#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/60/2206065.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206065_Fobs loop_ _publ_author_name 'Nakazawa, Hiroshi' 'Itazaki, Masumi' 'Owaribe, Mari' _publ_section_title ; Dicarbonyl(\h^5^-cyclopentadienyl)(trimethylsilyl isocyanide)iron(II) trifluoromethanesulfonate ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1073 _journal_page_last m1074 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.803 _cell_angle_gamma 90.000 _cell_length_a 17.3703 _cell_length_b 13.1308 _cell_length_c 8.0113 _exptl_crystal_F_000 864.00 _reflns_d_resolution_high 0.7702 _[local]_cod_data_source_file sj6080Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' OWM307' _shelx_refln_list_code 4 _shelx_f_calc_maximum 123.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 21.75 220.76 113.07 o 8 0 0 3134.49 3541.71 99.91 o 10 0 0 6288.06 6967.19 163.61 o 12 0 0 280.09 306.07 31.58 o 14 0 0 182.69 202.41 19.84 o 16 0 0 1828.97 1963.22 92.23 o 18 0 0 4918.36 4975.11 157.20 o 20 0 0 98.64 104.70 20.99 o 22 0 0 49.91 46.80 29.92 o 5 1 0 6817.05 6941.98 168.80 o 6 1 0 48.47 33.49 8.99 o 7 1 0 2101.86 1956.48 53.45 o 8 1 0 1390.17 1535.61 38.56 o 9 1 0 77.26 58.79 11.35 o 10 1 0 38.29 76.93 12.06 o 11 1 0 1765.42 1907.71 49.88 o 12 1 0 1880.45 1861.75 50.25 o 13 1 0 3473.14 3809.84 82.71 o 14 1 0 54.81 56.85 12.43 o 15 1 0 521.87 529.48 24.05 o 16 1 0 397.23 417.06 19.96 o 17 1 0 128.58 127.69 13.52 o 18 1 0 36.96 15.70 11.37 o 19 1 0 26.18 63.17 30.13 o 20 1 0 0.38 59.68 33.02 o 21 1 0 782.16 875.92 47.84 o 22 1 0 106.07 65.58 21.25 o 0 2 0 690.39 684.93 24.17 o 1 2 0 541.70 484.16 25.23 o 3 2 0 6097.85 6486.73 118.91 o 4 2 0 1496.66 1838.88 44.95 o 5 2 0 3207.63 3225.94 65.34 o 6 2 0 1097.83 1051.19 26.81 o 7 2 0 109.75 92.87 11.99 o 8 2 0 1242.28 1464.13 35.44 o 9 2 0 4961.41 5257.29 87.34 o 10 2 0 3287.94 3283.79 69.07 o 11 2 0 90.59 96.23 13.71 o 12 2 0 46.91 76.73 14.28 o 13 2 0 32.26 48.89 14.41 o 14 2 0 1019.68 1060.21 38.48 o 15 2 0 895.06 967.91 33.95 o 16 2 0 187.70 177.93 33.97 o 17 2 0 18.57 39.40 14.78 o 18 2 0 98.79 107.93 24.31 o 19 2 0 207.79 203.74 28.16 o 20 2 0 788.03 757.12 46.41 o 21 2 0 217.04 234.19 32.58 o 22 2 0 82.72 94.07 38.94 o 2 3 0 804.40 1021.85 36.75 o 3 3 0 990.33 1404.52 103.54 o 5 3 0 3676.21 4387.37 80.80 o 6 3 0 422.22 629.78 23.64 o 7 3 0 385.54 497.66 24.02 o 8 3 0 1876.91 1984.67 48.98 o 9 3 0 978.74 913.77 29.91 o 10 3 0 1310.95 1401.51 39.67 o 11 3 0 87.80 78.73 19.04 o 12 3 0 2732.75 2759.37 76.50 o 13 3 0 37.96 55.60 20.18 o 14 3 0 23.09 52.62 