#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2206179.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206179_Fobs loop_ _publ_author_name 'Lewis, Thomas C.' 'Tocher, Derek A.' _publ_section_title ; A low-temperature determination of triethylenediaminium dichloride dihydrate ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2202 _journal_page_last o2204 _journal_volume 61 _journal_year 2005 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.1407 _cell_length_b 8.7188 _cell_length_c 16.8945 _exptl_crystal_F_000 472.00 _reflns_d_resolution_high 0.7512 _[local]_cod_data_source_file dn6231Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' dabcodichloridedihydrate in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 97.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2921.86 3227.14 67.65 o 4 0 0 853.77 838.33 18.11 o 6 0 0 14.65 15.06 1.79 o 8 0 0 1.32 1.27 1.26 o 1 1 0 345.85 384.25 5.80 o 2 1 0 650.05 718.06 10.89 o 3 1 0 195.47 216.00 4.77 o 4 1 0 1111.11 1113.45 20.59 o 5 1 0 537.99 564.20 15.16 o 6 1 0 16.35 17.75 2.00 o 7 1 0 274.37 248.88 5.52 o 8 1 0 39.71 36.63 1.69 o 9 1 0 449.98 484.17 10.07 o 1 2 0 3697.18 3965.35 58.68 o 3 2 0 794.41 791.66 15.75 o 4 2 0 2430.49 2372.20 38.44 o 5 2 0 15.67 17.64 0.90 o 6 2 0 612.66 601.41 11.59 o 7 2 0 50.04 45.44 1.73 o 8 2 0 368.82 365.56 7.78 o 9 2 0 23.78 24.16 1.91 o 1 3 0 6946.07 6903.99 102.05 o 2 3 0 278.38 266.18 4.27 o 3 3 0 3326.22 3629.47 53.85 o 4 3 0 568.19 582.61 9.13 o 5 3 0 1241.17 1187.57 24.82 o 6 3 0 135.08 136.39 3.36 o 7 3 0 133.96 119.76 3.20 o 8 3 0 0.13 0.07 0.53 o 9 3 0 10.76 14.81 2.07 o 0 4 0 2117.15 2192.64 46.20 o 2 4 0 0.05 -0.10 0.26 o 3 4 0 223.33 228.99 4.51 o 4 4 0 214.78 209.12 4.47 o 5 4 0 1460.01 1479.34 27.21 o 6 4 0 649.75 614.57 11.87 o 7 4 0 628.37 650.59 12.70 o 8 4 0 12.61 13.54 1.46 o 1 5 0 214.89 223.84 3.70 o 2 5 0 1292.40 1368.07 20.63 o 3 5 0 319.31 325.82 5.36 o 4 5 0 1008.41 1009.01 17.29 o 5 5 0 44.88 45.38 1.60 o 6 5 0 240.44 228.15 5.07 o 7 5 0 85.21 86.94 2.61 o 8 5 0 5.06 3.46 1.04 o 0 6 0 2095.82 2244.68 58.00 o 1 6 0 1395.98 1307.59 59.94 o 2 6 0 52.44 57.93 1.78 o 3 6 0 926.66 953.29 18.00 o 4 6 0 408.92 439.22 10.03 o 5 6 0 118.17 121.01 4.52 o 6 6 0 1.15 3.63 1.35 o 7 6 0 0.22 2.44 1.27 o 1 7 0 14.62 16.80 1.70 o 2 7 0 560.24 582.16 11.44 o 3 7 0 29.91 28.74 1.33 o 4 7 0 123.97 129.29 3.77 o 5 7 0 6.39 8.36 1.13 o 6 7 0 26.22 29.60 3.31 o 7 7 0 26.88 29.34 3.61 o 0 8 0 