#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/61/2206136.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206136_Fobs loop_ _publ_author_name 'Jones, Peter G.' 'Bubenitschek, Peter' 'Hopf, Henning' 'Savinsky, Rainer' _publ_section_title ; syn-exo-4,7,12,15-Tetrakis(trimethylsilyl)-4,7,12,15-tetrahydro[2.2]paracyclophane ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2177 _journal_page_last o2178 _journal_volume 61 _journal_year 2005 _space_group_IT_number 98 _symmetry_space_group_name_Hall 'I 4bw 2bw' _symmetry_space_group_name_H-M 'I 41 2 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.9060 _cell_length_b 13.9060 _cell_length_c 16.2630 _exptl_crystal_F_000 1104.00 _reflns_d_resolution_high 0.7685 _[local]_cod_data_source_file bt66803sup2.hkl _[local]_cod_data_source_block 3 #BEGIN Tags that were not found in dictionaries: _shelx_title ' zoff in I4(1)22' _shelx_refln_list_code 4 _shelx_f_calc_maximum 185.72 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-y, x+1/2, z+1/4' 'y+1/2, -x, z+3/4' '-x+1/2, y, -z+3/4' 'x, -y+1/2, -z+1/4' 'y+1/2, x+1/2, -z+1/2' '-y, -x, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, -y+1, z+1' '-y+1/2, x+1, z+3/4' 'y+1, -x+1/2, z+5/4' '-x+1, y+1/2, -z+5/4' 'x+1/2, -y+1, -z+3/4' 'y+1, x+1, -z+1' '-y+1/2, -x+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 2 0 6593.53 6036.94 50.23 o 1 3 0 590.84 618.66 12.69 o 3 3 0 1838.88 1631.94 30.84 o 0 4 0 9542.82 10392.13 91.64 o 2 4 0 12140.79 12067.51 89.00 o 1 5 0 238.52 222.06 9.52 o 3 5 0 730.79 711.56 39.65 o 5 5 0 7056.05 6844.98 82.83 o 0 6 0 18444.09 16626.29 141.87 o 2 6 0 529.34 621.63 17.31 o 4 6 0 983.77 1076.98 23.65 o 6 6 0 6090.00 5927.67 86.36 o 1 7 0 6556.23 6388.88 55.91 o 3 7 0 1426.59 1508.02 28.58 o 5 7 0 768.71 705.62 22.11 o 7 7 0 2499.51 2253.17 58.16 o 0 8 0 240.86 165.06 16.30 o 2 8 0 3378.83 3576.11 46.06 o 4 8 0 1120.07 1063.78 26.43 o 6 8 0 516.84 559.82 21.18 o 8 8 0 109.28 80.19 15.86 o 1 9 0 2764.46 2778.37 62.56 o 3 9 0 307.01 398.78 18.95 o 5 9 0 1004.77 917.14 33.93 o 7 9 0 128.62 96.77 12.46 o 9 9 0 661.94 699.65 40.53 o 0 10 0 92.09 47.23 8.39 o 2 10 0 99.10 101.30 10.78 o 4 10 0 1112.68 1172.89 30.80 o 6 10 0 112.80 93.20 11.84 o 8 10 0 43.04 43.54 11.90 o 10 10 0 13.52 17.62 11.46 o 1 11 0 1271.82 1154.14 31.49 o 3 11 0 376.17 326.36 18.04 o 5 11 0 576.20 600.39 25.09 o 7 11 0 193.04 168.21 16.20 