#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/62/2206265.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206265_Fobs loop_ _publ_author_name 'Lewis, Thomas C.' 'Tocher, Derek A.' _publ_section_title ; A low-temperature determination of butyramide ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1985 _journal_page_last o1986 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.070 _cell_angle_gamma 90.000 _cell_length_a 9.8140 _cell_length_b 5.9232 _cell_length_c 9.7006 _exptl_crystal_F_000 192.00 _reflns_d_resolution_high 0.7487 _[local]_cod_data_source_file rn6052Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' butyramide in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 75.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 939.81 997.09 9.44 o 2 0 0 753.77 759.97 7.41 o 3 0 0 124.72 140.17 1.46 o 4 0 0 641.74 669.45 7.04 o 5 0 0 371.40 350.10 4.31 o 6 0 0 251.01 218.56 3.26 o 7 0 0 115.93 96.47 2.14 o 8 0 0 125.12 113.14 2.50 o 9 0 0 47.23 45.72 1.74 o 10 0 0 0.05 0.18 1.21 o 11 0 0 4.17 6.78 1.13 o 1 1 0 607.26 639.00 3.62 o 2 1 0 5663.75 5806.27 31.23 o 3 1 0 544.47 542.70 3.61 o 4 1 0 51.30 57.61 0.78 o 5 1 0 132.90 128.66 1.35 o 6 1 0 223.35 217.21 2.01 o 7 1 0 3.36 3.57 0.49 o 8 1 0 21.67 18.60 0.84 o 9 1 0 11.27 9.61 0.73 o 10 1 0 7.39 7.63 1.21 o 11 1 0 9.45 9.39 0.89 o 0 2 0 1692.66 1770.25 13.78 o 1 2 0 164.13 185.96 1.33 o 2 2 0 97.41 121.62 1.22 o 3 2 0 456.44 454.58 2.89 o 4 2 0 1089.04 1088.16 6.37 o 5 2 0 2.71 2.69 0.33 o 6 2 0 13.54 15.41 0.60 o 7 2 0 22.90 20.82 0.83 o 8 2 0 16.62 16.41 1.07 o 9 2 0 1.82 1.96 0.55 o 10 2 0 0.68 0.66 0.60 o 11 2 0 7.43 7.84 0.82 o 1 3 0 40.00 40.81 0.58 o 2 3 0 283.85 298.68 2.12 o 3 3 0 2.70 3.25 0.41 o 4 3 0 7.50 7.61 0.36 o 5 3 0 140.41 138.00 1.60 o 6 3 0 104.11 93.61 1.84 o 7 3 0 14.65 14.28 0.68 o 8 3 0 10.26 10.10 0.97 o 9 3 0 10.76 12.40 1.12 o 10 3 0 4.10 4.15 0.88 o 11 3 0 0.02 1.29 1.67 o 0 4 0 0.83 1.18 0.31 o 1 4 0 1.58 1.46 0.25 o 2 4 0 12.13 12.19 0.59 o 3 4 0 113.32 110.15 1.46 o 4 4 0 113.09 112.20 1.98 o 5 4 0 52.74 55.38 1.25 o 6 4 0 57.68 59.47 1.37 o 7 4 0 10.38 9.34 0.77 o 8 