#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2206120.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206120_Fobs loop_ _publ_author_name 'Rodriguez, Mark A.' 'Andrews, Nicholas L.' 'Boyle, Timothy J.' 'Frazer, Colleen S.' _publ_section_title ; N-Methylimidazolidinetrione ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2288 _journal_page_last o2290 _journal_volume 61 _journal_year 2005 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 4.8966 _cell_length_b 7.2049 _cell_length_c 14.7187 _exptl_crystal_F_000 264.00 _reflns_d_resolution_high 0.7691 _[local]_cod_data_source_file bd6004Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' na071s in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 67.14 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 923.79 959.01 12.44 o 4 0 0 268.05 275.06 7.11 o 6 0 0 170.16 185.90 7.12 o 1 1 0 667.50 665.52 6.69 o 2 1 0 60.56 64.84 1.45 o 3 1 0 55.49 52.24 1.91 o 4 1 0 4.41 6.71 1.14 o 5 1 0 136.87 132.89 4.03 o 6 1 0 0.04 -0.84 1.65 o 0 2 0 295.92 316.55 5.03 o 1 2 0 537.40 532.07 5.13 o 2 2 0 197.84 175.77 2.71 o 3 2 0 25.80 21.65 1.23 o 4 2 0 55.44 59.07 2.04 o 5 2 0 1.47 0.44 1.29 o 6 2 0 15.83 13.17 2.51 o 1 3 0 342.57 372.57 4.05 o 2 3 0 54.93 51.74 1.25 o 3 3 0 0.00 -0.45 1.06 o 4 3 0 148.47 152.21 3.27 o 5 3 0 0.57 -1.26 1.43 o 6 3 0 0.12 -0.99 3.78 o 0 4 0 1631.49 1710.61 21.80 o 1 4 0 20.09 28.12 1.07 o 2 4 0 45.89 46.02 1.53 o 3 4 0 147.61 154.85 4.66 o 4 4 0 155.75 148.65 5.00 o 5 4 0 93.45 95.23 4.08 o 1 5 0 109.82 101.90 2.09 o 2 5 0 2.94 3.26 1.06 o 3 5 0 32.49 33.44 3.28 o 4 5 0 11.67 10.14 1.74 o 5 5 0 1.58 0.89 2.12 o 0 6 0 150.57 153.50 6.30 o 1 6 0 1.24 -0.28 0.86 o 2 6 0 4.34 1.93 1.17 o 3 6 0 0.81 1.05 1.40 o 4 6 0 20.29 25.38 2.72 o 1 7 0 62.76 60.68 5.51 o 2 7 0 0.62 0.04 1.28 o 3 7 0 14.66 17.87 2.40 o 4 7 0 61.37 73.31 9.00 o 0 8 0 4.20 0.65 2.76 o 1 8 0 1.09 1.26 1.77 o 2 8 0 29.73 26.93 3.47 o 3 8 0 54.43 74.47 6.70 o 1 9 0 36.03 38.50 4.04 o 1 0 1 94.92 74.09 1.03 o 2 0 1 522.99 499.23 4.99 o 3 0 1 251.35 240.89 3.14 o 4 0 1 31.56 25.95 1.70 o 5 0 1 119.65 122.14 3.60 o 6 0 1 14.31 12.83 2.77 o 0 1 1 2830.07 2746.32 23.18 o 1 1 1 142.91 126.06 1.27 o 2 1 1 252.73 285.73 2.62 o 3 1 1 162.70 161.11 2.00 o 4 1 1 21.73 22.03 1.12 o 5 1 1 85.30 81.65 2.11 o 6 1 1 55.79 59.12 2.27 o 0 2 1 107.85 110.72 1.49 o 1 2 1 578.56 584.65 3.95 o 2 2 1 441.56 453.85 3.55 o 3 2 1 314.43 322.70 3.24 