833.76 1301.77 59.91 o 1 0 6 141.13 97.98 5.25 o 2 0 6 814.24 971.75 45.18 o 3 0 6 4599.28 5820.57 268.07 o 4 0 6 894.23 1056.26 49.93 o 5 0 6 20.84 25.53 6.03 o 6 0 6 54.57 57.16 6.46 o 1 1 6 12947.86 14858.26 666.63 o 2 1 6 758.64 727.18 34.12 o 3 1 6 1449.43 1606.60 74.82 o 4 1 6 155.72 150.89 9.85 o 5 1 6 390.52 378.16 19.89 o 6 1 6 152.51 163.86 10.56 o 0 2 6 9695.64 8260.49 370.98 o 1 2 6 3416.87 3387.94 155.92 o 2 2 6 230.28 223.89 11.34 o 3 2 6 82.95 95.70 6.73 o 4 2 6 286.87 336.28 17.64 o 5 2 6 67.46 75.74 7.24 o 6 2 6 21.75 25.57 5.35 o 1 3 6 267.88 274.83 13.45 o 2 3 6 162.29 174.57 9.60 o 3 3 6 58.01 68.74 5.70 o 4 3 6 179.96 176.77 11.07 o 5 3 6 134.66 119.89 9.03 o 6 3 6 49.98 64.89 6.46 o 0 4 6 4839.11 3630.99 167.28 o 1 4 6 827.96 812.21 38.01 o 2 4 6 404.16 438.51 21.28 o 3 4 6 365.59 389.15 19.58 o 4 4 6 759.64 792.95 38.29 o 5 4 6 26.63 28.32 5.83 o 6 4 6 13.36 0.00 9687.73 o 1 5 6 865.54 903.97 42.36 o 2 5 6 3075.48 3606.88 166.37 o 3 5 6 103.31 120.44 8.30 o 4 5 6 660.37 717.35 35.17 o 5 5 6 96.75 129.97 9.14 o 6 5 6 234.21 233.88 12.97 o 0 6 6 5165.24 4591.54 211.45 o 1 6 6 677.62 721.86 34.30 o 2 6 6 123.02 134.30 8.33 o 3 6 6 329.22 390.25 20.20 o 4 6 6 608.64 671.61 33.23 o 5 6 6 39.10 34.59 5.78 o 6 6 6 40.56 33.01 4.73 o 1 7 6 76.67 90.28 6.75 o 2 7 6 274.74 267.14 15.22 o 3 7 6 68.02 79.13 7.40 o 4 7 6 40.69 44.16 6.13 o 5 7 6 11.69 16.14 4.86 o 0 8 6 72.02 76.34 6.67 o 1 8 6 53.04 47.39 6.14 o 2 8 6 98.49 112.82 8.43 o 3 8 6 74.00 75.81 7.24 o 4 8 6 107.44 104.87 8.60 o 5 8 6 13.28 11.96 4.29 o 1 9 6 176.29 163.32 10.25 o 2 9 6 251.74 305.92 16.55 o 3 9 6 40.88 59.23 6.57 o 4 9 6 65.82 58.38 5.95 o 0 10 6 705.11 741.23 35.97 o 1 10 6 78.38 87.70 7.15 o 2 10 6 117.27 125.98 8.66 o 3 10 6 116.31 122.62 8.71 o 4 10 6 153.26 138.89 8.83 o 1 11 6 31.39 31.72 5.19 o 2 11 6 275.70 295.85 16.02 o 3 11 6 55.27 52.52 5.15 o 0 12 6 5.31 12.11 3.63 o 1 12 6 51.22 25.89 4.39 o 2 12 6 5.81 6.45 3.42 o 1 1 7 4807.28 4504.12 206.69 o 2 1 7 584.27 597.18 28.07 o 3 1 7 1146.30 1189.11 55.52 o 4 1 7 562.74 634.80 30.97 o 5 1 7 287.28 