1633.48 1611.54 54.48 o 1 8 0 1741.01 1685.23 31.34 o 2 8 0 733.62 712.99 13.93 o 3 8 0 89.15 84.41 2.66 o 4 8 0 238.06 242.16 8.35 o 5 8 0 2.43 1.86 0.76 o 6 8 0 4.37 3.73 1.61 o 1 9 0 6.06 8.33 0.98 o 2 9 0 0.32 0.63 0.67 o 3 9 0 129.79 141.76 3.77 o 4 9 0 258.29 265.74 6.92 o 5 9 0 1.32 2.05 1.68 o 6 9 0 122.64 158.33 9.87 o 0 10 0 95.08 94.17 5.48 o 1 10 0 63.98 69.53 2.59 o 2 10 0 469.51 468.15 9.87 o 3 10 0 36.89 39.89 1.91 o 4 10 0 336.23 361.96 9.12 o 1 11 0 311.30 333.64 9.99 o 2 11 0 100.32 105.62 3.72 o 3 11 0 195.29 200.51 8.88 o 1 0 1 1396.13 1346.21 21.64 o 2 0 1 3763.58 3790.42 56.01 o 3 0 1 568.05 580.72 8.92 o 4 0 1 176.28 154.82 2.72 o 5 0 1 559.43 551.49 10.53 o 6 0 1 96.71 102.71 2.74 o 7 0 1 231.55 205.53 4.75 o 8 0 1 12.94 12.54 1.12 o 9 0 1 15.16 19.62 1.77 o -9 1 1 389.66 402.65 8.66 o -8 1 1 180.70 170.68 4.30 o -7 1 1 342.60 330.59 6.88 o -6 1 1 338.08 326.06 6.71 o -5 1 1 1118.35 1116.41 20.52 o -4 1 1 632.34 659.31 11.12 o -3 1 1 3039.83 3021.64 41.50 o -2 1 1 781.43 781.99 11.73 o -1 1 1 1277.73 1247.71 18.99 o 0 1 1 153.41 153.85 3.26 o 1 1 1 1315.92 1302.30 19.00 o 2 1 1 774.20 774.84 12.73 o 3 1 1 2998.97 2955.25 48.23 o 4 1 1 642.63 660.28 9.47 o 5 1 1 1154.95 1108.62 18.38 o 6 1 1 330.68 323.59 6.69 o 7 1 1 325.83 319.38 6.85 o 8 1 1 176.60 173.97 4.31 o 9 1 1 393.88 407.40 10.20 o -9 2 1 18.46 22.11 1.52 o -8 2 1 61.28 61.83 2.20 o -7 2 1 155.74 150.24 3.80 o -6 2 1 708.52 666.52 12.70 o -5 2 1 106.22 91.34 3.45 o -4 2 1 371.00 382.77 6.06 o -3 2 1 1004.94 1092.44 17.31 o -2 2 1 843.46 892.99 20.50 o -1 2 1 4491.01 4698.59 112.74 o 0 2 1 41.27 42.01 1.00 o 1 2 1 4510.06 4745.64 85.56 o 2 2 1 853.54 931.63 13.72 o 3 2 1 973.75 1012.22 15.83 o 4 2 1 360.82 367.43 6.55 o 5 2 1 110.26 96.06 2.22 o 6 2 1 699.74 660.68 12.69 o 7 2 1 158.47 157.57 4.05 o 8 2 1 57.06 60.50 2.17 o 9 2 1 18.78 21.32 1.85 o -9 3 1 63.33 70.61 5.23 o -8 3 1 339.06 322.21 7.07 o -7 3 1 15.91 14.81 1.12 o -6 3 1 107.14 97.62 2.99 o -5 3 1 118.36 121.61 3.14 o -4 3 1 966.35 998.69 16.06 o -3 3 1 704.80 725.89 10.94 o -2 3 1 1192.37 1237.47 18.46 o -1 3 1 3670.96 3925.58 74.04 o 0 3 1 5387.37 5299.68 115.04 o 1 3 1 3776.65 3946.79 58.15 o 2 3 1 1173.18 1222.48 20.52 o 3 3 1 705.89 701.86 12.61 o 4 3 1 930.99 932.22 13.61 o 5 3 1 121.42 125.71 3.84 o 6 3 1 100.68 96.62 2.62 o 7 3 1 16.56 16.40 1.13 o 8 3 1 342.26 326.46 8.39 o 9 3 1 62.89 73.02 3.78 o -8 4 1 35.33 38.96 1.77 o -7 4 1 179.39 177.17 4.31 