#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:12:02 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180980 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/60/2206088.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206088_Fobs loop_ _publ_author_name 'Li, Xin-Hua' 'Lei, Xin-Xiang' 'Wang, Shun' _publ_section_title ; 4,4'-Bipyridinium bis(3,5-dicarboxybenzoate) benzene-1,3,5-tricarboxylic acid hexahydrate ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1802 _journal_page_last o1804 _journal_volume 61 _journal_year 2005 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.037 _cell_angle_gamma 90.000 _cell_length_a 10.9217 _cell_length_b 21.5274 _cell_length_c 16.4036 _exptl_crystal_F_000 1864.00 _reflns_d_resolution_high 0.8378 _cod_data_source_file wk6046Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' lx in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 534.01 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5.26 113.10 9.63 o 4 0 0 4486.31 4568.29 86.96 o 6 0 0 290.28 358.84 26.97 o 8 0 0 318.05 302.15 29.44 o 10 0 0 547.59 571.55 44.85 o 1 1 0 0.39 9.02 1.33 o 3 1 0 1213.31 1918.93 32.98 o 5 1 0 2183.68 1849.45 53.39 o 7 1 0 1985.48 1861.70 48.35 o 9 1 0 47.67 50.28 12.89 o 11 1 0 38.99 75.04 11.56 o 0 2 0 12156.16 14278.73 112.05 o 2 2 0 2122.72 1901.13 33.32 o 4 2 0 468.31 454.47 17.85 o 6 2 0 6186.04 6501.93 89.81 o 8 2 0 1138.88 1033.11 38.39 o 10 2 0 98.57 72.82 11.16 o 12 2 0 62.12 102.92 24.22 o 1 3 0 2345.90 2570.43 32.96 o 3 3 0 7207.38 8231.52 50.36 o 5 3 0 309.39 388.62 14.35 o 7 3 0 122.85 130.21 10.70 o 9 3 0 2176.09 1808.20 41.91 o 11 3 0 63.78 87.54 12.90 o 0 4 0 60978.13 59067.82 410.47 o 2 4 0 57.56 37.83 11.35 o 4 4 0 582.12 513.78 11.95 o 6 4 0 1003.48 1088.79 21.03 o 8 4 0 1.07 13.12 4.46 o 10 4 0 8.62 24.31 6.57 o 12 4 0 259.60 297.98 38.71 o 1 5 0 7384.66 7123.23 62.84 o 3 5 0 448.17 334.26 8.86 o 5 5 0 643.79 714.94 15.63 o 7 5 0 367.66 353.02 13.03 o 9 5 0 1372.44 1257.77 32.52 o 11 5 0 5.27 30.62 8.47 o 0 6 0 299.28 341.62 11.01 o 2 6 0 510.46 559.71 23.24 o 4 6 0 49.76 80.88 5.69 o 6 6 0 58.09 54.44 7.20 o 8 6 0 175.75 164.38 13.45 o 10 6 0 22.08 33.72 8.57 o 12 6 0 848.19 787.39 35.07 o 1 7 0 2.05 6.07 2.05 o 3 7 0 16.64 41.81 4.83 o 5 7 0 36.46 58.16 5.88 o 7 7 0 203.44 219.45 13.88 o 9 7 0 511.37 473.49 20.29 o 11 7 0 272.47 256.49 23.74 o 0 8 0 46950.23 47767.80 263.94 o 2 8 0 1672.02 1646.16 27.25 o 4 8 0 1222.36 1405.98 23.54 o 6 8 0 27.56 46.20 5.99 o 8 8 0 28.46 49.40 8.61 o 10 8 0 1.68 21.53 10.36 o 12 8 0 73.20 81.18 17.18 o 1 9 0 35.48 68.27 5.39 o 3 