o 4 2 1 49.29 49.30 1.30 o 5 2 1 73.82 75.24 2.07 o 6 2 1 8.21 4.95 1.63 o 0 3 1 1899.67 1960.59 17.12 o 1 3 1 69.09 62.62 1.07 o 2 3 1 467.29 505.10 3.79 o 3 3 1 24.84 23.53 0.94 o 4 3 1 250.02 249.46 3.30 o 5 3 1 40.36 39.03 3.47 o 6 3 1 39.15 50.17 4.62 o 0 4 1 393.07 422.89 4.69 o 1 4 1 265.31 301.80 2.62 o 2 4 1 37.06 37.48 1.02 o 3 4 1 59.36 55.29 1.46 o 4 4 1 73.84 73.82 1.99 o 5 4 1 0.04 -0.96 1.28 o 0 5 1 45.19 49.72 1.68 o 1 5 1 62.32 59.59 1.22 o 2 5 1 331.55 324.67 4.22 o 3 5 1 37.11 38.90 1.54 o 4 5 1 17.98 17.65 1.43 o 5 5 1 76.44 78.22 4.12 o 0 6 1 130.12 128.45 2.92 o 1 6 1 247.23 247.12 2.99 o 2 6 1 21.53 19.04 1.18 o 3 6 1 52.06 52.01 2.05 o 4 6 1 28.88 31.51 2.61 o 0 7 1 52.79 45.48 2.38 o 1 7 1 44.41 41.18 1.91 o 2 7 1 20.17 22.38 1.64 o 3 7 1 35.34 38.44 1.96 o 4 7 1 5.09 4.82 1.74 o 0 8 1 29.89 32.75 2.29 o 1 8 1 48.13 51.23 2.55 o 2 8 1 5.01 4.23 1.47 o 3 8 1 8.46 9.81 2.25 o 0 9 1 1.39 6.33 2.27 o 1 9 1 4.42 4.59 1.74 o 0 0 2 11.47 6.98 0.41 o 1 0 2 1053.23 1032.30 9.07 o 2 0 2 319.48 319.69 3.52 o 3 0 2 454.66 511.55 5.51 o 4 0 2 1.14 0.24 0.98 o 5 0 2 15.84 11.49 2.09 o 6 0 2 0.04 -1.65 1.65 o 0 1 2 753.63 702.93 6.25 o 1 1 2 595.64 582.74 3.83 o 2 1 2 152.42 172.09 1.58 o 3 1 2 23.86 28.48 0.84 o 4 1 2 17.49 16.78 0.98 o 5 1 2 116.79 115.30 2.48 o 6 1 2 47.14 48.00 2.28 o 0 2 2 169.53 176.07 2.08 o 1 2 2 1998.32 2072.70 12.66 o 2 2 2 194.84 211.72 2.04 o 3 2 2 39.95 36.55 1.05 o 4 2 2 13.41 12.80 0.88 o 5 2 2 109.56 105.38 2.59 o 6 2 2 4.28 3.19 1.49 o 0 3 2 267.57 259.16 3.28 o 1 3 2 83.53 79.79 1.01 o 2 3 2 149.55 134.07 2.00 o 3 3 2 163.42 167.84 2.22 o 4 3 2 18.95 17.06 1.07 o 5 3 2 48.94 47.63 2.21 o 0 4 2 5.03 3.73 0.59 o 1 4 2 104.58 98.61 1.29 o 2 4 2 411.77 437.64 4.00 o 3 4 2 64.34 57.64 1.50 o 4 4 2 128.63 119.92 2.68 o 5 4 2 34.72 32.57 2.86 o 0 5 2 342.89 345.12 4.31 o 1 5 2 81.34 79.46 1.40 o 2 5 2 2.27 1.86 0.64 o 3 5 2 459.35 461.52 5.73 o 4 5 2 26.10 25.07 1.62 o 5 5 2 8.22 10.18 1.53 o 0 6 2 23.78 19.81 1.27 o 1 6 2 166.59 167.04 2.52 o 2 6 2 213.27 213.28 3.24 o 3 6 2 53.81 53.73 2.08 o 4 6 2 59.87 67.08 2.78 o 0 7 2 27.87 25.67 2.52 o 1 7 2 104.39 100.38 2.63 o 2 7 2 18.09 15.17 1.46 o 3 7 2 26.16 27.97 1.98 o 4 7 2 5.22 3.50 1.67 o 0 8 2 1.39 -0.14 1.35 o 1 8 2 4.70 3.21 1.36 o 2 8 2 12.13 8.57 1.68 o 3 8 2 1.00 1.74 1.73 o 0 9 2 2.90 5.51 3.28 o 1 9 2 13.46 14.43 2.28 o 1 0 3 4508.20 4528.17 38.64 o 2 0 3 77.03 79.42 1.43 