#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:12:02 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180980 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/60/2206054.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206054_Fobs loop_ _publ_author_name 'Sun, Gang-Chun' 'Li, Yi-Zhi' 'Chen, Nai-Sheng' 'Wang, Liu-Fang' _publ_section_title ; (Perchlorato-\kO)[3,6,14,21-tetraaza-3,6-difuryl-27,28-dihydroxy-10,25-dimethyltetracyclo[18.4.3.3^8,12^.0^15,20^]octacosa-8,10,12(28),13,17,19,21,23,25,27(1)-decaene-\k^4^N,N',O,O']copper(II) perchlorate dimethylformamide solvate ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1065 _journal_page_last m1066 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.060 _cell_angle_gamma 90.000 _cell_length_a 9.7172 _cell_length_b 27.8630 _cell_length_c 14.9020 _exptl_crystal_F_000 1916.00 _reflns_d_resolution_high 0.8107 _cod_data_source_file sg6003Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sadd in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 593.65 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 73590.34 70200.17 71.00 o 4 0 0 14575.98 14403.39 672.31 o 6 0 0 10.80 161.66 66.57 o 8 0 0 3367.91 2957.58 61.48 o 10 0 0 602.28 720.58 119.59 o 1 1 0 27233.32 24177.59 69.68 o 2 1 0 13260.68 13416.82 224.64 o 3 1 0 113.52 170.67 23.97 o 4 1 0 12719.90 11891.61 438.29 o 5 1 0 4829.50 5045.91 104.47 o 6 1 0 819.26 876.46 81.15 o 7 1 0 1532.74 1485.73 31.42 o 8 1 0 1223.64 1481.27 56.03 o 9 1 0 1937.45 2143.05 61.00 o 10 1 0 50.92 102.61 35.57 o 11 1 0 392.92 526.42 72.29 o 0 2 0 46308.34 41540.51 330.30 o 1 2 0 5390.39 4762.54 184.77 o 2 2 0 1694.29 1567.03 64.12 o 3 2 0 206.91 257.18 32.17 o 4 2 0 17.77 84.99 29.80 o 5 2 0 2816.75 2663.15 94.23 o 6 2 0 10010.00 9601.38 57.00 o 7 2 0 1018.27 859.27 88.53 o 8 2 0 220.26 258.45 28.10 o 9 2 0 9.66 19.13 6.06 o 10 2 0 446.16 441.08 31.32 o 11 2 0 9.73 44.52 44.18 o 1 3 0 2814.39 2522.22 50.59 o 2 3 0 24996.37 24238.38 165.67 o 3 3 0 15468.08 14452.33 495.67 o 4 3 0 0.60 118.98 41.03 o 5 3 0 11045.25 12080.05 182.37 o 6 3 0 3819.22 3958.95 64.34 o 7 3 0 745.55 688.29 60.08 o 8 3 0 1390.84 1392.70 53.76 o 9 3 0 2285.29 2135.65 109.57 o 10 3 0 877.77 759.37 21.31 o 11 3 0 77.91 79.37 10.62 o 0 4 0 34235.12 32994.36 83.71 o 1 4 0 129.03 107.60 43.91 o 2 4 0 15414.35 15261.62 194.90 o 3 4 0 2430.07 2375.17 56.85 o 4 4 0 9346.99 8850.03 166.52 o 5 4 0 5813.46 4990.23 