9 0 1739.25 1719.63 31.93 o 5 9 0 235.79 285.52 15.45 o 7 9 0 4.46 17.89 6.12 o 9 9 0 9.00 29.09 9.98 o 11 9 0 102.27 126.44 19.82 o 0 10 0 73615.89 81945.96 433.56 o 2 10 0 1502.29 1473.76 27.37 o 4 10 0 308.05 352.62 21.33 o 6 10 0 4.09 15.51 7.03 o 8 10 0 0.00 15.26 6.15 o 10 10 0 43.70 123.92 19.74 o 12 10 0 30.33 67.39 13.59 o 1 11 0 0.01 7.72 2.96 o 3 11 0 415.46 606.05 16.81 o 5 11 0 348.54 331.74 18.26 o 7 11 0 377.65 465.53 22.93 o 9 11 0 40.38 87.01 22.15 o 11 11 0 236.87 263.09 31.52 o 0 12 0 4463.15 5214.30 63.35 o 2 12 0 421.72 331.09 13.06 o 4 12 0 854.83 672.62 25.01 o 6 12 0 1.95 11.20 7.18 o 8 12 0 10.41 34.70 18.16 o 10 12 0 44.05 116.68 27.66 o 1 13 0 3620.53 3743.25 38.60 o 3 13 0 189.63 210.74 15.27 o 5 13 0 151.16 156.97 15.83 o 7 13 0 6.44 15.87 8.62 o 9 13 0 76.13 168.18 23.54 o 11 13 0 255.96 363.32 36.19 o 0 14 0 2008.68 2106.36 41.54 o 2 14 0 184.04 146.37 11.19 o 4 14 0 814.36 765.53 28.72 o 6 14 0 4.75 23.18 7.34 o 8 14 0 938.28 907.48 82.42 o 10 14 0 178.95 211.34 29.86 o 1 15 0 1005.07 1023.86 23.32 o 3 15 0 111.02 109.21 13.98 o 5 15 0 0.74 9.56 6.82 o 7 15 0 127.95 152.53 23.61 o 9 15 0 2.14 56.40 26.69 o 0 16 0 1261.11 972.05 30.10 o 2 16 0 51.65 39.88 10.18 o 4 16 0 26.25 22.55 8.00 o 6 16 0 25.27 45.12 13.15 o 8 16 0 970.62 994.83 162.63 o 10 16 0 8.95 44.34 14.00 o 1 17 0 1536.62 1362.79 32.35 o 3 17 0 119.28 144.95 16.76 o 5 17 0 17.91 34.15 9.10 o 7 17 0 0.00 22.05 10.88 o 9 17 0 1797.41 1719.16 70.15 o 0 18 0 436.11 451.39 28.79 o 2 18 0 807.31 708.20 29.53 o 4 18 0 50.46 49.50 11.73 o 6 18 0 458.30 435.30 34.41 o 8 18 0 5.63 62.07 15.69 o 1 19 0 1115.12 912.04 34.23 o 3 19 0 1998.05 1737.97 48.76 o 5 19 0 1300.68 1114.01 51.26 o 7 19 0 111.48 144.02 24.26 o 0 20 0 436.90 385.10 29.74 o 2 20 0 89.05 112.07 15.74 o 4 20 0 418.20 369.05 25.80 o 6 20 0 102.85 176.49 43.07 o 8 20 0 38.20 94.52 18.33 o 1 21 0 1886.83 1540.35 51.54 o 3 21 0 27.56 43.07 10.37 o 5 21 0 621.70 588.17 38.63 o 7 21 0 140.11 191.47 28.10 o 0 22 0 50.38 66.79 15.53 o 2 22 0 193.79 204.83 22.04 o 4 22 0 5.75 36.16 12.30 o 6 22 0 71.47 96.76 25.04 o 1 23 0 16.82 31.59 15.71 o 3 23 0 520.41 528.18 29.13 o 5 23 0 23.81 56.08 14.13 o 0 24 0 3.58 26.14 13.48 o 2 24 0 0.01 30.18 8.24 o 4 24 0 190.70 232.58 30.28 o 1 25 0 534.17 615.92 32.16 o 3 25 0 201.01 278.61 58.89 o -9 1 1 85.26 124.34 14.07 o -7 1 1 0.00 13.27 6.06 o -5 1 1 2877.13 3085.15 86.54 o -3 1 1 165922.89 153908.25 8304.28 o -1 1 1 425.55 263.67 11.42 o 1 1 1 2474.73 2420.79 27.24 o 3 1 1 25708.98 25479.01 202.53 o 5 1 1 393.59 398.86 32.88 o 7 1 1 773.86 780.52 