27.35 o 15 3 0 6.67 22.22 23.55 o 16 3 0 295.40 368.94 33.32 o 17 3 0 3049.19 3388.47 101.13 o 18 3 0 153.91 158.25 26.52 o 19 3 0 45.50 46.70 23.94 o 20 3 0 97.82 107.91 54.89 o 21 3 0 152.86 126.43 47.72 o 22 3 0 330.46 357.24 39.07 o 0 4 0 207.40 450.18 31.45 o 1 4 0 2025.19 2247.32 41.72 o 2 4 0 3369.04 3569.64 71.83 o 5 4 0 7808.34 8783.36 182.78 o 6 4 0 224.05 204.00 17.00 o 7 4 0 6130.76 6743.68 137.81 o 8 4 0 1098.44 1270.74 40.57 o 9 4 0 1989.63 2079.25 45.24 o 10 4 0 8.90 11.47 20.45 o 11 4 0 1075.46 1171.94 39.09 o 12 4 0 745.22 771.19 34.76 o 13 4 0 2505.31 2378.11 65.22 o 14 4 0 2.13 56.16 27.37 o 15 4 0 171.19 243.86 31.16 o 16 4 0 15.55 37.53 21.91 o 17 4 0 572.90 545.82 38.00 o 18 4 0 193.68 209.12 28.16 o 19 4 0 312.70 327.03 33.45 o 20 4 0 132.46 102.88 63.43 o 21 4 0 378.85 414.87 40.39 o 1 5 0 178.13 155.15 12.65 o 2 5 0 8170.93 8655.10 195.60 o 3 5 0 751.08 779.60 25.84 o 4 5 0 2018.85 2105.09 46.33 o 5 5 0 5.41 43.37 22.62 o 6 5 0 4728.56 4971.03 118.49 o 7 5 0 136.57 215.62 19.04 o 8 5 0 11634.20 12603.11 282.92 o 9 5 0 183.37 271.34 21.31 o 10 5 0 1663.29 1920.48 49.11 o 11 5 0 12.88 51.00 16.46 o 12 5 0 63.79 85.22 17.77 o 13 5 0 21.56 25.96 26.94 o 14 5 0 130.25 175.66 26.71 o 15 5 0 36.41 60.37 24.66 o 16 5 0 863.32 753.30 41.24 o 17 5 0 2.80 40.17 31.90 o 18 5 0 631.02 582.62 37.98 o 19 5 0 34.45 51.12 19.62 o 20 5 0 992.37 1182.78 51.30 o 21 5 0 29.28 23.65 34.48 o 1 6 0 2656.40 2783.81 56.29 o 2 6 0 2731.02 3022.61 62.07 o 3 6 0 437.60 412.06 19.90 o 4 6 0 5355.08 5589.82 110.36 o 5 6 0 3077.57 3417.78 86.71 o 6 6 0 2843.74 3175.31 74.78 o 7 6 0 66.64 91.90 16.80 o 8 6 0 0.50 20.32 23.93 o 9 6 0 3722.03 4028.79 102.35 o 10 6 0 249.91 220.13 21.42 o 11 6 0 87.86 108.58 17.84 o 12 6 0 269.30 307.79 26.83 o 13 6 0 1911.40 2256.01 66.33 o 14 6 0 827.43 850.33 41.64 o 15 6 0 667.22 688.56 38.21 o 16 6 0 91.32 81.07 26.13 o 17 6 0 22.79 9.96 19.63 o 18 6 0 114.57 83.90 48.12 o 19 6 0 673.82 729.57 122.07 o 20 6 0 62.82 45.53 18.25 o 21 6 0 49.85 55.41 24.62 o 1 7 0 542.90 515.27 22.38 o 2 7 0 1271.14 1304.86 37.89 o 3 7 0 268.93 196.22 17.10 o 4 7 0 6832.65 7520.22 166.51 o 5 7 0 2898.26 3145.70 64.64 o 6 7 0 1721.70 1663.81 42.13 o 7 7 0 625.17 649.74 28.32 o 8 7 0 2018.40 2183.82 58.16 o 9 7 0 9.43 27.11 23.77 o 10 7 0 30.56 43.72 13.58 o 11 7 0 1597.32 1652.08 53.56 o 12 7 0 2744.78 3048.66 74.28 o 13 7 0 50.94 70.16 17.78 o 14 7 0 365.93 394.57 28.26 o 15 7 0 179.28 212.28 51.64 o 16 7 0 262.53 279.76 30.54 o 17 7 0 1273.63 1423.58 52.55 o 18 7 0 0.52 14.46 27.70 o 19 7 0 17.41 45.49 29.04 o 