o -6 4 1 279.74 265.01 6.62 o -5 4 1 22.63 22.32 1.12 o -4 4 1 319.97 344.88 6.94 o -3 4 1 245.83 256.52 4.86 o -2 4 1 752.14 809.07 14.67 o -1 4 1 579.07 630.43 9.61 o 1 4 1 585.63 630.60 9.62 o 2 4 1 739.69 789.26 12.19 o 3 4 1 246.99 253.89 6.58 o 4 4 1 320.18 352.14 5.75 o 5 4 1 21.88 22.79 1.04 o 6 4 1 283.52 279.92 5.85 o 7 4 1 180.68 180.43 4.30 o 8 4 1 35.34 34.90 2.12 o -8 5 1 135.64 138.89 4.50 o -7 5 1 21.99 23.37 1.35 o -6 5 1 166.89 159.89 4.31 o -5 5 1 55.23 58.29 1.88 o -4 5 1 549.71 553.21 9.37 o -3 5 1 550.20 543.93 8.44 o -2 5 1 2127.10 2199.89 32.08 o -1 5 1 825.58 924.26 15.10 o 0 5 1 4296.60 4474.41 72.44 o 1 5 1 807.64 922.13 15.37 o 2 5 1 2089.25 2101.48 32.09 o 3 5 1 564.56 528.63 8.46 o 4 5 1 556.73 551.49 8.94 o 5 5 1 60.22 61.82 1.57 o 6 5 1 168.45 153.81 3.74 o 7 5 1 24.71 26.61 1.76 o 8 5 1 135.56 135.25 5.64 o -7 6 1 249.01 252.81 6.48 o -6 6 1 14.36 14.45 2.80 o -5 6 1 358.27 344.33 7.14 o -4 6 1 145.86 141.03 3.29 o -3 6 1 102.85 99.98 2.28 o -2 6 1 312.03 310.65 6.44 o -1 6 1 302.94 286.87 7.16 o 0 6 1 1237.52 1205.86 23.60 o 1 6 1 312.02 297.60 7.14 o 2 6 1 318.43 320.33 6.48 o 3 6 1 103.22 100.03 3.76 o 4 6 1 139.56 134.72 3.39 o 5 6 1 361.43 346.88 8.30 o 6 6 1 15.61 14.12 3.59 o 7 6 1 249.44 253.27 11.80 o -7 7 1 28.80 37.03 3.93 o -6 7 1 483.43 506.46 20.58 o -5 7 1 391.67 386.29 9.18 o -4 7 1 591.61 583.39 13.26 o -3 7 1 113.69 104.11 2.73 o -2 7 1 174.31 180.12 4.14 o -1 7 1 240.09 233.07 5.10 o 0 7 1 6.72 7.35 0.77 o 1 7 1 244.26 237.88 5.48 o 2 7 1 174.72 179.99 4.72 o 3 7 1 103.25 94.29 2.70 o 4 7 1 584.21 599.71 13.34 o 5 7 1 391.50 381.71 9.21 o 6 7 1 481.33 513.03 11.99 o 7 7 1 29.68 32.15 3.74 o -6 8 1 23.26 19.74 2.96 o -5 8 1 71.76 74.01 3.81 o -4 8 1 340.85 329.78 8.14 o -3 8 1 190.65 190.36 5.28 o -2 8 1 124.69 137.83 3.78 o -1 8 1 333.15 316.85 6.74 o 0 8 1 116.04 108.48 2.94 o 1 8 1 327.32 316.52 6.76 o 2 8 1 124.80 135.85 3.49 o 3 8 1 184.13 179.30 4.43 o 4 8 1 345.66 337.38 8.21 o 5 8 1 71.32 74.86 2.78 o 6 8 1 19.65 18.01 1.49 o -5 9 1 201.69 219.78 7.98 o -4 9 1 177.73 166.15 5.30 o -3 9 1 20.34 20.89 1.36 o -2 9 1 232.63 225.56 5.24 o -1 9 1 26.12 28.82 1.49 o 0 9 1 88.96 97.83 2.87 o 1 9 1 24.17 26.41 1.48 o 2 9 1 229.39 221.50 5.23 o 3 9 1 21.12 21.02 1.71 o 4 9 1 180.11 180.12 5.03 o 5 9 1 197.27 209.40 5.92 o -4 10 1 18.35 24.79 4.52 o -3 10 1 150.19 156.74 4.70 o -2 10 1 28.99 29.50 1.69 o -1 10 1 7.38 8.60 1.10 o 0 10 1 239.73 239.05 5.67 