#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2206164.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206164_Fobs loop_ _publ_author_name 'Zhang, Hui' 'Fang, Liang' 'Yuan, Runzhang' _publ_section_title ; Diaquadibromobis(1H-imidazole)nickel(II) ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1391 _journal_page_last m1392 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.114 _cell_angle_gamma 90.000 _cell_length_a 7.8000 _cell_length_b 9.3659 _cell_length_c 8.4736 _exptl_crystal_F_000 380.00 _reflns_d_resolution_high 0.7487 _[local]_cod_data_source_file cv6519Isup2.hkl _[local]_cod_data_source_block I loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 12629.22 11162.14 236.15 o 2 0 0 8569.04 8469.05 202.11 o 3 0 0 37.05 42.03 2.84 o 4 0 0 750.89 750.81 20.05 o 5 0 0 4975.76 5191.85 126.40 o 6 0 0 15.60 15.24 5.45 o 7 0 0 5.49 10.45 5.71 o 8 0 0 3140.87 3146.41 95.20 o 9 0 0 2489.07 2548.57 147.88 o 10 0 0 1392.25 1474.19 68.63 o 1 1 0 2806.85 3089.09 52.89 o 2 1 0 15513.69 13828.98 235.78 o 3 1 0 8676.05 8357.45 142.30 o 4 1 0 729.09 771.18 15.81 o 5 1 0 325.80 320.90 10.80 o 6 1 0 2887.00 2939.73 61.99 o 7 1 0 2801.65 2827.18 60.22 o 8 1 0 653.52 648.32 17.63 o 9 1 0 68.23 61.15 10.04 o 10 1 0 185.93 188.47 16.24 o 0 2 0 140.34 194.10 16.73 o 1 2 0 540.95 616.19 11.39 o 2 2 0 297.05 271.19 5.95 o 3 2 0 8515.97 8697.14 148.48 o 4 2 0 12963.00 12997.50 221.54 o 5 2 0 7722.32 7851.73 134.37 o 6 2 0 2708.49 2761.56 58.28 o 7 2 0 122.85 117.57 6.70 o 8 2 0 144.79 158.40 9.24 o 9 2 0 218.48 219.63 14.42 o 10 2 0 119.33 115.63 13.16 o 1 3 0 9773.27 9725.22 165.52 o 2 3 0 9180.31 9320.77 159.29 o 3 3 0 5582.14 5693.23 97.68 o 4 3 0 1399.56 1460.39 26.54 o 5 3 0 140.34 150.32 5.22 o 6 3 0 1893.55 1923.73 42.20 o 7 3 0 2553.81 2583.84 55.91 o 8 3 0 1302.42 1264.64 30.27 o 9 3 0 2.52 2.76 8.00 o 10 3 0 177.83 182.77 15.02 o 0 4 0 18041.46 15209.69 365.53 o 1 4 0 20265.32 18554.66 331.58 o 2 4 0 2326.27 2372.98 41.96 o 3 4 0 119.96 126.03 4.52 o 4 4 0 1949.01 2038.18 36.69 o 5 4 0 1149.91 1151.00 26.28 o 6 4 0 337.35 353.75 11.85 o 7 4 0 691.72 699.82 18.79 o 8 4 0 998.73 1001.46 25.49 o 9 4 0 2102.55 2164.99 65.44 o 1 5 0 1434.58 1344.98 28.00 o 2 5 0 3729.07 3765.19 71.28 o 3 5 0 4112.62 4261.24 74.43 o 4 5 0 475.56 501.30 11.48 o 5 5 0 683.54 675.62 14.57 o 6 5 0 1259.36 1281.81 27.27 o 7 5 0 1235.75 1236.45 29.81 o 