159.08 o 6 4 0 14.04 85.13 26.73 o 7 4 0 0.68 60.32 39.50 o 8 4 0 424.30 439.67 36.82 o 9 4 0 5.11 58.09 22.80 o 10 4 0 2077.20 1863.95 68.34 o 11 4 0 36.80 64.96 96.41 o 1 5 0 778.08 887.00 34.12 o 2 5 0 11038.02 11648.18 66.33 o 3 5 0 90.17 64.46 14.17 o 4 5 0 219.86 269.47 40.72 o 5 5 0 10465.34 9531.30 42.74 o 6 5 0 683.74 820.94 150.30 o 7 5 0 147.66 245.40 30.91 o 8 5 0 12.09 43.62 51.78 o 9 5 0 131.36 295.35 42.62 o 10 5 0 1039.63 1069.50 44.64 o 11 5 0 115.17 290.59 76.32 o 0 6 0 2719.25 2536.86 40.65 o 1 6 0 26102.54 24520.05 501.53 o 2 6 0 4359.34 4193.73 115.04 o 3 6 0 6006.65 5665.98 139.52 o 4 6 0 7114.31 7066.68 123.23 o 5 6 0 3016.01 2968.42 62.72 o 6 6 0 256.21 327.70 48.05 o 7 6 0 1269.32 1345.20 51.97 o 8 6 0 353.51 360.25 52.95 o 9 6 0 725.18 764.84 40.88 o 10 6 0 263.97 306.51 49.51 o 11 6 0 5.30 19.85 15.37 o 1 7 0 3480.16 3596.21 147.12 o 2 7 0 3832.42 3496.42 199.24 o 3 7 0 400.13 412.96 41.15 o 4 7 0 1856.66 2122.98 73.02 o 5 7 0 32111.10 29781.15 88.85 o 6 7 0 2764.29 2845.51 37.32 o 7 7 0 81.04 205.23 25.04 o 8 7 0 71.36 189.37 33.67 o 9 7 0 33.76 49.41 18.25 o 10 7 0 49.50 152.64 78.72 o 11 7 0 855.79 916.62 72.23 o 0 8 0 619.34 517.42 57.68 o 1 8 0 3904.88 3844.13 49.46 o 2 8 0 846.41 943.57 32.51 o 3 8 0 33.19 55.60 35.61 o 4 8 0 4049.79 3685.21 59.03 o 5 8 0 5399.50 5267.29 51.44 o 6 8 0 1657.04 1778.26 67.56 o 7 8 0 135.39 170.24 78.89 o 8 8 0 870.26 895.63 44.16 o 9 8 0 215.12 321.22 68.28 o 10 8 0 359.16 481.02 75.67 o 11 8 0 23.57 87.41 64.04 o 1 9 0 3742.15 4087.65 103.20 o 2 9 0 6459.31 5587.06 108.17 o 3 9 0 2200.80 2080.59 46.58 o 4 9 0 288.55 428.80 43.10 o 5 9 0 9145.77 8109.61 34.77 o 6 9 0 340.46 339.13 41.25 o 7 9 0 784.46 735.35 59.65 o 8 9 0 1189.14 1459.39 88.75 o 9 9 0 1864.37 2301.41 99.71 o 10 9 0 1.40 45.80 89.38 o 11 9 0 2060.60 1958.75 89.26 o 0 10 0 2286.15 2412.27 90.44 o 1 10 0 5944.61 5494.09 67.02 o 2 10 0 705.23 831.06 129.99 o 3 10 0 6029.02 5744.62 39.24 o 4 10 0 25.60 103.39 55.77 o 5 10 0 1563.18 1508.86 67.81 o 6 10 0 8745.51 7807.33 46.34 o 7 10 0 29.13 69.05 44.25 o 8 10 0 1890.15 1854.68 72.21 o 9 10 0 26.50 105.57 59.02 o 10 10 0 209.94 268.39 70.22 o 11 10 0 4.77 63.25 34.24 o 1 11 0 23037.74 21970.13 590.90 o 2 11 0 1873.41 1626.27 172.53 o 3 11 0 9726.45 8878.18 39.23 o 4 11 0 672.01 1022.65 75.60 o 5 11 0 689.65 779.12 47.90 o 6 11 0 1896.22 1706.44 19.20 o 7 11 0 75.40 260.08 86.71 o 8 11 0 468.78 