#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/62/2206258.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206258_Fobs loop_ _publ_author_name 'Petrova, Rosica' 'Shivachev, Boris' 'Kosev, Krasimir' 'Stoyanova, Malinka' 'Angelova, Silvia' _publ_section_title ; (3RS,4RS)-3-(2-Furyl)-2-phenethyl-4-(pyrrolidin-1-ylcarbonyl)-3,4-dihydroisoquinolin-1(2H)-one ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2248 _journal_page_last o2250 _journal_volume 61 _journal_year 2005 _space_group_IT_number 29 _symmetry_space_group_name_Hall 'P 2c -2ac' _symmetry_space_group_name_H-M 'P c a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.9675 _cell_length_b 11.0663 _cell_length_c 32.7891 _exptl_crystal_F_000 1760.00 _reflns_d_resolution_high 0.8115 _[local]_cod_data_source_file ob6537Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a015 in P b c 21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 300.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-x+1/2, y, z+1/2' 'x+1/2, -y, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 333.29 307.28 21.72 o 4 0 0 1129.41 1133.63 46.47 o 6 0 0 0.76 4.44 31.52 o 8 0 0 401.96 417.73 42.50 o 10 0 0 0.46 -48.57 48.57 o 12 0 0 82.67 30.35 49.27 o 14 0 0 7.56 -56.51 64.21 o 0 1 0 12.72 9.81 11.67 o 1 1 0 13.48 4.20 13.08 o 2 1 0 7409.01 6808.09 75.42 o 3 1 0 38825.79 34383.71 198.47 o 4 1 0 37.38 19.15 22.42 o 5 1 0 450.38 414.23 40.40 o 6 1 0 70.86 28.95 29.65 o 7 1 0 66.57 60.48 25.22 o 8 1 0 65.60 27.55 44.83 o 9 1 0 110.17 103.44 33.16 o 10 1 0 214.36 278.33 39.93 o 11 1 0 669.73 721.04 69.35 o 12 1 0 15.03 98.30 38.76 o 13 1 0 180.11 136.13 60.71 o 14 1 0 87.51 146.87 51.14 o 0 2 0 11224.84 10704.24 91.76 o 1 2 0 527.61 562.96 27.55 o 2 2 0 54.13 42.73 15.64 o 3 2 0 8006.97 6802.96 97.60 o 4 2 0 695.88 660.80 41.33 o 5 2 0 7002.56 6830.28 120.48 o 6 2 0 15.69 9.34 29.65 o 7 2 0 196.99 155.51 32.69 o 8 2 0 128.24 97.14 36.43 o 9 2 0 37.95 18.21 42.26 o 10 2 0 6.19 8.17 45.30 o 11 2 0 81.51 13.78 48.57 o 12 2 0 543.81 605.69 63.74 o 13 2 0 260.24 321.99 60.94 o 14 2 0 0.20 -67.71 67.71 o 0 3 0 11.22 1.87 15.64 o 1 3 0 241.09 233.26 22.18 o 2 3 0 697.18 756.53 38.53 o 3 3 0 256.56 250.54 24.05 o 4 3 0 1.01 5.60 25.68 o 5 3 0 12.02 10.97 31.06 o 6 3 0 1193.40 1274.20 63.74 o 7 3 0 2.72 17.51 31.06 o 8 3 0 8.27 -10.04 38.76 o 9 3 0 15.29 3.74 40.40 o 10 3 0 599.33 631.61 61.64 o 11 3 0 228.44 218.79 48.10 o 12 3 0 4.83 -31.76 58.14 o 13 3 0 1.78 -17.75 66.78 o 14 3 0 69.76 38.99 50.44 o 0 4 0 3688.98 3565.98 78.22 o 1 4 0 337.07 334.60 31.29 o 2 4 0 377.50 389.24 33.39 o 3 4 0 0.15 20.78 18.21 o 4 4 0 236.87 209.21 27.32 o 5 4 0 3.99 55.81 21.48 o 6 4 0 38.96 88.96 27.09 o 7 4 0 87.38 57.44 30.59 o 8 4 0 53.87 52.07 