o 3 0 3 4.83 3.70 0.59 o 4 0 3 18.05 12.60 1.39 o 5 0 3 165.91 172.51 4.29 o 6 0 3 66.40 66.38 3.42 o 0 1 3 2250.23 2170.50 17.14 o 1 1 3 1967.74 1954.82 11.89 o 2 1 3 83.26 87.93 1.07 o 3 1 3 143.80 142.12 1.75 o 4 1 3 205.11 205.20 3.00 o 5 1 3 70.12 71.87 2.03 o 6 1 3 24.84 24.09 2.08 o 0 2 3 225.66 237.44 3.24 o 1 2 3 459.73 461.82 3.46 o 2 2 3 48.33 50.12 0.82 o 3 2 3 330.17 346.42 3.42 o 4 2 3 8.83 8.33 0.79 o 5 2 3 94.02 97.28 2.73 o 6 2 3 4.49 2.96 1.56 o 0 3 3 105.86 104.36 1.65 o 1 3 3 427.15 430.20 3.44 o 2 3 3 249.27 244.46 2.22 o 3 3 3 65.06 64.57 1.48 o 4 3 3 6.84 3.95 0.87 o 5 3 3 81.04 83.96 2.63 o 0 4 3 19.85 21.38 0.93 o 1 4 3 668.80 679.53 5.20 o 2 4 3 65.75 60.23 1.28 o 3 4 3 283.03 277.60 3.69 o 4 4 3 4.54 3.98 0.93 o 5 4 3 12.09 8.79 1.56 o 0 5 3 53.96 58.71 1.81 o 1 5 3 89.16 83.13 1.43 o 2 5 3 91.37 90.06 1.78 o 3 5 3 10.61 9.84 1.26 o 4 5 3 5.19 4.05 1.12 o 5 5 3 31.58 35.27 2.20 o 0 6 3 16.65 13.87 1.25 o 1 6 3 4.98 2.69 0.68 o 2 6 3 63.93 58.03 1.95 o 3 6 3 25.07 24.48 1.55 o 4 6 3 4.18 2.30 1.27 o 0 7 3 214.33 216.05 5.66 o 1 7 3 14.50 14.03 1.28 o 2 7 3 95.46 91.21 2.71 o 3 7 3 12.50 11.35 1.58 o 4 7 3 3.10 5.33 1.87 o 0 8 3 3.92 3.10 1.80 o 1 8 3 10.06 9.52 1.62 o 2 8 3 37.61 40.61 2.46 o 3 8 3 24.79 25.56 2.59 o 0 9 3 15.56 15.99 3.44 o 1 9 3 6.25 7.51 2.15 o 0 0 4 2935.31 2826.24 33.80 o 1 0 4 862.07 916.62 8.31 o 2 0 4 75.11 90.08 2.08 o 3 0 4 67.33 69.72 1.60 o 4 0 4 2.09 0.46 1.01 o 5 0 4 34.15 33.27 2.26 o 6 0 4 49.13 57.01 6.39 o 0 1 4 312.47 311.13 3.21 o 1 1 4 3908.03 4104.66 25.61 o 2 1 4 327.17 335.56 2.79 o 3 1 4 33.99 34.76 0.93 o 4 1 4 113.50 105.74 1.96 o 5 1 4 14.70 14.06 1.30 o 6 1 4 3.83 3.07 1.55 o 0 2 4 55.85 61.33 1.10 o 1 2 4 47.51 50.75 0.81 o 2 2 4 228.10 225.00 2.05 o 3 2 4 117.00 109.59 2.13 o 4 2 4 219.43 217.84 3.26 o 5 2 4 24.13 23.64 2.14 o 6 2 4 24.39 23.19 2.57 o 0 3 4 308.89 355.67 3.91 o 1 3 4 511.26 526.55 4.23 o 2 3 4 64.13 54.83 1.23 o 3 3 4 10.38 11.34 0.91 o 4 3 4 168.11 171.62 2.91 o 5 3 4 73.94 73.89 2.55 o 0 4 4 179.97 171.34 2.50 o 1 4 4 59.28 56.90 1.38 o 2 4 4 110.85 107.85 1.69 o 3 4 4 58.65 64.47 1.99 o 4 4 4 56.84 62.11 1.95 o 5 4 4 20.15 19.61 1.92 o 0 5 4 35.75 36.58 1.57 o 1 5 4 49.32 49.18 1.16 o 2 5 4 25.25 26.90 1.27 o 3 5 4 16.08 16.27 1.16 o 4 5 4 2.80 1.63 1.15 o 5 5 4 6.91 7.74 1.68 o 0 6 4 349.86 336.62 5.15 o 1 6 4 35.27 34.33 1.40 o 2 6 4 13.36 12.90 1.26 o 3 6 4 28.41 30.02 1.96 o 