8 5 0 383.42 388.01 15.98 o 9 5 0 4.51 2.64 8.14 o 0 6 0 710.31 690.42 24.93 o 1 6 0 454.67 463.20 10.95 o 2 6 0 627.57 622.86 29.05 o 3 6 0 3867.42 3978.46 70.09 o 4 6 0 4130.90 4172.82 79.38 o 5 6 0 3487.29 3672.13 68.83 o 6 6 0 2358.08 2436.76 53.10 o 7 6 0 95.28 107.38 7.55 o 8 6 0 84.75 91.70 9.97 o 9 6 0 120.32 88.56 13.54 o 1 7 0 2010.64 2096.91 38.93 o 2 7 0 3012.78 3014.93 54.28 o 3 7 0 2275.91 2285.08 41.89 o 4 7 0 667.96 658.13 15.51 o 5 7 0 101.02 106.35 6.70 o 6 7 0 896.99 933.49 25.46 o 7 7 0 848.22 931.14 60.90 o 8 7 0 502.88 468.42 24.85 o 0 8 0 4508.25 4620.03 129.95 o 1 8 0 3610.20 3800.62 84.77 o 2 8 0 1271.69 1246.32 35.68 o 3 8 0 67.93 83.19 8.72 o 4 8 0 590.03 604.75 15.16 o 5 8 0 237.56 219.09 9.33 o 6 8 0 8.81 25.47 6.95 o 7 8 0 212.34 227.38 13.86 o 1 9 0 316.63 312.01 12.32 o 2 9 0 1235.69 1234.88 30.98 o 3 9 0 446.47 433.31 14.89 o 4 9 0 5.84 15.17 6.11 o 5 9 0 2.16 -2.61 5.76 o 6 9 0 414.69 411.60 17.04 o 7 9 0 391.42 422.53 26.60 o 0 10 0 347.70 327.75 19.77 o 1 10 0 2.51 10.97 11.58 o 2 10 0 164.52 147.91 10.01 o 3 10 0 753.76 748.38 23.33 o 4 10 0 1118.23 1122.24 31.43 o 5 10 0 1221.57 1227.79 34.17 o 6 10 0 391.99 426.49 19.52 o 1 11 0 142.45 140.01 10.53 o 2 11 0 486.43 497.57 18.62 o 3 11 0 532.02 505.21 18.78 o 4 11 0 112.02 109.91 10.04 o 0 12 0 809.01 835.21 37.88 o 1 12 0 463.82 431.49 18.19 o 2 12 0 251.06 245.50 14.29 o -10 1 1 184.93 174.49 14.61 o -9 1 1 406.31 391.36 13.17 o -8 1 1 429.67 430.10 13.53 o -7 1 1 403.85 396.60 12.08 o -6 1 1 807.82 753.58 24.37 o -5 1 1 774.43 782.11 17.51 o -4 1 1 1993.52 2057.19 39.30 o -3 1 1 139.74 133.68 3.59 o -2 1 1 11.13 11.15 1.75 o -1 1 1 2079.08 2218.37 40.34 o 0 1 1 7781.58 7126.31 110.50 o 1 1 1 146.74 135.03 3.37 o 2 1 1 5223.02 5245.20 89.83 o 3 1 1 6079.95 6219.88 112.39 o 4 1 1 3500.78 3677.38 63.49 o 5 1 1 1698.90 1623.37 35.28 o 6 1 1 1006.68 1055.67 21.92 o 7 1 1 64.63 81.34 5.35 o 8 1 1 513.78 475.74 19.98 o 9 1 1 51.95 55.65 10.10 o 10 1 1 10.25 8.00 9.45 o -10 2 1 2.63 4.12 9.18 o -9 2 1 21.29 20.60 5.55 o -8 2 1 355.66 355.15 12.00 o -7 2 1 23.20 22.80 4.79 o -6 2 1 196.51 200.78 7.90 o -5 2 1 14.62 19.03 2.38 o -4 2 1 34.02 37.10 2.60 o -3 2 1 736.19 757.98 14.15 o -2 2 1 14.46 13.89 1.71 o -1 2 1 6778.10 6874.97 124.11 o 0 2 1 1599.70 1710.35 28.99 o 1 2 1 15.73 23.40 3.56 o 2 2 1 311.88 344.23 7.09 o 3 2 1 51.52 73.34 7.57 o 4 2 1 769.70 