33.16 o 9 4 0 34.37 23.82 44.60 o 10 4 0 8.57 -22.18 47.63 o 11 4 0 36.77 42.96 38.99 o 12 4 0 322.17 267.35 58.84 o 13 4 0 263.76 226.73 54.64 o 14 4 0 27.83 53.47 50.20 o 0 5 0 204.28 207.35 25.22 o 1 5 0 279.42 295.84 30.35 o 2 5 0 336.99 429.17 41.56 o 3 5 0 4649.42 4960.66 112.08 o 4 5 0 97.79 111.14 23.82 o 5 5 0 8.56 33.16 24.98 o 6 5 0 2801.81 2958.18 102.74 o 7 5 0 784.19 877.02 63.74 o 8 5 0 25.69 43.20 36.66 o 9 5 0 263.50 197.77 41.80 o 10 5 0 23.80 -9.34 51.14 o 11 5 0 8.37 5.14 52.77 o 12 5 0 13.48 0.00 59.54 o 13 5 0 3.17 4.20 52.77 o 0 6 0 16323.70 16739.22 206.88 o 1 6 0 440.51 444.11 41.80 o 2 6 0 0.21 5.14 29.89 o 3 6 0 9.85 -33.86 33.86 o 4 6 0 131.71 126.56 27.55 o 5 6 0 295.29 348.38 35.49 o 6 6 0 364.15 358.19 41.80 o 7 6 0 272.02 240.50 44.60 o 8 6 0 277.99 322.46 46.47 o 9 6 0 22.04 45.53 38.29 o 10 6 0 44.37 80.09 39.23 o 11 6 0 32.52 -16.58 53.00 o 12 6 0 48.24 -24.05 63.28 o 13 6 0 18.12 53.00 59.07 o 0 7 0 57.33 29.42 25.45 o 1 7 0 16.47 11.44 28.02 o 2 7 0 2586.00 2425.81 93.63 o 3 7 0 57.26 31.99 31.06 o 4 7 0 12.41 36.19 44.83 o 5 7 0 403.44 435.71 43.43 o 6 7 0 22.73 68.65 36.66 o 7 7 0 152.54 135.20 43.43 o 8 7 0 22.30 17.98 37.59 o 9 7 0 310.61 357.25 52.07 o 10 7 0 85.27 0.00 55.81 o 11 7 0 110.69 117.22 51.60 o 12 7 0 37.01 114.88 47.17 o 0 8 0 89.12 100.17 32.46 o 1 8 0 0.78 -43.20 43.20 o 2 8 0 0.79 27.55 31.99 o 3 8 0 37.16 -10.74 48.33 o 4 8 0 1075.75 1114.48 76.59 o 5 8 0 3391.67 3211.53 122.35 o 6 8 0 459.20 479.14 58.14 o 7 8 0 670.71 628.81 63.74 o 8 8 0 855.83 746.03 69.12 o 9 8 0 150.51 95.97 52.54 o 10 8 0 2.50 17.28 49.97 o 11 8 0 14.32 -62.34 62.34 o 0 9 0 494.83 505.29 50.90 o 1 9 0 124.94 113.71 37.59 o 2 9 0 70.69 73.79 37.36 o 3 9 0 2.90 -44.83 44.83 o 4 9 0 79.81 102.04 39.93 o 5 9 0 227.70 241.44 46.47 o 6 9 0 259.12 192.64 45.30 o 7 9 0 63.70 127.72 44.60 o 8 9 0 12.04 -63.74 63.74 o 9 9 0 58.31 -17.28 62.81 o 10 9 0 5.80 0.00 63.04 o 11 9 0 9.27 13.54 60.01 o 0 10 0 1475.64 1426.44 90.83 o 1 10 0 866.78 832.19 76.12 o 2 10 0 21.69 0.00 51.60 o 3 10 0 577.24 606.16 64.91 o 4 10 0 394.26 338.34 54.64 o 5 10 0 2.27 -35.02 48.80 o 6 10 0 87.58 52.54 57.21 o 7 10 0 106.76 133.56 48.10 o 8 10 0 3.85 35.49 57.91 o 9 10 0 67.69 75.65 44.83 o 10 10 0 7.29 27.09 61.18 o 0 11 0 53.51 29.89 42.73 o 1 11 0 42.74 50.20 58.61 o 2 11 0 846.89 793.66 67.48 o 3 11 0 79.22 107.64 47.40 o 4 11 0 141.56 153.88 52.77 o 5 11 0 60.93 5.60 64.45 o 6 11 0 272.65 291.87 58.37 o 7 11 0 61.73 106.47 53.47 o 8 11 0 165.28 164.15 60.24 o 0 12 0 94.68 56.27 62.58 o 1 12 0 100.39 116.75 46.23 o 2 12 0 10.20 -11.44 57.21 o 3 12 0 62.96 159.48 44.60 o 4 12 0 33.44 92.00 49.74 o 5 12 0 92.74 -31.06 68.18 o 6 12 0 2.62 -25.92 60.01 o 7 12 0 