20 7 0 12.44 -1.53 25.69 o 0 8 0 3940.97 4560.47 98.03 o 1 8 0 152.82 168.53 16.86 o 2 8 0 193.05 202.49 17.51 o 3 8 0 3907.54 3987.71 82.57 o 4 8 0 1322.41 1383.08 40.52 o 5 8 0 349.07 323.86 21.35 o 6 8 0 1488.36 1438.61 39.42 o 7 8 0 194.44 197.07 21.40 o 8 8 0 367.51 353.86 24.96 o 9 8 0 2026.99 2286.16 66.45 o 10 8 0 3504.60 3776.70 104.07 o 11 8 0 205.81 230.79 25.86 o 12 8 0 0.50 34.91 22.86 o 13 8 0 143.49 173.03 22.67 o 14 8 0 223.63 210.30 25.00 o 15 8 0 257.94 228.16 29.32 o 16 8 0 236.85 213.92 28.48 o 17 8 0 1.08 57.98 28.34 o 18 8 0 603.52 631.61 64.03 o 19 8 0 57.80 42.68 29.51 o 1 9 0 170.43 194.10 18.69 o 2 9 0 1475.02 1423.43 42.36 o 3 9 0 5801.94 6017.05 110.78 o 4 9 0 1134.29 1142.68 37.63 o 5 9 0 716.96 747.10 30.85 o 6 9 0 617.35 602.65 27.52 o 7 9 0 1783.11 1912.99 52.94 o 8 9 0 181.89 152.65 21.40 o 9 9 0 25.25 22.16 13.34 o 10 9 0 323.64 333.40 30.98 o 11 9 0 751.78 808.37 39.48 o 12 9 0 212.02 207.50 27.09 o 13 9 0 2685.29 2964.19 84.27 o 14 9 0 65.12 73.59 20.57 o 15 9 0 1500.99 1461.23 79.39 o 16 9 0 13.58 40.26 22.77 o 17 9 0 3.73 53.88 26.71 o 18 9 0 24.42 44.43 19.63 o 19 9 0 8.36 24.96 20.59 o 0 10 0 14632.25 15558.19 371.99 o 1 10 0 215.52 231.23 21.19 o 2 10 0 1687.69 1891.18 49.62 o 3 10 0 982.65 985.26 36.22 o 4 10 0 73.59 52.30 12.65 o 5 10 0 6.97 32.73 19.80 o 6 10 0 591.35 636.29 29.78 o 7 10 0 187.04 212.55 22.06 o 8 10 0 218.71 231.29 22.61 o 9 10 0 366.96 387.01 25.62 o 10 10 0 1253.08 1278.34 47.99 o 11 10 0 63.02 88.66 18.82 o 12 10 0 133.67 112.98 22.16 o 13 10 0 13.96 49.47 28.97 o 14 10 0 965.87 1124.44 50.25 o 15 10 0 331.90 399.18 31.79 o 16 10 0 195.94 225.62 27.75 o 17 10 0 17.30 38.27 25.30 o 18 10 0 825.80 843.46 51.03 o 1 11 0 752.75 809.15 32.44 o 2 11 0 871.64 895.08 35.87 o 3 11 0 34.66 43.53 13.66 o 4 11 0 748.99 833.43 33.68 o 5 11 0 360.18 414.93 25.57 o 6 11 0 104.95 107.58 17.38 o 7 11 0 1313.79 1427.53 44.81 o 8 11 0 184.48 191.79 20.84 o 9 11 0 63.25 67.58 15.89 o 10 11 0 117.97 118.03 18.31 o 11 11 0 817.47 762.37 34.70 o 12 11 0 819.03 832.36 39.22 o 13 11 0 431.86 453.46 31.43 o 14 11 0 0.04 11.90 22.31 o 15 11 0 2.64 41.20 26.97 o 16 11 0 47.57 58.78 21.99 o 17 11 0 412.67 357.13 36.25 o 0 12 0 3.93 6.88 18.55 o 1 12 0 65.57 77.49 17.01 o 2 12 0 669.28 700.83 32.95 o 3 12 0 150.54 168.33 21.45 o 4 12 0 972.56 1014.92 39.53 o 5 12 0 47.82 43.20 14.33 o 6 12 0 416.46 399.74 25.39 o 7 12 0 36.61 44.78 13.97 o 8 12 0 227.93 233.71 21.76 o 9 12 0 853.31 907.71 39.83 o 10 12 0 127.21 148.28 23.02 o 11 12 0 529.83 604.42 33.27 o 12 12 0 4.79 44.13 21.80 o 13 12 0 