#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/63/2206302.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206302_Fobs loop_ _publ_author_name 'Santos, Isabel C.' 'Belo, Dulce' 'Mendon\,ca, Joana' 'Figueira, Mauro Jo\~ao' 'Almeida, Manuel' 'Rovira, Concepcion' _publ_section_title ; 5,6-Dihydrothieno[2,3-d][1,3]dithiol-2-one ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2161 _journal_page_last o2163 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.651 _cell_angle_gamma 90.000 _cell_length_a 4.0743 _cell_length_b 11.1543 _cell_length_c 14.7779 _exptl_crystal_F_000 360.00 _reflns_d_resolution_high 0.7832 _[local]_cod_data_source_file su6203Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' betonab in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 104.02 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1101.21 1197.30 5.33 o 2 0 0 61.19 50.85 4.18 o 3 0 0 559.65 594.99 12.22 o 4 0 0 0.09 0.00 6.72 o 5 0 0 104.24 115.29 7.60 o 1 1 0 10819.91 10711.28 214.30 o 2 1 0 157.69 157.05 4.64 o 3 1 0 1.93 8.99 4.03 o 4 1 0 136.81 123.13 11.54 o 5 1 0 3.20 1.94 3.03 o 0 2 0 3275.19 3333.81 10.07 o 1 2 0 3647.38 3827.84 99.11 o 2 2 0 106.92 132.48 4.08 o 3 2 0 144.29 152.54 5.80 o 4 2 0 32.05 44.93 7.41 o 5 2 0 1.11 8.35 5.10 o 1 3 0 22.35 38.23 2.76 o 2 3 0 113.05 137.77 4.16 o 3 3 0 351.55 389.97 7.31 o 4 3 0 93.93 87.15 5.95 o 5 3 0 10.20 16.58 5.98 o 0 4 0 300.89 353.42 5.74 o 1 4 0 728.31 714.10 5.77 o 2 4 0 2976.10 3104.56 38.25 o 3 4 0 61.50 66.65 5.28 o 4 4 0 6.44 10.48 4.76 o 1 5 0 781.54 811.15 7.76 o 2 5 0 1451.77 1364.18 15.30 o 3 5 0 841.28 847.35 9.87 o 4 5 0 60.80 63.53 5.89 o 0 6 0 76.84 62.26 4.47 o 1 6 0 1632.17 1601.92 9.87 o 2 6 0 202.45 192.79 5.56 o 4 6 0 28.43 35.38 10.52 o 1 7 0 360.64 338.03 5.95 o 2 7 0 120.18 124.19 5.32 o 3 7 0 0.01 2.77 2.89 o 4 7 0 55.55 68.69 6.26 o 0 8 0 19.45 6.84 4.96 o 1 8 0 81.15 83.72 4.65 o 2 8 0 79.45 82.26 5.02 o 3 8 0 9.44 12.94 4.46 o 4 8 0 3.72 1.05 7.68 o 1 9 0 667.07 615.85 11.90 o 2 9 0 1.06 0.00 8.71 o 3 9 0 181.13 175.65 7.80 o 4 9 0 75.92 75.32 6.82 o 0 10 0 871.19 856.90 14.04 o 1 10 0 108.31 101.08 5.27 o 2 10 0 0.65 0.06 1.56 o 3 10 0 88.66 87.51 6.19 o 1 11 0 1.81 0.92 2.51 o 2 11 0 336.89 342.33 11.49 o 3 11 0 119.20 140.73 6.95 o 0 12 0 333.83 336.02 