11.63 -20.31 67.25 o 0 13 0 96.89 63.04 52.07 o 1 13 0 67.00 -31.52 67.95 o 2 13 0 219.56 285.80 59.31 o 3 13 0 45.94 58.61 75.65 o 4 13 0 7.26 115.58 47.87 o 2 0 1 45295.76 40078.56 157.26 o 4 0 1 34.46 41.33 21.37 o 6 0 1 554.90 577.73 33.37 o 8 0 1 101.01 55.79 19.88 o 10 0 1 158.58 206.71 29.23 o 12 0 1 1010.05 1107.08 63.34 o 14 0 1 254.53 239.48 45.24 o 1 1 1 3641.54 3406.65 61.41 o 2 1 1 193.42 224.23 14.48 o 3 1 1 19008.66 19006.95 815.84 o 4 1 1 1531.21 1466.42 37.31 o 5 1 1 711.32 742.92 31.74 o 6 1 1 1660.49 1698.68 48.56 o 7 1 1 201.80 169.01 23.47 o 8 1 1 1271.19 1254.73 52.34 o 9 1 1 173.48 191.57 25.37 o 10 1 1 206.60 163.48 31.70 o 11 1 1 240.02 302.59 33.32 o 12 1 1 190.10 212.20 34.88 o 13 1 1 342.35 366.98 44.25 o 14 1 1 12.21 41.23 43.34 o 1 2 1 1900.56 1961.05 130.06 o 2 2 1 10893.09 10266.72 106.59 o 3 2 1 3859.27 3496.67 209.45 o 4 2 1 2237.19 2343.92 61.99 o 5 2 1 2148.75 2303.38 52.42 o 6 2 1 112.79 112.90 17.65 o 7 2 1 169.40 171.82 22.70 o 8 2 1 215.62 222.81 36.08 o 9 2 1 58.91 105.00 23.61 o 10 2 1 159.44 199.05 30.03 o 11 2 1 328.63 311.67 33.94 o 12 2 1 20.01 57.66 33.66 o 13 2 1 39.10 -27.85 39.63 o 14 2 1 7.83 -10.26 48.64 o 1 3 1 533.04 554.58 24.19 o 2 3 1 2516.96 2713.66 46.73 o 3 3 1 107.82 101.00 15.88 o 4 3 1 372.34 374.51 25.39 o 5 3 1 32.87 35.52 15.19 o 6 3 1 592.72 583.39 35.66 o 7 3 1 120.35 148.85 26.85 o 8 3 1 294.60 272.67 29.06 o 9 3 1 213.18 247.45 28.22 o 10 3 1 176.87 193.84 30.38 o 11 3 1 45.90 50.99 30.13 o 12 3 1 75.66 47.12 36.51 o 13 3 1 15.59 60.00 44.83 o 14 3 1 141.33 172.92 42.69 o 1 4 1 1246.90 1088.37 34.73 o 2 4 1 6690.98 6857.36 80.49 o 3 4 1 2199.61 2146.87 49.20 o 4 4 1 1119.15 1081.92 39.70 o 5 4 1 430.78 468.97 65.96 o 6 4 1 183.01 231.06 53.70 o 7 4 1 0.71 -10.24 24.85 o 8 4 1 9.28 2.83 26.70 o 9 4 1 35.95 -8.73 31.61 o 10 4 1 22.56 -22.84 37.94 o 11 4 1 35.59 22.47 34.24 o 12 4 1 17.71 4.22 64.56 o 13 4 1 52.48 34.90 44.52 o 14 4 1 87.70 53.61 41.90 o 1 5 1 311.92 336.52 30.24 o 2 5 1 419.81 479.77 29.67 o 3 5 1 1165.69 1241.68 43.09 o 4 5 1 1869.82 2260.06 144.42 o 5 5 1 303.23 381.03 26.20 o 6 5 1 170.59 157.25 22.85 o 7 5 1 477.25 476.54 38.64 o 8 5 1 368.41 372.41 57.56 o 9 5 1 261.82 234.70 31.45 o 10 5 1 193.18 200.03 32.99 o 11 5 1 12.93 82.77 53.70 o 12 5 1 5.81 -5.84 39.21 o 13 5 1 6.85 12.72 42.75 o 1 6 1 76.47 89.56 17.58 o 2 6 1 33.44 -79.59 161.58 o 3 6 1 69.74 70.89 17.99 o 4 6 1 241.84 255.29 21.96 o 5 6 1 444.41 477.32 31.85 o 6 6 1 374.33 371.74 69.00 o 7 6 1 418.41 435.67 60.59 o 8 6 1 17.81 17.65 37.59 o 9 6 1 2.10 -33.79 33.79 o 10 6 1 149.40 155.23 33.23 o 11 6 1 26.74 77.31 60.48 o 12 6 1 7.31 57.46 56.39 o 13 6 1 1.06 -41.28 47.37 o 1 7 1 6.29 -18.93 24.26 o 2 7 1 248.34 260.29 