#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/63/2206329.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206329_Fobs loop_ _publ_author_name 'Sonar, Vijayakumar N.' 'Parkin, Sean' 'Crooks, Peter A.' _publ_section_title ; 6\a-Acetoxy-4,5\a-epoxy-3-methoxy-17-methylmorphin-7-ene ; _journal_coeditor_code AC6177 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2579 _journal_page_last o2581 _journal_volume 61 _journal_year 2005 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.6588 _cell_length_b 12.3368 _cell_length_c 15.4441 _exptl_crystal_F_000 728.00 _reflns_d_resolution_high .8411 _[local]_cod_data_source_file ac6177Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' k04243 - P212121' _shelx_refln_list_code 4 _shelx_f_calc_maximum 204.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1310.08 1257.12 31.49 o 4 0 0 8027.39 8639.74 186.34 o 6 0 0 119.56 162.72 21.00 o 8 0 0 32.05 39.37 26.24 o 10 0 0 109.66 73.49 49.86 o 1 1 0 5795.75 5332.92 107.60 o 2 1 0 693.26 645.62 13.12 o 3 1 0 1540.96 1501.19 28.87 o 4 1 0 27.46 28.87 7.87 o 5 1 0 224.37 259.82 13.12 o 6 1 0 563.19 593.13 26.24 o 7 1 0 37.17 36.74 15.75 o 8 1 0 489.09 448.78 31.49 o 9 1 0 70.76 65.61 26.24 o 10 1 0 24.71 -2.62 28.87 o 0 2 0 2334.59 2157.31 60.36 o 1 2 0 237.16 220.46 7.87 o 2 2 0 453.34 443.53 13.12 o 3 2 0 27.90 23.62 5.25 o 4 2 0 362.52 409.42 13.12 o 5 2 0 95.03 94.48 10.50 o 6 2 0 17.16 10.50 13.12 o 7 2 0 126.92 146.97 21.00 o 8 2 0 60.39 47.24 21.00 o 9 2 0 155.13 136.47 28.87 o 10 2 0 16.61 10.50 49.86 o 1 3 0 5013.69 4857.89 83.98 o 2 3 0 1044.58 1013.04 23.62 o 3 3 0 .92 5.25 5.25 o 4 3 0 684.26 734.85 26.24 o 5 3 0 216.32 230.95 13.12 o 6 3 0 .58 -5.25 10.50 o 7 3 0 32.94 28.87 15.75 o 8 3 0 129.47 104.98 21.00 o 9 3 0 26.92 28.87 26.24 o 10 3 0 83.90 55.11 36.74 o 0 4 0 10052.84 10004.46 238.83 o 1 4 0 4085.92 3755.61 65.61 o 2 4 0 99.77 99.73 7.87 o 3 4 0 10.22 7.87 5.25 o 4 4 0 289.87 359.55 18.37 o 5 4 0 433.49 459.28 21.00 o 6 4 0 106.97 104.98 15.75 o 7 4 0 24.55 2.62 15.75 o 8 4 0 30.43 28.87 23.62 o 9 4 0 23.64 31.49 36.74 o 1 5 0 1224.71 1306.98 26.24 o 2 5 0 134.06 123.35 7.87 o 3 5 0 68.11 57.74 7.87 o 4 5 0 111.03 112.85 13.12 o 