807.10 16.31 o 5 2 1 190.72 185.86 5.70 o 6 2 1 27.99 28.83 3.82 o 7 2 1 351.27 316.92 10.48 o 8 2 1 9.57 6.12 7.21 o 9 2 1 0.17 5.59 8.17 o 10 2 1 30.32 25.07 10.34 o -10 3 1 506.76 509.14 23.31 o -9 3 1 789.54 767.83 21.20 o -8 3 1 501.80 478.98 14.78 o -7 3 1 994.98 994.22 24.32 o -6 3 1 1.34 5.26 4.32 o -5 3 1 83.00 82.00 4.05 o -4 3 1 92.68 93.43 4.17 o -3 3 1 65.57 59.04 2.99 o -2 3 1 194.26 183.48 4.79 o -1 3 1 9851.65 9235.08 157.64 o 0 3 1 2815.44 3015.35 49.92 o 1 3 1 7332.67 7308.43 125.15 o 2 3 1 3491.17 3602.21 62.52 o 3 3 1 1977.26 2062.23 36.61 o 4 3 1 320.45 342.57 8.13 o 5 3 1 548.19 558.02 12.02 o 6 3 1 41.65 48.85 4.50 o 7 3 1 517.54 507.90 14.49 o 8 3 1 411.11 391.23 26.44 o 9 3 1 466.15 429.65 20.50 o -9 4 1 2.20 -0.77 6.58 o -8 4 1 62.96 72.64 6.90 o -7 4 1 111.63 105.97 7.06 o -6 4 1 151.34 138.38 7.11 o -5 4 1 126.85 127.27 5.69 o -4 4 1 620.84 614.24 12.83 o -3 4 1 1334.56 1390.18 25.54 o -2 4 1 202.06 160.30 6.87 o -1 4 1 21.77 29.81 2.23 o 0 4 1 29.36 33.33 3.74 o 1 4 1 832.73 800.69 15.33 o 2 4 1 1509.66 1563.38 28.21 o 3 4 1 1156.18 1156.87 21.67 o 4 4 1 31.23 24.28 3.34 o 5 4 1 276.49 279.17 8.34 o 6 4 1 457.31 454.88 12.18 o 7 4 1 107.77 104.35 6.83 o 8 4 1 141.35 140.94 11.70 o 9 4 1 17.90 23.75 9.07 o -9 5 1 0.53 5.11 6.93 o -8 5 1 34.95 28.14 5.92 o -7 5 1 579.99 575.86 16.69 o -6 5 1 1383.71 1399.29 31.01 o -5 5 1 1660.73 1649.83 32.32 o -4 5 1 2692.43 2653.85 47.32 o -3 5 1 1388.87 1406.02 26.16 o -2 5 1 347.82 336.19 8.17 o -1 5 1 1.46 2.11 2.31 o 0 5 1 24.84 29.15 3.49 o 1 5 1 99.87 101.45 4.45 o 2 5 1 2124.93 2202.42 45.49 o 3 5 1 2888.45 2940.23 56.51 o 4 5 1 3012.55 3097.52 54.87 o 5 5 1 2923.49 2890.16 51.63 o 6 5 1 1305.44 1311.70 27.97 o 7 5 1 166.18 164.63 12.89 o 8 5 1 0.09 2.68 7.20 o 9 5 1 2.14 -4.69 8.22 o -9 6 1 42.83 31.31 11.26 o -8 6 1 226.54 220.25 13.25 o -7 6 1 723.21 730.95 21.81 o -6 6 1 668.53 659.95 17.38 o -5 6 1 7.25 10.26 3.46 o -4 6 1 107.66 112.21 5.69 o -3 6 1 596.09 533.56 14.65 o -2 6 1 2919.94 2953.95 55.51 o -1 6 1 1135.78 1090.67 32.05 o 0 6 1 0.64 6.70 3.42 o 1 6 1 479.14 457.57 14.49 o 2 6 1 1102.26 1053.61 22.45 o 3 6 1 945.43 958.45 19.20 o 4 6 1 150.54 152.45 7.09 o 5 6 1 6.39 2.79 3.66 o 6 6 1 367.94 371.02 11.33 o 7 6 1 401.56 370.34 15.19 o 8 6 1 155.95 144.60 11.89 o -8 7 1 690.39 708.51 35.39 o -7 7 1 170.70 186.59 13.93 o -6 7 1 89.56 84.93 7.65 o -5 7 