428.49 40.08 o 9 11 0 198.41 208.26 62.83 o 10 11 0 138.09 158.07 67.37 o 11 11 0 476.34 575.73 106.16 o 0 12 0 16338.84 15748.09 186.94 o 1 12 0 23151.95 21584.21 268.55 o 2 12 0 2896.71 2844.24 129.15 o 3 12 0 881.15 903.13 28.18 o 4 12 0 76.01 210.51 81.37 o 5 12 0 398.21 443.64 45.58 o 6 12 0 1960.90 2212.81 88.32 o 7 12 0 1.81 21.62 20.42 o 8 12 0 331.04 475.14 114.70 o 9 12 0 2.59 129.83 81.95 o 10 12 0 2124.47 2152.02 76.40 o 11 12 0 155.58 313.26 95.52 o 1 13 0 10516.60 9759.60 139.86 o 2 13 0 24.37 88.13 90.52 o 3 13 0 6035.57 5440.03 64.59 o 4 13 0 98.21 296.73 110.42 o 5 13 0 143.97 215.29 78.92 o 6 13 0 2789.88 2725.87 87.69 o 7 13 0 271.56 272.40 26.29 o 8 13 0 59.17 72.18 52.57 o 9 13 0 510.61 503.12 46.55 o 10 13 0 764.73 805.91 47.08 o 11 13 0 211.24 214.00 15.91 o 0 14 0 201.89 252.18 95.90 o 1 14 0 15182.06 14696.37 373.39 o 2 14 0 6537.26 6137.35 36.52 o 3 14 0 29.58 38.11 51.11 o 4 14 0 784.23 898.27 49.50 o 5 14 0 58.63 126.63 59.72 o 6 14 0 1762.12 2063.25 103.62 o 7 14 0 902.95 923.36 78.27 o 8 14 0 2070.76 2212.94 81.54 o 9 14 0 20.33 74.24 126.86 o 10 14 0 82.91 85.84 12.03 o 1 15 0 8108.54 7547.40 112.56 o 2 15 0 988.85 1037.33 128.43 o 3 15 0 3041.40 3302.11 76.16 o 4 15 0 1464.28 1448.91 22.89 o 5 15 0 1976.65 2083.97 102.65 o 6 15 0 79.96 144.75 52.32 o 7 15 0 729.09 603.75 25.52 o 8 15 0 64.96 156.21 218.07 o 9 15 0 24.96 92.80 176.32 o 10 15 0 1009.52 986.75 153.12 o 0 16 0 24246.04 22422.89 236.63 o 1 16 0 6476.29 6052.09 65.26 o 2 16 0 35.55 53.89 126.37 o 3 16 0 1922.60 2058.41 72.03 o 4 16 0 3049.92 2877.16 149.25 o 5 16 0 715.55 926.43 174.77 o 6 16 0 3607.97 3732.02 142.29 o 7 16 0 22.42 30.93 139.20 o 8 16 0 39.77 57.23 3.09 o 9 16 0 765.22 739.29 63.41 o 10 16 0 896.75 907.87 88.16 o 1 17 0 176.19 267.57 78.88 o 2 17 0 1356.76 1421.35 24.75 o 3 17 0 10.05 29.39 78.88 o 4 17 0 7123.94 6297.88 3.09 o 5 17 0 2066.91 2197.76 61.87 o 6 17 0 5857.07 5198.23 21.65 o 7 17 0 217.00 327.89 106.72 o 8 17 0 57.86 207.25 95.89 o 9 17 0 382.48 481.00 102.08 o 10 17 0 27.07 98.98 179.41 o 0 18 0 1490.32 1777.08 72.69 o 1 18 0 2.91 75.78 47.95 o 2 18 0 3951.40 3985.67 153.12 o 3 18 0 82.62 162.40 26.29 o 4 18 0 7301.35 6823.74 126.82 o 5 18 0 533.77 567.61 102.08 o 6 18 0 697.43 655.77 21.65 o 7 18 0 2159.20 2194.67 184.05 o 8 18 0 5.82 54.13 81.97 o 9 18 0 297.87 375.83 109.81 o 10 18 0 340.36 437.70 85.06 o 1 19 0 294.61 312.42 88.16 o 2 19 0 387.56 366.55 