4 0 8.55 6.78 0.92 o 9 4 0 1.43 0.91 0.78 o 10 4 0 2.40 2.71 1.17 o 1 5 0 69.42 69.98 1.32 o 2 5 0 10.31 11.87 0.66 o 3 5 0 52.27 52.98 1.04 o 4 5 0 4.65 4.51 0.58 o 5 5 0 2.64 1.88 0.54 o 6 5 0 29.76 31.62 1.16 o 7 5 0 0.50 0.99 0.61 o 8 5 0 19.41 21.45 2.18 o 9 5 0 19.23 20.09 1.71 o 0 6 0 37.08 34.61 1.48 o 1 6 0 1.01 0.56 0.46 o 2 6 0 15.72 14.09 1.43 o 3 6 0 7.78 8.39 0.79 o 4 6 0 0.34 0.44 0.85 o 5 6 0 0.82 1.50 0.82 o 6 6 0 0.08 0.03 0.80 o 7 6 0 12.82 16.44 1.50 o 1 7 0 1.23 0.94 0.66 o 2 7 0 10.62 10.01 2.20 o 3 7 0 11.33 11.53 1.74 o 4 7 0 1.05 -0.09 1.19 o -12 1 1 1.62 1.64 1.00 o -11 1 1 2.22 2.87 0.68 o -10 1 1 25.49 23.70 1.02 o -9 1 1 29.51 27.04 1.00 o -8 1 1 4.85 2.84 0.51 o -7 1 1 28.04 26.99 0.87 o -6 1 1 39.52 35.17 0.86 o -5 1 1 12.29 13.26 0.45 o -4 1 1 1363.22 1401.38 8.67 o -3 1 1 26.31 23.84 0.37 o -2 1 1 797.66 828.95 4.70 o -1 1 1 11.17 11.12 0.37 o 0 1 1 103.03 109.75 1.42 o 1 1 1 536.84 521.48 3.03 o 2 1 1 1396.28 1382.41 7.69 o 3 1 1 30.56 32.11 0.45 o 4 1 1 97.91 99.17 1.09 o 5 1 1 53.71 47.89 0.83 o 6 1 1 0.02 0.12 0.35 o 7 1 1 29.87 29.72 0.92 o 8 1 1 8.25 7.82 0.65 o 9 1 1 2.14 3.35 0.58 o 10 1 1 0.20 0.30 0.51 o 11 1 1 2.69 3.70 0.72 o -12 2 1 6.38 4.93 1.69 o -11 2 1 0.49 0.44 0.66 o -10 2 1 0.78 1.57 0.61 o -9 2 1 2.40 2.57 0.59 o -8 2 1 17.44 17.89 0.84 o -7 2 1 51.38 47.93 0.97 o -6 2 1 161.11 157.08 1.69 o -5 2 1 7.71 8.84 0.43 o -4 2 1 0.00 0.06 0.14 o -3 2 1 108.69 107.85 0.98 o -2 2 1 1643.27 1751.63 9.70 o -1 2 1 136.31 131.97 1.40 o 0 2 1 11.07 10.59 0.26 o 1 2 1 0.06 -0.11 0.11 o 2 2 1 55.80 57.12 0.64 o 3 2 1 34.59 36.60 0.60 o 4 2 1 270.30 263.84 2.22 o 5 2 1 0.72 0.64 0.30 o 6 2 1 5.18 6.13 0.47 o 7 2 1 33.08 33.96 1.01 o 8 2 1 0.05 -0.01 0.43 o 9 2 1 9.66 7.59 0.89 o 10 2 1 4.79 4.97 0.80 o -11 3 1 0.02 -0.20 0.88 o -10 3 1 11.71 11.43 1.07 o -9 3 1 11.72 9.90 0.78 o -8 3 1 18.27 17.96 0.89 o -7 3 1 7.10 5.51 0.51 o -6 3 1 17.46 18.53 0.85 o -5 3 1 59.97 60.67 1.01 o -4 3 1 370.93 356.73 2.56 o -3 3 1 1.57 1.51 0.23 o -2 3 1 3.82 3.67 0.24 o -1 3 1 22.66 21.12 0.42 o 0 3 1 204.14 204.58 1.55 o 1 3 1 76.67 80.79 1.15 o 2 3 1 76.67 