4.07 42.92 23.76 o 14 12 0 986.59 1029.40 48.36 o 15 12 0 115.36 97.63 21.63 o 16 12 0 13.25 23.52 21.18 o 1 13 0 257.68 296.41 27.17 o 2 13 0 2404.06 2575.35 63.78 o 3 13 0 266.84 292.06 25.82 o 4 13 0 7.87 24.02 22.40 o 5 13 0 48.76 47.32 18.43 o 6 13 0 227.89 296.72 31.10 o 7 13 0 171.22 242.90 30.33 o 8 13 0 290.26 285.77 25.67 o 9 13 0 19.40 36.48 21.99 o 10 13 0 747.64 778.48 39.87 o 11 13 0 288.47 244.39 30.49 o 12 13 0 245.86 229.84 27.39 o 13 13 0 6.12 25.69 24.29 o 14 13 0 122.70 89.86 20.29 o 0 14 0 2.94 59.73 27.97 o 1 14 0 641.44 680.77 35.59 o 2 14 0 174.74 181.70 24.15 o 3 14 0 119.62 88.76 20.31 o 4 14 0 295.14 282.17 28.50 o 5 14 0 866.52 920.78 41.97 o 6 14 0 1.30 43.63 26.65 o 7 14 0 602.57 598.50 37.41 o 8 14 0 95.30 126.19 24.63 o 9 14 0 286.17 342.92 33.54 o 10 14 0 259.34 259.10 28.34 o 11 14 0 489.16 538.74 37.92 o 12 14 0 109.09 129.06 25.34 o 1 15 0 29.58 58.57 26.18 o 2 15 0 281.87 310.84 33.67 o 3 15 0 103.43 91.56 20.52 o 4 15 0 19.07 28.49 13.58 o 5 15 0 0.30 18.54 16.58 o 6 15 0 991.37 1017.10 45.94 o 7 15 0 67.98 89.49 21.75 o 8 15 0 1131.36 1126.90 49.51 o 9 15 0 2.16 47.44 27.78 o 10 15 0 38.96 40.50 18.89 o 0 16 0 139.44 214.95 30.95 o 1 16 0 766.37 794.10 47.39 o 2 16 0 7.14 24.75 26.27 o 3 16 0 168.91 162.71 27.79 o 4 16 0 354.97 406.64 34.68 o 5 16 0 117.17 102.94 22.32 o 6 16 0 42.55 61.50 18.87 o 7 16 0 122.85 117.57 31.21 o 1 17 0 0.62 21.88 24.39 o -21 0 1 130.98 110.29 26.87 o -19 0 1 304.73 312.50 35.26 o -17 0 1 80.76 162.80 22.75 o -15 0 1 162.80 165.20 23.91 o -13 0 1 1634.78 1512.66 49.01 o -11 0 1 2223.13 2482.85 64.76 o -9 0 1 10132.88 10009.34 177.50 o -7 0 1 0.06 394.48 37.78 o -5 0 1 1140.56 1222.69 40.52 o -3 0 1 565.03 757.17 30.78 o 3 0 1 35.22 389.97 51.93 o 5 0 1 1664.94 1827.53 48.40 o 7 0 1 3376.04 3017.70 109.77 o 9 0 1 9261.13 10080.96 225.24 o 11 0 1 5013.85 5180.84 125.07 o 13 0 1 1048.62 1125.03 39.09 o 15 0 1 76.80 86.67 34.78 o 17 0 1 951.24 922.13 33.93 o 19 0 1 289.38 337.02 33.53 o 21 0 1 29.36 32.32 28.53 o -22 1 1 81.58 35.74 18.07 o -21 1 1 10.85 32.07 21.46 o -20 1 1 274.55 332.89 37.33 o -19 1 1 408.38 490.32 84.85 o -18 1 1 528.95 585.50 41.74 o -17 1 1 440.62 377.96 42.28 o -16 1 1 1699.91 1774.36 61.42 o -15 1 1 550.92 593.72 17.39 o -14 1 1 119.28 94.30 16.35 o -13 1 1 11.24 53.22 14.26 o -12 1 1 1155.48 1470.31 44.83 o -11 1 1 1191.31 1323.84 48.16 o -10 1 1 2343.89 2305.16 62.32 o -9 1 1 248.69 190.50 20.05 o -8 1 1 2387.81 2195.16 63.34 o -7 1 1 773.01 761.07 31.56 o -6 1 1 241.40 260.53 18.79 o -5 1 1 96.60 145.67 36.61 o 1 1 1 1510.35 1358.95 