31.90 o 9 1 1 70.76 58.52 10.04 o 11 1 1 64.27 68.96 11.21 o -12 2 1 251.36 273.53 38.53 o -10 2 1 8.13 33.27 6.79 o -8 2 1 128.73 148.63 13.79 o -6 2 1 3344.69 3268.76 55.23 o -4 2 1 10358.89 9949.13 122.73 o -2 2 1 825.50 1159.25 14.27 o 0 2 1 13590.23 14601.90 137.03 o 2 2 1 0.49 27.30 3.35 o 4 2 1 3883.30 3659.44 44.88 o 6 2 1 0.45 20.77 5.82 o 8 2 1 75.83 75.13 15.11 o 10 2 1 113.47 119.07 14.45 o -11 3 1 45.00 68.54 19.20 o -9 3 1 312.98 332.20 21.41 o -7 3 1 469.14 406.90 15.30 o -5 3 1 5909.55 6016.89 53.29 o -3 3 1 14970.63 14246.81 166.82 o -1 3 1 1081.11 1205.03 13.89 o 1 3 1 101.21 100.73 4.30 o 3 3 1 2381.16 2131.39 30.83 o 5 3 1 131.72 132.67 11.15 o 7 3 1 650.24 551.40 24.60 o 9 3 1 3120.14 2790.93 55.77 o 11 3 1 17.74 50.98 11.13 o -12 4 1 388.91 391.31 46.78 o -10 4 1 78.66 127.21 15.49 o -8 4 1 0.89 9.25 4.04 o -6 4 1 446.88 384.26 13.50 o -4 4 1 227.11 268.63 9.42 o -2 4 1 17.04 5.73 2.78 o 0 4 1 7650.36 7325.50 82.21 o 2 4 1 7486.22 7322.84 71.58 o 4 4 1 2542.85 2872.22 43.10 o 6 4 1 469.22 349.07 13.21 o 8 4 1 728.16 724.92 21.95 o 10 4 1 95.74 104.03 16.82 o 12 4 1 416.56 409.11 48.54 o -11 5 1 184.81 217.03 21.05 o -9 5 1 338.40 394.03 17.96 o -7 5 1 168.10 216.05 11.07 o -5 5 1 5.05 16.55 4.24 o -3 5 1 1265.38 1398.56 38.13 o -1 5 1 1621.59 1703.28 20.30 o 1 5 1 7678.82 6934.17 41.37 o 3 5 1 1464.20 1838.55 20.23 o 5 5 1 4.25 4.70 2.48 o 7 5 1 34.34 35.94 6.76 o 9 5 1 796.93 816.13 26.55 o 11 5 1 1.14 34.63 9.38 o -12 6 1 68.29 97.83 14.89 o -10 6 1 13.54 37.54 9.79 o -8 6 1 110.94 134.75 10.55 o -6 6 1 159.16 137.59 11.25 o -4 6 1 1015.13 1098.91 20.25 o -2 6 1 591.66 661.73 13.70 o 0 6 1 19376.22 18965.12 156.84 o 2 6 1 423.85 389.27 8.73 o 4 6 1 4587.96 4625.27 39.03 o 6 6 1 4573.63 4297.38 43.92 o 8 6 1 2442.49 2231.33 42.26 o 10 6 1 70.65 104.40 12.69 o 12 6 1 1.37 41.47 8.92 o -11 7 1 195.31 195.15 25.31 o -9 7 1 700.93 653.77 28.50 o -7 7 1 21.65 27.60 5.09 o -5 7 1 14.67 36.96 5.45 o -3 7 1 8282.21 7647.20 86.87 o -1 7 1 7.14 2.57 2.53 o 1 7 1 346.05 251.70 6.93 o 3 7 1 1832.99 1606.37 24.98 o 5 7 1 4276.90 4114.37 39.87 o 7 7 1 166.71 200.72 14.48 o 9 7 1 306.17 320.27 18.86 o 11 7 1 11.63 50.98 9.91 o -12 8 1 94.65 124.44 24.35 o -10 8 1 9.00 30.53 9.56 o -8 8 1 512.22 463.44 29.35 o -6 8 1 1255.01 1205.64 30.29 o -4 8 1 0.01 19.11 4.30 o -2 8 1 890.32 951.78 18.43 o 0 8 1 1934.01 1785.39 23.34 o 2 8 1 5171.56 5436.43 42.37 o 4 8 1 9278.16 9612.40 80.42 o 6 8 1 699.26 635.12 23.16 o 8 8 1 271.69 257.06 19.42 o 10 8 1 11.85 28.85 8.83 o 12 8 1 166.57 183.34 21.41 o -11 9 1 46.02 57.68 13.11 o -9 9 1 6.67 