o 9 11 0 595.65 629.16 29.29 o 11 11 0 65.94 33.48 15.86 o 0 12 0 1170.82 1282.70 36.70 o 2 12 0 1038.91 1069.92 32.24 o 4 12 0 447.86 549.36 29.08 o 6 12 0 67.97 59.83 12.42 o 8 12 0 60.22 63.89 34.37 o 10 12 0 6.70 14.44 8.66 o 12 12 0 202.75 197.38 29.96 o 1 13 0 1303.26 1240.00 36.62 o 3 13 0 1079.03 971.06 49.35 o 5 13 0 10.41 26.36 9.60 o 7 13 0 625.18 628.91 30.53 o 9 13 0 241.58 221.21 21.18 o 11 13 0 89.40 117.88 33.04 o 0 14 0 224.91 212.68 18.31 o 2 14 0 210.14 227.24 18.66 o 4 14 0 351.85 377.22 49.79 o 6 14 0 261.06 261.55 21.33 o 8 14 0 30.23 24.67 11.84 o 10 14 0 39.30 53.85 13.30 o 1 15 0 283.23 294.45 24.67 o 3 15 0 0.12 -8.02 9.69 o 5 15 0 306.10 311.51 23.31 o 7 15 0 23.90 18.46 16.74 o 9 15 0 31.01 43.88 13.93 o 0 16 0 507.59 562.15 30.18 o 2 16 0 45.20 52.04 19.83 o 4 16 0 2.15 0.47 9.28 o 6 16 0 103.50 147.30 17.06 o 8 16 0 3.16 -4.41 8.26 o 1 17 0 13.14 11.54 9.52 o 3 17 0 35.38 44.06 13.08 o 5 17 0 187.41 214.54 44.50 o 0 18 0 1.57 -27.55 67.41 o 1 2 1 23015.03 24812.05 91.48 o 0 3 1 21068.24 21094.91 123.24 o 2 3 1 221.28 282.48 7.55 o 1 4 1 468.24 439.48 9.37 o 3 4 1 413.42 435.48 9.58 o 0 5 1 4460.88 4561.03 28.27 o 2 5 1 2666.65 3257.63 26.10 o 4 5 1 1861.54 2002.46 21.25 o 1 6 1 2115.40 2081.45 30.02 o 3 6 1 9001.51 9752.98 56.38 o 5 6 1 803.67 1026.36 17.17 o 0 7 1 299.77 205.32 8.02 o 2 7 1 1779.08 1742.13 21.19 o 4 7 1 2699.54 2618.74 27.29 o 6 7 1 618.86 614.88 15.79 o 1 8 1 659.96 608.72 13.25 o 3 8 1 521.48 662.48 14.83 o 5 8 1 2030.12 1935.20 26.10 o 7 8 1 1219.39 1153.08 22.12 o 0 9 1 1542.93 1497.60 27.09 o 2 9 1 3044.73 2734.37 29.89 o 4 9 1 470.37 411.24 15.52 o 6 9 1 62.20 35.26 6.23 o 8 9 1 6.55 21.04 9.00 o 1 10 1 629.75 602.29 23.15 o 3 10 1 297.43 295.42 12.34 o 5 10 1 408.93 397.82 23.39 o 7 10 1 1518.27 1542.94 39.43 o 9 10 1 746.30 720.35 20.92 o 0 11 1 309.29 230.49 10.89 o 2 11 1 2939.00 2853.52 34.06 o 4 11 1 576.28 577.13 17.03 o 6 11 1 267.38 238.64 12.54 o 8 11 1 295.00 308.35 22.26 o 10 11 1 1.93 9.03 6.17 o 1 12 1 10.71 6.63 15.27 o 3 12 1 239.86 221.31 14.12 o 5 12 1 452.65 455.10 19.59 o 7 12 1 244.70 229.62 13.22 o 9 12 1 3.50 -4.92 4.92 o 11 12 1 94.58 85.53 11.96 o 0 13 1 13.92 26.18 8.39 o 2 13 1 497.49 500.54 17.03 o 4 13 1 194.82 206.77 13.61 o 6 13 1 40.26 46.78 7.68 o 8 13 1 9.95 -7.58 13.89 o 10 13 1 76.04 47.47 9.56 o 12 13 1 17.27 15.69 7.76 o 1 14 1 62.43 102.84 9.63 o 3 14 