o 1 10 1 7.66 8.92 1.08 o 2 10 1 31.49 34.92 1.78 o 3 10 1 147.47 157.03 5.67 o 4 10 1 19.88 23.13 1.75 o -2 11 1 5.53 6.47 1.46 o -1 11 1 456.40 469.26 9.99 o 0 11 1 19.32 21.59 2.11 o 1 11 1 456.36 452.80 9.93 o 2 11 1 4.64 5.15 1.07 o 3 11 1 22.69 24.16 2.60 o 0 0 2 306.24 322.98 8.48 o 1 0 2 311.92 283.79 4.82 o 2 0 2 1485.06 1602.35 25.86 o 3 0 2 2354.36 2425.55 36.03 o 4 0 2 815.96 751.93 11.52 o 5 0 2 4.32 4.28 0.52 o 6 0 2 1810.93 1805.51 32.72 o 7 0 2 0.06 1.56 0.61 o 8 0 2 207.65 205.40 4.92 o 9 0 2 364.91 357.64 9.22 o -9 1 2 31.18 33.35 3.02 o -8 1 2 69.36 75.01 2.47 o -7 1 2 397.10 387.98 7.95 o -6 1 2 41.78 44.63 1.82 o -5 1 2 343.30 311.06 9.03 o -4 1 2 762.17 806.29 13.37 o -3 1 2 2326.35 2346.29 38.61 o -2 1 2 1288.31 1330.10 20.13 o -1 1 2 1030.73 1115.84 31.13 o 0 1 2 843.71 743.40 12.15 o 1 1 2 975.88 1081.02 17.70 o 2 1 2 1346.75 1364.85 21.81 o 3 1 2 2333.67 2454.95 38.61 o 4 1 2 759.75 796.57 12.27 o 5 1 2 349.49 339.84 5.93 o 6 1 2 40.68 44.43 2.04 o 7 1 2 396.64 381.41 7.91 o 8 1 2 69.75 72.44 2.91 o 9 1 2 28.53 31.70 2.14 o -9 2 2 21.73 26.18 2.34 o -8 2 2 422.27 418.98 8.78 o -7 2 2 204.91 201.43 4.78 o -6 2 2 695.50 681.29 14.67 o -5 2 2 265.66 240.18 5.05 o -4 2 2 991.80 972.36 16.10 o -3 2 2 82.35 98.29 1.64 o -2 2 2 2062.37 2166.39 32.06 o -1 2 2 958.76 1073.63 14.58 o 0 2 2 4738.51 4747.81 121.09 o 1 2 2 955.78 1053.90 17.67 o 2 2 2 2097.75 2148.28 32.07 o 3 2 2 69.23 82.84 1.87 o 4 2 2 970.41 955.58 14.63 o 5 2 2 265.31 238.85 4.54 o 6 2 2 696.21 668.46 11.59 o 7 2 2 215.71 215.06 4.82 o 8 2 2 429.20 424.17 10.36 o 9 2 2 23.06 24.95 2.01 o -9 3 2 155.07 174.56 6.08 o -8 3 2 418.67 412.99 8.65 o -7 3 2 138.03 129.14 3.39 o -6 3 2 278.88 268.37 6.55 o -5 3 2 166.80 155.86 3.23 o -4 3 2 1026.29 1057.52 19.49 o -3 3 2 37.00 32.91 1.00 o -2 3 2 48.76 50.14 1.04 o -1 3 2 2572.06 2585.22 42.20 o 0 3 2 1003.84 1002.98 16.43 o 1 3 2 2550.11 2621.72 35.80 o 2 3 2 46.55 47.38 1.09 o 3 3 2 39.23 35.42 1.00 o 4 3 2 1039.85 1058.94 16.04 o 5 3 2 162.44 153.23 3.63 o 6 3 2 280.70 271.06 5.20 o 7 3 2 137.25 127.47 4.04 o 8 3 2 421.59 410.03 10.19 o 9 3 2 153.97 167.64 9.49 o -8 4 2 34.64 36.23 1.70 o -7 4 2 10.50 8.33 0.90 o -6 4 2 117.82 109.60 3.28 o -5 4 2 17.20 15.38 0.88 o -4 4 2 408.27 387.59 11.07 o -3 4 2 852.67 854.36 18.53 o -2 4 2 329.09 336.27 5.50 o -1 4 2 459.05 459.52 7.96 o 0 4 2 549.88 570.47 9.57 o 1 4 2 471.94 477.64 6.72 o 2 4 2 303.31 296.21 4.63 o 3 4 2 879.79 