18.59 9.51 o -7 9 1 256.12 248.80 17.16 o -5 9 1 2017.39 1818.96 30.35 o -3 9 1 44310.34 47346.67 264.85 o -1 9 1 196.49 212.49 9.62 o 1 9 1 6560.72 7070.47 46.88 o 3 9 1 3932.11 4307.62 50.68 o 5 9 1 2344.41 1964.60 74.67 o 7 9 1 621.54 671.59 25.86 o 9 9 1 195.96 170.72 15.90 o 11 9 1 21.11 50.37 9.91 o -12 10 1 55.76 103.44 16.88 o -10 10 1 106.33 167.28 40.59 o -8 10 1 62.13 97.98 17.27 o -6 10 1 1395.88 1201.82 33.54 o -4 10 1 2347.10 2288.55 33.64 o -2 10 1 216.04 204.63 10.76 o 0 10 1 8670.35 9764.39 60.36 o 2 10 1 4950.61 5133.91 44.76 o 4 10 1 1.30 8.59 4.73 o 6 10 1 518.41 533.65 36.34 o 8 10 1 273.76 219.81 16.88 o 10 10 1 132.90 142.19 17.57 o -11 11 1 0.01 36.60 12.93 o -9 11 1 13.45 29.43 9.63 o -7 11 1 107.65 102.94 22.84 o -5 11 1 2779.84 2826.03 81.87 o -3 11 1 104.10 189.64 15.89 o -1 11 1 236.97 237.63 11.35 o 1 11 1 8260.53 9634.70 61.67 o 3 11 1 285.84 301.88 11.46 o 5 11 1 499.91 498.26 22.37 o 7 11 1 964.60 1023.21 36.41 o 9 11 1 20.45 54.78 12.80 o 11 11 1 1.39 42.32 13.21 o -10 12 1 39.75 76.85 19.13 o -8 12 1 80.66 97.90 28.48 o -6 12 1 1540.07 1383.59 37.74 o -4 12 1 2453.64 2565.71 112.13 o -2 12 1 22.63 25.47 5.60 o 0 12 1 41.75 35.46 5.65 o 2 12 1 1901.69 2044.90 29.02 o 4 12 1 577.46 571.76 46.23 o 6 12 1 200.39 147.38 15.84 o 8 12 1 102.68 95.53 14.33 o 10 12 1 2.42 52.70 10.99 o -11 13 1 5.99 52.34 12.64 o -9 13 1 79.22 131.71 20.51 o -7 13 1 10.05 41.44 12.16 o -5 13 1 3917.13 4178.66 110.21 o -3 13 1 256.60 291.07 13.64 o -1 13 1 46.71 56.76 7.74 o 1 13 1 975.46 907.48 18.20 o 3 13 1 369.71 371.11 22.86 o 5 13 1 115.13 122.15 14.40 o 7 13 1 283.67 264.30 23.32 o 9 13 1 391.53 440.13 33.77 o 11 13 1 10.05 45.95 12.50 o -10 14 1 18.93 44.60 16.24 o -8 14 1 24.17 33.21 10.49 o -6 14 1 73.85 113.34 19.55 o -4 14 1 1166.86 1233.04 35.75 o -2 14 1 97.50 163.18 13.78 o 0 14 1 3535.09 3355.59 42.44 o 2 14 1 5646.59 5507.01 67.23 o 4 14 1 1.03 6.18 5.98 o 6 14 1 0.36 14.16 7.09 o 8 14 1 16.09 44.84 12.80 o 10 14 1 1.60 42.05 11.96 o -9 15 1 1251.07 1286.49 145.16 o -7 15 1 31.46 48.55 13.81 o -5 15 1 16.76 15.89 7.21 o -3 15 1 548.52 440.48 21.76 o -1 15 1 47.89 45.54 7.83 o 1 15 1 4208.53 4003.97 100.33 o 3 15 1 2554.21 2468.49 52.55 o 5 15 1 25.79 63.69 12.33 o 7 15 1 20.17 32.29 8.97 o 9 15 1 2619.73 2506.31 100.58 o -10 16 1 4.32 47.16 14.36 o -8 16 1 159.93 197.56 28.11 o -6 16 1 8.46 14.90 13.90 o -4 16 1 4.91 11.46 6.99 o -2 16 1 519.94 496.40 19.03 o 0 16 1 844.04 799.04 23.45 o 2 16 1 43.04 33.63 7.92 o 4 16 1 3156.03 2731.93 58.45 o 6 16 1 1871.42 1817.69 49.74 o 8 16 1 3082.81 3186.74 181.07 o 10 