6.19 o 3 19 0 277.20 405.22 74.24 o 4 19 0 1360.59 1498.69 72.69 o 5 19 0 16530.66 15172.45 86.61 o 6 19 0 49.81 51.04 58.77 o 7 19 0 2507.30 2602.98 97.44 o 8 19 0 1076.37 1078.00 201.06 o 9 19 0 466.97 436.15 174.77 o 0 20 0 20516.35 19626.75 216.53 o 1 20 0 6023.59 5755.01 228.90 o 2 20 0 798.09 832.09 18.56 o 3 20 0 1243.10 1908.54 225.81 o 4 20 0 10070.62 9211.74 231.99 o 5 20 0 3492.62 3328.35 40.21 o 6 20 0 11.65 47.95 47.95 o 7 20 0 197.14 344.90 202.61 o 8 20 0 5.27 66.51 139.20 o 9 20 0 425.78 465.54 91.25 o 1 21 0 1308.88 1747.69 179.41 o 2 21 0 43.47 61.87 47.95 o 3 21 0 1056.41 1155.33 208.80 o 4 21 0 13698.92 13270.09 153.12 o 5 21 0 1353.60 1897.72 213.44 o 6 21 0 1582.72 2016.81 221.17 o 7 21 0 12.71 30.93 41.76 o 8 21 0 224.10 293.86 61.87 o 9 21 0 123.52 162.40 116.00 o 0 22 0 728.45 777.96 202.61 o 1 22 0 23.78 142.29 199.52 o 2 22 0 224.02 270.66 9.28 o 3 22 0 270.71 309.33 37.12 o 4 22 0 1403.15 1687.37 134.56 o 5 22 0 2.61 7.73 6.19 o 6 22 0 583.49 584.63 21.65 o 7 22 0 3.12 13.92 7.73 o 8 22 0 4.30 58.77 81.97 o 9 22 0 55.74 184.05 176.32 o 1 23 0 34.80 44.85 54.13 o 2 23 0 4622.00 4194.46 32.48 o 3 23 0 5555.91 5032.74 146.93 o 4 23 0 13.79 34.03 106.72 o 5 23 0 12763.56 11500.75 160.85 o 6 23 0 404.00 330.98 68.05 o 7 23 0 30.26 71.15 193.33 o 8 23 0 400.80 491.83 137.65 o 0 24 0 4751.31 4718.77 170.13 o 1 24 0 2545.60 2671.03 86.61 o 2 24 0 1975.79 2213.23 106.72 o 3 24 0 4.80 43.31 51.04 o 4 24 0 159.39 179.41 6.19 o 5 24 0 41.34 78.88 81.97 o 6 24 0 42.60 112.90 30.93 o 7 24 0 284.77 383.56 61.87 o 8 24 0 238.84 262.93 41.76 o 1 25 0 786.46 853.74 108.26 o 2 25 0 252.12 262.93 9.28 o 3 25 0 327.31 279.94 3.09 o 4 25 0 29.87 77.33 170.13 o 5 25 0 861.78 996.03 126.82 o 6 25 0 481.23 476.36 63.41 o 7 25 0 8.98 88.16 187.14 o 8 25 0 2.97 4.64 54.13 o 0 26 0 3536.65 3486.11 116.00 o 1 26 0 525.28 635.67 98.98 o 2 26 0 710.56 804.25 167.04 o 3 26 0 1139.08 1166.16 94.34 o 4 26 0 6.52 60.32 173.22 o 5 26 0 170.04 185.60 44.85 o 6 26 0 5.83 21.65 10.83 o 7 26 0 625.03 597.00 23.20 o 1 27 0 815.55 802.70 184.05 o 2 27 0 20.83 102.08 210.34 o 3 27 0 77.38 241.27 140.74 o 4 27 0 490.52 640.31 191.78 o 5 27 0 1590.60 1483.22 103.62 o 6 27 0 112.00 182.50 40.21 o 7 27 0 0.28 34.03 210.34 o 0 28 0 6246.41 5652.94 88.16 o 1 28 0 11.43 66.51 211.89 o 2 28 0 3.78 30.93 176.32 o 3 28 0 612.41 567.61 23.20 o 4 28 0 478.84 471.72 77.33 o 5 28 0 33.34 44.85 89.70 