297.13 16.31 o 6 1 7 3.51 10.34 3.74 o 0 2 7 1128.79 830.72 38.56 o 1 2 7 14079.98 16827.38 754.41 o 2 2 7 165.70 194.89 10.04 o 3 2 7 1275.26 1443.90 67.31 o 4 2 7 108.67 113.57 8.54 o 5 2 7 128.60 141.84 9.73 o 6 2 7 9.57 5.74 5.05 o 1 3 7 895.86 876.45 40.91 o 2 3 7 1754.97 1897.48 87.99 o 3 3 7 63.89 52.15 5.08 o 4 3 7 541.11 575.70 28.58 o 5 3 7 426.86 447.25 22.92 o 6 3 7 34.37 36.53 5.67 o 0 4 7 781.61 560.35 26.52 o 1 4 7 502.23 458.61 21.96 o 2 4 7 19.57 28.04 3.88 o 3 4 7 557.85 546.18 26.78 o 4 4 7 52.51 60.23 6.86 o 5 4 7 97.98 96.95 8.12 o 6 4 7 7.83 10.96 4.65 o 1 5 7 24.36 20.71 3.72 o 2 5 7 24.42 32.61 5.01 o 3 5 7 15.94 27.44 5.07 o 4 5 7 227.34 276.65 15.49 o 5 5 7 10.68 20.19 5.43 o 6 5 7 16.00 24.70 4.62 o 0 6 7 1299.60 1007.68 47.51 o 1 6 7 380.03 371.59 18.56 o 2 6 7 5.51 16.23 4.41 o 3 6 7 657.73 686.93 33.63 o 4 6 7 62.19 86.77 7.54 o 5 6 7 40.56 51.80 5.93 o 6 6 7 34.29 20.57 4.66 o 1 7 7 769.14 816.47 39.09 o 2 7 7 1301.35 1536.90 72.04 o 3 7 7 85.97 115.55 8.54 o 4 7 7 122.67 145.36 9.85 o 5 7 7 377.20 370.45 19.40 o 0 8 7 3.41 5.63 4.77 o 1 8 7 518.23 588.46 28.88 o 2 8 7 24.60 18.63 5.61 o 3 8 7 462.68 501.08 25.28 o 4 8 7 52.28 57.33 6.75 o 5 8 7 89.76 80.32 6.37 o 1 9 7 264.40 269.28 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393.72 20.90 o 1 6 23 244.31 252.09 14.78 o 2 6 23 4.83 0.00 8467.23 o 3 6 23 219.97 212.94 12.59 o 4 6 23 1.04 6.51 3.99 o 1 7 23 288.70 337.58 18.09 o 2 7 23 9.03 9.67 4.91 o 3 7 23 33.61 32.70 5.40 o 4 7 23 16.79 14.98 3.95 o 0 8 23 59.44 63.62 7.12 o 1 8 23 173.65 179.56 11.36 o 2 8 23 11.03 9.96 4.65 o 3 8 23 140.25 149.20 9.43 o 1 9 23 51.35 52.13 5.95 o 2 9 23 0.42 7.24 4.01 o 0 10 23 3.06 7.36 2.91 o 1 10 23 11.33 13.24 4.35 o 0 0 24 782.88 945.60 45.10 o 1 0 24 115.22 99.46 7.77 o 2 0 24 109.85 131.38 9.02 o 3 0 24 2469.11 2644.47 123.17 o 4 0 24 14.21 16.32 5.25 o 5 0 24 20.00 17.38 4.70 o 1 1 24 640.57 643.23 31.77 o 2 1 24 298.60 316.17 16.97 o 3 1 24 203.14 177.40 11.69 o 4 1 24 1.04 0.00 9129.38 o 5 1 24 118.54 127.54 8.46 o 0 2 24 52.36 43.46 6.58 o 1 2 24 172.02 