16 1 152.47 193.05 27.12 o -9 17 1 5.89 66.39 16.15 o -7 17 1 1143.25 1025.52 50.13 o -5 17 1 204.58 185.76 25.45 o -3 17 1 3.77 27.73 8.51 o -1 17 1 51.56 64.17 9.70 o 1 17 1 124.41 146.06 12.36 o 3 17 1 506.94 491.51 24.95 o 5 17 1 1826.46 1657.17 47.39 o 7 17 1 338.23 488.25 34.47 o 9 17 1 415.35 372.70 58.75 o -8 18 1 405.26 390.34 72.65 o -6 18 1 496.76 501.09 37.41 o -4 18 1 119.51 123.17 17.80 o -2 18 1 143.56 158.48 17.35 o 0 18 1 9.70 10.10 5.15 o 2 18 1 10.27 22.78 8.43 o 4 18 1 0.58 13.65 7.03 o 6 18 1 488.45 522.99 35.69 o 8 18 1 1370.28 1363.83 61.06 o -7 19 1 166.77 198.84 28.18 o -5 19 1 0.68 35.11 13.62 o -3 19 1 3.10 20.65 9.01 o -1 19 1 425.04 394.69 23.49 o 1 19 1 168.71 152.38 14.84 o 3 19 1 5.70 17.55 7.52 o 5 19 1 16.66 47.48 10.98 o 7 19 1 31.47 66.88 18.30 o -8 20 1 84.64 134.10 24.01 o -6 20 1 365.07 436.80 39.68 o -4 20 1 550.50 484.28 33.69 o -2 20 1 15.97 37.14 9.39 o 0 20 1 243.94 198.87 14.98 o 2 20 1 13.25 16.07 8.26 o 4 20 1 2055.34 1865.09 53.35 o 6 20 1 52.30 65.08 35.91 o 8 20 1 89.33 97.37 50.91 o -7 21 1 190.69 248.49 32.60 o -5 21 1 0.12 23.10 10.46 o -3 21 1 0.89 21.52 8.46 o -1 21 1 12.20 12.10 6.91 o 1 21 1 354.58 342.28 26.21 o 3 21 1 655.65 519.56 28.03 o 5 21 1 6.27 17.03 11.70 o 7 21 1 11.62 29.11 11.70 o -6 22 1 331.71 473.98 43.00 o -4 22 1 107.73 135.48 26.42 o -2 22 1 363.31 359.90 26.70 o 0 22 1 74.26 71.11 12.52 o 2 22 1 219.33 271.75 24.81 o 4 22 1 13.01 19.65 11.52 o 6 22 1 178.67 223.61 65.36 o -5 23 1 21.84 36.45 11.27 o -3 23 1 22.70 41.70 28.62 o -1 23 1 500.06 432.85 25.56 o 1 23 1 275.82 308.55 26.32 o 3 23 1 134.31 154.00 19.35 o 5 23 1 19.55 30.74 11.52 o -4 24 1 8.57 64.38 19.81 o -2 24 1 37.73 33.42 22.70 o 0 24 1 336.80 374.96 35.40 o 2 24 1 35.46 77.50 13.86 o 4 24 1 49.22 112.26 50.36 o -1 25 1 87.76 104.27 16.58 o 1 25 1 42.81 68.37 25.73 o -10 0 2 486.03 437.54 39.35 o -8 0 2 33.31 77.33 17.34 o -6 0 2 20360.52 20514.78 250.14 o -4 0 2 6874.72 7278.27 104.57 o -2 0 2 149.04 102.20 6.46 o 0 0 2 5486.66 5501.10 49.95 o 2 0 2 15007.73 14565.96 89.64 o 4 0 2 2045.52 1717.05 33.59 o 6 0 2 4376.45 3899.60 101.27 o 8 0 2 999.87 846.77 37.70 o 10 0 2 0.41 20.64 13.48 o 12 0 2 140.13 151.90 31.37 o -11 1 2 6.09 29.32 8.81 o -9 1 2 6.71 15.14 5.47 o -7 1 2 425.58 425.37 22.41 o -5 1 2 383.58 449.74 13.09 o -3 1 2 285166.84 271589.50 1332.70 o -1 1 2 226.46 223.55 10.29 o 1 1 2 14.83 29.96 2.17 o 3 1 2 15702.55 16763.44 134.61 o 5 1 2 592.36 424.80 15.94 o 7 1 2 678.11 587.26 22.31 o 9 1 2 253.96 236.34 16.28 o 11 1 2 0.14 15.38 8.34 o -12 2 2 2.08 47.34 11.13 o -10 2 2 269.54 