#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/63/2206312.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206312_Fobs loop_ _publ_author_name 'Messouri, Ibtissam' 'El Bali, Brahim' 'Capitelli, Francesco' 'Piniella, Juan F.' 'Lachkar, Mohammed' 'Slimani, Zineb' _publ_section_title ; Diammonium tris[hexaaquamagnesium(II)] tetrakis[hydrogenphosphate(III)], (NH~4~)~2~[Mg(H~2~O)~6~]~3~(HPO~3~)~4~ ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i129 _journal_page_last i131 _journal_volume 61 _journal_year 2005 _space_group_IT_number 12 _symmetry_space_group_name_Hall '-C 2y' _symmetry_space_group_name_H-M 'C 1 2/m 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.377 _cell_angle_gamma 90.000 _cell_length_a 34.3300 _cell_length_b 7.0380 _cell_length_c 6.1666 _exptl_crystal_F_000 796.00 _reflns_d_resolution_high 0.7699 _[local]_cod_data_source_file wm6070Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bali 10 (ex bali24)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 153.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, -y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 10 0 0 4179.76 4374.45 42.29 o 14 0 0 4164.63 4742.77 102.40 o 16 0 0 17.97 13.72 1.75 o 18 0 0 3565.89 3750.70 57.37 o 20 0 0 2786.44 2813.82 27.85 o 22 0 0 156.33 160.54 3.62 o 24 0 0 10842.24 10218.90 192.60 o 26 0 0 714.85 880.20 15.09 o 28 0 0 147.21 152.60 7.35 o 30 0 0 2302.12 2108.12 34.18 o 32 0 0 139.66 165.35 7.66 o 34 0 0 11.61 11.72 5.09 o 36 0 0 77.17 59.43 6.20 o 38 0 0 43.28 51.03 6.16 o 40 0 0 0.93 -0.97 5.65 o 44 0 0 382.58 393.59 14.18 o 7 1 0 432.08 544.62 7.95 o 11 1 0 328.40 286.44 2.81 o 13 1 0 7.60 7.96 1.02 o 15 1 0 696.38 935.49 7.63 o 17 1 0 4060.24 4054.22 28.85 o 19 1 0 200.11 223.54 3.16 o 21 1 0 1830.84 1971.02 17.73 o 23 1 0 20.06 33.93 2.25 o 25 1 0 2414.46 2357.76 20.36 o 27 1 0 1204.50 1267.16 18.23 o 29 1 0 698.45 726.97 8.26 o 31 1 0 119.87 104.26 3.28 o 33 1 0 1978.08 1921.86 23.06 o 35 1 0 28.73 38.69 3.38 o 37 1 0 223.18 226.14 7.12 o 39 1 0 452.08 435.42 9.87 o 41 1 0 692.67 715.82 18.71 o 43 1 0 82.07 84.74 5.48 o 0 2 0 7711.49 7518.42 134.21 o 2 2 0 222.28 222.87 2.32 o 4 2 0 1267.00 1349.92 8.14 o 6 2 0 7995.28 8331.20 73.37 o 8 2 0 3142.79 3138.02 18.46 o 10 2 0 376.76 411.61 3.22 o 12 2 