1 473.17 455.17 13.31 o -4 7 1 151.09 151.49 7.38 o -3 7 1 135.21 142.38 6.54 o -2 7 1 1548.39 1464.42 51.01 o -1 7 1 2525.56 2462.39 47.70 o 0 7 1 5451.48 5410.72 127.41 o 1 7 1 2930.51 3029.31 57.85 o 2 7 1 2150.37 2158.52 39.77 o 3 7 1 64.77 71.69 5.07 o 4 7 1 229.47 243.64 7.95 o 5 7 1 38.37 40.57 4.98 o 6 7 1 122.84 123.16 7.78 o 7 7 1 111.20 123.41 11.26 o 8 7 1 515.50 540.71 26.67 o -7 8 1 445.05 439.98 18.96 o -6 8 1 156.45 166.41 9.98 o -5 8 1 1.12 0.45 4.60 o -4 8 1 201.33 205.32 10.12 o -3 8 1 1236.24 1210.95 27.74 o -2 8 1 1379.19 1342.45 30.57 o -1 8 1 158.87 149.19 10.22 o 0 8 1 29.24 24.19 5.31 o 1 8 1 1071.01 1066.21 36.62 o 2 8 1 2092.91 2134.06 44.98 o 3 8 1 700.30 712.13 18.17 o 4 8 1 62.86 79.21 6.54 o 5 8 1 44.19 42.31 5.87 o 6 8 1 811.62 831.69 27.93 o 7 8 1 563.93 608.97 34.06 o -7 9 1 263.51 305.03 18.41 o -6 9 1 861.19 936.15 44.43 o -5 9 1 1787.73 1814.38 42.81 o -4 9 1 1635.97 1645.77 39.32 o -3 9 1 1235.65 1192.43 30.17 o -2 9 1 95.19 85.00 10.58 o -1 9 1 158.25 162.45 10.66 o 0 9 1 684.82 659.72 19.10 o 1 9 1 18.92 24.30 6.19 o 2 9 1 272.99 274.33 11.12 o 3 9 1 1272.07 1269.96 31.10 o 4 9 1 1748.87 1781.50 45.35 o 5 9 1 2154.75 2188.57 50.39 o 6 9 1 745.29 778.14 29.59 o 7 9 1 117.64 122.70 18.16 o -6 10 1 523.14 545.84 24.76 o -5 10 1 157.49 171.81 12.24 o -4 10 1 354.77 339.12 13.79 o -3 10 1 856.90 802.85 22.97 o -2 10 1 1348.50 1310.87 33.35 o -1 10 1 522.78 499.44 20.88 o 0 10 1 22.60 21.39 6.85 o 1 10 1 379.89 391.83 15.82 o 2 10 1 875.31 869.02 25.96 o 3 10 1 1325.91 1309.51 38.49 o 4 10 1 96.44 92.54 9.11 o 5 10 1 86.43 103.15 9.39 o 6 10 1 223.42 229.48 28.38 o -4 11 1 156.50 164.67 11.21 o -3 11 1 1.14 1.52 6.76 o -2 11 1 573.28 522.48 19.14 o -1 11 1 1819.41 1784.88 46.60 o 0 11 1 2009.05 1954.91 50.40 o 1 11 1 1702.49 1674.05 44.26 o 2 11 1 348.39 357.90 17.61 o 3 11 1 25.65 24.80 7.72 o 4 11 1 131.98 127.84 10.89 o -2 12 1 601.53 581.65 21.16 o -1 12 1 366.13 395.27 17.39 o 0 12 1 52.69 53.73 9.42 o 1 12 1 687.11 709.68 24.14 o 2 12 1 813.22 812.50 26.61 o -10 0 2 1282.85 1317.14 57.42 o -9 0 2 3161.46 3150.86 97.20 o -8 0 2 2261.64 2314.29 71.94 o -7 0 2 439.43 434.34 18.44 o -6 0 2 112.07 112.01 8.65 o -5 0 2 290.61 294.22 13.29 o -4 0 2 1821.60 1881.39 56.53 o -3 0 2 20.39 20.07 3.87 o -2 0 2 2096.53 2179.58 53.56 o -1 0 2 24401.56 20245.18 484.40 o 0 0 2 17273.57 14576.47 378.53 o 1 0 2 