4 6 4 29.37 30.99 1.94 o 0 7 4 4.36 2.44 1.23 o 1 7 4 18.33 19.00 1.38 o 2 7 4 11.89 11.86 1.41 o 3 7 4 1.48 1.84 1.36 o 4 7 4 30.79 36.84 5.68 o 0 8 4 18.46 20.86 2.47 o 1 8 4 29.82 36.39 2.64 o 2 8 4 31.54 34.91 2.18 o 3 8 4 15.43 17.38 2.74 o 0 9 4 14.43 15.10 3.27 o 1 9 4 16.47 20.78 2.52 o 1 0 5 165.26 197.20 2.39 o 2 0 5 31.08 31.93 1.03 o 3 0 5 12.60 15.42 0.94 o 4 0 5 188.12 195.76 5.47 o 5 0 5 8.53 3.84 1.65 o 6 0 5 38.97 49.10 4.38 o 0 1 5 977.74 981.47 12.70 o 1 1 5 800.12 798.22 5.57 o 2 1 5 589.41 650.98 4.62 o 3 1 5 83.05 77.87 1.32 o 4 1 5 60.45 60.40 1.74 o 5 1 5 2.32 0.61 1.06 o 6 1 5 14.11 14.64 2.05 o 0 2 5 896.28 898.09 9.04 o 1 2 5 397.39 409.95 3.25 o 2 2 5 120.22 104.65 1.47 o 3 2 5 38.43 42.14 1.23 o 4 2 5 92.48 84.26 2.12 o 5 2 5 0.50 -0.01 1.12 o 0 3 5 29.71 30.37 0.91 o 1 3 5 305.99 307.79 2.93 o 2 3 5 148.59 161.28 2.03 o 3 3 5 41.84 43.70 1.47 o 4 3 5 99.07 101.89 2.28 o 5 3 5 10.01 7.83 1.41 o 0 4 5 0.66 0.19 0.63 o 1 4 5 364.74 357.48 3.23 o 2 4 5 34.91 34.90 1.19 o 3 4 5 107.42 110.22 2.25 o 4 4 5 112.62 112.96 2.48 o 5 4 5 13.76 10.40 1.59 o 0 5 5 353.53 365.82 5.71 o 1 5 5 110.52 106.53 1.91 o 2 5 5 431.23 401.53 5.02 o 3 5 5 99.63 99.20 2.25 o 4 5 5 24.97 23.55 1.66 o 5 5 5 6.02 8.82 1.69 o 0 6 5 1.98 1.51 1.09 o 1 6 5 180.73 175.03 2.69 o 2 6 5 33.44 36.88 2.68 o 3 6 5 29.73 26.20 1.83 o 4 6 5 18.95 22.00 1.96 o 0 7 5 121.39 116.18 3.50 o 1 7 5 7.72 4.19 1.41 o 2 7 5 18.10 19.78 1.64 o 3 7 5 7.25 5.79 1.53 o 0 8 5 2.29 2.61 2.12 o 1 8 5 6.80 5.33 1.73 o 2 8 5 21.05 18.57 2.08 o 0 9 5 28.10 23.99 6.37 o 0 0 6 4.21 2.92 0.56 o 1 0 6 40.88 41.95 1.09 o 2 0 6 280.41 307.18 3.69 o 3 0 6 4.55 1.94 0.73 o 4 0 6 52.62 55.39 3.85 o 5 0 6 32.65 28.22 2.53 o 0 1 6 1127.87 1179.43 10.66 o 1 1 6 700.23 752.79 5.40 o 2 1 6 104.68 110.61 1.34 o 3 1 6 231.64 235.26 2.52 o 4 1 6 18.44 17.17 1.08 o 5 1 6 1.33 -0.14 1.24 o 0 2 6 76.95 76.24 1.35 o 1 2 6 162.79 177.23 1.82 o 2 2 6 227.86 241.03 2.78 o 3 2 6 7.91 6.46 0.79 o 4 2 6 248.34 246.95 3.80 o 5 2 6 24.22 22.85 1.73 o 0 3 6 57.18 64.59 1.33 o 1 3 6 236.76 241.34 2.54 o 2 3 6 225.10 224.92 2.57 o 3 3 6 119.05 114.54 2.21 o 4 3 6 44.28 45.08 1.69 o 5 3 6 15.02 15.70 1.66 o 0 4 6 0.00 0.77 0.74 o 1 4 6 131.55 141.80 1.96 o 2 4 6 111.97 109.32 1.94 o 3 4 6 31.52 32.34 1.42 o 4 4 6 152.22 143.88 2.86 o 5 4 6 36.58 38.32 2.56 o 0 5 6 168.44 165.47 3.71 o 1 5 6 1.02 1.19 0.65 o 2 5 6 3.50 1.62 0.73 o 3 5 