26.27 o 3 7 1 440.23 426.13 28.38 o 4 7 1 17.81 35.10 28.21 o 5 7 1 965.45 864.63 47.95 o 6 7 1 175.69 141.61 31.19 o 7 7 1 107.15 116.27 28.63 o 8 7 1 55.62 148.55 25.51 o 9 7 1 48.08 48.47 32.94 o 10 7 1 132.51 195.58 44.48 o 11 7 1 9.00 -0.47 68.88 o 12 7 1 81.72 105.25 38.30 o 1 8 1 103.12 140.36 25.17 o 2 8 1 559.09 571.16 51.72 o 3 8 1 71.00 122.21 34.91 o 4 8 1 225.49 249.31 31.10 o 5 8 1 1896.39 1804.96 70.34 o 6 8 1 122.23 154.55 45.88 o 7 8 1 242.28 223.85 33.65 o 8 8 1 252.03 251.59 39.32 o 9 8 1 97.76 56.30 36.23 o 10 8 1 12.47 53.97 34.67 o 11 8 1 8.37 11.10 47.99 o 1 9 1 178.22 189.73 29.01 o 2 9 1 149.91 211.41 68.53 o 3 9 1 82.09 11.30 37.24 o 4 9 1 481.92 438.48 37.30 o 5 9 1 672.44 663.36 51.25 o 6 9 1 49.13 77.47 33.86 o 7 9 1 66.21 51.94 31.17 o 8 9 1 94.85 154.76 31.91 o 9 9 1 4.27 36.89 35.47 o 10 9 1 1.84 -36.58 44.79 o 11 9 1 12.15 38.29 45.04 o 1 10 1 188.47 152.20 31.69 o 2 10 1 1134.60 1112.53 162.63 o 3 10 1 892.28 923.86 72.03 o 4 10 1 60.73 61.34 31.08 o 5 10 1 243.16 231.72 61.41 o 6 10 1 37.75 50.87 34.57 o 7 10 1 221.79 231.34 35.87 o 8 10 1 30.74 65.51 45.42 o 9 10 1 28.49 -17.45 42.50 o 10 10 1 58.48 36.01 46.17 o 1 11 1 167.21 181.01 44.13 o 2 11 1 190.91 175.31 34.49 o 3 11 1 95.78 32.05 54.76 o 4 11 1 23.21 3.97 62.69 o 5 11 1 9.60 -5.14 39.72 o 6 11 1 125.19 132.57 56.51 o 7 11 1 127.62 184.41 37.16 o 8 11 1 40.12 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12841.51 12442.05 75.54 o 2 2 2 270.65 244.87 49.03 o 3 2 2 5608.45 5151.89 61.42 o 4 2 2 4388.39 4432.06 63.73 o 5 2 2 553.37 619.24 31.95 o 6 2 2 228.92 242.06 32.22 o 7 2 2 767.04 886.32 57.44 o 8 2 2 22.14 68.93 35.61 o 9 2 2 15.48 20.19 41.80 o 10 2 2 275.60 270.54 35.73 o 11 2 2 27.77 12.01 37.68 o 12 2 2 25.18 11.75 39.63 o 13 2 2 18.56 -8.44 148.62 o 14 2 2 12.24 -47.77 74.60 o 0 3 2 30680.41 30400.59 136.05 o 1 3 2 1407.91 1461.52 33.85 o 2 3 2 973.45 989.53 29.96 o 3 3 2 320.80 337.75 22.04 o 4 3 2 219.91 226.45 17.33 o 5 3 2 2149.58 2439.76 56.21 o 6 3 2 488.18 582.33 65.73 o 7 3 2 67.12 54.40 19.13 o 8 3 2 98.28 96.21 24.87 o 9 3 2 24.19 24.74 33.24 o 10 3 2 186.97 174.01 37.71 o 11 3 2 33.96 84.24 54.64 o 12 3 2 595.36 587.65 49.27 o 13 3 2 54.88 31.78 45.30 o 14 3 2 18.10 53.24 45.81 o 0 4 2 567.54 567.48 26.99 o 1 4 2 372.14 359.49 22.50 o 2 4 2 2674.28 2610.88 51.84 o 3 4 2 709.05 663.62 31.76 o 4 4 2 1837.72 1897.82 51.10 o 5 4 2 296.02 343.67 29.77 o 6 4 2 18.79 33.40 20.92 o 7 4 2 104.07 111.53 22.12 o 8 4 2 34.83 78.53 46.82 o 9 4 2 332.98 278.40 33.24 o 10 4 2 22.17 -15.38 30.95 o 11 4 2 117.73 262.17 138.35 o 12 4 2 75.93 89.86 34.46 o 13 4 2 57.25 58.36 34.60 o 14 4 2 23.37 -48.27 48.27 o 0 5 2 5214.94 5474.72 106.83 o 1 5 2 1772.49 1856.68 