855.15 13.29 o 4 4 2 421.49 405.81 6.03 o 5 4 2 14.77 14.80 0.86 o 6 4 2 111.65 110.55 2.60 o 7 4 2 11.25 9.19 1.18 o 8 4 2 33.40 33.87 2.09 o -8 5 2 58.37 61.38 2.26 o -7 5 2 504.20 493.27 9.97 o -6 5 2 421.05 386.84 8.91 o -5 5 2 725.79 704.17 13.42 o -4 5 2 42.07 45.73 1.29 o -3 5 2 142.48 125.17 2.65 o -2 5 2 90.66 91.86 2.07 o -1 5 2 57.63 70.88 1.57 o 0 5 2 279.82 239.25 4.32 o 1 5 2 56.02 68.02 2.31 o 2 5 2 98.85 102.10 1.76 o 3 5 2 146.63 131.59 3.71 o 4 5 2 41.17 42.21 1.30 o 5 5 2 721.32 699.57 11.04 o 6 5 2 411.07 378.71 8.04 o 7 5 2 506.65 492.69 14.33 o 8 5 2 63.34 65.85 3.42 o -8 6 2 49.72 47.22 4.08 o -7 6 2 211.24 225.24 6.13 o -6 6 2 89.02 87.40 4.51 o -5 6 2 419.03 413.20 8.34 o -4 6 2 187.40 179.13 4.05 o -3 6 2 408.85 403.40 9.82 o -2 6 2 310.29 299.72 5.36 o -1 6 2 364.31 352.61 6.29 o 0 6 2 21.95 18.21 0.95 o 1 6 2 374.57 363.07 13.76 o 2 6 2 303.50 289.46 12.43 o 3 6 2 420.98 400.77 12.08 o 4 6 2 187.35 185.56 4.25 o 5 6 2 425.09 415.10 9.70 o 6 6 2 87.00 69.69 5.03 o 7 6 2 205.17 195.45 10.23 o -7 7 2 67.31 68.27 5.20 o -6 7 2 345.92 315.09 14.32 o -5 7 2 3.96 3.67 2.11 o -4 7 2 311.31 309.69 12.35 o -3 7 2 244.02 256.53 5.57 o -2 7 2 8.33 10.73 1.01 o -1 7 2 372.62 384.19 7.64 o 0 7 2 60.13 62.06 1.96 o 1 7 2 349.32 365.74 7.64 o 2 7 2 6.83 9.74 0.90 o 3 7 2 239.86 256.07 5.64 o 4 7 2 322.76 305.90 7.98 o 5 7 2 3.75 3.74 0.84 o 6 7 2 337.75 340.11 8.38 o 7 7 2 70.61 77.08 4.98 o -6 8 2 58.47 54.90 4.51 o -5 8 2 147.14 152.97 7.12 o -4 8 2 313.28 318.14 7.81 o -3 8 2 119.14 113.97 3.10 o -2 8 2 276.30 270.20 5.86 o -1 8 2 2.32 1.80 1.05 o 0 8 2 0.18 0.63 0.56 o 1 8 2 1.32 1.26 0.64 o 2 8 2 266.81 263.05 5.88 o 3 8 2 118.66 118.19 3.19 o 4 8 2 314.64 318.47 7.89 o 5 8 2 151.66 158.67 4.65 o 6 8 2 59.52 61.41 4.18 o -5 9 2 161.16 154.03 7.44 o -4 9 2 9.35 11.32 1.67 o -3 9 2 80.44 87.04 2.97 o -2 9 2 133.86 142.12 3.71 o -1 9 2 4.84 6.65 0.92 o 0 9 2 571.32 566.52 11.41 o 1 9 2 4.89 6.54 0.88 o 2 9 2 134.33 136.42 3.68 o 3 9 2 77.07 81.35 2.65 o 4 9 2 9.07 10.02 1.23 o 5 9 2 161.58 161.63 4.84 o -4 10 2 124.91 140.47 9.42 o -3 10 2 60.54 62.07 3.54 o -2 10 2 391.93 408.17 11.10 o -1 10 2 31.54 30.31 1.69 o 0 10 2 177.63 181.19 4.59 o 1 10 2 31.13 33.45 1.72 o 2 10 2 400.81 391.56 8.63 o 3 10 2 59.43 61.67 2.37 o 4 10 2 130.48 138.89 4.46 o -2 11 2 27.53 37.10 4.90 o -1 11 2 38.96 46.46 2.17 o 0 11 2 165.11 174.07 4.68 o 1 11 2 39.16 43.25 2.12 o 2 11 2 25.90 30.24 2.00 o 1 0 3 7943.99 