84.13 1.11 o 3 3 1 34.38 31.96 0.59 o 4 3 1 20.18 22.38 0.56 o 5 3 1 19.69 20.58 0.68 o 6 3 1 28.74 27.70 0.95 o 7 3 1 4.82 2.44 0.67 o 8 3 1 0.01 -0.22 0.63 o 9 3 1 0.49 1.17 0.69 o 10 3 1 0.95 0.76 0.79 o -10 4 1 1.46 1.49 0.93 o -9 4 1 0.27 0.45 0.80 o -8 4 1 2.37 0.94 0.70 o -7 4 1 16.66 14.71 0.85 o -6 4 1 69.38 73.26 1.25 o -5 4 1 28.54 24.13 0.88 o -4 4 1 13.35 14.86 0.52 o -3 4 1 0.43 0.58 0.26 o -2 4 1 108.49 107.44 1.15 o -1 4 1 13.38 14.86 0.45 o 0 4 1 0.01 -0.15 0.30 o 1 4 1 127.05 126.82 1.44 o 2 4 1 80.17 74.78 1.11 o 3 4 1 67.47 67.97 1.36 o 4 4 1 4.23 4.10 0.54 o 5 4 1 0.20 0.03 0.42 o 6 4 1 7.41 8.61 0.95 o 7 4 1 0.03 0.51 0.55 o 8 4 1 0.05 0.74 0.71 o 9 4 1 10.13 11.43 1.14 o -9 5 1 5.36 8.38 1.23 o -8 5 1 24.31 28.10 1.37 o -7 5 1 0.43 0.68 0.63 o -6 5 1 25.75 28.54 1.22 o -5 5 1 2.48 3.61 0.72 o -4 5 1 0.30 0.07 0.42 o -3 5 1 26.01 23.25 0.85 o -2 5 1 7.76 7.54 0.56 o -1 5 1 27.08 23.97 0.71 o 0 5 1 100.61 98.60 1.59 o 1 5 1 69.97 66.28 1.12 o 2 5 1 35.79 36.32 0.87 o 3 5 1 2.68 2.65 0.40 o 4 5 1 2.23 1.75 0.52 o 5 5 1 0.02 0.50 0.51 o 6 5 1 0.52 1.36 0.60 o 7 5 1 42.94 52.75 1.79 o 8 5 1 4.01 2.57 0.96 o -8 6 1 1.38 0.81 1.51 o -7 6 1 15.13 21.85 2.36 o -6 6 1 1.40 0.76 0.86 o -5 6 1 0.50 1.27 0.80 o -4 6 1 1.29 0.69 1.10 o -3 6 1 18.60 18.03 1.15 o -2 6 1 1.24 1.29 0.53 o -1 6 1 98.22 102.08 2.08 o 0 6 1 1.64 0.84 0.49 o 1 6 1 0.37 0.25 0.52 o 2 6 1 28.80 29.69 2.25 o 3 6 1 5.49 7.33 1.12 o 4 6 1 18.65 22.34 1.24 o 5 6 1 38.45 43.49 1.60 o 6 6 1 0.65 1.28 0.72 o 7 6 1 1.36 3.88 0.89 o -5 7 1 1.48 6.15 1.45 o -4 7 1 2.40 2.76 0.97 o -3 7 1 8.77 8.05 1.89 o -2 7 1 3.96 2.88 0.68 o -1 7 1 3.84 3.62 0.71 o 0 7 1 0.48 1.01 0.71 o 1 7 1 26.30 27.46 1.72 o 2 7 1 0.79 0.85 0.74 o 3 7 1 7.60 8.89 1.84 o 4 7 1 12.84 13.06 2.24 o -12 0 2 1.27 0.98 0.89 o -11 0 2 24.27 24.82 2.24 o -10 0 2 14.31 11.73 2.34 o -9 0 2 0.02 -0.41 0.57 o -8 0 2 374.19 346.31 4.84 o -7 0 2 0.03 -0.14 0.53 o -6 0 2 163.35 150.86 1.84 o -5 0 2 192.40 196.64 2.12 o -4 0 2 257.63 244.18 2.39 o -3 0 2 98.61 83.73 1.05 o -2 0 2 2579.22 2618.41 20.05 o -1 0 2 2106.91 2263.93 17.38 o 0 0 2 2985.00 