11.19 o 1 12 0 143.20 165.75 15.63 o 2 12 0 172.37 195.19 7.30 o 1 13 0 130.70 137.64 6.69 o 2 13 0 77.66 69.64 8.58 o 0 14 0 14.69 18.07 7.04 o -5 1 1 12.14 6.96 7.25 o -4 1 1 178.03 175.63 9.54 o -3 1 1 97.20 98.57 7.35 o -2 1 1 110.01 88.05 5.32 o 1 1 1 1541.81 1466.63 9.18 o 2 1 1 1270.83 1490.10 12.63 o 3 1 1 109.02 109.69 7.53 o 4 1 1 0.01 3.31 5.24 o 5 1 1 116.20 133.45 10.57 o -5 2 1 1.50 27.02 8.16 o -4 2 1 2.27 0.21 2.14 o -3 2 1 234.32 195.51 8.23 o -2 2 1 881.93 793.66 9.82 o 0 2 1 1482.50 1487.57 7.57 o 1 2 1 7340.76 7178.04 20.31 o 2 2 1 81.45 80.44 5.27 o 3 2 1 294.93 281.68 9.51 o 4 2 1 263.98 261.57 10.57 o 5 2 1 1.58 0.00 4.91 o -5 3 1 1.60 0.30 2.81 o -4 3 1 154.49 151.13 9.38 o -3 3 1 578.56 553.12 11.79 o -2 3 1 10.05 15.31 4.43 o 1 3 1 82.20 158.99 4.95 o 2 3 1 452.39 382.69 8.10 o 3 3 1 0.13 10.83 6.02 o 4 3 1 291.87 279.13 10.93 o 5 3 1 0.86 0.00 7.85 o -4 4 1 6.30 2.60 5.06 o -3 4 1 6.53 14.63 6.16 o -2 4 1 2835.81 2799.59 18.46 o -1 4 1 1154.21 1143.61 10.32 o 0 4 1 5477.94 5618.77 19.61 o 1 4 1 519.86 520.30 7.46 o 2 4 1 158.08 150.85 6.70 o 3 4 1 898.97 882.61 14.24 o 4 4 1 41.25 24.69 7.91 o -4 5 1 13.81 12.70 6.91 o -3 5 1 72.07 72.26 7.41 o -2 5 1 0.82 0.00 4.17 o -1 5 1 314.56 328.48 6.71 o 0 5 1 179.59 202.58 5.27 o 1 5 1 855.40 885.85 9.73 o 2 5 1 23.07 17.79 5.51 o 3 5 1 124.40 127.97 8.39 o 4 5 1 1.36 18.91 7.11 o -4 6 1 2.09 0.00 6.24 o -3 6 1 104.28 100.53 7.86 o -2 6 1 36.94 28.52 5.82 o -1 6 1 148.88 171.03 6.27 o 0 6 1 161.60 148.73 5.58 o 1 6 1 69.17 62.77 5.01 o 2 6 1 600.32 583.26 11.06 o 3 6 1 195.94 207.58 9.42 o 4 6 1 152.37 158.44 9.61 o -4 7 1 3.45 4.80 5.82 o -3 7 1 3.43 5.08 5.26 o -2 7 1 130.97 103.83 7.33 o -1 7 1 57.36 61.92 6.00 o 0 7 1 940.11 832.19 10.69 o 1 7 1 2361.78 2150.38 17.19 o 2 7 1 23.43 18.16 6.13 o 3 7 1 285.68 281.68 10.24 o 4 7 1 33.99 20.75 8.04 o -4 8 1 72.71 76.01 9.50 o -3 8 1 539.88 509.91 12.79 o -2 8 1 534.97 510.40 11.33 o -1 8 1 478.44 485.60 10.57 o 0 8 1 1945.51 1915.60 17.17 o 1 8 1 769.77 751.26 11.95 o 2 8 1 1931.26 1958.76 20.26 o 3 8 1 22.63 10.76 6.37 o 4 8 1 42.66 63.29 8.67 o -4 9 1 144.46 134.71 10.63 o -3 9 1 200.78 197.65 10.42 o -2 9 1 109.86 101.85 7.48 o -1 9 1 465.57 486.08 11.06 o 0 9 1 1255.05 1309.94 15.77 o 1 9 1 2382.07 2315.14 20.98 o 2 9 1 19.49 