1 124.12 139.63 11.70 o 5 14 1 214.26 219.29 13.62 o 7 14 1 26.48 31.56 7.45 o 9 14 1 60.77 54.80 9.69 o 11 14 1 55.36 71.36 10.89 o 0 15 1 354.49 334.69 16.67 o 2 15 1 620.39 611.69 27.60 o 4 15 1 375.54 391.39 23.91 o 6 15 1 79.92 65.95 9.55 o 8 15 1 187.98 183.40 21.91 o 10 15 1 61.47 43.88 15.90 o 1 16 1 144.62 132.48 11.75 o 3 16 1 62.81 79.09 10.60 o 5 16 1 18.34 30.74 9.06 o 7 16 1 157.92 180.68 14.09 o 0 17 1 164.39 164.66 15.55 o 2 17 1 72.12 73.38 10.42 o 4 17 1 57.59 72.74 10.86 o 6 17 1 135.69 164.35 14.61 o 1 18 1 133.58 138.20 19.21 o 1 1 2 2059.29 1787.82 17.41 o 0 2 2 9021.98 9531.82 65.37 o 2 2 2 15876.30 15841.32 67.28 o 1 3 2 3837.27 3652.51 22.00 o 3 3 2 1585.92 1974.26 24.61 o 0 4 2 2610.74 2721.73 41.46 o 2 4 2 6755.78 6856.95 57.36 o 4 4 2 1037.53 772.81 37.01 o 1 5 2 2738.82 2869.62 29.65 o 3 5 2 1335.81 1434.91 24.93 o 5 5 2 1720.70 1732.57 30.51 o 0 6 2 96.69 113.43 6.68 o 2 6 2 3264.79 3836.30 30.78 o 4 6 2 3105.74 3759.15 45.42 o 6 6 2 1200.67 1363.07 29.27 o 1 7 2 3023.73 3119.87 50.24 o 3 7 2 177.51 247.69 13.35 o 5 7 2 1360.54 1510.83 22.33 o 7 7 2 14.12 1.32 6.23 o 0 8 2 2063.26 2096.76 52.53 o 2 8 2 3743.23 3641.55 43.12 o 4 8 2 1266.15 1191.22 20.33 o 6 8 2 104.63 112.33 7.89 o 8 8 2 3573.26 3595.73 57.31 o 1 9 2 2222.35 1917.36 33.81 o 3 9 2 884.87 815.74 18.57 o 5 9 2 1055.60 923.34 19.81 o 7 9 2 1051.62 1036.85 22.02 o 9 9 2 129.68 108.38 13.08 o 0 10 2 502.30 567.76 16.04 o 2 10 2 180.59 200.79 11.73 o 4 10 2 2982.29 2950.71 45.91 o 6 10 2 408.71 457.95 15.84 o 8 10 2 275.95 221.91 12.32 o 10 10 2 640.79 646.44 29.89 o 1 11 2 493.92 480.23 15.06 o 3 11 2 86.51 66.74 8.96 o 5 11 2 199.31 165.40 10.58 o 7 11 2 442.28 376.05 17.04 o 9 11 2 109.39 104.59 10.33 o 11 11 2 2.46 37.01 11.22 o 0 12 2 259.84 210.50 11.30 o 2 12 2 20.82 12.57 5.46 o 4 12 2 626.12 599.44 18.34 o 6 12 2 148.00 126.76 11.96 o 8 12 2 90.08 61.87 8.86 o 10 12 2 100.40 73.63 10.73 o 12 12 2 8.87 18.06 10.59 o 1 13 2 61.87 64.56 7.61 o 3 13 2 81.74 85.43 9.25 o 5 13 2 283.14 286.57 14.50 o 7 13 2 123.59 126.04 14.63 o 9 13 2 19.07 7.58 6.61 o 11 13 2 18.35 25.73 7.48 o 0 14 2 161.82 125.99 16.41 o 2 14 2 534.77 553.36 18.87 o 4 14 2 49.65 57.33 7.93 o 6 14 2 29.52 24.83 7.76 o 8 14 2 215.49 235.58 15.42 o 10 14 2 25.25 19.07 13.78 o 1 15 2 290.61 312.46 15.78 o 3 15 2 26.74 42.96 8.52 o 5 15 2 179.55 229.67 14.53 o 7 15 2 119.59 138.69 