9574.29 9526.38 273.09 o 2 0 2 942.17 993.26 30.63 o 3 0 2 87.79 97.53 4.24 o 4 0 2 1620.51 1654.00 41.64 o 5 0 2 371.50 388.28 12.60 o 6 0 2 44.70 43.93 4.51 o 7 0 2 1530.77 1484.31 64.40 o 8 0 2 3027.61 2961.76 120.95 o 9 0 2 1968.49 1938.27 84.56 o 10 0 2 548.10 595.67 55.02 o -10 1 2 120.22 135.89 8.79 o -9 1 2 173.51 153.64 8.64 o -8 1 2 740.65 722.78 19.59 o -7 1 2 3268.88 3204.34 68.06 o -6 1 2 1990.06 1921.18 41.78 o -5 1 2 110.55 113.53 5.83 o -4 1 2 2925.24 3037.76 57.37 o -3 1 2 6968.11 6908.41 118.38 o -2 1 2 14624.38 13765.37 269.13 o -1 1 2 1047.14 1177.73 21.03 o 0 1 2 211.02 215.07 7.78 o 1 1 2 8442.31 8304.40 141.11 o 2 1 2 11383.56 10939.94 185.80 o 3 1 2 8119.88 8209.77 140.18 o 4 1 2 99.68 96.40 4.22 o 5 1 2 273.56 258.63 8.64 o 6 1 2 3392.94 3526.18 61.86 o 7 1 2 1674.10 1647.82 49.75 o 8 1 2 889.65 859.86 30.33 o 9 1 2 0.76 2.93 8.23 o -10 2 2 121.78 149.97 13.81 o -9 2 2 223.02 226.33 10.32 o -8 2 2 4.68 9.17 4.91 o -7 2 2 975.93 935.28 22.96 o -6 2 2 4227.79 4139.36 86.18 o -5 2 2 14389.13 13390.59 247.55 o -4 2 2 11519.81 11609.17 197.70 o -3 2 2 2559.70 2515.35 44.02 o -2 2 2 124.81 135.39 4.62 o -1 2 2 1401.89 1491.25 27.52 o 0 2 2 13359.91 12902.39 252.49 o 1 2 2 1777.50 1874.79 32.98 o 2 2 2 631.88 624.82 11.95 o 3 2 2 8010.06 8149.54 139.21 o 4 2 2 13881.01 13651.49 232.66 o 5 2 2 10630.94 10601.88 181.29 o 6 2 2 2137.62 2225.88 43.52 o 7 2 2 531.20 482.78 19.52 o 8 2 2 67.15 64.83 9.51 o 9 2 2 385.04 374.19 19.06 o -10 3 2 190.85 199.65 12.54 o -9 3 2 52.20 45.36 6.56 o -8 3 2 1198.76 1159.06 28.34 o -7 3 2 2340.16 2331.94 50.76 o -6 3 2 1264.02 1271.07 29.29 o -5 3 2 151.77 139.97 5.75 o -4 3 2 408.28 395.36 8.86 o -3 3 2 5048.47 4953.89 85.56 o -2 3 2 9081.04 8976.25 153.71 o -1 3 2 3311.59 3336.67 65.42 o 0 3 2 856.65 931.03 15.46 o 1 3 2 4442.70 4539.40 78.29 o 2 3 2 5086.21 5108.31 88.11 o 3 3 2 3080.54 3183.01 60.18 o 4 3 2 658.07 684.51 13.92 o 5 3 2 613.05 618.96 13.18 o 6 3 2 1961.09 1955.94 39.13 o 7 3 2 2578.94 2601.89 75.10 o 8 3 2 279.62 296.17 16.10 o 9 3 2 7.72 8.39 8.76 o -9 4 2 1505.71 1513.88 36.67 o -8 4 2 1731.91 1753.55 40.19 o -7 4 2 688.76 684.61 18.56 o -6 4 2 182.44 172.84 11.74 o -5 4 2 665.20 692.81 14.40 o -4 4 2 379.61 340.81 9.37 o -3 4 2 112.81 104.55 4.08 o -2 4 2 4203.88 4140.58 71.86 o -1 4 2 10160.61 9769.17 187.01 o 0 4 2 9537.28 9490.83 176.20 o 1 4 2 9127.67 8950.92 