59.78 o 2 5 2 1554.39 1557.90 44.86 o 3 5 2 1266.41 1361.27 67.36 o 4 5 2 38.00 72.75 19.15 o 5 5 2 303.70 314.42 22.68 o 6 5 2 271.16 323.20 27.05 o 7 5 2 302.60 338.96 31.60 o 8 5 2 14.11 38.88 30.63 o 9 5 2 492.26 494.18 48.57 o 10 5 2 14.47 12.11 51.02 o 11 5 2 26.26 24.78 33.10 o 12 5 2 14.99 33.02 41.58 o 13 5 2 14.87 25.29 70.05 o 0 6 2 807.86 819.70 38.39 o 1 6 2 2079.55 2117.84 56.36 o 2 6 2 143.38 123.97 27.44 o 3 6 2 10.19 -9.89 24.85 o 4 6 2 59.52 40.10 19.07 o 5 6 2 255.67 260.57 25.42 o 6 6 2 114.88 85.09 26.20 o 7 6 2 510.88 500.33 37.17 o 8 6 2 81.33 83.56 59.07 o 9 6 2 19.06 16.54 34.06 o 10 6 2 30.60 45.67 36.43 o 11 6 2 27.39 43.61 39.69 o 12 6 2 45.89 36.91 44.15 o 13 6 2 5.77 72.71 38.12 o 0 7 2 472.38 501.67 59.43 o 1 7 2 69.59 45.66 21.61 o 2 7 2 164.91 154.33 27.09 o 3 7 2 954.23 1044.98 47.54 o 4 7 2 395.49 395.45 32.51 o 5 7 2 456.89 453.94 34.15 o 6 7 2 273.58 287.65 34.21 o 7 7 2 169.91 97.98 36.43 o 8 7 2 195.62 149.77 52.30 o 9 7 2 2.22 62.02 26.81 o 10 7 2 12.77 -12.30 54.52 o 11 7 2 19.16 72.72 49.50 o 12 7 2 17.55 4.33 58.84 o 0 8 2 262.51 205.96 26.75 o 1 8 2 178.45 203.12 27.79 o 2 8 2 517.44 505.96 37.37 o 3 8 2 127.01 137.49 35.61 o 4 8 2 455.39 439.04 33.24 o 5 8 2 704.38 688.24 44.47 o 6 8 2 28.35 46.64 26.80 o 7 8 2 250.45 311.33 34.29 o 8 8 2 315.63 311.97 54.64 o 9 8 2 10.46 74.54 59.78 o 10 8 2 141.76 169.37 31.92 o 11 8 2 12.33 57.31 47.28 o 0 9 2 399.11 372.50 33.43 o 1 9 2 327.36 349.48 31.04 o 2 9 2 133.73 152.58 27.89 o 3 9 2 16.38 -11.01 41.45 o 4 9 2 59.52 97.64 27.09 o 5 9 2 153.36 116.08 30.75 o 6 9 2 21.93 49.47 39.34 o 7 9 2 178.67 176.19 37.36 o 8 9 2 176.43 140.32 34.17 o 9 9 2 0.88 -3.01 39.37 o 10 9 2 6.91 5.62 45.66 o 11 9 2 9.43 21.65 44.08 o 0 10 2 359.99 351.04 37.01 o 1 10 2 272.85 260.70 44.36 o 2 10 2 121.65 118.84 31.70 o 3 10 2 177.20 199.05 33.09 o 4 10 2 77.76 77.53 36.89 o 5 10 2 73.14 61.18 33.09 o 6 10 2 160.87 130.11 68.53 o 7 10 2 40.68 68.68 35.53 o 8 10 2 8.98 -9.78 48.10 o 9 10 2 120.89 188.21 37.30 o 10 10 2 43.49 18.86 40.02 o 0 11 2 787.61 622.75 99.59 o 1 11 2 710.21 746.01 58.14 o 2 11 2 53.82 69.75 63.04 o 3 11 2 82.13 115.08 30.21 o 4 11 2 79.95 70.51 57.56 o 5 11 2 479.33 518.32 47.80 o 6 11 2 9.36 37.55 61.29 o 7 11 2 29.14 102.88 32.63 o 8 11 2 0.52 -39.86 49.11 o 0 12 2 331.78 296.62 42.82 o 1 12 2 232.66 216.02 39.70 o 2 12 2 28.27 20.56 36.89 o 3 12 2 6.19 23.92 41.65 o 4 12 2 39.02 23.06 67.95 o 5 12 2 75.06 111.22 57.32 o 6 12 2 5.26 -11.77 69.00 o 0 13 2 5.59 26.13 44.18 o 1 13 2 155.80 117.70 50.90 o 2 13 2 46.47 118.15 38.98 o 3 13 2 26.02 21.32 96.90 o 4 13 2 30.09 -11.86 47.00 o 2 0 3 26025.90 23853.17 189.02 o 4 0 3 820.91 858.17 33.51 o 6 0 3 100.68 105.47 16.31 o 8 0 