188.30 11.53 o 2 2 24 25.85 13.06 5.74 o 3 2 24 69.31 81.50 7.44 o 4 2 24 31.24 33.14 5.79 o 5 2 24 3.84 0.00 8101.41 o 1 3 24 42.62 36.26 5.87 o 2 3 24 198.62 198.55 12.16 o 3 3 24 98.39 106.87 8.52 o 4 3 24 34.64 28.40 5.56 o 5 3 24 21.17 26.65 4.60 o 0 4 24 405.43 511.19 25.87 o 1 4 24 155.70 192.42 11.86 o 2 4 24 25.96 40.08 5.65 o 3 4 24 197.30 233.32 13.29 o 4 4 24 124.37 110.15 8.26 o 5 4 24 2.52 0.00 7900.52 o 1 5 24 1248.87 1445.10 68.35 o 2 5 24 358.13 378.14 19.74 o 3 5 24 372.22 393.56 20.44 o 4 5 24 9.81 3.54 4.47 o 0 6 24 349.68 408.28 21.43 o 1 6 24 419.02 412.18 21.54 o 2 6 24 2.23 1.65 7.25 o 3 6 24 58.46 61.59 6.70 o 4 6 24 70.84 57.58 5.68 o 1 7 24 8.87 4.13 5.33 o 2 7 24 8.21 0.71 19.39 o 3 7 24 3.71 5.16 4.21 o 4 7 24 10.61 21.47 3.89 o 0 8 24 87.76 68.69 7.02 o 1 8 24 15.76 16.97 5.08 o 2 8 24 5.33 6.37 4.39 o 3 8 24 25.65 17.13 4.25 o 1 9 24 104.85 124.63 8.44 o 2 9 24 57.11 57.23 5.49 o 0 10 24 48.88 25.43 4.92 o 1 10 24 26.21 13.86 4.45 o 1 1 25 237.05 246.96 14.28 o 2 1 25 280.13 278.49 15.54 o 3 1 25 64.94 53.46 6.80 o 4 1 25 22.32 23.37 5.22 o 5 1 25 16.98 18.40 4.47 o 0 2 25 877.21 1117.74 53.12 o 1 2 25 168.61 191.30 11.51 o 2 2 25 52.90 47.18 6.44 o 3 2 25 52.67 47.80 6.48 o 4 2 25 391.94 364.19 19.38 o 5 2 25 18.68 19.52 4.51 o 1 3 25 17.49 7.84 5.61 o 2 3 25 680.40 786.14 38.31 o 3 3 25 1.95 0.00 8947.59 o 4 3 25 12.78 14.20 5.07 o 5 3 25 1.26 7.76 3.81 o 0 4 25 450.57 467.37 24.09 o 1 4 25 15.34 0.00 11328.01 o 2 4 25 27.85 29.29 5.85 o 3 4 25 33.32 47.32 5.98 o 4 4 25 79.37 64.31 6.67 o 1 5 25 12.32 16.23 5.66 o 2 5 25 3.68 12.59 5.52 o 3 5 25 10.62 0.00 9005.34 o 4 5 25 14.48 0.00 8473.39 o 0 6 25 70.85 75.48 7.49 o 1 6 25 76.24 93.53 7.68 o 2 6 25 1.59 1.46 7.93 o 3 6 25 24.44 29.91 5.17 o 4 6 25 99.24 96.90 7.15 o 1 7 25 63.79 68.67 6.83 o 2 7 25 357.37 389.93 20.50 o 3 7 25 28.70 29.91 4.75 o 0 8 25 456.05 537.79 27.07 o 1 8 25 10.19 3.06 4.76 o 2 8 25 1.93 11.85 4.16 o 3 8 25 18.19 18.60 4.17 o 1 9 25 17.14 18.82 4.49 o 2 9 25 28.67 23.37 4.57 o 0 10 25 8.40 6.78 4.13 o 0 0 26 2173.78 2891.17 133.98 o 1 0 