#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:12:02 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180980 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/60/2206018.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206018_Fobs loop_ _publ_author_name 'Trilleras, Jorge' 'Quiroga, Jairo' 'Cobo, Justo' 'Low, John N.' 'Glidewell, Christopher' _publ_section_title ; 3-(5-Chloro-3-methyl-1-phenylpyrazol-4-yl)-1,5-di-2-thienylpentane-1,5-dione: centrosymmetric dimers formed by C---H···\p(thiophene) hydrogen bonds ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1892 _journal_page_last o1894 _journal_volume 61 _journal_year 2005 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.6729 _cell_length_b 17.8962 _cell_length_c 16.2619 _exptl_crystal_F_000 1888.00 _reflns_d_resolution_high 0.7694 _cod_data_source_file lh6436Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 446' _shelx_refln_list_code 4 _shelx_f_calc_maximum 422.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 178808.38 165977.39 3058.73 o 6 0 0 18760.51 20039.21 433.57 o 8 0 0 575.21 702.13 65.12 o 10 0 0 15982.96 16683.23 598.34 o 12 0 0 39.34 63.09 69.78 o 14 0 0 925.23 1033.21 140.76 o 16 0 0 22.06 -78.73 142.46 o 18 0 0 144.92 147.24 140.25 o 4 1 0 156824.23 147124.50 1943.50 o 6 1 0 2423.49 2584.62 48.12 o 8 1 0 12818.03 13233.33 170.68 o 10 1 0 909.79 1032.02 42.18 o 12 1 0 157.83 136.04 43.83 o 14 1 0 5135.51 6013.95 385.84 o 16 1 0 157.33 227.61 84.48 o 18 1 0 23.33 292.58 107.92 o 2 2 0 930.12 552.99 43.11 o 4 2 0 1077.66 936.39 24.48 o 6 2 0 11245.12 10665.33 123.55 o 8 2 0 3108.41 3243.96 61.34 o 10 2 0 96.45 87.57 26.23 o 12 2 0 2088.78 2197.82 74.99 o 14 2 0 486.51 540.32 195.72 o 16 2 0 905.39 845.22 120.82 o 18 2 0 766.08 1013.33 165.22 o 2 3 0 37673.97 34814.45 366.22 o 4 3 0 4527.98 4568.63 63.81 o 6 3 0 10795.28 10421.07 141.56 o 8 3 0 1160.12 1085.95 32.04 o 10 3 0 2840.74 2720.31 62.71 o 12 3 0 1036.83 848.91 75.26 o 14 3 0 2230.54 2278.54 161.72 o 16 3 0 198.86 236.39 97.82 o 18 3 0 953.44 1187.26 285.53 o 0 4 0 15084.73 14252.60 308.32 o 2 4 0 8903.62 8730.06 104.16 o 4 4 0 4495.16 4199.23 83.20 o 6 4 0 18697.90 17121.13 185.97 o 8 4 0 1640.86 1591.48 46.05 o 10 4 0 12.59 -11.70 21.34 o 12 4 0 181.87 175.84 39.36 o 14 4 0 9.78 51.84 62.09 o 16 4 0 7.09 21.31 94.93 o 18 4 0 0.17 -154.20 159.09 o 2 5 0 19682.98 17501.87 232.90 o 4 5 0 1050.78 901.77 23.99 o 6 5 0 2126.61 2008.65 42.61 o 8 5 0 597.05 584.46 28.66 o 10 5 0 2902.60 2845.90 73.31 o 12 5 0 2495.74 2323.44 90.32 o 14 5 0 2061.17 2199.23 181.91 o 16 