o 6 28 0 537.96 579.99 98.98 o 1 29 0 1697.72 1902.36 106.72 o 2 29 0 288.37 371.19 129.92 o 3 29 0 81.34 197.97 86.61 o 4 29 0 7.51 23.20 111.36 o 5 29 0 51.94 69.60 58.77 o 6 29 0 1082.16 1331.65 69.60 o 0 30 0 149.25 400.58 218.07 o 1 30 0 324.91 463.99 112.90 o 2 30 0 307.75 445.43 188.69 o 3 30 0 1147.58 1255.86 44.85 o 4 30 0 364.15 491.83 123.73 o 5 30 0 1.05 34.03 210.34 o 1 31 0 388.42 388.20 85.06 o 2 31 0 2109.71 1995.15 40.21 o 3 31 0 763.18 785.69 216.53 o 4 31 0 285.49 326.34 137.65 o 5 31 0 223.14 177.86 30.93 o 0 32 0 1526.66 1594.58 187.14 o 1 32 0 622.52 682.06 129.92 o 2 32 0 4.34 63.41 54.13 o 3 32 0 575.14 627.93 98.98 o 4 32 0 133.98 244.37 86.61 o 1 33 0 254.47 414.50 126.82 o 2 33 0 688.30 671.24 40.21 o 3 33 0 3009.73 2770.02 98.98 o 0 34 0 240.23 323.25 86.61 o 1 34 0 33.44 71.15 109.81 o -11 0 1 506.29 504.20 176.32 o -9 0 1 2313.03 2072.49 7.73 o -7 0 1 1619.38 1466.21 27.84 o -5 0 1 4372.61 4466.67 106.72 o -3 0 1 340.55 490.28 168.58 o -1 0 1 5894.73 5625.10 179.41 o 1 0 1 5208.97 4932.21 190.24 o 3 0 1 823.06 1076.46 18.56 o 5 0 1 7362.42 7269.17 86.61 o 7 0 1 12.81 60.32 117.54 o 9 0 1 307.83 349.54 51.04 o 11 0 1 10.59 52.59 176.32 o -11 1 1 199.62 279.23 34.41 o -10 1 1 281.26 328.12 33.99 o -9 1 1 786.73 697.90 12.62 o -8 1 1 1000.97 1017.10 52.54 o -7 1 1 10.75 84.95 67.08 o -6 1 1 141.79 174.34 22.87 o -5 1 1 7508.90 7080.11 148.43 o -4 1 1 6868.85 6616.57 20.56 o -3 1 1 27042.07 26924.95 219.10 o -2 1 1 449.20 440.25 32.75 o -1 1 1 1523.60 1653.61 81.23 o 0 1 1 38963.02 35029.10 290.31 o 1 1 1 4849.70 4680.52 254.45 o 2 1 1 5866.39 6202.70 61.76 o 3 1 1 12833.04 11967.65 55.48 o 4 1 1 4680.14 4171.73 62.90 o 5 1 1 614.20 652.85 20.71 o 6 1 1 6114.59 5924.39 148.86 o 7 1 1 165.25 249.43 29.42 o 8 1 1 94.63 78.80 69.45 o 9 1 1 4.08 21.84 14.83 o 10 1 1 916.85 877.20 54.98 o 11 1 1 25.75 77.05 35.83 o -11 2 1 172.72 283.67 61.54 o -10 2 1 58.41 113.11 49.11 o -9 2 1 1724.51 1571.26 189.34 o -8 2 1 1034.37 1041.14 32.09 o -7 2 1 361.66 393.54 34.28 o -6 2 1 64.04 79.33 54.93 o -5 2 1 980.78 1071.08 88.84 o -4 2 1 814.46 1231.23 68.31 o -3 2 1 9526.67 9337.41 108.60 o -2 2 1 1581.40 1825.51 65.73 o -1 2 1 604.20 647.91 56.58 o 0 2 1 10650.49 9499.45 100.45 o 1 2 1 17338.44 15519.04 40.07 o 2 2 1 13809.17 14250.27 172.05 o 3 2 1 4656.42 4654.26 87.09 o 4 2 1 121.82 148.88 45.18 o 5 2 1 21561.69 20360.70 258.03 o 6 2 1 281.13 352.29 54.55 o 7 2 