12.63 o 9 15 2 33.78 51.43 9.85 o 0 16 2 125.30 138.23 19.21 o 2 16 2 42.52 65.31 9.55 o 4 16 2 136.58 165.90 23.98 o 6 16 2 19.82 16.46 8.06 o 8 16 2 7.18 4.21 6.88 o 1 17 2 83.48 68.13 17.38 o 3 17 2 286.09 342.52 18.21 o 5 17 2 21.77 26.76 8.49 o 0 18 2 167.23 166.03 27.35 o 0 1 3 10786.47 11312.06 36.56 o 1 2 3 12256.51 12990.61 87.50 o 0 3 3 34491.68 34831.15 99.71 o 2 3 3 3955.88 4022.75 41.72 o 1 4 3 491.25 441.15 16.92 o 3 4 3 4064.50 5308.01 32.48 o 0 5 3 4093.40 3713.36 35.61 o 2 5 3 1194.00 1143.44 18.06 o 4 5 3 450.85 563.60 16.92 o 1 6 3 5257.78 5220.69 38.58 o 3 6 3 873.39 745.55 13.95 o 5 6 3 1706.48 1653.23 22.25 o 0 7 3 333.80 377.99 11.25 o 2 7 3 513.93 553.33 12.84 o 4 7 3 1616.62 1498.72 29.46 o 6 7 3 1493.76 1430.56 28.24 o 1 8 3 3504.45 3241.14 38.23 o 3 8 3 802.86 816.86 16.92 o 5 8 3 4440.32 4191.77 39.17 o 7 8 3 865.37 802.62 19.16 o 0 9 3 360.37 400.93 17.68 o 2 9 3 75.88 88.01 10.78 o 4 9 3 11.80 2.84 4.79 o 6 9 3 795.06 824.14 21.37 o 8 9 3 151.35 146.10 10.33 o 1 10 3 1586.74 1440.53 33.00 o 3 10 3 115.19 108.57 12.08 o 5 10 3 648.38 641.61 17.74 o 7 10 3 659.94 652.99 18.71 o 9 10 3 25.62 11.70 6.49 o 0 11 3 126.88 108.40 8.13 o 2 11 3 72.67 65.64 7.89 o 4 11 3 236.20 216.76 11.96 o 6 11 3 258.15 263.12 23.25 o 8 11 3 182.29 185.26 12.10 o 10 11 3 171.67 140.86 11.90 o 1 12 3 2160.36 2107.46 32.96 o 3 12 3 243.85 270.95 15.14 o 5 12 3 158.12 171.96 11.40 o 7 12 3 384.01 390.11 16.58 o 9 12 3 44.47 57.38 8.59 o 11 12 3 88.15 83.75 11.52 o 0 13 3 514.88 489.50 17.87 o 2 13 3 76.68 65.75 8.02 o 4 13 3 197.64 201.84 12.29 o 6 13 3 301.10 338.54 17.44 o 8 13 3 273.20 272.12 15.72 o 10 13 3 284.27 292.63 16.82 o 12 13 3 173.70 153.97 16.86 o 1 14 3 418.37 444.42 28.62 o 3 14 3 60.54 64.03 8.67 o 5 14 3 275.79 236.18 14.07 o 7 14 3 120.55 137.75 17.93 o 9 14 3 22.91 8.85 7.76 o 11 14 3 61.09 52.18 10.53 o 0 15 3 31.22 43.31 10.34 o 2 15 3 32.49 21.99 9.91 o 4 15 3 0.82 -4.63 13.93 o 6 15 3 52.74 47.26 10.90 o 8 15 3 31.59 -7.20 17.34 o 1 16 3 205.44 172.26 13.12 o 3 16 3 13.46 20.21 7.26 o 5 16 3 54.03 43.30 9.16 o 7 16 3 60.31 50.20 9.89 o 0 17 3 1.65 15.01 7.95 o 2 17 3 69.84 78.52 10.65 o 4 17 3 35.82 34.78 9.29 o 0 0 4 17457.13 17820.02 76.02 o 1 1 4 873.79 758.83 15.26 o 0 2 4 7681.97 9220.53 38.11 o 2 2 4 8086.52 9047.62 55.45 o 1 3 4 2763.88 3105.03 23.19 o 3 3 4 465.37 497.34 18.95 o 0 4 4 2102.63 2277.46 20.79 o 