26 360.63 421.36 21.62 o 2 0 26 106.62 102.94 8.06 o 3 0 26 37.08 32.92 6.29 o 4 0 26 56.14 51.97 6.10 o 5 0 26 53.14 55.13 5.61 o 1 1 26 68.63 50.84 7.22 o 2 1 26 95.18 111.77 8.63 o 3 1 26 163.45 186.08 11.56 o 4 1 26 18.20 11.06 5.23 o 5 1 26 3.71 8.82 4.00 o 0 2 26 110.44 159.92 10.33 o 1 2 26 53.25 59.82 6.61 o 2 2 26 4.48 18.27 5.52 o 3 2 26 344.97 367.98 19.47 o 4 2 26 27.67 22.93 5.76 o 5 2 26 2.75 3.97 3.90 o 1 3 26 15.56 16.97 5.73 o 2 3 26 171.34 170.05 11.45 o 3 3 26 69.20 56.77 6.78 o 4 3 26 13.58 24.74 4.85 o 5 3 26 53.36 49.77 5.07 o 0 4 26 1198.20 1319.39 62.80 o 1 4 26 194.27 198.43 12.26 o 2 4 26 39.02 44.76 5.77 o 3 4 26 14.29 8.89 5.09 o 4 4 26 205.68 193.00 11.57 o 1 5 26 49.50 53.94 6.61 o 2 5 26 497.80 590.90 29.31 o 3 5 26 83.42 90.93 7.57 o 4 5 26 26.03 29.21 4.62 o 0 6 26 132.75 153.99 10.42 o 1 6 26 10.73 0.00 10091.15 o 2 6 26 7.11 14.45 4.97 o 3 6 26 5.45 0.00 7891.30 o 4 6 26 146.88 117.65 8.29 o 1 7 26 21.26 16.97 5.45 o 2 7 26 45.31 43.81 6.00 o 3 7 26 1.50 0.00 7422.37 o 0 8 26 35.47 35.48 5.81 o 1 8 26 1.40 13.74 4.23 o 2 8 26 1.30 0.00 7648.72 o 3 8 26 5.87 6.30 3.76 o 1 9 26 2.12 6.33 4.01 o 2 9 26 81.27 66.90 5.88 o 1 1 27 151.41 149.65 10.37 o 2 1 27 144.72 184.80 11.52 o 3 1 27 62.70 52.57 6.80 o 4 1 27 21.62 16.75 5.14 o 5 1 27 21.65 23.73 4.31 o 0 2 27 13.74 26.38 5.71 o 1 2 27 191.05 203.68 12.20 o 2 2 27 238.68 245.63 14.12 o 3 2 27 213.22 227.97 13.26 o 4 2 27 96.94 108.84 8.21 o 1 3 27 299.65 354.53 18.82 o 2 3 27 697.70 850.54 41.18 o 3 3 27 67.19 70.57 6.80 o 4 3 27 37.15 30.25 5.45 o 0 4 27 712.91 870.78 42.35 o 1 4 27 89.38 96.42 8.39 o 2 4 27 15.99 18.63 5.22 o 3 4 27 58.48 52.46 6.74 o 4 4 27 53.65 55.63 5.86 o 1 5 27 8.13 24.28 5.48 o 2 5 27 54.91 45.84 6.30 o 3 5 27 23.42 30.37 5.16 o 4 5 27 9.88 3.76 4.15 o 0 6 27 204.23 222.83 15.70 o 1 6 27 35.34 30.96 6.06 o 2 6 27 17.87 23.40 5.27 o 3 6 27 13.87 5.18 4.66 o 1 7 27 135.28 165.28 10.31 o 2 7 27 93.08 120.00 8.45 o 3 7 27 32.86 33.53 4.73 o 0 8 27 101.68 97.49 7.54 o 1 8 27 32.82 44.86 5.16 o 2 8 27 10.90 21.68 4.19 o 1 9 27 15.52 9.91 4.21 