24.69 6.50 o 3 9 1 69.36 83.60 8.37 o -3 10 1 8.62 9.58 6.47 o -2 10 1 25.28 28.40 6.62 o -1 10 1 87.79 91.76 7.10 o 0 10 1 227.51 234.79 9.01 o 1 10 1 4.67 0.00 2.79 o 2 10 1 367.91 380.99 11.06 o 3 10 1 118.12 116.41 9.17 o -3 11 1 0.48 1.09 4.09 o -2 11 1 137.07 134.21 9.09 o -1 11 1 11.18 9.64 5.49 o 0 11 1 153.70 158.44 8.50 o 1 11 1 27.57 32.37 6.20 o 2 11 1 198.41 177.36 9.58 o 3 11 1 157.23 174.18 11.22 o -2 12 1 97.24 93.02 9.04 o -1 12 1 1.76 3.28 4.96 o 0 12 1 165.50 166.22 9.28 o 1 12 1 8.32 9.92 6.25 o 2 12 1 17.17 10.40 7.03 o -2 13 1 0.01 3.72 5.84 o -1 13 1 1099.15 1186.76 19.53 o 0 13 1 46.52 59.54 7.73 o 1 13 1 4.35 13.41 6.54 o 2 13 1 331.13 323.75 12.95 o 0 14 1 99.19 127.23 9.58 o -5 0 2 100.06 92.82 10.29 o -4 0 2 240.21 251.79 10.02 o -3 0 2 92.33 86.62 7.30 o -2 0 2 4379.27 4397.82 20.24 o -1 0 2 2228.43 2167.60 11.16 o 2 0 2 1931.53 2182.85 15.27 o 3 0 2 48.78 32.37 7.07 o 4 0 2 3.01 6.62 6.22 o 5 0 2 23.48 34.63 9.11 o -5 1 2 0.02 13.97 7.90 o -4 1 2 41.65 46.99 7.32 o -3 1 2 700.98 703.07 12.14 o -2 1 2 331.71 402.56 7.87 o -1 1 2 435.58 389.54 6.02 o 1 1 2 4980.15 5574.74 17.90 o 2 1 2 2022.83 2017.07 14.68 o 3 1 2 631.35 607.71 11.82 o 4 1 2 10.08 23.10 7.02 o 5 1 2 3.96 0.00 7.51 o -5 2 2 0.47 1.41 4.87 o -4 2 2 2.39 0.21 2.15 o -3 2 2 6.06 15.92 6.18 o -2 2 2 2.81 0.19 1.54 o -1 2 2 1084.98 1055.46 8.49 o 0 2 2 111.19 115.01 3.50 o 1 2 2 0.20 0.00 3.08 o 2 2 2 4041.15 4183.67 21.15 o 3 2 2 13.21 2.71 4.92 o 4 2 2 475.73 486.56 12.98 o 5 2 2 0.02 21.85 8.86 o -5 3 2 50.21 34.63 9.36 o -4 3 2 31.78 33.87 7.61 o -3 3 2 235.54 264.74 9.22 o -2 3 2 3.79 0.00 2.54 o -1 3 2 1379.94 1514.59 11.02 o 0 3 2 116.98 129.95 4.23 o 1 3 2 692.89 614.19 7.57 o 2 3 2 789.52 760.86 10.23 o 3 3 2 865.27 935.83 14.00 o 4 3 2 31.99 31.50 7.95 o -4 4 2 161.62 152.47 9.95 o -3 4 2 174.53 174.47 8.63 o -2 4 2 416.41 465.64 8.93 o -1 4 2 3330.15 3356.50 16.41 o 0 4 2 3757.54 3827.84 16.18 o 1 4 2 496.21 537.34 7.58 o 2 4 2 45.29 59.03 5.86 o 3 4 2 172.65 163.15 8.91 o 4 4 2 6.29 8.09 6.45 o -4 5 2 640.74 632.69 15.35 o -3 5 2 207.17 205.38 9.06 o -2 5 2 888.39 896.91 11.75 o -1 5 2 2908.08 3015.82 17.96 o 0 5 2 810.83 716.42 8.75 o 1 5 2 977.78 915.29 10.55 o 2 5 2 4.90 19.00 5.32 o 3 5 2 230.45 231.13 9.61 o 4 5 2 67.46 80.44 8.80 o -4 