5 0 616.52 646.70 111.01 o 18 5 0 23.79 -103.71 117.89 o 0 6 0 23181.31 21816.53 603.77 o 2 6 0 20072.85 19779.02 227.03 o 4 6 0 22894.96 24879.11 275.25 o 6 6 0 738.57 937.10 30.34 o 8 6 0 4.11 -0.78 21.12 o 10 6 0 1641.81 1541.77 53.24 o 12 6 0 84.25 86.56 39.35 o 14 6 0 67.54 -61.68 61.68 o 16 6 0 1.33 -61.06 96.87 o 18 6 0 2.67 90.88 137.01 o 2 7 0 11989.26 12240.05 170.11 o 4 7 0 2492.05 2145.74 49.41 o 6 7 0 1013.90 1233.13 31.80 o 8 7 0 1020.89 1029.49 45.27 o 10 7 0 5090.46 5261.97 136.31 o 12 7 0 2775.45 2804.26 109.13 o 14 7 0 25.12 50.64 69.41 o 16 7 0 11.66 48.50 181.66 o 18 7 0 106.82 -66.93 142.25 o 0 8 0 4994.87 5245.30 123.14 o 2 8 0 715.94 696.78 31.97 o 4 8 0 6056.70 6937.91 110.11 o 6 8 0 113.71 100.52 11.86 o 8 8 0 46.36 36.55 15.81 o 10 8 0 785.43 706.29 48.24 o 12 8 0 3223.53 3227.43 197.98 o 14 8 0 16.21 31.74 66.38 o 16 8 0 611.77 346.23 151.07 o 2 9 0 1.79 13.68 19.37 o 4 9 0 747.83 649.97 27.29 o 6 9 0 2923.07 2864.64 68.83 o 8 9 0 5145.55 5437.05 116.17 o 10 9 0 941.31 893.41 56.59 o 12 9 0 1.19 -3.55 42.37 o 14 9 0 543.51 472.48 89.58 o 16 9 0 262.23 228.86 115.03 o 0 10 0 280.12 448.82 59.74 o 2 10 0 2460.55 2386.48 63.65 o 4 10 0 4645.50 4726.52 83.00 o 6 10 0 1652.78 1692.52 51.27 o 8 10 0 4.67 62.16 26.93 o 10 10 0 270.73 254.88 36.85 o 12 10 0 1697.28 1807.84 87.70 o 14 10 0 194.01 176.28 83.45 o 16 10 0 278.75 205.27 146.88 o 2 11 0 1.83 -8.23 26.61 o 4 11 0 3375.05 3619.56 92.85 o 6 11 0 626.86 643.76 36.48 o 8 11 0 59.79 36.17 38.68 o 10 11 0 652.54 673.65 56.56 o 12 11 0 432.89 423.06 61.71 o 14 11 0 406.61 545.65 82.77 o 16 11 0 1.12 75.74 128.66 o 0 12 0 5001.07 5207.25 115.13 o 2 12 0 3593.28 3465.61 75.08 o 4 12 0 2709.82 2616.53 80.95 o 6 12 0 10.59 36.49 39.57 o 8 12 0 690.59 594.03 52.89 o 10 12 0 807.39 886.11 80.90 o 12 12 0 1805.34 1858.82 126.08 o 14 12 0 989.09 1321.10 116.02 o 16 12 0 14.47 -148.34 150.30 o 2 13 0 6932.47 7446.97 163.70 o 4 13 0 520.41 596.76 45.55 o 6 13 0 32.35 48.36 37.29 o 8 13 0 263.92 243.07 42.10 o 10 13 0 111.49 130.84 61.45 o 12 13 0 2045.51 2117.24 142.12 o 14 13 0 682.04 624.70 101.35 o 0 14 0 198.43 146.95 60.58 o 2 14 0 456.89 406.35 47.46 o 4 14 0 4892.98 4832.67 140.52 o 6 14 0 199.25 168.11 40.96 o 8 14 0 4491.05 4423.35 181.99 o 10 14 0 1376.45 1496.35 105.81 o 12 14 0 416.98 214.63 72.96 o 14 14 0 598.98 655.28 104.05 o 2 15 0 16425.78 16467.67 393.29 o 4 15 0 2229.88 2315.25 226.51 o 6 15 0 137.27 156.52 43.66 o 8 15 0 1047.18 794.78 101.49 o 10 15 0 418.39 329.03 62.49 o 12 15 0 727.46 907.38 101.16 o 14 15 0 9.33 26.49 85.68 o 0 16 