34.44 o 4 1 1 289.20 1423.16 41.58 o 5 1 1 618.16 675.85 21.22 o 6 1 1 14.84 55.20 11.85 o 7 1 1 1408.66 1363.60 37.72 o 8 1 1 100.82 380.40 21.64 o 9 1 1 1.10 27.08 15.11 o 10 1 1 1881.46 2004.45 52.63 o 11 1 1 2543.02 2525.06 61.02 o 12 1 1 3484.14 3495.78 80.39 o 13 1 1 71.83 39.64 15.09 o 14 1 1 55.52 63.51 16.00 o 15 1 1 1022.62 972.20 35.60 o 16 1 1 1134.32 1248.47 41.70 o 17 1 1 149.21 175.53 18.19 o 18 1 1 37.85 104.38 19.58 o 19 1 1 560.18 548.67 38.72 o 20 1 1 862.83 779.29 44.81 o 21 1 1 11.28 18.20 23.77 o 22 1 1 242.58 195.14 56.70 o -22 2 1 2.60 39.14 26.36 o -21 2 1 0.48 16.94 27.10 o -20 2 1 320.27 237.76 54.30 o -19 2 1 1295.47 1489.52 61.95 o -18 2 1 13.09 6.50 24.77 o -17 2 1 90.80 93.00 31.38 o -16 2 1 142.93 140.39 37.72 o -15 2 1 659.29 642.54 36.60 o -14 2 1 3782.37 4141.36 100.03 o -13 2 1 187.11 241.84 25.65 o -12 2 1 90.40 82.66 17.62 o -11 2 1 272.77 430.66 29.87 o -10 2 1 119.91 95.97 17.11 o -9 2 1 5320.47 5733.02 105.04 o -8 2 1 243.41 587.17 29.21 o -7 2 1 803.74 1107.99 30.61 o -6 2 1 1110.49 1122.83 28.91 o -5 2 1 1958.15 1857.28 46.83 o -4 2 1 304.34 391.72 30.76 o 3 2 1 4756.47 4417.83 103.87 o 4 2 1 809.79 697.59 26.33 o 5 2 1 427.88 730.89 24.47 o 6 2 1 859.40 1007.67 32.18 o 7 2 1 2951.29 3133.24 70.35 o 8 2 1 2571.15 2518.32 62.56 o 9 2 1 4491.72 4970.30 106.73 o 10 2 1 147.97 152.63 16.61 o 11 2 1 1189.62 1248.23 38.09 o 12 2 1 5.59 23.99 23.15 o 13 2 1 252.78 239.46 23.22 o 14 2 1 2911.15 3237.70 81.27 o 15 2 1 176.00 270.43 22.45 o 16 2 1 233.07 234.42 23.26 o 17 2 1 499.70 454.02 25.98 o 18 2 1 71.99 48.14 15.26 o 19 2 1 1837.51 2029.93 59.40 o 20 2 1 88.87 102.00 23.35 o 21 2 1 2.19 33.46 29.59 o 22 2 1 57.22 41.79 32.04 o -22 3 1 507.85 628.71 59.32 o -21 3 1 363.69 407.55 41.13 o -20 3 1 17.10 36.41 50.71 o -19 3 1 0.48 58.92 34.02 o -18 3 1 14.72 81.47 35.77 o -17 3 1 509.89 520.01 37.30 o -16 3 1 11.25 44.04 21.15 o -15 3 1 547.56 543.12 49.66 o -14 3 1 134.84 141.29 31.51 o -13 3 1 1656.32 1714.83 52.98 o -12 3 1 1782.63 1657.64 48.59 o -11 3 1 832.20 969.12 39.56 o -10 3 1 727.96 692.90 32.77 o -9 3 1 303.87 247.18 19.27 o -8 3 1 3637.75 3469.60 75.64 o -7 3 1 1968.32 2105.34 56.16 o -5 3 1 4945.35 4773.15 87.65 o -4 3 1 10927.80 10975.25 212.80 o -3 3 1 6590.22 6438.23 239.91 o -2 3 1 6.55 2.49 28.15 o -1 3 1 1682.72 1459.18 45.88 o 0 3 1 1384.30 1335.21 39.95 o 1 3 1 5279.56 4930.52 90.34 o 2 3 1 263.77 259.40 20.44 o 4 3 1 2722.80 4075.47 91.70 o 5 3 1 3912.95 4001.03 81.26 o 7 3 1 3114.96 2997.39 69.47 o 8 3 1 2158.62 2429.97 67.28 o 9 3 1 67.94 111.18 14.48 o 10 3 