6 131.69 130.74 2.64 o 4 5 6 14.77 12.21 1.28 o 5 5 6 6.79 0.98 3.98 o 0 6 6 0.75 0.67 1.09 o 1 6 6 99.54 100.07 2.21 o 2 6 6 75.46 74.52 2.15 o 3 6 6 3.65 1.47 1.31 o 4 6 6 21.31 25.50 1.85 o 0 7 6 3.81 6.53 1.51 o 1 7 6 13.12 10.79 1.28 o 2 7 6 11.76 10.46 1.61 o 3 7 6 59.61 68.89 3.74 o 0 8 6 21.31 23.14 3.39 o 1 8 6 32.89 35.64 2.40 o 2 8 6 38.45 39.09 2.60 o 1 0 7 337.46 328.04 3.73 o 2 0 7 174.60 159.06 2.52 o 3 0 7 10.32 7.21 0.86 o 4 0 7 0.29 -0.67 1.22 o 5 0 7 3.09 3.78 1.78 o 0 1 7 5.01 3.76 0.64 o 1 1 7 278.13 282.43 2.91 o 2 1 7 843.08 841.91 6.22 o 3 1 7 6.11 6.37 0.66 o 4 1 7 327.75 320.80 4.43 o 5 1 7 3.41 4.54 1.36 o 0 2 7 371.02 336.56 3.81 o 1 2 7 177.72 176.60 1.88 o 2 2 7 68.42 65.87 1.28 o 3 2 7 161.77 167.21 2.45 o 4 2 7 2.03 2.27 0.92 o 5 2 7 78.27 81.86 3.09 o 0 3 7 0.33 -0.18 0.62 o 1 3 7 114.51 107.67 1.63 o 2 3 7 291.17 291.36 3.11 o 3 3 7 72.99 66.28 1.73 o 4 3 7 15.38 12.42 1.28 o 5 3 7 8.86 6.31 1.70 o 0 4 7 25.37 26.11 2.63 o 1 4 7 0.10 -0.53 0.53 o 2 4 7 51.21 49.09 1.81 o 3 4 7 57.38 61.28 1.83 o 4 4 7 0.73 0.66 0.96 o 5 4 7 11.75 13.66 1.78 o 0 5 7 28.71 25.15 1.74 o 1 5 7 283.47 281.06 4.16 o 2 5 7 4.15 2.54 0.86 o 3 5 7 20.13 22.19 1.39 o 4 5 7 5.16 4.69 1.19 o 0 6 7 43.97 43.47 2.34 o 1 6 7 32.67 30.66 1.76 o 2 6 7 64.51 59.68 2.30 o 3 6 7 10.51 7.50 1.29 o 4 6 7 7.53 8.90 1.71 o 0 7 7 69.13 74.48 3.44 o 1 7 7 101.36 100.62 2.91 o 2 7 7 23.43 24.15 2.05 o 3 7 7 9.42 10.58 1.84 o 0 8 7 1.74 1.85 1.73 o 1 8 7 28.49 27.52 2.23 o 2 8 7 0.98 -1.15 1.73 o 0 0 8 103.90 88.40 2.26 o 1 0 8 117.16 107.40 1.82 o 2 0 8 0.09 -0.24 0.53 o 3 0 8 273.22 276.13 4.34 o 4 0 8 2.32 0.95 1.37 o 5 0 8 7.76 5.57 2.89 o 0 1 8 58.17 61.90 1.32 o 1 1 8 365.20 358.09 3.13 o 2 1 8 216.14 211.13 2.40 o 3 1 8 0.39 0.54 0.57 o 4 1 8 48.18 47.50 2.50 o 5 1 8 1.01 -0.10 1.30 o 0 2 8 566.96 597.34 6.16 o 1 2 8 32.85 39.79 0.91 o 2 2 8 512.48 514.86 5.17 o 3 2 8 253.38 243.65 3.16 o 4 2 8 55.45 54.55 1.98 o 5 2 8 2.19 2.26 1.40 o 0 3 8 151.10 153.95 3.33 o 1 3 8 103.52 117.76 1.77 o 2 3 8 31.06 35.48 1.14 o 3 3 8 4.28 2.46 0.79 o 4 3 8 54.15 55.79 1.95 o 5 3 8 85.47 95.58 3.36 o 0 4 8 204.23 221.68 4.39 o 1 4 8 28.91 31.79 1.30 o 2 4 8 73.89 68.76 1.63 o 3 4 8 183.81 187.65 3.14 o 4 4 8 6.10 5.14 1.11 o 5 4 8 2.38 3.61 1.44 o 0 5 8 0.18 -0.91 0.91 o 1 5 8 74.27 69.49 1.79 o 2 5 8 99.78 100.18 2.38 o 3 5 8 13.79 13.15 1.33 o 4 5 8 1.89 0.60 1.15 o 0 6 8 21.23 21.52 1.82 