0 88.71 108.12 70.10 o 2 16 0 4454.54 4429.40 176.60 o 4 16 0 222.10 250.64 62.22 o 6 16 0 330.04 471.13 65.23 o 8 16 0 705.36 804.64 81.92 o 10 16 0 1107.18 1022.52 100.81 o 12 16 0 12.27 99.57 78.81 o 2 17 0 1474.00 1296.63 61.18 o 4 17 0 28.94 -69.87 69.87 o 6 17 0 1052.85 1092.42 139.72 o 8 17 0 237.80 283.65 74.30 o 10 17 0 258.38 128.01 71.69 o 12 17 0 58.19 124.89 82.38 o 0 18 0 3107.97 3097.30 187.16 o 2 18 0 1286.00 1334.08 78.91 o 4 18 0 591.53 433.22 79.55 o 6 18 0 415.79 496.91 77.39 o 8 18 0 1073.89 1129.57 113.29 o 10 18 0 100.82 75.10 77.68 o 12 18 0 48.80 162.41 148.09 o 2 19 0 528.58 698.22 66.96 o 4 19 0 2957.62 3116.47 187.30 o 6 19 0 694.29 685.72 87.34 o 8 19 0 2858.44 3276.75 178.39 o 10 19 0 492.50 552.67 100.34 o 0 20 0 3233.44 3415.19 205.47 o 2 20 0 14.15 -12.45 72.29 o 4 20 0 559.21 526.98 94.86 o 6 20 0 527.03 689.31 121.34 o 8 20 0 567.37 656.77 136.90 o 2 21 0 178.97 104.43 69.39 o 4 21 0 1519.37 1460.66 156.87 o 6 21 0 479.62 616.73 95.45 o 8 21 0 33.89 18.41 194.95 o 0 22 0 1662.35 1951.72 190.42 o 2 22 0 2421.20 2532.78 170.63 o 4 22 0 664.40 693.11 93.53 o 6 22 0 73.38 252.66 233.81 o 2 23 0 320.84 337.55 105.11 o 2 1 1 5458.96 1944.74 285.78 o 3 1 1 9463.83 8930.87 89.53 o 4 1 1 498.98 531.85 12.24 o 5 1 1 1366.46 1415.29 22.29 o 6 1 1 3608.96 3798.47 42.74 o 7 1 1 625.29 685.16 17.22 o 8 1 1 3786.69 4201.77 51.62 o 9 1 1 39.64 24.25 14.48 o 10 1 1 2966.16 3038.86 54.98 o 11 1 1 395.62 341.76 22.28 o 12 1 1 1553.59 1605.86 60.78 o 13 1 1 187.94 154.99 30.66 o 14 1 1 2248.88 2226.44 105.77 o 15 1 1 692.52 708.70 75.86 o 16 1 1 194.06 168.67 66.50 o 17 1 1 5.89 19.41 70.63 o 18 1 1 806.37 845.46 96.50 o 19 1 1 115.08 -87.73 87.73 o 1 2 1 143.75 55.21 12.95 o 2 2 1 7428.28 7069.06 85.08 o 3 2 1 9381.73 8988.28 85.86 o 4 2 1 57247.31 55592.40 509.79 o 5 2 1 850.44 714.78 15.35 o 6 2 1 10078.20 10391.77 90.48 o 7 2 1 5241.79 5248.47 69.68 o 8 2 1 2536.96 2718.49 37.30 o 9 2 1 602.60 689.18 22.18 o 10 2 1 48.54 77.47 15.43 o 11 2 1 709.95 728.16 29.30 o 12 2 1 2.61 34.70 23.20 o 13 2 1 1.81 9.47 27.28 o 14 2 1 2721.70 2939.27 175.70 o 15 2 1 871.41 902.37 72.48 o 16 2 1 89.46 35.97 61.82 o 17 2 1 135.83 155.36 78.24 o 18 2 1 315.60 278.72 90.80 o 1 3 1 2811.25 2784.49 74.51 o 2 3 1 25504.07 25115.72 212.55 o 3 3 1 45831.68 45018.07 383.79 o 4 3 1 2545.77 2751.33 31.92 o 5 3 1 1204.04 1385.04 21.50 o 6 3 1 345.85 376.17 13.83 o 7 3 1 31453.60 33440.34 274.20 o 8 3 1 162.47 165.21 13.76 o 9 3 1 1384.70 1415.85 31.34 o 10 3 1 185.90 223.51 18.04 o 11 3 1 6184.78 6746.09 114.33 o 12 3 1 180.41 