6 2 12.59 0.00 5.83 o -3 6 2 58.08 50.03 7.09 o -2 6 2 68.70 58.86 6.02 o -1 6 2 455.59 465.16 8.46 o 0 6 2 3321.53 3402.11 19.07 o 1 6 2 355.73 324.93 7.86 o 2 6 2 70.42 65.92 6.37 o 3 6 2 11.46 5.59 5.72 o 4 6 2 0.05 3.43 5.57 o -4 7 2 26.52 14.47 7.38 o -3 7 2 162.70 172.74 9.17 o -2 7 2 9.75 0.00 4.00 o -1 7 2 439.64 431.03 9.50 o 0 7 2 605.20 580.62 9.98 o 1 7 2 604.22 594.36 10.63 o 2 7 2 470.40 415.78 10.67 o 3 7 2 51.17 51.74 7.21 o 4 7 2 3.70 10.40 7.10 o -4 8 2 30.40 33.61 8.09 o -3 8 2 1.99 2.33 4.45 o -2 8 2 154.90 137.25 8.17 o -1 8 2 78.57 72.26 6.68 o 0 8 2 2.86 0.00 3.50 o 1 8 2 57.07 52.69 6.33 o 2 8 2 160.31 146.34 8.43 o 3 8 2 47.73 46.99 7.47 o 4 8 2 0.93 13.81 7.29 o -4 9 2 22.47 16.97 7.54 o -3 9 2 123.95 126.74 9.07 o -2 9 2 231.56 206.95 9.41 o -1 9 2 17.59 12.93 5.57 o 0 9 2 623.01 627.21 12.01 o 1 9 2 39.06 26.69 6.41 o 2 9 2 353.55 372.52 10.51 o 3 9 2 0.04 0.00 5.91 o -3 10 2 1.07 7.07 6.08 o -2 10 2 198.97 199.80 9.24 o -1 10 2 11.17 9.18 5.29 o 0 10 2 177.00 181.45 8.52 o 1 10 2 827.24 838.49 14.51 o 2 10 2 0.41 11.41 5.89 o 3 10 2 18.40 8.53 6.82 o -3 11 2 7.58 9.85 6.43 o -2 11 2 12.28 12.01 6.65 o -1 11 2 339.91 357.95 10.73 o 0 11 2 10.57 23.62 5.72 o 1 11 2 264.98 247.31 9.94 o 2 11 2 51.81 69.87 7.47 o 3 11 2 103.94 115.23 9.82 o -2 12 2 373.40 349.33 12.22 o -1 12 2 87.58 81.43 8.66 o 0 12 2 497.59 546.47 13.24 o 1 12 2 122.96 106.29 8.54 o 2 12 2 0.01 0.00 0.12 o -2 13 2 49.75 47.89 7.99 o -1 13 2 194.41 207.58 10.99 o 0 13 2 35.35 30.29 7.55 o 1 13 2 106.57 105.61 8.96 o 0 14 2 1.42 0.00 6.47 o -5 1 3 29.56 29.69 9.38 o -4 1 3 39.70 39.96 7.85 o -3 1 3 171.10 151.93 8.33 o -2 1 3 1613.98 1783.44 13.81 o -1 1 3 66.74 51.89 4.24 o 0 1 3 57.21 65.04 3.16 o 1 1 3 614.49 565.49 7.26 o 2 1 3 1085.30 1142.88 11.79 o 3 1 3 923.86 937.84 14.68 o 4 1 3 10.25 5.64 6.21 o 5 1 3 0.00 0.00 7.96 o -5 2 3 11.63 3.93 6.88 o -4 2 3 94.11 96.42 9.42 o -3 2 3 209.65 181.75 8.52 o -1 2 3 25.71 66.28 4.43 o 1 2 3 8.18 6.34 3.46 o 2 2 3 3757.82 4028.65 22.14 o 3 2 3 448.78 511.39 11.83 o 5 2 3 71.55 67.17 10.36 o -5 3 3 35.00 45.95 9.61 o -4 3 3 3.51 13.73 6.78 o -3 3 3 1314.41 1407.15 16.35 o -2 3 3 0.49 2.78 3.78 o -1 3 3 69.60 114.77 4.67 o 0 3 3 3881.17 3722.05 15.96 o 1 3 3 514.12 464.70 7.04 o 2 3 3 7.05 14.55 4.99 o 3 3 3 