o 1 6 8 13.11 12.67 1.25 o 2 6 8 73.21 72.35 2.49 o 3 6 8 5.67 2.66 1.35 o 4 6 8 3.76 1.19 1.80 o 0 7 8 40.90 42.85 2.61 o 1 7 8 40.97 45.72 2.04 o 2 7 8 1.01 -0.27 1.22 o 3 7 8 6.40 5.43 1.85 o 0 8 8 8.61 9.77 2.19 o 1 8 8 10.34 8.00 1.87 o 1 0 9 107.26 119.92 2.04 o 2 0 9 21.81 21.40 1.23 o 3 0 9 78.24 85.57 2.36 o 4 0 9 8.19 7.82 1.47 o 5 0 9 13.41 13.70 2.80 o 0 1 9 3.46 5.82 0.63 o 1 1 9 174.24 179.68 2.48 o 2 1 9 140.54 149.94 1.92 o 3 1 9 112.80 113.50 2.20 o 4 1 9 4.06 3.07 1.05 o 5 1 9 24.37 23.57 2.03 o 0 2 9 0.40 1.23 0.89 o 1 2 9 31.13 30.96 0.97 o 2 2 9 663.27 663.41 5.66 o 3 2 9 80.56 75.88 1.73 o 4 2 9 1.04 2.31 1.04 o 5 2 9 10.69 11.39 1.77 o 0 3 9 355.06 328.25 5.52 o 1 3 9 28.57 25.04 1.04 o 2 3 9 7.59 9.12 0.79 o 3 3 9 134.94 135.02 2.55 o 4 3 9 2.36 0.35 0.95 o 5 3 9 16.93 18.13 2.11 o 0 4 9 16.54 16.93 1.53 o 1 4 9 67.43 63.00 1.69 o 2 4 9 57.17 56.39 1.57 o 3 4 9 12.52 11.15 1.14 o 4 4 9 2.07 2.51 1.09 o 0 5 9 245.65 246.33 5.05 o 1 5 9 15.47 14.77 1.11 o 2 5 9 219.44 213.54 3.66 o 3 5 9 4.70 4.10 1.16 o 4 5 9 25.69 27.03 1.92 o 0 6 9 6.40 6.11 1.38 o 1 6 9 141.51 143.12 3.59 o 2 6 9 29.68 29.02 2.24 o 3 6 9 7.16 6.35 1.47 o 0 7 9 0.86 1.48 1.57 o 1 7 9 3.11 0.63 1.20 o 2 7 9 21.42 24.84 1.95 o 0 8 9 15.58 16.76 2.42 o 1 8 9 11.74 12.34 1.94 o 0 0 10 723.24 768.18 15.06 o 1 0 10 726.66 724.72 8.39 o 2 0 10 34.78 34.48 1.58 o 3 0 10 21.52 17.36 1.42 o 4 0 10 11.77 13.16 1.87 o 5 0 10 0.84 -0.22 2.33 o 0 1 10 15.38 13.13 1.00 o 1 1 10 45.74 44.44 1.02 o 2 1 10 39.20 39.07 1.48 o 3 1 10 102.09 98.58 2.11 o 4 1 10 3.37 3.46 1.14 o 5 1 10 11.20 12.24 1.84 o 0 2 10 8.67 8.28 0.91 o 1 2 10 10.97 8.95 0.68 o 2 2 10 167.42 158.29 2.25 o 3 2 10 14.95 12.07 1.04 o 4 2 10 5.71 5.69 1.28 o 5 2 10 0.98 1.92 1.58 o 0 3 10 39.29 43.90 2.05 o 1 3 10 10.39 11.37 0.84 o 2 3 10 57.47 56.98 1.51 o 3 3 10 271.73 268.69 3.83 o 4 3 10 12.74 13.55 1.41 o 5 3 10 20.90 21.98 2.55 o 0 4 10 32.10 33.34 1.97 o 1 4 10 116.85 114.81 2.18 o 2 4 10 4.64 4.05 0.94 o 3 4 10 26.64 28.13 1.51 o 4 4 10 7.54 6.76 1.29 o 0 5 10 63.89 64.35 2.64 o 1 5 10 14.29 13.94 1.22 o 2 5 10 11.02 11.04 1.22 o 3 5 10 30.71 29.48 1.94 o 4 5 10 0.91 0.19 1.51 o 0 6 10 4.58 1.52 1.34 o 1 6 10 15.86 17.26 1.47 o 2 6 10 26.62 33.16 2.02 o 3 6 10 6.74 4.67 1.51 o 0 7 10 139.59 157.62 7.03 o 1 7 10 48.25 53.25 2.32 o 2 7 10 0.32 -1.45 1.45 o 1 0 11 11.53 13.39 1.09 o 2 0 11 5.03 6.92 1.04 o 3 0 11 400.15 408.50 