3 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141.61 34.28 o 4 3 28 82.85 124.97 48.10 o 5 3 28 40.11 27.88 40.04 o 6 3 28 41.06 -18.01 41.51 o 7 3 28 1.10 17.41 75.30 o 8 3 28 4.36 -6.31 37.84 o 9 3 28 37.81 5.02 51.95 o 10 3 28 1.18 3.71 46.71 o 0 4 28 298.63 266.91 33.70 o 1 4 28 28.33 -30.65 37.56 o 2 4 28 87.88 107.65 32.43 o 3 4 28 58.53 40.38 35.28 o 4 4 28 238.94 296.73 38.34 o 5 4 28 48.82 12.23 42.48 o 6 4 28 66.37 16.62 69.93 o 7 4 28 8.15 -34.32 58.84 o 8 4 28 19.43 89.94 34.41 o 9 4 28 20.04 80.61 49.38 o 0 5 28 21.78 -37.13 57.44 o 1 5 28 88.83 123.56 63.16 o 2 5 28 23.91 54.19 33.04 o 3 5 28 185.02 199.97 112.66 o 4 5 28 48.32 37.64 33.19 o 5 5 28 42.94 36.48 41.21 o 6 5 28 1.77 -41.97 41.97 o 7 5 28 0.34 -25.05 42.29 o 8 5 28 23.88 4.42 49.03 o 9 5 28 1.80 9.37 38.71 o 0 6 28 72.69 23.79 38.63 o 1 6 28 47.34 23.46 36.83 o 2 6 28 8.05 -10.40 37.46 o 3 6 28 44.97 135.87 32.85 o 4 6 28 47.61 -15.04 53.82 o 5 6 28 0.46 47.91 70.17 o 6 6 28 12.74 14.66 40.16 o 7 6 28 14.66 34.17 35.59 o 8 6 28 9.32 180.66 229.65 o 0 7 28 18.15 31.00 86.04 o 1 7 28 32.80 -10.79 56.97 o 2 7 28 148.04 152.74 35.84 o 3 7 28 30.45 26.74 44.16 o 4 7 28 12.13 3.64 39.23 o 5 7 28 11.67 215.39 150.26 o 6 7 28 25.87 27.58 49.80 o 7 7 28 39.40 -4.17 48.28 o 0 8 28 222.95 185.18 40.99 o 1 8 28 18.07 15.87 41.82 o 2 8 28 0.35 8.04 37.92 o 3 8 28 9.07 48.78 37.65 o 4 8 28 8.76 -20.01 44.73 o 5 8 28 3.00 -10.48 45.22 o 6 8 28 9.51 54.19 39.19 o 0 9 28 23.70 57.95 37.88 o 1 9 28 56.91 62.72 65.61 o 2 9 28 7.51 -37.08 42.71 o 3 9 28 9.38 46.85 38.06 o 4 9 28 25.81 -22.14 80.09 o 2 0 29 39.95 42.83 45.18 o 4 0 29 115.57 119.46 31.58 o 6 0 29 71.71 46.24 38.64 o 8 0 29 55.17 40.42 40.37 o 10 0 29 52.70 39.35 51.72 o 1 1 29 1016.94 967.29 61.97 o 2 1 29 693.63 695.12 45.64 o 3 1 29 444.12 465.17 41.69 o 4 1 29 14.44 -37.13 37.13 o 5 1 29 48.75 46.98 48.10 o 6 1 29 123.50 155.49 36.46 o 7 1 29 3.72 2.66 35.20 o 8 1 29 23.82 52.14 35.70 o 9 1 29 11.14 38.86 40.73 o 10 1 29 0.46 -7.93 58.72 o 1 2 29 188.47 151.96 34.46 o 2 2 29 65.95 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165.67 32.94 o 3 2 30 17.60 27.27 31.11 o 4 2 30 153.41 119.00 55.92 o 5 2 30 29.93 53.54 46.58 o 6 2 30 20.13 85.92 48.22 o 7 2 30 41.75 50.82 37.96 o 8 2 30 50.45 51.21 38.20 o 9 2 30 8.94 -2.35 72.38 o 0 3 30 225.52 240.70 34.59 o 1 3 30 70.57 64.38 57.44 o 2 3 30 13.46 26.77 31.66 o 3 3 30 17.90 -2.63 40.36 o 4 3 30 18.63 39.27 33.82 o 5 3 30 23.88 4.61 41.37 o 6 3 30 20.95 37.46 42.92 o 7 3 30 4.04 -42.83 42.83 o 8 3 30 78.73 39.94 84.64 o 9 3 30 0.57 -13.27 57.91 o 0 4 30 335.94 335.63 38.53 o 1 4 30 41.72 58.29 29.31 o 2 4 30 17.73 65.80 30.82 o 3 4 30 224.99 178.30 41.15 o 4 4 30 150.93 85.59 