10.29 12.47 6.46 o 4 3 3 46.58 33.11 8.41 o -4 4 3 677.04 663.20 15.16 o -3 4 3 192.44 195.82 8.85 o -2 4 3 501.27 531.80 9.55 o -1 4 3 2073.62 2075.24 13.90 o 0 4 3 973.41 1055.46 9.20 o 1 4 3 2557.06 2489.25 15.23 o 2 4 3 265.27 257.00 7.68 o 3 4 3 209.99 213.59 9.24 o 4 4 3 76.55 83.01 8.93 o -4 5 3 57.29 46.55 8.33 o -3 5 3 64.45 53.32 7.32 o -2 5 3 8.68 12.63 4.95 o -1 5 3 225.42 264.04 6.38 o 0 5 3 659.26 657.04 8.39 o 1 5 3 1888.33 1874.79 15.10 o 2 5 3 199.18 192.47 7.86 o 3 5 3 141.39 134.21 8.59 o 4 5 3 6.00 6.01 6.52 o -4 6 3 25.57 23.30 7.79 o -3 6 3 265.96 238.15 9.75 o -2 6 3 86.15 104.72 7.14 o -1 6 3 769.98 613.64 9.72 o 0 6 3 2189.77 2430.87 17.20 o 1 6 3 339.02 341.23 8.05 o 2 6 3 849.76 807.23 12.39 o 3 6 3 201.97 183.80 9.45 o 4 6 3 323.99 329.67 12.66 o -4 7 3 34.31 26.01 7.67 o -3 7 3 50.94 39.27 7.23 o -2 7 3 35.42 32.48 6.21 o -1 7 3 2024.61 1924.19 17.21 o 0 7 3 405.17 380.13 8.50 o 1 7 3 29.71 32.48 5.84 o 2 7 3 280.08 277.67 9.44 o 3 7 3 295.74 290.90 10.40 o 4 7 3 99.74 108.32 9.98 o -4 8 3 95.17 86.42 9.53 o -3 8 3 4.47 1.07 3.81 o -2 8 3 1006.54 987.89 15.07 o -1 8 3 165.80 167.35 7.90 o 0 8 3 295.54 298.38 8.66 o 1 8 3 228.26 215.50 8.01 o 2 8 3 50.83 48.04 7.10 o 3 8 3 430.84 445.17 12.41 o 4 8 3 42.77 69.33 8.71 o -3 9 3 296.27 289.05 11.12 o -2 9 3 68.45 77.93 7.32 o -1 9 3 917.26 873.56 14.17 o 0 9 3 97.86 106.06 7.41 o 1 9 3 36.76 33.11 6.40 o 2 9 3 327.47 319.06 10.51 o 3 9 3 51.95 56.55 7.86 o -3 10 3 14.25 11.19 6.92 o -2 10 3 137.74 121.40 8.65 o -1 10 3 176.68 164.54 8.39 o 0 10 3 62.04 58.36 6.83 o 1 10 3 0.12 0.19 1.84 o 2 10 3 365.67 335.63 11.58 o 3 10 3 11.61 18.34 7.47 o -3 11 3 2.99 8.03 6.54 o -2 11 3 180.54 187.36 9.85 o -1 11 3 65.02 61.06 7.33 o 0 11 3 114.97 101.18 7.90 o 1 11 3 756.04 756.65 14.99 o 2 11 3 10.57 13.17 6.72 o 3 11 3 332.97 293.13 13.06 o -2 12 3 8.62 0.00 3.09 o -1 12 3 0.71 1.44 4.16 o 0 12 3 47.59 54.75 7.58 o 1 12 3 50.66 33.49 7.70 o 2 12 3 215.23 253.86 11.12 o -2 13 3 2.70 11.56 6.89 o -1 13 3 4.20 3.47 5.61 o 0 13 3 768.49 856.90 17.22 o 1 13 3 124.12 126.74 9.57 o 0 14 3 64.09 73.94 8.81 o -5 0 4 80.84 57.20 10.55 o -4 0 4 450.78 434.66 12.27 o -3 0 4 225.21 203.83 8.72 o -2 0 4 202.16 279.50 7.29 o -1 0 4 3557.34 3247.53 14.91 o 1 0 4 10.25 33.49 4.16 o 2 0 4 509.14 