6.80 o 4 0 11 22.55 21.54 2.28 o 5 0 11 71.48 82.79 5.27 o 0 1 11 0.21 0.64 0.70 o 1 1 11 103.89 96.00 1.65 o 2 1 11 125.99 128.48 2.17 o 3 1 11 99.48 94.42 2.12 o 4 1 11 16.63 14.55 2.50 o 5 1 11 0.07 -1.50 2.11 o 0 2 11 18.78 17.03 1.18 o 1 2 11 32.34 30.80 1.15 o 2 2 11 22.38 17.13 1.02 o 3 2 11 130.58 131.46 2.71 o 4 2 11 0.17 0.74 1.19 o 5 2 11 35.61 35.75 4.05 o 0 3 11 70.52 77.43 2.61 o 1 3 11 83.68 77.80 1.85 o 2 3 11 11.12 10.83 1.09 o 3 3 11 204.61 212.49 3.70 o 4 3 11 61.63 73.00 2.74 o 0 4 11 166.79 161.17 4.01 o 1 4 11 51.80 50.95 1.68 o 2 4 11 23.36 22.27 2.05 o 3 4 11 14.50 10.70 1.43 o 4 4 11 11.14 10.80 1.54 o 0 5 11 22.17 21.37 3.39 o 1 5 11 6.94 6.97 1.12 o 2 5 11 10.15 9.75 1.26 o 3 5 11 1.82 -1.13 1.46 o 0 6 11 0.26 0.61 1.46 o 1 6 11 11.97 11.07 1.36 o 2 6 11 0.09 -1.03 1.44 o 3 6 11 9.17 3.73 1.58 o 0 7 11 10.97 9.45 2.08 o 1 7 11 16.23 15.00 1.70 o 2 7 11 7.95 10.14 3.47 o 0 0 12 141.88 132.61 4.75 o 1 0 12 47.43 46.44 1.76 o 2 0 12 17.13 11.96 1.23 o 3 0 12 0.47 1.11 1.30 o 4 0 12 0.32 -0.33 1.61 o 0 1 12 32.18 33.21 1.57 o 1 1 12 11.83 11.59 0.86 o 2 1 12 68.69 64.74 1.63 o 3 1 12 15.66 11.85 1.11 o 4 1 12 5.40 5.36 1.42 o 0 2 12 195.56 188.88 4.08 o 1 2 12 184.77 185.66 2.91 o 2 2 12 96.21 95.75 2.14 o 3 2 12 211.20 209.78 3.40 o 4 2 12 18.36 19.60 1.75 o 0 3 12 0.08 -1.15 1.15 o 1 3 12 125.62 121.06 3.19 o 2 3 12 8.42 6.96 1.12 o 3 3 12 35.77 34.84 1.96 o 4 3 12 14.11 19.21 2.79 o 0 4 12 44.70 43.86 2.42 o 1 4 12 5.97 6.18 1.13 o 2 4 12 64.44 63.96 2.18 o 3 4 12 16.31 13.06 1.70 o 4 4 12 21.74 22.48 2.37 o 0 5 12 14.43 13.69 1.77 o 1 5 12 46.67 45.70 2.44 o 2 5 12 55.18 57.86 2.72 o 3 5 12 14.70 14.40 1.78 o 0 6 12 48.15 49.01 2.94 o 1 6 12 81.41 89.60 2.72 o 2 6 12 24.23 22.48 1.92 o 0 7 12 0.89 -0.61 1.78 o 1 7 12 10.36 8.79 1.62 o 1 0 13 9.66 10.01 1.29 o 2 0 13 0.33 -0.58 0.95 o 3 0 13 1.58 -0.54 1.45 o 4 0 13 0.01 -0.32 2.15 o 0 1 13 57.08 56.24 2.21 o 1 1 13 11.90 11.13 0.97 o 2 1 13 190.73 195.80 3.15 o 3 1 13 20.49 20.27 1.35 o 4 1 13 6.86 5.99 2.44 o 0 2 13 5.12 5.13 1.16 o 1 2 13 14.54 12.87 1.21 o 2 2 13 2.66 2.35 0.84 o 3 2 13 18.60 17.68 1.46 o 4 2 13 7.75 7.81 1.86 o 0 3 13 38.55 37.13 2.17 o 1 3 13 45.93 45.80 1.68 o 2 3 13 96.99 95.13 2.70 o 3 3 13 33.60 34.29 1.98 o 4 3 13 6.46 4.74 1.78 o 0 4 13 0.34 -0.36 1.22 o 1 4 13 43.53 47.75 1.86 o 2 4 13 84.11 81.76 2.67 o 3 4 13 12.05 9.66 1.70 o 0 5 13 37.70 36.43 2.47 o 1 5 13 13.94 