72.62 o 5 4 30 7.83 -1.59 51.14 o 6 4 30 3.76 -42.61 42.61 o 7 4 30 10.04 14.31 40.75 o 8 4 30 16.37 27.74 46.47 o 0 5 30 185.47 204.58 58.49 o 1 5 30 22.55 35.27 39.69 o 2 5 30 325.60 352.74 40.17 o 3 5 30 110.04 49.96 40.62 o 4 5 30 161.62 131.54 36.52 o 5 5 30 116.95 128.56 34.59 o 6 5 30 5.29 59.66 38.03 o 7 5 30 6.08 6.38 37.69 o 8 5 30 4.18 -3.16 65.15 o 0 6 30 51.89 41.78 38.06 o 1 6 30 29.96 14.08 36.22 o 2 6 30 3.46 -28.69 43.01 o 3 6 30 9.96 -24.20 44.13 o 4 6 30 69.23 3.75 60.24 o 5 6 30 59.88 18.38 39.54 o 6 6 30 4.27 32.02 98.77 o 7 6 30 0.91 -6.74 46.22 o 0 7 30 161.01 257.49 37.97 o 1 7 30 23.19 57.16 38.41 o 2 7 30 29.94 39.12 39.23 o 3 7 30 15.05 -49.25 99.82 o 4 7 30 18.84 11.79 49.97 o 5 7 30 31.72 -51.25 51.25 o 6 7 30 106.85 100.61 45.65 o 0 8 30 0.95 -40.44 45.23 o 1 8 30 2.89 -38.88 49.09 o 2 8 30 4.30 26.51 39.10 o 3 8 30 52.51 1.35 43.80 o 4 8 30 20.36 69.80 41.48 o 0 9 30 2.44 -49.94 49.94 o 1 9 30 73.48 63.98 47.68 o 2 0 31 1052.60 1017.22 63.61 o 4 0 31 317.03 370.36 40.22 o 6 0 31 66.79 87.35 42.15 o 8 0 31 31.28 40.34 34.50 o 1 1 31 236.56 267.44 40.28 o 2 1 31 143.28 97.58 43.20 o 3 1 31 110.14 78.83 34.07 o 4 1 31 136.18 111.02 43.20 o 5 1 31 10.78 26.17 39.23 o 6 1 31 107.36 73.58 71.80 o 7 1 31 77.08 122.60 50.79 o 8 1 31 29.40 -0.29 38.96 o 9 1 31 37.88 192.44 104.96 o 1 2 31 25.99 -24.08 38.51 o 2 2 31 33.32 12.89 37.81 o 3 2 31 76.90 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34 19.33 39.00 42.47 o 2 4 34 27.77 -44.16 44.16 o 3 4 34 3.32 39.66 36.97 o 4 4 34 2.93 -40.75 89.66 o 5 4 34 13.24 52.87 37.87 o 6 4 34 5.75 7.09 44.82 o 0 5 34 6.12 5.06 43.78 o 1 5 34 7.17 -40.45 43.56 o 2 5 34 61.59 120.01 51.25 o 3 5 34 54.56 16.20 48.79 o 4 5 34 0.42 82.71 39.69 o 5 5 34 100.45 133.26 77.29 o 0 6 34 65.75 24.07 43.90 o 1 6 34 0.02 -22.91 46.22 o 2 6 34 20.11 74.73 43.63 o 3 6 34 5.20 15.54 45.97 o 4 6 34 5.91 -3.14 69.58 o 0 7 34 21.49 13.73 46.31 o 1 7 34 1.24 -28.13 52.29 o 2 7 34 19.96 -21.06 150.14 o 2 0 35 14.37 53.46 93.98 o 4 0 35 22.50 60.73 57.21 o 6 0 35 33.34 13.43 42.02 o 1 1 35 42.36 -10.93 43.42 o 2 1 35 27.29 -45.96 45.96 o 3 1 35 0.90 -14.21 57.21 o 4 1 35 3.26 74.14 35.33 o 5 1 35 7.86 -34.67 45.15 o 6 1 35 5.78 -47.66 47.66 o 7 1 35 8.49 -49.12 49.12 o 1 2 35 15.17 31.01 49.38 o 2 2 35 25.01 3.75 35.74 o 3 2 35 141.47 126.14 43.01 o 4 2 35 52.69 79.58 66.66 o 5 2 35 34.11 60.13 64.68 o 6 2 35 4.43 -11.43 45.55 o 7 2 35 51.52 70.88 43.99 o 1 3 35 4.48 -35.47 46.74 o 2 3 35 56.13 106.47 96.55 o 3 3 35 49.55 49.35 62.58 o 4 3 35 69.86 102.64 38.98 o 5 3 35 65.13 67.44 39.08 o 6 3 35 43.58 4.17 51.93 o 1 4 35 3.87 -17.95 41.91 o 2 4 35 0.18 -48.38 48.38 o 3 4 35 2.99 12.70 40.07 o 4 4 35 37.24 21.63 39.09 o 5 4 35 