o 0 0 28 55.68 69.86 7.58 o 1 0 28 141.88 162.09 10.50 o 2 0 28 213.74 214.57 12.75 o 3 0 28 550.76 614.98 30.47 o 4 0 28 15.11 11.42 4.95 o 1 1 28 290.59 329.85 17.88 o 2 1 28 61.45 71.07 7.65 o 3 1 28 66.80 65.09 6.95 o 4 1 28 7.74 4.04 4.53 o 0 2 28 19.23 17.76 5.80 o 1 2 28 83.81 86.44 7.87 o 2 2 28 103.00 125.53 9.24 o 3 2 28 20.28 25.72 5.33 o 4 2 28 1.19 0.00 8675.63 o 1 3 28 42.90 54.89 6.50 o 2 3 28 37.51 53.16 6.67 o 3 3 28 52.66 46.45 6.29 o 4 3 28 3.79 11.44 4.17 o 0 4 28 263.16 260.64 15.16 o 1 4 28 130.49 149.23 10.16 o 2 4 28 17.51 21.33 5.34 o 3 4 28 153.12 193.99 11.59 o 4 4 28 16.64 13.69 4.31 o 1 5 28 87.45 109.69 8.40 o 2 5 28 17.39 20.91 5.50 o 3 5 28 89.67 113.22 7.97 o 4 5 28 14.14 14.54 3.98 o 0 6 28 77.67 94.41 7.94 o 1 6 28 179.01 185.40 11.75 o 2 6 28 0.64 11.03 4.69 o 3 6 28 19.26 22.50 4.59 o 1 7 28 40.57 53.72 5.76 o 2 7 28 5.09 0.00 7767.38 o 3 7 28 7.97 11.44 3.83 o 0 8 28 43.00 49.59 5.64 o 1 8 28 18.65 20.50 4.41 o 2 8 28 5.59 10.76 3.89 o 1 1 29 211.37 191.08 12.34 o 2 1 29 168.90 196.13 12.50 o 3 1 29 60.13 71.96 6.86 o 4 1 29 11.95 12.43 4.40 o 0 2 29 197.83 237.50 13.64 o 1 2 29 467.16 559.04 27.96 o 2 2 29 84.35 123.98 8.84 o 3 2 29 43.27 57.27 6.35 o 4 2 29 96.81 101.64 7.47 o 1 3 29 125.34 152.19 10.36 o 2 3 29 35.26 58.70 6.31 o 3 3 29 117.81 120.62 8.81 o 4 3 29 19.63 15.96 4.38 o 0 4 29 43.29 52.34 6.51 o 1 4 29 68.59 103.50 8.31 o 2 4 29 25.70 39.03 6.00 o 3 4 29 18.32 16.72 5.01 o 4 4 29 2.36 0.00 7575.20 o 1 5 29 11.90 17.38 5.20 o 2 5 29 11.53 1.00 13.56 o 3 5 29 4.28 16.69 4.35 o 0 6 29 38.00 22.00 5.53 o 1 6 29 112.74 101.57 8.38 o 2 6 29 12.74 17.72 4.71 o 3 6 29 19.89 18.99 4.45 o 1 7 29 63.42 67.80 6.47 o 2 7 29 43.78 42.91 5.05 o 0 8 29 71.46 68.19 6.62 o 1 8 29 29.74 31.46 5.13 o 0 0 30 2515.01 3469.26 161.01 o 1 0 30 2.06 6.33 5.31 o 2 0 30 3.54 0.00 8553.86 o 3 0 30 77.81 103.21 7.84 o 4 0 30 297.33 305.21 16.14 o 1 1 30 187.37 197.98 12.46 o 2 1 30 696.88 792.90 38.91 o 3 1 30 56.53 52.08 6.44 o 4 1 30 12.31 20.43 4.37 o 0 2 30 191.29 243.94 13.95 o 1 2 30 95.62 94.58 8.24 o 2 2 30 