2958.26 22.61 o 1 0 2 832.06 859.56 6.92 o 2 0 2 33.62 36.11 0.69 o 3 0 2 30.83 32.72 0.85 o 4 0 2 40.31 33.69 0.76 o 5 0 2 48.14 45.89 1.37 o 6 0 2 25.98 23.19 1.12 o 7 0 2 139.85 128.09 2.64 o 8 0 2 12.99 11.26 1.04 o 9 0 2 51.63 50.42 1.85 o 10 0 2 8.48 8.72 1.11 o 11 0 2 5.96 3.85 1.48 o -12 1 2 0.47 1.47 1.01 o -11 1 2 0.27 0.03 0.52 o -10 1 2 15.64 14.01 0.86 o -9 1 2 14.12 13.66 0.83 o -8 1 2 0.05 0.18 0.42 o -7 1 2 19.55 22.35 0.79 o -6 1 2 376.79 369.35 2.89 o -5 1 2 3.22 4.13 0.27 o -4 1 2 28.93 32.72 0.49 o -3 1 2 338.03 369.54 2.33 o -2 1 2 425.13 442.99 4.77 o -1 1 2 4.96 7.74 0.23 o 0 1 2 668.91 633.13 4.58 o 1 1 2 1017.62 1053.61 5.94 o 2 1 2 180.58 189.84 1.40 o 3 1 2 229.19 233.84 1.72 o 4 1 2 70.36 71.24 0.81 o 5 1 2 61.78 58.29 1.95 o 6 1 2 10.82 9.80 0.62 o 7 1 2 14.54 15.25 0.77 o 8 1 2 17.16 15.55 0.85 o 9 1 2 62.94 59.43 2.28 o 10 1 2 4.48 5.54 0.92 o -12 2 2 1.47 2.94 1.02 o -11 2 2 0.50 -0.04 0.56 o -10 2 2 0.94 0.50 0.55 o -9 2 2 0.15 0.79 0.51 o -8 2 2 6.03 6.18 0.62 o -7 2 2 12.00 10.20 0.56 o -6 2 2 21.31 21.94 0.66 o -5 2 2 26.10 29.34 0.59 o -4 2 2 495.39 561.82 3.85 o -3 2 2 37.18 36.13 0.74 o -2 2 2 109.65 137.54 1.21 o -1 2 2 704.71 753.68 4.39 o 0 2 2 164.90 152.45 1.54 o 1 2 2 148.72 156.52 1.55 o 2 2 2 14.05 16.46 0.37 o 3 2 2 428.59 421.29 2.81 o 4 2 2 78.44 72.54 0.89 o 5 2 2 45.25 44.47 0.87 o 6 2 2 52.23 49.61 1.19 o 7 2 2 64.28 63.45 1.34 o 8 2 2 2.61 1.93 0.66 o 9 2 2 4.55 3.83 0.77 o 10 2 2 2.72 2.54 0.86 o -11 3 2 8.98 10.12 1.03 o -10 3 2 1.43 3.19 0.65 o -9 3 2 1.55 0.76 0.55 o -8 3 2 0.16 0.89 0.49 o -7 3 2 1.40 0.90 0.44 o -6 3 2 2.47 1.83 0.38 o -5 3 2 22.96 22.74 0.57 o -4 3 2 1.51 1.38 0.24 o -3 3 2 173.88 170.55 1.71 o -2 3 2 291.67 318.61 2.22 o -1 3 2 363.98 374.58 2.56 o 0 3 2 340.53 362.62 4.30 o 1 3 2 239.60 238.65 2.05 o 2 3 2 48.24 47.87 0.80 o 3 3 2 9.54 10.78 0.58 o 4 3 2 34.23 32.36 1.40 o 5 3 2 366.47 359.02 3.56 o 6 3 2 27.51 26.53 0.97 o 7 3 2 27.01 28.92 1.30 o 8 3 2 4.93 5.58 1.04 o 9 3 2 4.22 3.59 0.86 o -10 4 2 0.13 -0.23 0.94 o -9 4 2 7.82 7.38 1.16 o -8 4 2 18.46 20.72 1.16 o -7 4 2 6.18 5.17 0.80 o -6 4 2 19.31 