27.21 30.93 74.14 o 1 5 35 7.51 36.05 46.30 o 2 5 35 41.20 76.62 32.52 o 3 5 35 127.32 334.87 168.59 o 4 5 35 2.35 16.55 56.04 o 5 5 35 61.57 21.31 62.58 o 1 6 35 5.98 -19.52 57.79 o 2 6 35 15.46 -23.58 68.77 o 3 6 35 69.09 75.30 43.78 o 0 0 36 251.95 280.58 109.04 o 2 0 36 310.00 332.80 41.93 o 4 0 36 70.08 132.08 89.08 o 6 0 36 10.69 124.29 76.24 o 0 1 36 16.90 -35.91 45.48 o 1 1 36 3.06 15.86 39.11 o 2 1 36 109.21 123.39 38.70 o 3 1 36 15.59 18.99 42.54 o 4 1 36 52.41 75.78 45.30 o 5 1 36 46.22 21.14 44.51 o 6 1 36 4.50 8.60 80.44 o 0 2 36 142.59 165.67 37.89 o 1 2 36 3.94 18.41 79.74 o 2 2 36 9.55 -20.78 60.13 o 3 2 36 57.84 32.63 43.45 o 4 2 36 2.65 -9.88 38.87 o 5 2 36 6.01 13.99 44.71 o 6 2 36 24.62 97.88 39.23 o 0 3 36 21.60 22.71 44.01 o 1 3 36 23.08 -40.75 44.74 o 2 3 36 48.96 6.25 42.83 o 3 3 36 25.46 -35.74 74.60 o 4 3 36 10.23 17.83 76.47 o 5 3 36 12.35 -6.84 46.56 o 0 4 36 39.15 37.12 39.79 o 1 4 36 6.08 18.96 40.18 o 2 4 36 18.03 -35.73 144.30 o 3 4 36 36.81 28.56 40.94 o 4 4 36 8.69 10.07 45.17 o 5 4 36 36.78 -14.83 58.72 o 0 5 36 42.30 20.17 44.25 o 1 5 36 19.76 41.66 39.78 o 2 5 36 4.62 -42.00 81.49 o 3 5 36 16.72 27.20 42.85 o 0 6 36 26.60 17.75 51.49 o 1 6 36 68.86 107.91 44.85 o 2 0 37 203.45 226.94 44.31 o 4 0 37 0.28 4.14 40.55 o 1 1 37 26.46 69.93 35.70 o 2 1 37 140.92 117.52 98.19 o 3 1 37 8.44 19.22 83.24 o 4 1 37 4.50 63.19 64.10 o 5 1 37 78.71 -11.00 49.36 o 1 2 37 52.30 165.75 119.67 o 2 2 37 42.14 101.81 58.37 o 3 2 37 8.25 -47.85 47.85 o 4 2 37 3.00 52.78 36.90 o 5 2 37 32.91 54.74 51.16 o 1 3 37 17.22 -39.13 58.72 o 2 3 37 8.16 -72.73 72.73 o 3 3 37 2.78 2.68 57.09 o 4 3 37 4.86 20.69 49.27 o 1 4 37 57.20 17.87 43.14 o 2 4 37 52.70 171.42 40.07 o 3 4 37 13.90 37.00 51.72 o 4 4 37 10.76 -40.87 45.50 o 1 5 37 14.46 -19.66 106.94 o 2 5 37 26.37 85.59 39.71 o 0 0 38 25.55 39.38 42.88 o 2 0 38 12.48 -62.61 72.03 o 4 0 38 66.44 19.66 86.86 o 0 1 38 46.08 58.62 54.76 o 1 1 38 71.39 134.20 37.17 o 2 1 38 14.19 -26.55 49.61 o 3 1 38 30.76 28.80 39.26 o 4 1 38 28.44 112.75 78.81 o 0 2 38 129.56 132.38 45.42 o 1 2 38 7.71 -42.98 50.44 o 2 2 38 55.67 23.32 51.91 o 3 2 38 31.12 39.89 57.79 o 4 2 38 9.07 75.98 44.48 o 0 3 38 121.92 158.48 41.41 o 1 3 38 5.94 -50.09 50.09 o 2 3 38 14.11 -33.89 50.35 o 3 3 38 30.75 47.09 89.31 o 0 4 38 12.92 87.88 42.15 o 1 4 38 53.14 101.22 39.62 o 2 4 38 2.87 6.69 44.07 o 2 0 39 4.95 -8.75 67.71 o 1 1 39 34.50 -20.54 48.03 o 2 1 39 2.30 -14.07 40.97 o 3 1 39 0.94 -53.32 53.32 o 1 2 39 74.94 43.36 69.12 o 2 2 39 3.55 -26.65 50.03 o 3 2 39 26.92 55.88 52.63 o 1 3 39 17.05 51.24 43.22 o 2 3 39 24.09 -27.35 48.34 o 0 0 40 59.38 82.32 48.22 o 2 0 40 5.17 31.62 51.26 o 0 1 40 26.81 1.20 48.68 o 1 1 40 0.51 69.98 45.95 o