0 7059.64 7153.65 63.18 o 14 2 0 745.36 753.17 8.09 o 16 2 0 236.38 214.01 2.24 o 18 2 0 2113.27 2171.90 13.63 o 20 2 0 4154.68 4093.22 29.68 o 22 2 0 194.50 207.16 3.52 o 24 2 0 1081.69 1049.96 8.81 o 26 2 0 800.52 766.02 8.24 o 28 2 0 200.39 214.73 4.11 o 30 2 0 50.46 47.26 2.46 o 32 2 0 2021.83 1969.09 23.34 o 34 2 0 7.04 10.92 3.94 o 36 2 0 152.26 147.30 5.60 o 38 2 0 42.96 45.30 4.23 o 40 2 0 6.29 16.63 4.53 o 42 2 0 1821.82 1796.14 28.39 o 1 3 0 18.72 31.55 3.20 o 3 3 0 121.04 117.42 1.93 o 5 3 0 103.25 149.88 2.69 o 7 3 0 32.92 50.49 1.21 o 9 3 0 5466.90 5182.71 31.47 o 11 3 0 771.51 789.57 5.60 o 13 3 0 240.47 250.24 2.73 o 15 3 0 7611.46 7421.62 47.91 o 17 3 0 186.85 198.75 6.38 o 19 3 0 853.03 802.91 7.20 o 21 3 0 264.73 276.77 3.92 o 23 3 0 1318.41 1321.36 10.75 o 25 3 0 1546.42 1546.11 12.48 o 27 3 0 1873.60 1870.26 14.51 o 29 3 0 992.34 1002.09 10.67 o 31 3 0 37.31 37.12 4.02 o 33 3 0 2044.24 2072.92 37.94 o 35 3 0 553.47 528.73 10.65 o 37 3 0 315.19 346.18 9.00 o 39 3 0 2242.40 2241.62 28.39 o 41 3 0 1947.97 1958.47 29.04 o 2 4 0 13.70 45.64 10.95 o 4 4 0 10.21 11.47 1.27 o 6 4 0 4773.39 4942.33 29.88 o 8 4 0 1925.78 1988.25 12.54 o 10 4 0 226.98 208.89 3.01 o 12 4 0 4153.48 4040.56 26.30 o 14 4 0 1.14 5.92 1.32 o 16 4 0 37.37 37.50 3.59 o 18 4 0 115.38 117.01 2.78 o 20 4 0 1620.54 1595.34 12.55 o 22 4 0 144.40 145.33 3.34 o 24 4 0 5222.12 5267.88 42.52 o 26 4 0 6.10 13.46 3.28 o 28 4 0 215.84 201.72 3.95 o 30 4 0 1423.81 1418.83 15.31 o 32 4 0 690.56 693.96 12.19 o 34 4 0 0.10 -2.42 3.77 o 36 4 0 5.58 13.97 4.09 o 38 4 0 40.02 40.53 6.48 o 40 4 0 42.35 33.46 4.86 o 1 5 0 734.65 726.89 6.82 o 3 5 0 576.45 621.14 5.49 o 5 5 0 1963.64 1922.58 13.97 o 7 5 0 42.92 64.06 3.66 o 9 5 0 6295.47 6109.54 37.27 o 11 5 0 212.44 226.09 3.38 o 13 5 0 68.83 64.22 3.19 o 15 5 0 708.73 679.48 7.16 o 17 5 0 2985.91 2963.16 22.91 o 19 5 0 11.32 7.60 2.08 o 21 5 0 604.15 566.55 6.94 o 23 5 0 0.06 -0.89 2.24 o 25 5 0 668.04 659.96 7.46 o 27 5 0 2140.27 2159.75 16.99 o 29 5 0 549.70 542.06 8.41 o 31 5 0 56.26 54.40 7.05 o 33 5 0 920.69 879.17 22.05 o 35 5 0 29.84 30.13 4.38 o 37 5 0 83.00 81.61 5.13 o 0 6 0 19505.72 18666.83 333.48 o 2 6 0 7.63 51.03 13.98 o 4 6 0 816.00 830.48 7.13 o 6 6 0 281.67 301.44 5.09 o 8 6 0 3760.54 3687.03 29.55 