551.58 9.22 o 3 0 4 85.01 91.35 8.12 o 4 0 4 0.67 0.00 5.49 o -5 1 4 239.75 259.46 12.99 o -4 1 4 288.62 275.86 11.58 o -3 1 4 180.17 166.78 8.73 o -2 1 4 9.91 59.03 5.36 o -1 1 4 385.30 421.13 6.71 o 0 1 4 7.65 29.69 3.56 o 2 1 4 385.52 518.31 9.43 o 3 1 4 3.85 10.69 6.20 o 4 1 4 28.28 44.05 8.10 o -5 2 4 40.27 49.41 9.95 o -4 2 4 4.60 3.28 5.80 o -3 2 4 932.55 963.38 14.21 o -2 2 4 0.79 0.21 1.73 o -1 2 4 855.07 970.84 9.51 o 0 2 4 6794.00 6677.40 19.60 o 1 2 4 174.30 164.82 5.32 o 2 2 4 1561.96 1532.46 14.50 o 3 2 4 436.83 430.57 11.31 o 4 2 4 180.19 163.98 10.05 o -5 3 4 0.19 1.48 5.27 o -4 3 4 38.07 22.89 7.83 o -3 3 4 88.49 96.63 8.36 o -2 3 4 2304.85 2436.24 17.21 o -1 3 4 773.77 743.52 8.92 o 0 3 4 192.12 253.86 5.56 o 1 3 4 771.61 881.32 9.70 o 2 3 4 18.76 18.16 5.11 o 3 3 4 1272.09 1276.25 17.13 o 4 3 4 168.77 165.09 10.08 o -4 4 4 357.60 338.42 12.03 o -3 4 4 29.03 22.38 7.01 o -2 4 4 764.91 690.41 10.88 o -1 4 4 22.94 75.63 4.74 o 0 4 4 224.78 173.61 5.17 o 1 4 4 708.05 671.08 9.04 o 2 4 4 249.70 260.16 8.09 o 3 4 4 0.36 0.00 5.36 o 4 4 4 87.18 92.19 9.20 o -4 5 4 47.14 66.45 8.35 o -3 5 4 1554.10 1556.44 18.05 o -2 5 4 183.30 185.88 7.44 o -1 5 4 54.15 97.06 5.15 o 0 5 4 643.24 829.06 10.04 o 1 5 4 312.90 242.53 6.79 o 2 5 4 227.95 203.52 8.09 o 3 5 4 94.67 98.57 8.01 o 4 5 4 116.44 151.93 9.67 o -3 6 4 0.10 0.00 4.36 o -2 6 4 783.90 737.59 12.44 o 0 6 4 445.02 397.32 8.25 o 1 6 4 587.66 585.36 10.02 o 2 6 4 393.82 390.41 10.33 o 3 6 4 0.04 9.31 5.91 o 4 6 4 102.46 108.55 9.76 o -4 7 4 14.29 11.64 7.21 o -3 7 4 45.94 51.58 7.20 o -2 7 4 446.95 427.42 10.82 o -1 7 4 94.17 89.08 6.58 o 0 7 4 1053.69 1056.87 12.76 o 1 7 4 741.75 707.12 11.59 o 2 7 4 348.00 316.73 10.08 o 3 7 4 374.16 371.69 11.34 o 4 7 4 3.41 0.00 7.92 o -4 8 4 49.93 25.80 8.63 o -3 8 4 18.20 20.56 6.72 o -2 8 4 8.05 2.33 4.39 o -1 8 4 566.27 579.57 11.54 o 0 8 4 37.67 35.01 5.81 o 1 8 4 27.79 32.00 6.05 o 2 8 4 155.66 151.66 8.33 o 3 8 4 45.24 48.80 7.61 o 4 8 4 10.68 17.06 8.20 o -3 9 4 83.85 109.24 8.88 o -2 9 4 156.58 157.62 8.75 o -1 9 4 18.14 25.68 5.96 o 0 9 4 222.59 238.48 8.75 o 1 9 4 244.06 233.79 9.00 o 2 9 4 21.50 43.76 6.63 o 3 9 4 132.05 153.00 9.98 o -3 10 4 3.17 4.89 5.69 o -2 10 4 129.16 144.24 8.90 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