13.05 1.32 o 2 5 13 4.42 3.41 1.20 o 3 5 13 7.12 6.16 2.19 o 0 6 13 0.06 -1.06 1.69 o 1 6 13 44.70 46.31 2.27 o 2 6 13 2.59 2.71 1.52 o 0 0 14 84.76 91.82 4.22 o 1 0 14 1.28 1.33 1.13 o 2 0 14 398.11 433.45 8.68 o 3 0 14 0.02 -1.52 1.52 o 4 0 14 15.27 10.72 2.80 o 0 1 14 146.30 157.25 4.64 o 1 1 14 25.58 26.84 1.47 o 2 1 14 10.72 7.99 1.03 o 3 1 14 18.09 17.79 1.61 o 4 1 14 11.78 13.81 1.96 o 0 2 14 1.45 0.39 1.34 o 1 2 14 2.98 2.43 0.94 o 2 2 14 40.26 39.51 1.82 o 3 2 14 20.98 19.46 1.64 o 4 2 14 2.15 1.40 1.93 o 0 3 14 161.50 167.55 4.26 o 1 3 14 4.20 2.81 1.00 o 2 3 14 16.29 15.14 1.49 o 3 3 14 28.63 26.68 2.14 o 0 4 14 8.84 12.17 1.77 o 1 4 14 26.12 24.24 1.62 o 2 4 14 81.97 85.48 2.81 o 3 4 14 23.79 25.02 2.19 o 0 5 14 0.12 -1.81 1.81 o 1 5 14 0.36 -0.13 1.21 o 2 5 14 5.25 5.87 1.57 o 0 6 14 13.54 13.60 2.20 o 1 6 14 10.77 9.01 1.64 o 1 0 15 20.74 24.51 3.93 o 2 0 15 11.42 14.10 3.45 o 3 0 15 5.45 4.60 2.48 o 0 1 15 3.21 4.16 1.59 o 1 1 15 121.74 124.23 3.06 o 2 1 15 37.28 34.63 1.77 o 3 1 15 3.00 2.17 1.31 o 0 2 15 98.10 106.01 4.05 o 1 2 15 17.85 18.19 1.54 o 2 2 15 58.63 59.89 2.25 o 3 2 15 21.62 21.57 1.73 o 0 3 15 3.75 4.49 1.68 o 1 3 15 27.34 27.34 1.68 o 2 3 15 52.14 56.16 2.45 o 3 3 15 17.21 13.19 1.92 o 0 4 15 1.05 0.79 1.49 o 1 4 15 5.68 3.83 1.22 o 2 4 15 7.80 5.73 1.52 o 0 5 15 5.24 7.25 1.93 o 1 5 15 24.31 28.40 2.14 o 2 5 15 2.87 0.56 3.97 o 0 0 16 3.73 1.84 1.79 o 1 0 16 69.05 71.30 3.49 o 2 0 16 3.13 4.66 1.92 o 3 0 16 1.38 -0.27 2.45 o 0 1 16 8.77 6.63 1.81 o 1 1 16 51.98 53.34 2.30 o 2 1 16 4.02 5.16 1.35 o 3 1 16 7.67 5.30 2.59 o 0 2 16 1.18 2.35 1.54 o 1 2 16 5.40 5.31 1.25 o 2 2 16 3.98 3.77 1.46 o 3 2 16 13.30 15.96 1.83 o 0 3 16 4.97 5.45 2.01 o 1 3 16 31.38 32.95 2.09 o 2 3 16 0.38 -1.35 1.35 o 0 4 16 48.45 52.43 3.62 o 1 4 16 33.39 29.68 1.95 o 2 4 16 19.77 24.93 2.71 o 0 5 16 9.11 10.33 5.42 o 1 0 17 91.44 98.75 4.23 o 2 0 17 0.35 -0.91 1.91 o 0 1 17 23.46 24.07 2.60 o 1 1 17 8.02 9.52 1.52 o 2 1 17 37.93 35.88 2.45 o 0 2 17 11.51 9.18 2.41 o 1 2 17 98.00 100.56 3.10 o 2 2 17 6.10 8.14 1.76 o 0 3 17 0.15 -0.60 1.83 o 1 3 17 25.79 23.37 2.02 o 2 3 17 14.86 9.73 2.50 o 0 4 17 3.29 1.89 2.11 o 1 4 17 54.50 46.84 3.61 o 0 0 18 2.18 -3.46 3.46 o 1 0 18 10.37 6.00 2.84 o 2 0 18 0.52 -1.12 2.28 o 0 1 18 7.66 10.60 4.57 o 1 1 18 56.33 63.15 3.04 o 2 1 18 3.40 6.25 2.10 o 0 2 18 16.61 14.50 2.51 o 1 2 18 29.08 30.92 2.21 o 0 3 18 12.79 13.31 4.00 o