167.85 26.28 o 13 3 1 103.33 73.10 30.50 o 14 3 1 11.26 43.82 47.57 o 15 3 1 695.08 619.06 69.97 o 16 3 1 42.53 45.07 63.68 o 17 3 1 51.30 -85.46 85.46 o 18 3 1 17.23 -16.67 78.60 o 0 4 1 12.09 0.54 10.16 o 1 4 1 1398.95 1534.47 16.49 o 2 4 1 2926.68 2827.43 28.94 o 3 4 1 111.24 98.17 6.66 o 4 4 1 27217.11 26760.82 240.63 o 5 4 1 3136.86 3145.87 35.61 o 6 4 1 887.56 752.99 18.81 o 7 4 1 4802.21 5352.41 56.34 o 8 4 1 32.24 10.57 11.91 o 9 4 1 2516.15 2589.51 51.02 o 10 4 1 97.32 108.52 16.32 o 11 4 1 150.08 151.81 21.31 o 12 4 1 1971.92 1901.15 56.14 o 13 4 1 221.79 115.40 33.55 o 14 4 1 675.01 652.40 89.59 o 15 4 1 28.32 49.46 50.87 o 16 4 1 146.11 135.69 65.22 o 17 4 1 69.82 82.32 66.53 o 18 4 1 12.25 6.26 84.77 o 1 5 1 20.10 21.68 8.59 o 2 5 1 36.14 2.83 5.56 o 3 5 1 23.98 -3.10 7.61 o 4 5 1 30.86 19.51 7.91 o 5 5 1 198.58 162.54 12.56 o 6 5 1 6227.42 6268.21 60.96 o 7 5 1 3283.79 3485.68 44.70 o 8 5 1 2096.68 1921.09 35.38 o 9 5 1 19.96 29.96 15.21 o 10 5 1 8001.54 8824.43 129.66 o 11 5 1 3773.20 4020.61 70.35 o 12 5 1 335.78 288.57 30.61 o 13 5 1 197.66 170.73 31.98 o 14 5 1 672.20 686.16 112.51 o 15 5 1 27.93 -18.20 60.78 o 16 5 1 464.02 407.55 92.41 o 17 5 1 19.93 31.84 86.44 o 18 5 1 336.42 316.02 84.52 o 0 6 1 10485.37 10999.46 181.64 o 1 6 1 8541.78 8066.79 73.85 o 2 6 1 2270.95 2477.10 28.22 o 3 6 1 920.70 760.63 16.22 o 4 6 1 252.20 200.93 12.43 o 5 6 1 1497.58 1774.28 24.04 o 6 6 1 204.72 190.11 15.46 o 7 6 1 1708.76 1757.93 35.00 o 8 6 1 420.05 409.82 20.19 o 9 6 1 2235.17 2244.09 50.77 o 10 6 1 0.40 -12.01 17.26 o 11 6 1 1870.39 1882.37 49.08 o 12 6 1 2154.96 2333.58 67.38 o 13 6 1 35.62 33.84 35.24 o 14 6 1 617.70 731.41 62.59 o 15 6 1 149.67 72.39 79.74 o 16 6 1 235.69 182.83 73.94 o 17 6 1 199.90 247.61 82.09 o 18 6 1 0.17 17.58 80.02 o 1 7 1 0.64 -5.25 9.73 o 2 7 1 392.93 314.63 14.12 o 3 7 1 19520.52 19838.74 157.80 o 4 7 1 248.69 196.78 18.41 o 5 7 1 1700.93 1636.35 23.60 o 6 7 1 71.76 83.30 12.61 o 7 7 1 3891.36 4208.02 52.47 o 8 7 1 417.25 405.61 20.05 o 9 7 1 185.76 184.25 18.11 o 10 7 1 4452.45 4698.85 81.96 o 11 7 1 1145.83 1138.61 42.80 o 12 7 1 2628.45 2597.69 72.40 o 13 7 1 548.33 502.47 42.89 o 14 7 1 532.76 593.59 64.41 o 15 7 1 10.27 -31.10 49.80 o 16 7 1 297.67 319.57 71.88 o 17 7 1 12.39 30.49 75.97 o 18 7 1 428.99 476.19 96.65 o 0 8 1 9718.36 9430.98 137.72 o 1 8 1 7462.82 7678.74 74.73 o 2 8 1 2784.30 2527.21 42.29 o 3 8 1 1571.40 1834.44 25.27 o 4 8 1 1139.31 1154.95 25.16 o 5 8 1 6924.70 7001.26 74.54 o 6 8 1 413.81 417.92 15.98 o 7 8 1 2697.66 2553.40 44.61 o 8 8 1 2778.73 2888.69 