5 5 0 32.76 23.62 10.50 o 6 5 0 36.26 23.62 13.12 o 7 5 0 80.93 49.86 18.37 o 8 5 0 585.91 530.14 44.62 o 9 5 0 .96 -15.75 36.74 o 0 6 0 25608.27 28903.25 742.72 o 1 6 0 3588.37 3789.73 68.24 o 2 6 0 41.96 41.99 7.87 o 3 6 0 39.80 39.37 7.87 o 4 6 0 233.18 233.58 15.75 o 5 6 0 458.31 448.78 23.62 o 6 6 0 45.41 57.74 15.75 o 7 6 0 307.57 291.32 31.49 o 8 6 0 97.11 83.98 36.74 o 9 6 0 .00 -23.62 39.37 o 1 7 0 985.56 1020.92 28.87 o 2 7 0 42.29 36.74 10.50 o 3 7 0 162.90 131.22 13.12 o 4 7 0 344.32 346.43 21.00 o 5 7 0 4.40 15.75 13.12 o 6 7 0 126.82 102.35 15.75 o 7 7 0 94.26 78.73 23.62 o 8 7 0 144.05 104.98 31.49 o 9 7 0 3.08 55.11 41.99 o 0 8 0 2700.14 2897.41 102.35 o 1 8 0 31.42 15.75 10.50 o 2 8 0 10.27 .00 10.50 o 3 8 0 .92 5.25 10.50 o 4 8 0 3361.45 3653.26 97.11 o 5 8 0 .02 15.75 18.37 o 6 8 0 133.12 125.97 34.12 o 7 8 0 23.69 34.12 26.24 o 8 8 0 2.96 36.74 31.49 o 1 9 0 499.83 524.89 26.24 o 2 9 0 53.54 31.49 13.12 o 3 9 0 37.51 2.62 15.75 o 4 9 0 335.31 359.55 36.74 o 5 9 0 310.99 267.70 34.12 o 6 9 0 5.98 5.25 26.24 o 7 9 0 69.96 49.86 41.99 o 8 9 0 5.82 .00 36.74 o 0 10 0 921.02 1026.17 62.99 o 1 10 0 47.16 15.75 21.00 o 2 10 0 382.26 388.42 26.24 o 3 10 0 342.84 299.19 31.49 o 4 10 0 4.30 -10.50 23.62 o 5 10 0 33.36 57.74 34.12 o 6 10 0 317.24 280.82 55.11 o 7 10 0 1.65 5.25 44.62 o 1 11 0 62.93 76.11 21.00 o 2 11 0 19.19 -7.87 23.62 o 3 11 0 7.96 -7.87 31.49 o 4 11 0 6.79 -10.50 28.87 o 5 11 0 34.29 -5.25 39.37 o 6 11 0 7.48 52.49 62.99 o 0 12 0 132.26 136.47 31.49 o 1 12 0 389.88 433.04 34.12 o 2 12 0 36.61 36.74 21.00 o 3 12 0 2.81 10.50 31.49 o 4 12 0 12.68 -5.25 52.49 o 5 12 0 15.71 26.24 41.99 o 1 13 0 3.13 -13.12 23.62 o 2 13 0 1.71 21.00 60.36 o 3 13 0 .72 -70.86 70.86 o 4 13 0 30.60 -36.74 86.61 o 0 14 0 121.90 78.73 52.49 o 1 14 0 106.09 55.11 47.24 o 2 14 0 27.17 49.86 57.74 o 3 14 0 50.25 104.98 76.11 o 1 0 1 9.52 13.12 2.62 o 2 0 1 393.26 396.29 10.50 o 3 0 1 148.42 136.47 7.87 o 4 0 1 441.72 501.27 15.75 o 5 0 1 381.96 372.67 15.75 o 6 0 1 57.07 49.86 13.12 o 7 0 1 677.13 732.23 36.74 o 8 0 1 543.17 566.88 34.12 o 9 0 1 31.37 .00 26.24 o 10 0 1 38.89 2.62 28.87 o 0 1 1 2633.12 2398.76 41.99 o 1 1 1 3284.22 3028.10 41.48 o 2 