0.04 0.00 9402.92 o 3 2 30 85.86 97.61 7.70 o 4 2 30 28.37 32.57 4.88 o 1 3 30 27.41 36.75 5.82 o 2 3 30 40.31 40.08 6.27 o 3 3 30 3.74 7.30 4.72 o 4 3 30 11.57 10.39 3.92 o 0 4 30 375.88 445.36 23.18 o 1 4 30 76.35 85.38 7.69 o 2 4 30 31.02 27.68 5.69 o 3 4 30 11.91 20.33 4.67 o 4 4 30 35.71 32.97 4.64 o 1 5 30 7.80 15.12 5.14 o 2 5 30 176.31 230.87 13.22 o 3 5 30 1.01 0.00 8092.42 o 0 6 30 189.05 204.56 12.45 o 1 6 30 14.59 11.75 4.84 o 2 6 30 10.82 17.25 4.52 o 3 6 30 36.95 30.67 4.98 o 1 7 30 1.72 0.00 8035.87 o 2 7 30 6.25 1.86 4.08 o 0 8 30 16.13 0.00 10628.68 o 1 8 30 2.04 5.51 3.96 o 1 1 31 22.02 21.02 5.72 o 2 1 31 310.57 324.32 18.00 o 3 1 31 4.96 12.30 4.74 o 4 1 31 17.89 3.17 4.43 o 0 2 31 81.62 126.94 9.03 o 1 2 31 58.28 59.53 6.77 o 2 2 31 122.49 132.97 9.33 o 3 2 31 1.95 0.00 8488.58 o 4 2 31 123.43 111.93 7.84 o 1 3 31 52.98 51.26 7.04 o 2 3 31 114.78 128.11 9.25 o 3 3 31 43.74 56.64 5.80 o 4 3 31 5.98 7.61 3.82 o 0 4 31 192.05 225.97 13.31 o 1 4 31 33.76 30.62 5.94 o 2 4 31 26.84 22.50 5.34 o 3 4 31 8.66 15.27 4.28 o 1 5 31 34.13 26.54 5.45 o 2 5 31 8.15 12.22 4.52 o 3 5 31 6.92 8.05 4.05 o 0 6 31 153.05 139.30 9.82 o 1 6 31 13.93 10.94 4.77 o 2 6 31 10.40 10.03 4.38 o 1 7 31 6.58 3.37 4.03 o 2 7 31 50.86 52.52 5.37 o 0 8 31 98.71 109.20 12.73 o 0 0 32 282.20 361.04 19.28 o 1 0 32 5.09 6.55 4.95 o 2 0 32 5.60 14.95 4.76 o 3 0 32 43.84 46.19 5.70 o 4 0 32 137.84 137.45 8.87 o 1 1 32 20.67 28.08 5.93 o 2 1 32 106.71 100.35 8.41 o 3 1 32 21.85 12.54 4.95 o 4 1 32 0.89 2.87 3.66 o 0 2 32 33.79 30.91 5.72 o 1 2 32 20.09 29.41 5.74 o 2 2 32 33.77 34.77 5.66 o 3 2 32 5.75 8.10 4.37 o 1 3 32 124.91 142.92 10.04 o 2 3 32 25.57 20.67 5.40 o 3 3 32 23.13 24.81 4.78 o 0 4 32 42.54 40.33 6.19 o 1 4 32 53.74 46.51 6.24 o 2 4 32 40.74 33.80 5.32 o 3 4 32 85.02 51.78 6.15 o 1 5 32 11.06 16.11 4.82 o 2 5 32 69.93 70.38 6.47 o 3 5 32 5.47 0.00 8383.10 o 0 6 32 17.96 32.78 4.98 o 1 6 32 47.82 26.31 5.04 o 2 6 32 1.36 0.00 7509.17 o 1 7 32 25.14 13.39 7.02 o 1 1 33 38.49 52.34 6.40 o 2 1 33 51.41 58.54 6.19 o 3 1 33 29.62 34.50 5.06 o 0 2 33 20.18 