o 10 6 0 268.01 268.82 4.95 o 12 6 0 931.09 874.02 12.58 o 14 6 0 171.83 170.65 3.67 o 16 6 0 10.08 13.83 8.21 o 18 6 0 2650.96 2625.21 24.04 o 20 6 0 1442.84 1411.21 12.37 o 22 6 0 23.88 23.88 2.63 o 24 6 0 1002.64 983.04 9.85 o 26 6 0 25.36 29.98 2.84 o 28 6 0 43.33 46.28 4.55 o 30 6 0 8.01 5.32 5.36 o 32 6 0 138.44 129.98 8.48 o 1 7 0 88.15 77.51 3.92 o 3 7 0 744.60 761.04 8.98 o 5 7 0 169.35 166.34 5.41 o 7 7 0 13.43 12.14 4.25 o 9 7 0 3946.81 4024.66 44.60 o 11 7 0 102.45 133.88 5.47 o 13 7 0 7.71 14.97 4.72 o 15 7 0 2050.78 2123.54 20.80 o 17 7 0 543.85 548.80 8.28 o 19 7 0 55.22 51.23 3.27 o 21 7 0 287.63 300.33 6.04 o 23 7 0 42.92 53.38 3.94 o 25 7 0 337.97 335.58 21.83 o 27 7 0 282.52 307.12 8.11 o 0 8 0 2171.37 2091.75 32.67 o 2 8 0 4.04 8.60 3.75 o 4 8 0 1.56 0.82 3.29 o 6 8 0 793.03 790.09 12.12 o 8 8 0 280.64 274.66 6.98 o 10 8 0 1.85 0.69 3.43 o 12 8 0 6.74 16.75 5.85 o 14 8 0 92.80 104.40 5.04 o 16 8 0 42.12 34.67 5.62 o 18 8 0 9.56 10.13 3.70 o 20 8 0 574.14 550.59 18.20 o 1 9 0 4.09 4.61 10.59 o 3 9 0 185.84 179.27 6.46 o 5 9 0 54.23 49.72 4.55 o 7 9 0 2.39 4.67 3.09 o -44 0 1 5.13 1.88 5.29 o -42 0 1 35.90 35.97 6.60 o -40 0 1 460.76 442.26 13.78 o -38 0 1 1029.68 1033.46 22.97 o -36 0 1 96.11 109.47 7.15 o -34 0 1 614.30 628.17 15.66 o -32 0 1 358.58 377.89 11.82 o -30 0 1 388.23 417.44 17.12 o -28 0 1 12891.16 12096.90 219.36 o -26 0 1 151.79 165.75 5.58 o -24 0 1 894.12 892.25 8.64 o -22 0 1 2291.23 2163.62 23.23 o -20 0 1 1.62 4.02 2.21 o -18 0 1 4681.61 4732.75 38.58 o -16 0 1 1373.22 1506.83 13.93 o -14 0 1 487.14 410.04 4.23 o -12 0 1 1608.92 1954.52 14.85 o -10 0 1 1558.27 1717.55 19.99 o -8 0 1 2567.59 2419.60 39.14 o 10 0 1 1744.10 1883.49 28.42 o 14 0 1 396.45 322.69 6.96 o 16 0 1 358.28 346.66 7.75 o 18 0 1 367.77 337.31 8.20 o 20 0 1 1831.09 1953.88 28.95 o 22 0 1 1919.14 1943.36 30.19 o 24 0 1 479.93 521.25 12.23 o 26 0 1 3145.68 3052.11 47.69 o 28 0 1 130.00 137.89 7.00 o 30 0 1 121.54 129.29 6.42 o 32 0 1 1025.68 1090.69 21.62 o 34 0 1 632.76 625.18 15.64 o 36 0 1 361.57 381.28 12.78 o 38 0 1 134.96 115.47 8.31 o 42 0 1 225.41 220.18 10.17 o 44 0 1 0.62 2.08 6.02 o -43 1 1 29.63 31.14 6.98 o -41 1 1 1006.33 962.05 15.67 o -39 1 1 147.92 147.86 6.41 o -37 1 1 1148.31 1117.04 16.72 o -35 1 1 29.35 39.32 