#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2206038.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206038_Fobs loop_ _publ_author_name 'Hoki, Tomonori' 'Senju, Takatoshi' 'Mizuguchi, Jin' _publ_section_title ; The monoclinic form of 2,9-dichloro-5,12-dihydroquino[2,3-b]acridine-7,14-dithione dimethylacetamide disolvate ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1927 _journal_page_last o1929 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _[local]_cod_data_source_file ob6519Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_calc _refln_observed_status 1 0 0 10.63 0.16 18.31 o 2 0 0 9600.08 1.93 6973.62 o 3 0 0 437.23 0.16 276.68 o 4 0 0 5292.56 0.92 3450.41 o 5 0 0 249.64 0.19 340.39 o 6 0 0 11170.38 3.20 10405.54 o 7 0 0 658.44 0.19 658.19 o 8 0 0 1472.26 0.29 1359.10 o 9 0 0 2686.35 0.58 2722.02 o 10 0 0 491.95 0.61 365.94 o 11 0 0 1211.74 0.53 1100.65 o 12 0 0 81.72 0.96 78.72 o 13 0 0 852.06 0.59 847.09 o 14 0 0 6.35 7.90 3.64 o 15 0 0 1704.04 0.64 1609.33 o 16 0 0 5.86 3.57 2.92 o 1 1 0 436.39 0.06 493.47 o 2 1 0 3484.54 0.42 4778.96 o 3 1 0 1682.64 0.18 1353.61 o 4 1 0 3284.44 0.48 3334.50 o 5 1 0 4.54 0.64 1.20 o 6 1 0 34.93 0.17 48.98 o 7 1 0 878.53 0.21 864.55 o 8 1 0 2899.82 0.59 2643.00 o 9 1 0 709.69 0.30 699.23 o 10 1 0 2.37 7.18 0.43 o 11 1 0 16.65 2.37 19.02 o 12 1 0 97.22 0.88 111.42 o 13 1 0 1002.36 0.83 958.65 o 14 1 0 603.68 0.55 567.13 o 15 1 0 3.20 8.35 1.23 o 16 1 0 9.49 2.34 6.15 o 0 2 0 8.82 0.71 43.13 o 1 2 0 18547.72 6.45 14119.06 o 2 2 0 31680.44 17.56 24787.12 o 3 2 0 246.18 0.21 261.18 o 4 2 0 150.31 0.23 201.99 o 5 2 0 1084.38 0.28 888.12 o 6 2 0 80.46 0.41 145.16 o 7 2 0 1739.72 0.40 1786.95 o 8 2 0 1571.33 0.42 1269.53 o 9 2 0 68.23 0.71 34.66 o 10 2 0 5018.31 1.46 5076.95 o 11 2 0 66.26 0.92 56.81 o 12 2 0 14.98 2.96 16.37 o 13 2 0 46.38 1.42 37.35 o 14 2 0 18.84 1.99 21.41 o 15 2 0 178.76 0.74 170.78 o 16 2 0 22.37 0.94 50.38 o 1 3 0 8.47 0.50 1.37 o 2 3 0 11.49 0.14 16.64 o 3 3 0 295.15 0.05 164.12 o 4 3 0 2475.06 0.41 2131.63 o 5 3 0 4.80 2.56 0.09 o 6 3 0 381.42 0.23 383.92 o 7 3 0 256.32 0.34 308.44 o 8 3 0 430.98 0.36 440.10 o 9 3 0 85.56 0.81 102.00 o 10 3 0 137.59 0.76 132.65 o 11 3 0 65.77 1.08 54.22 o 12 3 0 47.89 1.28 40.24 o 13 3 0 693.27 0.81 656.49 o 14 3 0 1.30 18.92 0.80 o 15 3 0 225.90 0.41 207.21 o 16 3 0 -1.30 9.49 4.44 o 0 4 0 5375.82 1.08 5736.35 o 1 4 0 249.96 0.09 274.75 o 2 4 0 1190.94 0.17 1226.76 o 3 4 0 194.32 0.15 190.84 o 4 4 0 1270.21 0.25 1141.18 o 5 4 0 2.92 3.88 12.30 o 6 4 0 209.09 0.28 176.46 o 7 4 0 112.57 0.45 138.45 o 8 4 0 3250.14 0.98 3326.84 o 9 4 0 4265.40 1.51 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