153.02 o 2 4 2 2290.55 2366.14 42.04 o 3 4 2 432.48 479.77 15.03 o 4 4 2 374.08 363.43 9.62 o 5 4 2 422.72 397.93 9.98 o 6 4 2 2.71 -0.27 3.88 o 7 4 2 960.94 956.04 32.20 o 8 4 2 1901.68 1960.05 59.64 o 9 4 2 1256.41 1234.74 48.40 o -9 5 2 10.76 7.39 7.68 o -8 5 2 1032.92 1080.93 40.43 o -7 5 2 858.03 873.02 22.29 o -6 5 2 1698.76 1681.81 37.63 o -5 5 2 28.62 37.41 3.79 o -4 5 2 2025.50 1986.33 36.22 o -3 5 2 6521.86 6425.24 111.28 o -2 5 2 1934.07 1805.60 35.47 o -1 5 2 3643.74 3593.30 83.62 o 0 5 2 206.01 221.53 8.01 o 1 5 2 3126.77 3100.04 54.72 o 2 5 2 7184.52 7166.88 123.65 o 3 5 2 3399.64 3419.26 60.42 o 4 5 2 709.02 718.40 15.15 o 5 5 2 1052.98 1053.50 23.12 o 6 5 2 858.41 827.36 26.02 o 7 5 2 1235.22 1186.82 38.41 o 8 5 2 580.60 540.44 22.47 o 9 5 2 26.63 26.90 9.74 o -9 6 2 178.30 169.60 13.29 o -8 6 2 7.09 11.03 8.10 o -7 6 2 447.60 443.95 17.96 o -6 6 2 2751.20 2730.97 70.95 o -5 6 2 3687.70 3738.47 74.66 o -4 6 2 5386.60 5349.60 105.40 o -3 6 2 2122.18 2131.88 44.18 o -2 6 2 144.30 126.91 10.14 o -1 6 2 1926.42 1855.73 43.35 o 0 6 2 1212.53 1164.56 26.98 o 1 6 2 385.94 378.94 12.50 o 2 6 2 1072.97 1058.43 22.20 o 3 6 2 2412.98 2474.20 44.79 o 4 6 2 5550.03 5650.94 98.69 o 5 6 2 4336.22 4564.43 80.02 o 6 6 2 2037.78 2050.87 42.21 o 7 6 2 22.40 17.47 7.65 o 8 6 2 17.18 14.40 8.34 o -8 7 2 380.14 412.97 19.35 o -7 7 2 816.13 824.77 27.42 o -6 7 2 828.23 886.14 28.28 o -5 7 2 23.52 36.01 5.02 o -4 7 2 91.78 91.08 9.90 o -3 7 2 1618.66 1539.40 33.49 o -2 7 2 2138.96 1939.73 53.90 o -1 7 2 751.82 734.71 22.50 o 0 7 2 83.23 90.02 7.74 o 1 7 2 731.94 714.48 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-2 3 10 499.20 513.72 20.71 o -1 3 10 48.95 53.11 9.03 o 0 3 10 291.12 285.99 21.82 o 1 3 10 767.34 804.13 28.40 o 2 3 10 711.89 701.63 26.58 o 3 3 10 114.17 115.50 12.57 o -4 4 10 15.58 6.36 7.35 o -3 4 10 102.92 121.10 13.62 o -2 4 10 1004.28 1031.32 33.05 o -1 4 10 1578.08 1611.81 47.31 o 0 4 10 1152.09 1125.38 35.89 o 1 4 10 435.32 455.77 34.38 o 2 4 10 20.67 20.32 9.10 o -3 5 10 739.46 834.57 49.10 o -2 5 10 208.52 229.00 14.45 o -1 5 10 0.09 5.85 8.48 o 0 5 10 387.40 382.20 24.29 o 1 5 10 556.27 552.43 22.81 o -3 1 11 57.61 24.30 24.43 o -2 1 11 40.43 44.25 14.64 o -1 1 11 43.45 38.08 10.91 o 0 1 11 37.97 31.05 10.76 o 1 1 11 73.14 68.41 12.57 o -2 2 11 16.56 11.10 9.91 o -1 2 11 1.74 -4.75 9.09 o 0 2 11 14.37 17.33 11.77 o