2.75 o -33 1 1 5.97 6.91 3.47 o -31 1 1 841.95 914.32 10.19 o -29 1 1 4675.42 4492.08 34.36 o -27 1 1 65.83 59.30 2.20 o -25 1 1 1344.04 1379.74 10.95 o -23 1 1 2117.86 2186.60 18.25 o -21 1 1 2171.89 2180.48 16.26 o -19 1 1 420.94 415.49 4.52 o -17 1 1 1605.94 1630.08 20.94 o -15 1 1 3017.77 3167.09 24.95 o -13 1 1 843.80 978.97 7.06 o -11 1 1 2478.61 2636.07 17.04 o -9 1 1 106.12 94.77 2.34 o -7 1 1 622.30 569.28 3.96 o -5 1 1 7287.01 6939.42 57.78 o 5 1 1 1931.00 2031.83 15.46 o 7 1 1 63.68 93.82 1.34 o 9 1 1 817.77 752.30 5.30 o 11 1 1 296.06 317.34 2.89 o 13 1 1 6756.24 6855.74 54.46 o 15 1 1 3537.20 3673.23 28.72 o 17 1 1 12438.72 11789.08 160.14 o 19 1 1 777.39 783.18 9.14 o 21 1 1 1717.06 1779.48 15.63 o 23 1 1 10146.30 9863.75 88.62 o 25 1 1 172.88 174.21 5.67 o 27 1 1 1913.02 1862.53 21.33 o 29 1 1 24.87 42.50 3.70 o 31 1 1 299.59 296.52 7.24 o 33 1 1 5.68 1.06 3.25 o 35 1 1 155.16 147.54 11.74 o 37 1 1 15.89 21.10 3.84 o 39 1 1 121.06 127.90 7.93 o 41 1 1 439.13 468.29 10.48 o 43 1 1 26.65 32.82 6.21 o -42 2 1 184.96 196.70 7.06 o -40 2 1 512.67 511.12 11.18 o -38 2 1 2061.84 2149.36 26.82 o -36 2 1 681.80 680.81 11.54 o -34 2 1 424.30 427.31 6.97 o -32 2 1 1241.36 1232.18 10.98 o -30 2 1 712.23 754.40 7.69 o -28 2 1 41.80 42.57 2.29 o -26 2 1 580.14 613.51 6.49 o -24 2 1 4249.17 4101.27 29.11 o -22 2 1 1818.83 1877.69 14.56 o -20 2 1 8013.31 7683.03 54.43 o -18 2 1 191.59 189.18 5.10 o -16 2 1 15926.20 14612.59 319.29 o -14 2 1 3940.67 3799.21 24.75 o -12 2 1 3678.85 3557.51 23.36 o -10 2 1 1781.09 1511.36 10.79 o -6 2 1 2104.86 1661.07 11.45 o -4 2 1 1954.75 1598.04 20.08 o 0 2 1 327.54 284.56 2.95 o 2 2 1 2212.37 1903.15 14.11 o 8 2 1 4786.85 3881.37 29.16 o 12 2 1 1391.19 1167.74 8.77 o 16 2 1 1992.76 1955.72 14.54 o 18 2 1 8726.86 8106.04 57.81 o 20 2 1 14.95 22.52 2.45 o 22 2 1 458.08 443.37 4.50 o 24 2 1 309.95 330.57 4.23 o 26 2 1 3376.33 3266.69 35.85 o 28 2 1 582.35 583.84 9.91 o 30 2 1 511.57 488.67 9.54 o 32 2 1 1238.23 1274.94 24.44 o 34 2 1 0.29 2.30 3.99 o 36 2 1 489.41 508.74 10.19 o 38 2 1 1266.75 1210.50 17.92 o 40 2 1 1108.54 1098.11 17.43 o 42 2 1 426.07 462.28 14.40 o -41 3 1 1087.84 1015.43 16.77 o -39 3 1 298.53 288.88 8.59 o -37 3 1 931.90 976.84 15.79 o -35 3 1 135.48 147.86 6.38 o -33 3 1 413.78 