2 4 4 1815.21 1880.65 19.63 o 4 4 4 3689.01 4075.66 44.23 o 1 5 4 319.28 358.86 9.68 o 3 5 4 682.38 616.35 15.65 o 5 5 4 22.81 25.76 25.55 o 0 6 4 11950.99 11607.43 93.36 o 2 6 4 4068.18 4453.45 33.96 o 4 6 4 1326.71 1399.60 20.04 o 6 6 4 2958.76 2998.06 45.79 o 1 7 4 975.03 910.53 26.84 o 3 7 4 1024.80 973.83 17.42 o 5 7 4 11.88 -4.51 6.36 o 7 7 4 3581.43 3707.23 54.52 o 0 8 4 3.27 9.77 4.47 o 2 8 4 1787.18 1739.25 28.94 o 4 8 4 1668.13 1655.27 24.42 o 6 8 4 239.07 311.21 20.73 o 8 8 4 858.41 868.91 29.89 o 1 9 4 2210.99 2043.66 44.90 o 3 9 4 551.45 539.95 20.99 o 5 9 4 1392.46 1296.67 23.89 o 7 9 4 2092.61 1970.05 30.72 o 9 9 4 200.18 160.54 18.06 o 0 10 4 1349.00 1250.74 25.92 o 2 10 4 635.00 672.66 17.48 o 4 10 4 54.17 54.70 8.14 o 6 10 4 688.34 717.63 20.86 o 8 10 4 586.68 603.16 19.37 o 10 10 4 3.74 8.34 9.28 o 1 11 4 1063.87 880.92 29.00 o 3 11 4 900.35 836.13 25.69 o 5 11 4 611.59 607.77 18.38 o 7 11 4 0.97 3.63 5.49 o 9 11 4 73.40 117.21 11.15 o 11 11 4 124.11 79.55 15.88 o 0 12 4 57.94 77.88 8.39 o 2 12 4 157.02 163.46 11.19 o 4 12 4 226.74 218.47 12.29 o 6 12 4 69.03 41.28 7.68 o 8 12 4 134.44 140.97 11.40 o 10 12 4 358.98 435.25 19.47 o 12 12 4 1.52 2.40 10.15 o 1 13 4 777.36 773.02 44.20 o 3 13 4 32.37 28.60 6.80 o 5 13 4 72.04 56.28 10.90 o 7 13 4 245.66 268.90 15.19 o 9 13 4 50.21 46.72 13.23 o 11 13 4 38.54 28.04 16.15 o 0 14 4 1.28 -0.34 7.35 o 2 14 4 274.19 194.79 13.72 o 4 14 4 289.73 320.99 22.00 o 6 14 4 92.12 117.14 13.33 o 8 14 4 33.67 36.81 8.65 o 10 14 4 297.72 300.26 18.15 o 1 15 4 246.29 240.68 15.02 o 3 15 4 322.20 351.34 16.80 o 5 15 4 96.09 97.99 11.52 o 7 15 4 156.41 135.45 17.30 o 9 15 4 15.96 22.41 8.54 o 0 16 4 17.78 11.93 9.28 o 2 16 4 111.32 92.94 10.82 o 4 16 4 21.43 2.45 22.06 o 6 16 4 102.63 124.12 12.75 o 1 17 4 8.73 -6.37 14.30 o 3 17 4 0.66 -6.49 7.82 o 5 17 4 55.55 73.97 11.83 o 0 1 5 5196.22 6326.82 32.71 o 1 2 5 9774.90 11417.18 82.80 o 0 3 5 336.39 354.14 8.92 o 2 3 5 6451.85 6449.61 57.70 o 1 4 5 908.59 833.19 13.87 o 3 4 5 293.46 262.33 12.72 o 0 5 5 6983.00 8005.75 44.00 o 2 5 5 3100.63 3576.45 38.16 o 4 5 5 2921.82 2978.68 28.52 o 1 6 5 5154.91 5436.31 59.52 o 3 6 5 98.48 91.84 11.45 o 5 6 5 1356.30 1342.71 21.14 o 0 7 5 3822.10 4174.75 35.40 o 2 7 5 1560.61 1484.39 27.73 o 4 7 5 1119.97 1025.05 18.93 o 6 7 5 1485.33 1444.18 40.45 o 1 8 5 276.27 243.11 10.26 o 3 8 5 865.56 958.87 19.03 o 5 8 