49.45 o 9 8 1 3.29 -3.27 15.16 o 10 8 1 2660.66 2809.10 63.64 o 11 8 1 390.43 340.68 30.11 o 12 8 1 521.05 512.50 34.89 o 13 8 1 7.47 31.24 35.59 o 14 8 1 29.56 35.88 56.47 o 15 8 1 18.08 11.17 51.93 o 16 8 1 34.29 3.16 80.77 o 17 8 1 62.10 43.97 76.48 o 1 9 1 1933.87 1834.17 36.41 o 2 9 1 924.82 995.81 23.05 o 3 9 1 1.51 33.44 13.28 o 4 9 1 11.50 -5.46 12.36 o 5 9 1 277.22 274.39 17.59 o 6 9 1 344.57 337.36 18.09 o 7 9 1 77.97 104.34 16.26 o 8 9 1 643.79 610.74 27.50 o 9 9 1 1923.41 1927.66 43.40 o 10 9 1 1321.98 1321.25 41.86 o 11 9 1 97.41 79.09 22.96 o 12 9 1 630.92 595.27 39.04 o 13 9 1 404.53 394.60 39.42 o 14 9 1 1875.66 1976.54 89.62 o 15 9 1 384.93 494.52 71.78 o 16 9 1 1954.50 2136.94 134.69 o 17 9 1 6.14 -85.19 85.19 o 0 10 1 1.18 -13.70 18.85 o 1 10 1 11.76 15.70 15.27 o 2 10 1 2.04 6.00 16.09 o 3 10 1 1150.84 1196.10 25.13 o 4 10 1 5013.44 5114.78 61.98 o 5 10 1 2211.69 2124.86 35.97 o 6 10 1 5229.27 5280.81 80.16 o 7 10 1 33.31 27.77 18.93 o 8 10 1 2868.94 2799.49 56.89 o 9 10 1 1626.24 1671.79 47.38 o 10 10 1 34.83 31.96 18.04 o 11 10 1 209.17 219.92 23.61 o 12 10 1 1594.10 1603.51 53.92 o 13 10 1 518.63 473.01 52.31 o 14 10 1 53.06 -30.10 59.69 o 15 10 1 31.95 26.37 54.66 o 16 10 1 35.12 -46.26 77.83 o 17 10 1 304.24 174.67 97.62 o 1 11 1 5171.68 5212.89 70.56 o 2 11 1 2459.93 2429.31 42.43 o 3 11 1 7088.09 7157.62 84.38 o 4 11 1 0.28 3.48 16.75 o 5 11 1 542.78 619.47 24.47 o 6 11 1 2373.87 2164.08 43.60 o 7 11 1 1553.63 1531.89 39.56 o 8 11 1 6082.88 5957.14 108.13 o 9 11 1 50.15 -8.90 33.49 o 10 11 1 853.10 933.16 45.70 o 11 11 1 238.44 187.23 31.38 o 12 11 1 53.00 -2.94 36.16 o 13 11 1 340.01 442.79 50.01 o 14 11 1 155.74 184.47 53.77 o 15 11 1 21.86 66.71 57.58 o 16 11 1 117.79 208.43 92.15 o 0 12 1 646.62 726.23 34.06 o 1 12 1 1390.21 1252.38 34.74 o 2 12 1 215.49 178.09 20.91 o 3 12 1 704.32 786.83 23.67 o 4 12 1 2221.11 2057.80 44.13 o 5 12 1 903.84 1008.20 32.93 o 6 12 1 4226.82 4449.56 74.74 o 7 12 1 2421.47 2498.29 69.99 o 8 12 1 234.55 201.04 31.68 o 9 12 1 2681.91 2640.85 76.22 o 10 12 1 1411.24 1377.41 57.64 o 11 12 1 599.62 627.71 52.56 o 12 12 1 128.73 152.31 41.81 o 13 12 1 620.02 646.68 71.69 o 14 12 1 0.19 -53.60 53.60 o 15 12 1 76.80 87.20 63.55 o 16 12 1 36.60 -73.80 95.39 o 1 13 1 568.79 592.96 29.63 o 2 13 1 49.88 54.18 31.48 o 3 13 1 1501.53 1457.95 34.38 o 4 13 1 56.70 52.85 29.03 o 5 13 1 3299.67 3260.89 73.99 o 6 13 1 6.71 14.91 23.09 o 7 13 1 104.88 56.70 29.72 o 8 13 1 622.86 562.26 35.05 o 9 13 1 1023.82 989.42 61.73 o 10 13 1 239.77 208.18 36.43 o 11 13 1 991.09 929.26 54.15 