#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:12:20 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180981 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/61/2206175.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206175_Fobs loop_ _publ_author_name 'Zhang, Zhi-Gang' 'Sun, Yuan-Yuan' 'Jiang, Xiao-Ming' _publ_section_title ; Acetonitrile[2-(3,5-dimethylpyrazol-1-yl)-1,3-benzothiazole]dinitratocobalt(II) ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1307 _journal_page_last m1309 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 84.279 _cell_angle_beta 86.952 _cell_angle_gamma 84.890 _cell_length_a 9.4069 _cell_length_b 10.7765 _cell_length_c 18.1740 _exptl_crystal_F_000 924.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file dn6222Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p055p in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 262.75 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2.36 46.46 2.67 o 2 0 0 33181.30 31465.45 304.69 o 3 0 0 54.12 65.70 7.06 o 4 0 0 103.44 127.12 9.99 o 6 0 0 871.36 794.09 29.66 o 7 0 0 22.91 47.67 13.47 o 8 0 0 166.68 225.97 56.48 o 9 0 0 141.33 157.25 26.26 o 10 0 0 479.17 382.59 33.16 o 11 0 0 110.45 147.16 36.27 o -11 1 0 163.93 235.25 50.78 o -10 1 0 187.10 212.45 43.53 o -9 1 0 1492.19 1491.30 99.49 o -7 1 0 450.55 389.09 28.15 o -6 1 0 31.69 48.22 11.72 o -5 1 0 2882.56 2693.75 52.09 o -4 1 0 145.95 151.28 11.03 o -3 1 0 47513.45 45868.26 304.69 o -2 1 0 64.31 110.78 10.99 o -1 1 0 16852.86 16988.80 138.87 o 0 1 0 370.01 357.54 9.33 o 1 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