399.33 9.49 o -31 3 1 291.27 316.99 4.88 o -29 3 1 3387.69 3263.09 24.86 o -27 3 1 815.24 797.12 8.01 o -25 3 1 258.70 259.32 4.04 o -23 3 1 1108.02 1123.51 9.81 o -21 3 1 1793.28 1769.78 14.91 o -19 3 1 136.85 125.64 3.30 o -17 3 1 39.62 39.69 2.58 o -15 3 1 160.04 175.22 3.40 o -13 3 1 4366.69 4459.45 29.95 o -11 3 1 869.90 985.83 26.29 o -9 3 1 4933.52 5494.75 35.66 o -7 3 1 5103.26 5291.14 34.68 o -5 3 1 181.87 166.65 2.00 o -3 3 1 886.16 913.58 6.25 o -1 3 1 3872.84 4504.40 38.05 o 1 3 1 371.25 401.49 3.46 o 3 3 1 4.30 20.30 2.13 o 5 3 1 4362.81 4530.08 44.81 o 7 3 1 1340.61 1353.08 8.57 o 9 3 1 2053.99 2269.51 16.13 o 11 3 1 6007.14 6020.05 41.80 o 13 3 1 9642.18 9667.11 137.22 o 15 3 1 171.40 158.59 2.82 o 17 3 1 1210.77 1212.95 9.22 o 19 3 1 41.75 47.84 2.75 o 21 3 1 412.41 414.38 6.74 o 23 3 1 7113.84 7019.75 70.00 o 25 3 1 838.06 787.04 12.97 o 27 3 1 1682.66 1656.90 32.73 o 29 3 1 59.53 57.14 3.49 o 31 3 1 1886.05 1871.86 30.90 o 33 3 1 2.02 0.22 4.74 o 35 3 1 762.33 738.26 18.21 o 37 3 1 193.85 180.41 7.79 o 39 3 1 117.07 115.43 5.53 o 41 3 1 970.73 978.57 16.13 o -38 4 1 1111.65 1137.93 17.75 o -36 4 1 116.52 118.83 4.79 o -34 4 1 464.59 465.49 7.71 o -32 4 1 9.98 9.81 3.96 o -30 4 1 536.16 518.30 6.73 o -28 4 1 2904.93 2842.50 22.03 o -26 4 1 235.96 227.83 4.24 o -24 4 1 471.91 484.06 8.45 o -22 4 1 1536.68 1581.69 12.82 o -20 4 1 499.61 496.22 5.77 o -18 4 1 361.96 345.74 4.67 o -16 4 1 205.95 219.32 3.50 o -14 4 1 590.17 514.03 5.53 o -12 4 1 318.54 331.18 4.28 o -10 4 1 0.47 1.46 1.32 o -8 4 1 1181.95 1278.13 8.72 o -6 4 1 1308.16 1296.71 11.31 o -4 4 1 2444.95 2340.78 15.02 o -2 4 1 2007.75 2162.70 14.66 o 0 4 1 69.62 79.59 1.69 o 2 4 1 1775.84 1836.97 13.60 o 4 4 1 1382.54 1441.08 12.33 o 6 4 1 3456.47 3564.82 46.12 o 8 4 1 1130.39 1088.17 8.08 o 10 4 1 0.30 5.05 1.71 o 12 4 1 1203.26 1166.35 8.11 o 14 4 1 2805.14 2895.48 18.71 o 16 4 1 126.10 115.92 2.68 o 18 4 1 2177.60 2174.38 21.87 o 20 4 1 25.57 16.67 1.95 o 22 4 1 1032.21 1034.98 14.38 o 24 4 1 242.43 236.98 6.12 o 26 4 1 0.16 1.08 3.18 o 28 4 1 49.80 51.14 4.03 o 30 4 1 53.95 52.08 3.64 o 32 4 1 1109.32 1115.98 24.38 o 34 4 1 550.37 553.99 10.87 o 36 4 1 351.21 342.66 11.30 o 38 4 1 66.65 64.40 5.37 o -37 5 1 488.65 451.17 8.38 o -35 5 1 3.16 3.21 8.52 