16.01 0.75 o -5 4 2 4.48 5.68 1.08 o -4 4 2 36.78 35.15 0.73 o -3 4 2 118.16 114.72 1.71 o -2 4 2 162.26 156.71 1.64 o -1 4 2 72.77 77.44 1.07 o 0 4 2 23.64 25.61 0.65 o 1 4 2 1.87 1.52 0.34 o 2 4 2 81.56 76.79 1.15 o 3 4 2 465.21 458.24 3.68 o 4 4 2 47.75 48.55 1.93 o 5 4 2 16.19 18.46 0.88 o 6 4 2 5.38 6.18 0.81 o 7 4 2 23.48 22.59 1.85 o 8 4 2 16.52 16.81 1.23 o 9 4 2 2.45 5.46 2.54 o -9 5 2 6.70 6.69 1.14 o -8 5 2 8.82 10.33 1.18 o -7 5 2 0.81 0.72 0.59 o -6 5 2 0.43 -0.54 0.67 o -5 5 2 46.07 42.07 1.81 o -4 5 2 0.73 0.41 0.43 o -3 5 2 1.26 0.41 0.34 o -2 5 2 24.34 25.42 0.83 o -1 5 2 1.63 1.29 0.36 o 0 5 2 67.54 67.87 1.30 o 1 5 2 208.54 212.90 2.93 o 2 5 2 14.62 13.90 0.63 o 3 5 2 6.01 7.39 0.63 o 4 5 2 4.73 5.11 0.63 o 5 5 2 46.79 44.65 1.31 o 6 5 2 34.89 36.99 1.26 o 7 5 2 1.16 1.05 0.66 o 8 5 2 5.39 7.10 1.12 o -7 6 2 3.13 3.72 1.46 o -6 6 2 0.12 0.89 0.83 o -5 6 2 0.06 0.59 0.75 o -4 6 2 1.11 3.06 0.83 o -3 6 2 0.13 0.56 0.61 o -2 6 2 2.16 1.43 0.53 o -1 6 2 16.31 15.93 1.62 o 0 6 2 37.42 36.54 1.32 o 1 6 2 0.26 0.35 0.52 o 2 6 2 22.46 23.48 1.00 o 3 6 2 20.82 20.90 1.69 o 4 6 2 3.28 2.36 0.79 o 5 6 2 2.74 4.15 0.88 o 6 6 2 0.34 0.66 0.82 o -5 7 2 14.99 15.74 1.55 o -4 7 2 0.06 0.05 0.91 o -3 7 2 2.39 2.01 0.68 o -2 7 2 1.01 1.14 0.61 o -1 7 2 4.94 5.88 1.16 o 0 7 2 3.09 4.29 1.17 o 1 7 2 2.51 2.47 0.76 o 2 7 2 13.13 12.43 2.55 o 3 7 2 1.16 0.47 1.05 o -12 1 3 13.97 15.33 0.99 o -11 1 3 0.65 1.54 0.59 o -10 1 3 18.14 16.50 0.91 o -9 1 3 5.67 4.88 0.59 o -8 1 3 9.62 10.28 0.73 o -7 1 3 1.77 2.27 0.38 o -6 1 3 127.97 136.52 1.26 o -5 1 3 12.22 14.58 0.40 o -4 1 3 87.59 92.10 0.89 o -3 1 3 4.35 5.25 0.23 o -2 1 3 5.87 4.32 0.24 o -1 1 3 273.90 270.11 2.41 o 0 1 3 504.34 503.81 4.47 o 1 1 3 7.93 9.36 0.28 o 2 1 3 20.56 22.37 0.52 o 3 1 3 0.49 0.26 0.17 o 4 1 3 45.71 46.27 0.77 o 5 1 3 46.87 48.90 0.90 o 6 1 3 7.58 6.80 0.57 o 7 1 3 0.05 0.56 0.41 o 8 1 3 2.59 3.01 0.57 o 9 1 3 0.53 0.69 0.53 o 10 1 3 1.71 2.80 0.85 o -12 2 3 0.00 0.53 1.48 o -11 2 3 1.02 0.82 0.67 o -10 2 3 31.42 34.10 1.15 o -9 2 3 0.84 0.80 0.50 o -8 2 3 9.04 7.08 0.75 o -7 2 3 8.99 10.75 0.56 o -6 2 3 