5 172.87 159.58 9.77 o 7 8 5 1761.62 1728.10 29.80 o 0 9 5 965.54 918.43 18.91 o 2 9 5 3158.81 3098.13 34.32 o 4 9 5 4251.58 4285.70 79.65 o 6 9 5 644.76 598.74 20.73 o 8 9 5 1250.96 1171.50 25.75 o 1 10 5 229.81 197.43 10.80 o 3 10 5 977.56 1017.63 21.56 o 5 10 5 308.94 298.07 13.30 o 7 10 5 101.39 109.65 9.91 o 9 10 5 303.10 325.63 15.63 o 0 11 5 22.47 4.26 6.19 o 2 11 5 101.62 91.02 8.79 o 4 11 5 1679.52 1678.15 29.48 o 6 11 5 59.13 44.24 9.11 o 8 11 5 434.36 433.27 17.83 o 10 11 5 194.05 196.96 13.96 o 1 12 5 74.58 66.08 7.89 o 3 12 5 286.48 268.06 13.59 o 5 12 5 187.19 149.23 15.64 o 7 12 5 109.79 140.46 11.46 o 9 12 5 36.11 72.54 10.57 o 11 12 5 116.06 126.85 19.21 o 0 13 5 25.08 19.10 7.38 o 2 13 5 91.73 111.98 10.14 o 4 13 5 670.19 649.71 21.10 o 6 13 5 127.63 126.93 16.28 o 8 13 5 407.56 417.74 19.15 o 10 13 5 100.84 84.61 12.06 o 1 14 5 109.04 109.47 10.73 o 3 14 5 7.69 19.57 7.08 o 5 14 5 17.49 14.11 7.09 o 7 14 5 240.26 270.02 16.52 o 9 14 5 80.20 90.44 14.88 o 0 15 5 115.28 138.99 25.18 o 2 15 5 41.19 36.27 9.81 o 4 15 5 218.48 218.54 14.42 o 6 15 5 55.36 83.81 11.18 o 8 15 5 38.27 19.10 12.21 o 1 16 5 18.79 2.56 9.54 o 3 16 5 177.15 232.71 15.45 o 5 16 5 7.99 17.88 9.03 o 7 16 5 10.18 18.85 11.45 o 0 17 5 185.51 160.01 24.29 o 2 17 5 164.65 166.50 17.93 o 4 17 5 31.36 30.47 8.65 o 1 1 6 25526.13 27660.34 116.82 o 0 2 6 11975.10 11725.61 50.11 o 2 2 6 695.40 679.03 74.90 o 1 3 6 2199.85 2200.44 22.14 o 3 3 6 0.39 14.54 6.23 o 0 4 6 4147.83 3502.09 35.23 o 2 4 6 2474.54 2813.81 31.42 o 4 4 6 297.82 369.97 18.06 o 1 5 6 3044.52 3110.67 28.07 o 3 5 6 2905.51 2992.39 29.34 o 5 5 6 210.76 229.16 13.71 o 0 6 6 14.57 5.85 4.06 o 2 6 6 7236.92 7358.42 70.59 o 4 6 6 4792.95 5033.02 41.00 o 6 6 6 356.50 289.43 32.60 o 1 7 6 207.79 229.53 9.64 o 3 7 6 1308.80 1400.28 22.11 o 5 7 6 1493.46 1377.76 27.09 o 7 7 6 582.00 554.72 29.52 o 0 8 6 3029.10 2951.96 33.36 o 2 8 6 2439.76 2275.97 28.42 o 4 8 6 711.56 746.40 18.06 o 6 8 6 874.31 929.93 21.11 o 8 8 6 3.11 -5.68 8.37 o 1 9 6 718.54 750.19 17.86 o 3 9 6 189.20 151.31 10.30 o 5 9 6 625.53 554.95 21.11 o 7 9 6 1271.50 1278.39 26.40 o 9 9 6 63.99 70.28 13.08 o 0 10 6 60.88 56.60 7.59 o 2 10 6 570.50 507.07 15.82 o 4 10 6 349.40 358.27 14.45 o 6 10 6 131.18 108.83 10.68 o 8 10 6 179.48 160.98 12.00 o 10 10 6 167.48 192.22 32.16 o 1 11 6 1084.43 1107.71 25.95 o 3 11 6 327.26 338.24 14.23 o 5 11 6 