o -33 5 1 3.92 8.15 3.40 o -31 5 1 738.54 744.57 8.66 o -29 5 1 2498.29 2525.15 21.29 o -27 5 1 7.17 12.57 7.63 o -25 5 1 807.86 813.74 8.63 o -23 5 1 635.96 599.14 7.07 o -21 5 1 1842.94 1821.67 14.54 o -19 5 1 194.22 201.90 4.31 o -17 5 1 1980.17 2047.22 15.56 o -15 5 1 1589.12 1562.40 12.60 o -13 5 1 1204.55 1107.78 9.61 o -11 5 1 297.52 289.55 4.46 o -9 5 1 1988.54 1945.45 14.74 o -7 5 1 137.18 148.45 4.40 o -5 5 1 5050.43 5080.91 38.97 o -3 5 1 2.15 0.64 3.61 o -1 5 1 13020.28 12598.16 113.26 o 1 5 1 506.25 517.05 6.41 o 3 5 1 12176.55 11806.84 192.51 o 5 5 1 1022.91 1046.32 9.74 o 7 5 1 719.10 761.31 6.27 o 9 5 1 51.46 57.23 1.98 o 11 5 1 1993.98 1938.86 15.87 o 13 5 1 351.47 369.29 4.15 o 15 5 1 2854.44 2860.02 21.28 o 17 5 1 3274.48 3122.78 28.81 o 19 5 1 1015.52 1065.64 9.84 o 21 5 1 751.21 728.84 9.21 o 23 5 1 5289.14 5304.14 62.37 o 25 5 1 706.28 711.32 21.44 o 27 5 1 1329.63 1336.10 26.12 o 29 5 1 2.33 7.91 5.60 o 31 5 1 11.21 6.78 5.58 o 35 5 1 82.79 81.07 7.51 o -32 6 1 49.76 52.66 4.58 o -30 6 1 97.49 91.28 4.37 o -28 6 1 1038.25 1013.76 12.11 o -26 6 1 347.42 350.14 6.61 o -24 6 1 31.90 43.51 3.47 o -22 6 1 301.72 302.79 6.01 o -20 6 1 748.53 775.69 9.84 o -18 6 1 812.37 795.75 9.82 o -16 6 1 400.13 389.99 8.82 o -14 6 1 1323.61 1330.32 13.33 o -12 6 1 153.75 182.30 5.38 o -10 6 1 2068.20 2065.30 18.40 o -8 6 1 1592.34 1607.18 18.13 o -6 6 1 3481.24 3445.70 28.50 o -4 6 1 2.10 5.82 8.12 o -2 6 1 2324.32 2270.70 17.39 o 0 6 1 1124.24 1141.80 10.71 o 2 6 1 307.02 293.91 4.51 o 4 6 1 852.10 853.09 8.87 o 6 6 1 2547.11 2562.43 19.13 o 8 6 1 4616.54 4456.02 32.23 o 10 6 1 766.33 772.72 9.84 o 12 6 1 2090.48 1998.59 17.78 o 14 6 1 2254.65 2203.24 23.01 o 16 6 1 2.05 4.58 2.98 o 18 6 1 707.15 760.88 9.41 o 20 6 1 512.53 489.57 8.23 o 22 6 1 60.68 68.71 6.67 o 24 6 1 132.46 133.39 7.55 o 26 6 1 14.65 16.15 5.63 o 28 6 1 153.74 155.92 8.17 o 30 6 1 5.28 12.65 5.83 o 32 6 1 369.70 380.13 13.93 o -27 7 1 10.75 12.52 3.24 o -25 7 1 29.90 40.28 3.64 o -23 7 1 529.18 505.77 8.22 o -21 7 1 623.00 605.32 9.12 o -19 7 1 113.75 108.76 4.47 o -17 7 1 52.07 51.26 8.47 o -15 7 1 346.46 347.30 9.05 o -13 7 1 813.02 849.61 13.00 o -11 7 1 170.70 172.22 8.40 o -9 7 1 0.23 -0.96 2.51 o -7 7 1 397.14 415.69 8.73 o -5 7 1 82.51 85.16 4.35 o -3 