301.81 19.73 o -8 2 2 537.25 482.41 17.47 o -6 2 2 2741.63 2467.42 34.21 o -4 2 2 2055.11 2118.27 39.26 o -2 2 2 4150.27 4255.99 36.72 o 0 2 2 68.53 80.17 3.24 o 2 2 2 208.22 253.88 6.10 o 4 2 2 5982.00 5628.66 62.76 o 6 2 2 6027.38 5947.06 134.75 o 8 2 2 0.01 12.46 5.68 o 10 2 2 22.07 32.65 8.53 o 12 2 2 166.55 193.56 25.77 o -11 3 2 13.17 35.77 15.13 o -9 3 2 2740.80 2288.83 55.62 o -7 3 2 49.70 60.11 7.69 o -5 3 2 515.56 420.77 14.42 o -3 3 2 81940.59 81676.13 605.97 o -1 3 2 4637.05 4296.54 36.39 o 1 3 2 3766.89 4060.73 26.33 o 3 3 2 12009.79 13216.81 132.18 o 5 3 2 1531.87 1450.08 30.72 o 7 3 2 984.59 986.92 29.22 o 9 3 2 155.95 192.59 17.47 o 11 3 2 29.44 41.29 8.48 o -12 4 2 174.20 165.66 31.37 o -10 4 2 63.11 62.39 11.44 o -8 4 2 46.42 82.71 10.25 o -6 4 2 221.54 289.68 11.92 o -4 4 2 11.87 49.41 6.46 o -2 4 2 1353.67 1542.56 36.15 o 0 4 2 8598.38 9362.16 91.09 o 2 4 2 5995.02 5825.10 169.92 o 4 4 2 1550.19 1388.42 28.62 o 6 4 2 742.61 749.52 24.65 o 8 4 2 507.06 541.06 29.59 o 10 4 2 782.60 656.64 34.75 o 12 4 2 0.95 34.85 12.74 o -11 5 2 105.78 106.37 15.05 o -9 5 2 130.50 136.31 13.07 o -7 5 2 90.17 111.19 13.35 o -5 5 2 2050.52 2051.73 45.85 o -3 5 2 27788.48 27842.74 145.81 o -1 5 2 6541.26 6549.78 52.22 o 1 5 2 126.67 120.41 4.93 o 3 5 2 21.27 5.37 3.12 o 5 5 2 3196.19 3308.66 37.62 o 7 5 2 3.15 6.04 5.66 o 9 5 2 2874.62 2708.56 56.44 o 11 5 2 7.82 27.02 9.06 o -12 6 2 593.79 475.51 45.13 o -10 6 2 235.48 199.25 39.49 o -8 6 2 28.12 64.24 10.05 o -6 6 2 323.22 232.25 11.68 o -4 6 2 351.12 261.64 12.23 o -2 6 2 1734.97 1450.11 30.67 o 0 6 2 7880.15 7532.97 87.52 o 2 6 2 11518.73 12286.38 73.43 o 4 6 2 8.59 4.01 3.92 o 6 6 2 13422.94 13810.56 109.03 o 8 6 2 14.09 52.72 8.25 o 10 6 2 38.37 59.67 9.73 o 12 6 2 34.40 86.71 13.50 o -11 7 2 79.36 81.27 15.95 o -9 7 2 24.03 48.41 19.81 o -7 7 2 176.61 201.28 12.55 o -5 7 2 798.89 704.27 21.49 o -3 7 2 10020.20 10220.85 72.48 o -1 7 2 880.05 763.89 15.54 o 1 7 2 11169.76 10870.52 104.65 o 3 7 2 2.29 8.78 3.35 o 5 7 2 2288.73 2419.33 28.19 o 7 7 2 7.75 41.30 8.66 o 9 7 2 1523.16 1506.09 37.61 o 11 7 2 3.60 24.14 8.97 o -12 8 2 48.26 64.04 14.30 o -10 8 2 235.79 232.85 26.71 o -8 8 2 74.74 112.54 18.69 o -6 8 2 4133.16 4195.52 102.79 o -4 8 2 602.30 575.49 20.23 o -2 8 2 1128.90 1081.32 22.20 o 0 8 2 30203.00 29929.87 219.48 o 2 8 2 2626.91 2648.60 35.99 o 4 8 2 3341.61 3541.60 41.41 o 6 8 2 432.40 385.45 28.96 o 8 8 2 243.75 265.26 17.97 o 10 8 2 260.08 320.47 21.30 o 12 8 2 1.03 42.77 18.26 o -11 9 2 7.42 41.02 17.06 o -9 9 2 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