34.80 5.98 o 1 2 33 492.93 598.71 30.06 o 2 2 33 1.28 11.46 4.79 o 3 2 33 142.78 133.64 9.27 o 1 3 33 309.49 374.43 19.78 o 2 3 33 6.61 6.96 4.63 o 3 3 33 96.04 70.10 6.71 o 0 4 33 3.03 0.00 8440.52 o 1 4 33 16.10 5.56 5.08 o 2 4 33 0.20 0.47 18.83 o 3 4 33 68.41 55.03 5.95 o 1 5 33 2.00 3.26 4.29 o 2 5 33 1.76 4.97 4.13 o 0 6 33 26.55 25.27 4.56 o 1 6 33 16.69 1.51 7.14 o 2 6 33 0.75 0.00 8025.23 o 0 0 34 1.19 0.00 11872.65 o 1 0 34 9.73 0.65 18.10 o 2 0 34 1.12 0.00 8618.97 o 3 0 34 47.21 57.22 5.38 o 1 1 34 24.11 21.09 5.66 o 2 1 34 22.35 19.69 5.13 o 3 1 34 13.70 2.68 4.43 o 0 2 34 32.16 38.00 5.59 o 1 2 34 55.54 58.08 6.63 o 2 2 34 9.69 18.99 4.51 o 3 2 34 20.06 9.86 4.61 o 1 3 34 27.40 31.88 5.68 o 2 3 34 2.58 0.00 8820.77 o 3 3 34 24.92 21.97 4.36 o 0 4 34 37.05 37.22 5.67 o 1 4 34 61.70 53.73 6.37 o 2 4 34 31.11 18.80 4.75 o 1 5 34 180.76 176.60 10.86 o 2 5 34 236.92 224.22 12.93 o 0 6 34 90.05 35.79 16.74 o 1 6 34 37.67 0.00 11903.07 o 1 1 35 0.85 0.08 131.16 o 2 1 35 26.91 23.08 5.23 o 3 1 35 1.26 1.88 3.80 o 0 2 35 91.50 95.10 7.74 o 1 2 35 5.55 10.54 4.56 o 2 2 35 3.05 4.01 4.24 o 3 2 35 9.87 0.00 8636.15 o 1 3 35 23.16 25.84 5.00 o 2 3 35 31.51 17.76 5.03 o 0 4 35 95.74 77.96 7.08 o 1 4 35 58.84 71.46 6.33 o 2 4 35 6.41 7.78 3.86 o 1 5 35 8.83 0.00 9366.95 o 0 6 35 70.11 0.00 17971.07 o 0 0 36 302.81 300.41 16.80 o 1 0 36 51.44 44.42 5.54 o 2 0 36 0.36 5.96 3.97 o 1 1 36 15.88 5.56 4.65 o 2 1 36 77.68 42.29 6.54 o 0 2 36 61.28 67.49 6.58 o 1 2 36 16.98 21.57 4.70 o 2 2 36 29.16 35.03 4.83 o 1 3 36 5.38 4.79 4.33 o 2 3 36 197.49 141.24 9.99 o 0 4 36 115.32 114.32 26.12 o 1 4 36 8.42 0.00 9434.24 o 1 5 36 9.32 0.00 10267.11 o 1 1 37 33.78 33.58 4.99 o 2 1 37 26.33 0.00 12843.58 o 0 2 37 45.28 45.73 5.93 o 1 2 37 90.36 58.17 15.23 o 2 2 37 2.15 0.00 8549.82 o 1 3 37 46.98 0.00 14080.55 o 0 4 37 43.75 0.00 13792.36 o 1 4 37 11.82 0.00 10323.93 o 0 0 38 31.54 0.00 16228.51 o 1 0 38 91.07 0.00 21091.08 o 1 1 38 56.12 0.00 15666.54 o 0 2 38 6.27 8.94 4.16 o 1 2 38 3.65 0.00 8953.96 o 1 3 38 0.94 0.00 8568.44 o 0 2 39 43.16 0.00 12811.22 o