o 12 13 1 77.61 61.99 47.09 o 13 13 1 2.37 33.59 57.78 o 14 13 1 1093.09 1118.73 92.30 o 15 13 1 326.65 312.99 81.53 o 0 14 1 6591.59 6512.22 140.29 o 1 14 1 1943.12 1917.23 46.69 o 2 14 1 2294.09 2273.81 71.76 o 3 14 1 1584.56 1560.07 49.33 o 4 14 1 508.62 453.77 32.93 o 5 14 1 5117.30 5160.03 119.22 o 6 14 1 1379.52 1442.91 72.00 o 7 14 1 306.83 335.01 44.27 o 8 14 1 169.22 128.52 42.69 o 9 14 1 562.84 474.93 42.17 o 10 14 1 711.70 764.09 58.09 o 11 14 1 153.22 215.77 42.56 o 12 14 1 92.97 162.32 52.53 o 13 14 1 0.01 -60.35 60.35 o 14 14 1 5.58 -7.73 58.04 o 15 14 1 18.83 55.05 133.61 o 1 15 1 1377.38 1329.98 53.89 o 2 15 1 0.46 -26.05 26.05 o 3 15 1 146.42 155.76 38.12 o 4 15 1 896.84 850.13 45.46 o 5 15 1 26.44 -14.21 37.09 o 6 15 1 85.14 83.50 30.77 o 7 15 1 174.35 157.23 39.90 o 8 15 1 75.46 100.17 38.40 o 9 15 1 532.12 532.74 45.31 o 10 15 1 286.14 312.47 44.80 o 11 15 1 10.01 22.29 54.40 o 12 15 1 914.83 1064.42 82.07 o 13 15 1 46.39 37.82 70.96 o 14 15 1 15.85 14.20 77.02 o 0 16 1 796.14 735.34 61.63 o 1 16 1 177.34 158.04 28.49 o 2 16 1 738.66 755.55 37.81 o 3 16 1 685.42 669.79 49.11 o 4 16 1 0.12 -18.34 33.25 o 5 16 1 45.80 29.73 40.20 o 6 16 1 261.20 262.95 42.21 o 7 16 1 16.56 8.33 39.45 o 8 16 1 218.60 152.53 43.19 o 9 16 1 61.18 20.81 38.96 o 10 16 1 426.26 248.32 55.08 o 11 16 1 42.45 89.89 62.66 o 12 16 1 18.45 -54.07 54.07 o 13 16 1 429.13 478.28 72.86 o 1 17 1 46.61 56.45 30.10 o 2 17 1 685.06 608.64 34.15 o 3 17 1 16.07 65.84 37.26 o 4 17 1 5.30 -38.22 38.22 o 5 17 1 18.77 9.07 39.62 o 6 17 1 8.92 -44.68 44.88 o 7 17 1 313.41 331.67 50.57 o 8 17 1 764.87 844.73 62.54 o 9 17 1 62.35 84.12 48.19 o 10 17 1 314.69 408.80 52.82 o 11 17 1 103.32 94.97 55.33 o 12 17 1 221.92 187.87 59.31 o 0 18 1 1163.01 1120.85 76.19 o 1 18 1 1292.02 1347.39 61.00 o 2 18 1 253.71 246.96 36.68 o 3 18 1 10.95 -26.03 46.36 o 4 18 1 1353.41 1568.79 75.12 o 5 18 1 595.74 696.60 58.35 o 6 18 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6 10 1122.85 1153.92 63.04 o 12 6 10 1544.87 1704.48 74.07 o 13 6 10 382.08 302.27 56.95 o 14 6 10 261.08 285.61 69.33 o 15 6 10 34.53 -21.63 116.24 o 1 7 10 133.60 175.78 11.60 o 2 7 10 113.43 109.31 10.64 o 3 7 10 92.12 104.08 12.24 o 4 7 10 1766.84 1660.82 31.63 o 5 7 10 1462.46 1556.80 29.41 o 6 7 10 32.04 38.01 11.19 o 7 7 10 1825.20 1864.23 47.77 o 8 7 10 150.39 134.57 22.06 o 9 7 10 179.20 110.27 25.90 o 10 7 10 183.40 100.53 31.38 o 11 7 10 986.64 833.86 58.17 o 12 7 10 20.18 18.33 40.88 o 13 7 10 51.38 165.31 58.75 o 14 7 10 1061.58 1080.45 113.02 o 15 7 10 1416.49 1637.34 190.12 