7081.95 125.46 o 2 0 3 3030.37 3004.72 44.58 o 4 0 3 793.94 808.08 14.41 o 5 0 3 1416.42 1429.60 23.53 o 6 0 3 2.20 2.72 0.61 o 7 0 3 714.68 693.85 13.40 o 8 0 3 357.91 349.63 8.85 o 9 0 3 1.44 1.93 0.95 o -9 1 3 3.31 2.54 1.06 o -8 1 3 210.51 216.66 5.98 o -7 1 3 100.13 96.67 3.93 o -6 1 3 372.63 368.53 14.29 o -5 1 3 156.66 159.37 3.31 o -4 1 3 434.30 465.52 7.49 o -3 1 3 714.54 742.36 12.25 o -2 1 3 4354.44 4440.64 66.53 o -1 1 3 4840.96 4839.53 74.95 o 0 1 3 1101.55 1188.18 26.74 o 1 1 3 4828.70 4847.44 124.58 o 2 1 3 4374.82 4563.91 66.62 o 3 1 3 703.29 735.53 12.22 o 4 1 3 446.42 486.94 8.17 o 5 1 3 161.97 165.97 3.40 o 6 1 3 370.29 353.64 9.60 o 7 1 3 102.02 94.47 2.70 o 8 1 3 210.13 206.01 5.94 o 9 1 3 3.06 1.87 0.95 o -9 2 3 141.15 155.94 7.65 o -8 2 3 70.59 67.08 2.34 o -7 2 3 200.97 191.37 5.18 o -6 2 3 520.48 501.20 11.02 o -5 2 3 713.36 696.85 13.11 o -4 2 3 324.65 313.46 5.27 o -3 2 3 573.23 568.19 8.13 o -2 2 3 3827.23 3877.27 57.62 o -1 2 3 2093.03 2254.41 30.53 o 0 2 3 17.28 25.68 1.75 o 1 2 3 2043.11 2229.58 36.98 o 2 2 3 3829.19 3916.22 57.64 o 3 2 3 565.34 558.27 9.45 o 4 2 3 340.08 329.87 5.73 o 5 2 3 712.69 686.70 11.75 o 6 2 3 521.02 486.09 8.70 o 7 2 3 202.87 199.94 4.79 o 8 2 3 75.78 70.27 2.87 o 9 2 3 137.55 138.78 5.67 o -9 3 3 103.72 117.01 6.38 o -8 3 3 235.91 236.68 5.49 o -7 3 3 398.51 391.38 9.09 o -6 3 3 525.01 504.46 11.30 o -5 3 3 428.41 420.06 8.32 o -4 3 3 92.97 99.53 2.22 o -3 3 3 448.02 456.19 7.08 o -2 3 3 1412.01 1527.32 22.23 o -1 3 3 1818.62 1966.37 29.12 o 0 3 3 52.27 55.43 1.37 o 1 3 3 1827.62 1952.14 29.15 o 2 3 3 1396.24 1506.79 25.26 o 3 3 3 441.38 441.54 7.08 o 4 3 3 94.44 97.20 1.97 o 5 3 3 440.82 419.70 7.64 o 6 3 3 531.27 506.40 8.95 o 7 3 3 394.44 379.71 8.22 o 8 3 3 230.17 230.66 6.48 o 9 3 3 103.62 112.99 7.25 o -8 4 3 2.15 2.11 0.68 o -7 4 3 107.33 107.93 3.40 o -6 4 3 206.29 207.58 4.76 o -5 4 3 1308.21 1342.49 22.22 o -4 4 3 413.97 416.00 9.21 o -3 4 3 2881.01 2936.49 42.37 o -2 4 3 2358.89 2501.41 40.83 o -1 4 3 797.49 859.63 14.35 o 1 4 3 812.38 870.66 12.14 o 2 4 3 2382.89 2512.60 34.65 o 3 4 3 2845.85 2832.96 43.51 o 4 4 3 429.63 418.04 6.82 o 5 4 3 1303.85 1314.20 21.80 o 6 4 3 209.00 210.15 4.89 o 7 4 3 106.84 106.55 3.16 o 8 4 3 1.64 1.65 0.87 o -8 5 3 82.03 91.57 2.87 o -7 5 3 154.11 156.32 4.47 o -6 5 3 812.32 772.25 14.78 o -5 5 3 29.46 30.90 1.34 o -4 5 3 360.21 340.92 7.88 o -3 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