7 1 4.44 8.46 3.53 o -1 7 1 48.59 45.79 3.33 o 1 7 1 48.41 56.29 4.24 o 3 7 1 922.69 909.89 7.93 o 5 7 1 247.07 257.59 3.98 o 7 7 1 257.15 257.49 4.95 o 9 7 1 37.65 39.52 2.91 o 11 7 1 162.51 156.89 4.83 o 13 7 1 1021.78 1009.67 11.38 o 15 7 1 311.14 313.85 6.21 o 17 7 1 1305.37 1211.52 15.92 o 19 7 1 45.00 35.80 6.58 o 21 7 1 406.93 394.19 13.00 o 23 7 1 1446.77 1442.60 29.39 o 25 7 1 104.65 106.08 8.28 o 27 7 1 577.05 564.93 16.28 o -20 8 1 657.89 655.34 12.04 o -18 8 1 30.80 30.06 6.10 o -16 8 1 500.16 501.81 10.12 o -14 8 1 383.71 384.91 8.81 o -12 8 1 719.40 706.12 12.01 o -10 8 1 10.06 20.23 7.32 o -8 8 1 740.56 717.46 11.80 o -6 8 1 320.69 338.40 8.13 o -4 8 1 184.53 197.83 6.32 o -2 8 1 916.00 890.39 13.49 o 0 8 1 134.39 132.19 4.46 o 2 8 1 72.32 82.15 5.90 o 4 8 1 708.95 697.07 9.36 o 6 8 1 1243.72 1231.96 13.24 o 8 8 1 102.90 105.85 4.47 o 10 8 1 206.29 208.59 9.83 o 12 8 1 259.52 247.95 8.90 o 14 8 1 1699.00 1641.56 20.77 o 16 8 1 208.60 203.64 7.57 o 20 8 1 0.47 -1.42 6.42 o -5 9 1 744.66 772.17 13.15 o -1 9 1 426.04 447.14 9.56 o 1 9 1 43.58 48.14 4.58 o 3 9 1 397.98 393.94 12.09 o 5 9 1 413.73 425.75 9.53 o -42 0 2 40.53 45.85 7.07 o -40 0 2 370.43 383.63 13.40 o -38 0 2 1145.64 1159.56 24.32 o -36 0 2 0.74 -1.71 3.01 o -34 0 2 2860.77 2853.19 47.69 o -32 0 2 794.62 840.50 11.80 o -30 0 2 1236.39 1241.36 23.62 o -28 0 2 15.77 18.76 3.08 o -26 0 2 1664.52 1679.22 18.41 o -24 0 2 369.24 381.83 5.02 o -22 0 2 4.92 5.20 1.37 o -20 0 2 1035.08 939.16 9.33 o -18 0 2 14498.15 13546.55 137.10 o -16 0 2 13646.94 12743.80 217.18 o -14 0 2 4298.32 4021.29 30.64 o -12 0 2 391.41 426.86 4.58 o -10 0 2 46.98 83.80 2.40 o -8 0 2 80.24 48.36 2.95 o -4 0 2 254.62 257.81 5.65 o -2 0 2 92.63 143.66 3.15 o 0 0 2 193.68 211.09 2.47 o 4 0 2 7722.18 7865.61 102.96 o 8 0 2 476.75 456.12 8.26 o 10 0 2 786.63 675.26 11.61 o 12 0 2 5289.60 5526.57 84.08 o 14 0 2 80.02 67.25 3.41 o 16 0 2 7141.48 6820.48 90.95 o 18 0 2 21590.17 19747.55 297.00 o 20 0 2 4866.00 5082.25 89.13 o 22 0 2 28.99 26.67 4.45 o 24 0 2 6971.83 6654.35 89.84 o 26 0 2 5396.32 5212.52 96.71 o 28 0 2 1.39 17.23 8.40 o 30 0 2 903.74 902.04 18.78 o 34 0 2 435.29 464.43 13.47 o 36 0 2 248.16 229.55 10.37 o 38 0 2 242.99 240.51 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