1 1297.16 1147.46 38.03 o 11 3 1 1990.69 1868.57 49.98 o 12 3 1 1211.52 1198.83 42.01 o 13 3 1 1017.47 1242.75 45.27 o 14 3 1 67.32 87.49 17.25 o 15 3 1 284.36 291.77 23.29 o 16 3 1 217.66 180.06 20.41 o 17 3 1 240.48 269.23 33.45 o 18 3 1 4.21 10.55 30.39 o 19 3 1 298.66 356.63 34.27 o 20 3 1 18.31 83.48 53.80 o 21 3 1 649.78 661.80 72.61 o 22 3 1 437.95 480.80 39.70 o -21 4 1 7.55 46.44 19.56 o -20 4 1 142.47 136.20 39.12 o -19 4 1 292.97 300.68 33.54 o -18 4 1 509.00 674.75 43.89 o -17 4 1 2.98 56.43 37.42 o -16 4 1 896.56 879.44 43.68 o -15 4 1 111.55 151.18 28.93 o -14 4 1 926.82 945.34 42.77 o -13 4 1 0.49 13.20 28.31 o -12 4 1 16.61 63.38 18.89 o -11 4 1 719.75 712.62 31.84 o -10 4 1 3038.40 3055.22 63.72 o -9 4 1 1895.53 2018.81 53.53 o -8 4 1 527.30 966.26 34.44 o -7 4 1 727.84 823.36 29.57 o -6 4 1 13483.67 13597.36 335.21 o -5 4 1 184.95 230.54 35.01 o -3 4 1 2598.88 2508.79 65.59 o -2 4 1 266.37 215.09 15.49 o -1 4 1 7271.58 6906.20 125.92 o 0 4 1 2037.69 1877.46 49.76 o 2 4 1 86.75 68.33 11.37 o 3 4 1 2501.81 2410.88 57.39 o 4 4 1 10918.00 12662.04 220.89 o 5 4 1 662.45 664.78 27.63 o 6 4 1 8172.82 9005.70 178.00 o 7 4 1 1229.76 1291.83 39.52 o 8 4 1 3192.37 3064.89 64.53 o 9 4 1 2227.71 2225.85 56.38 o 10 4 1 3110.67 3154.71 65.79 o 11 4 1 553.64 588.54 27.09 o 12 4 1 243.95 246.98 20.78 o 13 4 1 13.25 32.57 22.36 o 14 4 1 157.55 256.97 24.08 o 15 4 1 49.17 58.68 14.21 o 16 4 1 313.48 407.56 33.97 o 17 4 1 24.97 19.49 17.72 o 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385.73 38.81 o -1 8 9 161.34 113.54 27.53 o 0 8 9 0.20 28.17 19.56 o 1 8 9 52.05 49.67 62.04 o 2 8 9 0.54 24.18 33.72 o 3 8 9 27.33 45.32 26.87 o -6 0 10 302.52 300.98 31.95 o -4 0 10 136.15 252.19 36.58 o -2 0 10 352.71 419.61 41.46 o 0 0 10 177.93 203.49 31.19 o 2 0 10 214.71 185.25 27.91 o 4 0 10 2.93 23.07 31.58 o -6 1 10 68.91 95.65 23.37 o -5 1 10 16.50 60.78 26.62 o -4 1 10 78.36 79.67 23.24 o -3 1 10 8.55 26.41 20.80 o -2 1 10 120.32 96.98 21.92 o -1 1 10 431.34 496.81 49.58 o 0 1 10 235.64 234.38 33.51 o 1 1 10 89.15 65.00 20.24 o 2 1 10 0.67 26.38 20.27 o 3 1 10 228.80 281.54 33.86 o 4 1 10 54.41 61.83 23.21 o -6 2 10 34.64 31.74 22.47 o -5 2 10 12.37 21.08 21.23 o -4 2 10 23.16 42.88 24.35 o -3 2 10 40.90 51.55 17.66 o -2 2 10 179.85 183.63 29.04 o -1 2 10 3.29 31.25 25.62 o 0 2 10 88.99 63.96 28.23 o 1 2 10 68.09 55.47 19.39 o 2 2 10 151.99 202.38 32.24 o 3 2 10 239.28 232.68 32.56 o 4 2 10 8.57 3.85 32.59 o -5 3 10 392.81 380.40 36.37 o -4 3 10 139.46 134.29 27.11 o -3 3 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