1 1 200.60 174.62 3.94 o 3 1 1 922.33 879.69 13.83 o 4 1 1 137.14 137.90 5.57 o 5 1 1 509.29 518.34 11.96 o 6 1 1 532.15 540.12 17.56 o 7 1 1 815.65 890.75 26.86 o 8 1 1 255.51 237.95 19.42 o 9 1 1 24.77 16.36 15.69 o 10 1 1 43.46 22.19 20.16 o 0 2 1 10445.25 9936.23 188.96 o 1 2 1 3943.49 3612.87 52.67 o 2 2 1 1419.14 1381.47 20.80 o 3 2 1 2294.17 2360.02 31.38 o 4 2 1 2264.62 2472.10 32.44 o 5 2 1 695.85 734.85 16.70 o 6 2 1 325.11 273.34 13.83 o 7 2 1 35.53 29.27 11.96 o 8 2 1 496.85 533.23 24.13 o 9 2 1 48.19 15.88 22.31 o 10 2 1 214.85 240.03 31.49 o 0 3 1 2042.58 2023.46 44.62 o 1 3 1 309.75 265.10 5.57 o 2 3 1 374.30 329.42 7.42 o 3 3 1 609.83 637.78 11.96 o 4 3 1 2336.92 2635.38 38.01 o 5 3 1 9.77 1.87 6.30 o 6 3 1 118.56 128.60 11.13 o 7 3 1 270.20 295.74 17.56 o 8 3 1 19.50 18.37 16.70 o 9 3 1 129.63 125.40 25.00 o 10 3 1 12.57 -3.71 31.38 o 0 4 1 32240.84 32874.06 569.51 o 1 4 1 348.52 325.62 7.87 o 2 4 1 1054.56 1051.91 15.69 o 3 4 1 145.63 142.52 6.56 o 4 4 1 2767.34 2841.01 60.36 o 5 4 1 90.14 89.64 14.43 o 6 4 1 429.07 450.54 17.56 o 7 4 1 11.36 2.62 11.13 o 8 4 1 75.88 47.52 19.68 o 9 4 1 41.44 31.32 27.10 o 0 5 1 4733.78 5115.08 86.61 o 1 5 1 1184.42 1218.66 17.56 o 2 5 1 94.74 86.28 9.19 o 3 5 1 278.43 275.85 8.20 o 4 5 1 113.00 110.27 6.75 o 5 5 1 437.12 416.97 18.37 o 6 5 1 47.46 34.33 23.62 o 7 5 1 47.87 26.65 11.96 o 8 5 1 38.75 35.69 21.84 o 9 5 1 76.36 92.23 25.19 o 0 6 1 1074.16 1099.65 31.49 o 1 6 1 668.44 695.64 12.99 o 2 6 1 451.19 446.30 11.13 o 3 6 1 58.09 48.22 6.30 o 4 6 1 773.00 786.54 16.98 o 5 6 1 61.81 45.97 6.75 o 6 6 1 7.63 16.94 10.08 o 7 6 1 142.00 108.36 21.00 o 8 6 1 27.39 17.72 20.25 o 9 6 1 30.83 29.82 31.49 o 0 7 1 714.94 742.72 23.62 o 1 7 1 897.95 916.15 18.28 o 2 7 1 405.79 381.50 12.60 o 3 7 1 140.40 129.54 13.12 o 4 7 1 47.57 40.17 10.08 o 5 7 1 58.20 55.35 14.43 o 6 7 1 107.42 109.23 52.49 o 7 7 1 173.22 141.96 30.18 o 8 7 1 5.50 -5.34 43.30 o 9 7 1 58.18 67.17 35.43 o 0 8 1 2102.24 2236.05 57.74 o 1 8 1 31.19 30.18 7.42 o 2 8 1 113.84 112.79 11.81 o 3 8 1 924.95 977.90 30.24 o 4 8 1 923.34 955.11 32.53 o 5 8 1 132.94 91.74 27.56 o 6 8 1 147.67 107.55 21.28 o 7 8 1 49.65 54.31 44.62 o 8 8 1 67.51 77.50 