o 0 8 10 2118.15 1958.23 56.28 o 1 8 10 1386.75 1348.53 35.22 o 2 8 10 631.48 648.90 19.48 o 3 8 10 71.99 72.74 12.29 o 4 8 10 349.94 326.48 16.85 o 5 8 10 2756.46 2683.95 47.56 o 6 8 10 868.57 773.89 27.16 o 7 8 10 1753.47 1713.44 48.23 o 8 8 10 1116.99 1060.07 50.38 o 9 8 10 1448.94 1301.96 47.96 o 10 8 10 886.30 802.13 44.50 o 11 8 10 1.16 49.74 49.69 o 12 8 10 79.49 93.89 50.95 o 13 8 10 238.98 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20.77 o 3 11 10 207.60 229.22 20.69 o 4 11 10 284.36 265.31 23.89 o 5 11 10 128.51 117.90 25.87 o 6 11 10 1093.61 1035.62 38.66 o 7 11 10 117.34 121.90 26.80 o 8 11 10 15.19 55.38 29.42 o 9 11 10 0.22 31.72 30.88 o 10 11 10 23.22 46.54 32.91 o 11 11 10 60.47 85.84 72.45 o 12 11 10 82.41 13.99 77.02 o 13 11 10 38.38 87.56 81.69 o 14 11 10 126.45 -3.41 150.47 o 0 12 10 2490.82 2349.20 94.36 o 1 12 10 206.23 210.63 27.52 o 2 12 10 1360.97 1325.34 39.71 o 3 12 10 0.19 5.87 19.89 o 4 12 10 25.45 4.59 19.27 o 5 12 10 0.01 -7.87 21.01 o 6 12 10 28.23 26.07 32.78 o 7 12 10 2949.92 2773.67 81.81 o 8 12 10 2677.42 2718.76 93.00 o 9 12 10 1943.28 2020.27 82.88 o 10 12 10 53.59 114.57 55.58 o 11 12 10 68.69 52.16 64.06 o 12 12 10 233.28 164.97 111.18 o 13 12 10 323.64 264.00 96.82 o 1 13 10 393.68 334.19 31.32 o 2 13 10 337.45 309.72 25.82 o 3 13 10 1363.21 1231.42 43.19 o 4 13 10 64.93 14.44 22.91 o 5 13 10 295.78 284.77 33.95 o 6 13 10 404.19 397.76 39.28 o 7 13 10 353.06 349.73 59.06 o 8 13 10 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27.28 o 2 1 11 6.75 14.58 5.54 o 3 1 11 814.90 829.26 16.94 o 4 1 11 5061.20 5155.57 69.93 o 5 1 11 112.15 103.88 11.72 o 6 1 11 0.14 8.34 10.17 o 7 1 11 3589.88 3700.67 68.01 o 8 1 11 53.46 55.71 14.82 o 9 1 11 171.00 190.00 22.34 o 10 1 11 224.90 229.40 23.92 o 11 1 11 14.95 48.45 29.68 o 12 1 11 560.97 559.71 44.89 o 13 1 11 346.32 302.22 46.80 o 14 1 11 0.26 -56.79 77.21 o 15 1 11 213.63 231.00 112.74 o 16 1 11 86.83 91.39 107.25 o 0 2 11 10639.55 10857.51 215.70 o 1 2 11 230.46 222.39 11.67 o 2 2 11 4984.33 5265.52 65.43 o 3 2 11 1448.68 1476.52 29.28 o 4 2 11 112.53 134.15 9.40 o 5 2 11 1247.66 1330.01 26.92 o 6 2 11 1264.23 1363.29 28.71 o 7 2 11 146.87 154.02 15.95 o 8 2 11 182.06 162.65 20.03 o 9 2 11 496.39 513.38 26.20 o 10 2 11 41.73 49.20 23.42 o 11 2 11 0.40 -30.88 41.16 o 12 2 11 232.96 288.25 43.82 o 13 2 11 283.78 338.08 50.59 o 14 2 11 13.05 -24.71 98.09 o 15 2 11 14.96 -77.08 86.27 o 16 2 11 1.93 80.93 113.00 o 1 3 11 744.23 751.42 16.45 o 2 3 11 957.21 1039.66 19.20 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