14.37 12.54 0.54 o -5 2 3 7.18 7.30 0.34 o -4 2 3 492.65 503.71 3.24 o -3 2 3 15.46 15.45 0.44 o -2 2 3 15.42 14.76 0.38 o -1 2 3 435.93 448.73 4.74 o 0 2 3 1.13 1.78 0.21 o 1 2 3 419.05 476.82 3.40 o 2 2 3 402.95 407.64 2.95 o 3 2 3 5.23 3.68 0.27 o 4 2 3 1.31 1.39 0.31 o 5 2 3 46.95 46.64 0.93 o 6 2 3 41.94 39.78 1.30 o 7 2 3 76.19 77.96 1.86 o 8 2 3 1.88 1.68 0.68 o 9 2 3 1.23 1.63 0.73 o -12 3 3 5.05 8.71 1.94 o -11 3 3 3.50 5.40 0.88 o -10 3 3 4.09 4.10 0.88 o -9 3 3 3.07 1.78 0.64 o -8 3 3 4.38 6.39 0.87 o -7 3 3 0.11 -0.36 0.36 o -6 3 3 14.41 13.42 0.59 o -5 3 3 23.04 21.63 0.57 o -4 3 3 10.64 12.37 0.43 o -3 3 3 136.71 124.21 2.28 o -2 3 3 37.25 43.12 0.60 o -1 3 3 104.18 109.52 1.34 o 0 3 3 83.21 83.09 1.14 o 1 3 3 23.66 22.49 0.70 o 2 3 3 5.64 6.19 0.40 o 3 3 3 6.36 5.91 0.43 o 4 3 3 164.10 156.11 2.06 o 5 3 3 52.52 54.71 1.57 o 6 3 3 0.03 -0.08 0.44 o 7 3 3 2.92 2.58 0.70 o 8 3 3 0.54 2.41 0.71 o 9 3 3 2.65 3.05 0.88 o -11 4 3 0.00 -1.37 1.37 o -10 4 3 0.10 0.04 0.69 o -9 4 3 2.68 3.98 0.72 o -8 4 3 1.58 3.43 0.56 o -7 4 3 26.01 24.14 0.92 o -6 4 3 4.03 6.40 0.55 o -5 4 3 116.92 99.74 1.34 o -4 4 3 1.71 1.71 0.37 o -3 4 3 5.70 6.01 0.49 o -2 4 3 30.72 29.11 0.84 o -1 4 3 14.05 14.87 0.66 o 0 4 3 0.57 1.24 0.35 o 1 4 3 62.43 59.24 1.00 o 2 4 3 47.67 48.11 1.08 o 3 4 3 104.51 102.25 1.64 o 4 4 3 0.00 0.15 0.39 o 5 4 3 0.14 0.41 0.49 o 6 4 3 7.17 8.80 0.80 o 7 4 3 0.00 1.42 0.73 o 8 4 3 2.85 4.91 1.21 o -9 5 3 0.12 0.15 1.25 o -8 5 3 1.71 3.16 0.85 o -7 5 3 49.34 45.68 1.92 o -6 5 3 22.83 20.04 1.07 o -5 5 3 4.16 3.71 0.61 o -4 5 3 28.46 23.20 0.96 o -3 5 3 37.32 38.60 1.03 o -2 5 3 0.54 0.78 0.37 o -1 5 3 64.32 59.79 1.27 o 0 5 3 2.63 2.73 0.45 o 1 5 3 66.79 62.77 1.32 o 2 5 3 2.37 3.08 0.49 o 3 5 3 5.60 5.07 0.71 o 4 5 3 3.73 4.96 1.02 o 5 5 3 0.42 0.08 0.68 o 6 5 3 0.23 0.90 0.73 o 7 5 3 5.51 7.33 1.33 o -8 6 3 0.00 2.29 1.52 o -7 6 3 1.52 1.72 0.97 o -6 6 3 0.12 -0.06 0.74 o -5 6 3 26.35 27.21 1.63 o -4 6 3 32.14 32.62 1.30 o -3 6 3 40.72 41.78 1.43 o -2 6 3 20.76 20.45 1.15 o -1 6 3 38.60 35.78 1.11 o 0 6 3 0.01 0.62 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