195.71 203.72 12.29 o 7 11 6 1338.60 1381.66 29.54 o 9 11 6 259.07 203.32 27.73 o 11 11 6 52.00 33.87 12.78 o 0 12 6 432.04 416.18 15.93 o 2 12 6 758.31 699.17 23.66 o 4 12 6 724.42 732.02 21.56 o 6 12 6 50.38 64.04 9.31 o 8 12 6 42.75 35.74 14.12 o 10 12 6 5.39 -6.55 6.55 o 12 12 6 36.79 52.78 15.26 o 1 13 6 133.99 114.80 10.52 o 3 13 6 235.50 231.08 13.72 o 5 13 6 438.47 421.08 18.06 o 7 13 6 19.17 5.91 8.78 o 9 13 6 284.91 339.50 25.56 o 11 13 6 357.20 411.15 20.90 o 0 14 6 0.28 -2.34 11.49 o 2 14 6 208.19 193.88 12.87 o 4 14 6 85.64 86.32 10.42 o 6 14 6 0.29 7.25 6.57 o 8 14 6 27.79 39.37 12.29 o 10 14 6 17.77 -12.52 12.52 o 1 15 6 63.39 62.21 12.23 o 3 15 6 44.83 24.40 8.03 o 5 15 6 31.45 8.38 8.52 o 7 15 6 219.72 260.21 16.96 o 0 16 6 130.80 149.58 12.95 o 2 16 6 59.54 70.76 10.13 o 4 16 6 192.21 215.53 15.39 o 6 16 6 68.63 83.90 11.48 o 1 17 6 97.35 116.54 19.97 o 3 17 6 2.96 -1.48 6.17 o 0 1 7 9025.11 9982.81 49.11 o 1 2 7 84.99 48.32 5.49 o 0 3 7 28.08 36.34 7.82 o 2 3 7 2517.14 2339.31 24.87 o 1 4 7 51.95 93.55 14.75 o 3 4 7 3102.38 3188.07 31.29 o 0 5 7 652.48 543.32 12.97 o 2 5 7 797.34 657.32 14.52 o 4 5 7 2310.74 2422.10 28.09 o 1 6 7 2553.12 2595.13 33.34 o 3 6 7 156.44 197.98 9.55 o 5 6 7 1657.38 1754.04 25.88 o 0 7 7 1080.99 1010.19 22.00 o 2 7 7 484.15 442.56 13.74 o 4 7 7 239.08 198.58 15.73 o 6 7 7 1385.84 1256.29 24.00 o 1 8 7 1508.08 1520.06 30.65 o 3 8 7 472.56 486.90 14.97 o 5 8 7 91.80 92.70 10.81 o 7 8 7 538.91 546.28 21.75 o 0 9 7 174.86 171.71 11.19 o 2 9 7 1714.32 1708.52 27.37 o 4 9 7 1850.54 1808.88 28.91 o 6 9 7 214.62 209.57 11.87 o 8 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400.04 36.63 o 1 2 19 65.28 54.38 11.29 o 0 3 19 55.66 58.35 10.71 o 2 3 19 234.80 237.00 17.81 o 1 4 19 177.27 158.35 15.07 o 3 4 19 264.25 287.66 19.02 o 0 5 19 445.69 413.46 22.89 o 2 5 19 138.46 131.82 15.26 o 4 5 19 62.36 81.31 11.90 o 1 6 19 479.18 477.17 23.23 o 3 6 19 65.38 72.75 13.37 o 5 6 19 78.30 50.60 12.86 o 0 7 19 364.92 350.88 21.02 o 2 7 19 26.61 16.92 15.39 o 0 0 20 608.31 645.32 37.07 o 1 1 20 0.05 -7.93 14.10 o 0 2 20 23.54 20.85 10.17 o 2 2 20 3.07 7.93 12.76 o 1 3 20 861.50 802.11 29.30 o 3 3 20 12.82 -7.45 10.15 o 0 4 20 1.80 -11.19 11.19 o 2 4 20 126.49 125.85 14.40 o 4 4 20 1.82 21.15 21.15 o 1 5 20 86.07 86.52 12.75 o 3 5 20 102.38 115.33 14.37 o 0 1 21 26.18 30.21 10.63 o 1 2 21 177.19 188.23 16.67 o