1 147.37 278.11 48.83 o 8 2 1 892.16 869.88 63.98 o 9 2 1 345.35 365.18 54.99 o 10 2 1 623.37 548.58 65.20 o 11 2 1 14.57 44.05 14.93 o -11 3 1 300.35 323.32 41.63 o -10 3 1 1238.77 1142.92 27.58 o -9 3 1 13.42 127.81 48.31 o -8 3 1 3357.00 2999.57 75.59 o -7 3 1 1174.30 1193.49 204.19 o -6 3 1 2763.92 2966.14 56.21 o -5 3 1 9569.19 8874.53 127.30 o -4 3 1 8776.25 8490.80 55.06 o -3 3 1 10651.45 10537.66 207.11 o -2 3 1 11940.82 10998.27 593.54 o -1 3 1 4402.14 3675.94 40.04 o 0 3 1 4013.82 3882.09 41.50 o 1 3 1 4818.27 4358.57 103.59 o 2 3 1 4047.25 3810.31 139.69 o 3 3 1 1082.49 1138.77 138.43 o 4 3 1 2843.04 3257.08 50.32 o 5 3 1 2.82 39.05 35.73 o 6 3 1 7440.08 6838.81 179.84 o 7 3 1 2348.74 2169.71 39.29 o 8 3 1 0.87 67.63 61.19 o 9 3 1 704.22 730.79 29.03 o 10 3 1 104.81 138.34 35.47 o 11 3 1 75.84 127.73 28.50 o -11 4 1 325.37 326.60 27.16 o -10 4 1 379.98 473.71 65.07 o -9 4 1 1999.20 1929.77 43.66 o -8 4 1 215.67 333.92 47.36 o -7 4 1 1451.02 1412.56 193.34 o -6 4 1 548.18 500.72 12.38 o -5 4 1 7747.14 7045.38 147.65 o -4 4 1 5340.72 4996.01 164.99 o -3 4 1 7731.90 7270.42 59.17 o -2 4 1 7767.53 7689.30 105.03 o -1 4 1 15052.99 15059.49 103.63 o 0 4 1 467.32 269.42 10.76 o 1 4 1 2228.12 2546.37 43.73 o 2 4 1 6782.84 6667.41 79.92 o 3 4 1 1716.57 1660.32 147.88 o 4 4 1 3572.38 3306.40 156.91 o 5 4 1 313.96 478.42 25.27 o 6 4 1 1141.31 1403.29 57.39 o 7 4 1 10182.77 9104.87 65.15 o 8 4 1 5.07 40.59 47.91 o 9 4 1 6.24 113.11 33.39 o 10 4 1 2.55 28.60 30.68 o 11 4 1 12.29 48.37 26.13 o -11 5 1 95.52 178.61 46.28 o -10 5 1 2365.99 2223.45 36.72 o -9 5 1 40.75 51.87 16.48 o -8 5 1 451.04 425.43 72.02 o -7 5 1 2083.30 1864.79 197.26 o -6 5 1 66.86 87.26 15.37 o -5 5 1 1968.22 1981.68 49.43 o -4 5 1 13536.71 12589.01 148.96 o -3 5 1 13055.72 12447.81 95.39 o -2 5 1 1956.55 2045.42 67.94 o -1 5 1 9032.83 9960.39 96.58 o 0 5 1 833.59 968.13 14.90 o 1 5 1 31874.44 30787.52 90.75 o 2 5 1 6543.15 6525.94 83.52 o 3 5 1 6436.17 5771.79 19.21 o 4 5 1 893.36 755.40 26.88 o 5 5 1 53.80 103.75 33.07 o 6 5 1 984.74 853.90 31.21 o 7 5 1 678.67 671.93 31.74 o 8 5 1 1087.47 1120.06 107.97 o 9 5 1 432.39 516.43 61.97 o 10 5 1 1095.96 994.20 81.34 o 11 5 1 148.60 190.16 24.23 o -11 6 1 63.27 101.12 23.16 o -10 6 1 6.59 162.82 67.37 o -9 6 1 3336.86 3004.48 30.38 o -8 6 1 51.29 77.74 36.31 o -7 6 1 623.44 601.06 27.87 o -6 6 1 81.85 222.48 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