31.38 o 0 9 1 113.98 115.48 15.75 o 1 9 1 146.27 131.68 11.96 o 2 9 1 60.64 56.86 15.75 o 3 9 1 631.77 624.46 22.04 o 4 9 1 1010.15 1099.66 38.97 o 5 9 1 209.30 194.89 22.70 o 6 9 1 128.44 132.48 27.10 o 7 9 1 19.05 -22.81 35.87 o 8 9 1 127.38 146.53 44.62 o 0 10 1 1577.81 1800.38 60.36 o 1 10 1 1264.27 1339.07 38.01 o 2 10 1 23.96 13.36 10.08 o 3 10 1 60.36 44.00 15.69 o 4 10 1 143.16 95.81 20.41 o 5 10 1 373.64 353.75 32.79 o 6 10 1 137.03 203.34 35.30 o 7 10 1 93.95 79.96 57.74 o 0 11 1 364.79 322.81 28.87 o 1 11 1 220.25 207.47 18.56 o 2 11 1 24.51 6.56 16.70 o 3 11 1 59.79 44.51 23.28 o 4 11 1 17.40 1.43 21.00 o 5 11 1 50.71 34.29 31.49 o 6 11 1 25.33 26.82 29.52 o 0 12 1 302.55 241.45 28.87 o 1 12 1 37.30 47.52 19.68 o 2 12 1 24.71 23.62 17.56 o 3 12 1 26.75 7.16 24.07 o 4 12 1 34.87 17.34 37.05 o 5 12 1 32.23 -19.25 32.79 o 0 13 1 57.70 36.74 26.24 o 1 13 1 314.01 359.57 27.84 o 2 13 1 56.36 28.65 32.03 o 3 13 1 1.30 .81 38.44 o 4 13 1 14.70 2.94 38.44 o 0 14 1 687.15 768.97 49.86 o 1 14 1 107.73 106.53 52.49 o 2 14 1 52.14 54.52 47.09 o 3 14 1 185.40 214.31 73.29 o 0 0 2 6618.28 6193.74 165.34 o 1 0 2 593.24 545.89 10.50 o 2 0 2 208.40 181.09 5.25 o 3 0 2 604.75 556.39 13.12 o 4 0 2 569.83 629.87 15.75 o 5 0 2 7.35 10.50 7.87 o 6 0 2 603.84 590.50 26.24 o 7 0 2 2859.58 3091.62 86.61 o 8 0 2 74.52 65.61 23.62 o 9 0 2 89.31 65.61 28.87 o 10 0 2 26.12 .00 28.87 o 0 1 2 9155.94 8335.30 141.72 o 1 1 2 9800.70 8892.96 127.38 o 2 1 2 1539.49 1401.98 19.42 o 3 1 2 405.72 409.00 8.20 o 4 1 2 749.96 781.05 14.85 o 5 1 2 7.44 .37 6.56 o 6 1 2 516.01 527.13 16.39 o 7 1 2 250.13 259.39 15.69 o 8 1 2 26.56 7.87 15.75 o 9 1 2 162.66 130.03 18.56 o 10 1 2 83.76 46.27 25.00 o 0 2 2 4262.22 4015.43 70.86 o 1 2 2 1091.34 976.37 18.23 o 2 2 2 5336.13 5153.79 97.11 o 3 2 2 1544.62 1695.24 25.00 o 4 2 2 1292.93 1385.96 22.27 o 5 2 2 162.52 164.04 9.28 o 6 2 2 122.83 106.39 19.68 o 7 2 2 409.89 414.87 34.12 o 8 2 2 159.40 139.10 36.74 o 9 2 2 13.27 15.75 18.56 o 10 2 2 60.73 30.32 26.48 o 0 3 2 21751.93 20515.45 385.80 o 1 3 2 3102.62 3011.86 40.99 o 2 3 2 166.39 151.83 11.81 o 3 3 2 1877.18 1968.35 27.84 o 4 3 2 173.94 174.25 8.20 o 5 3 2 219.25 224.19 15.75 o 6 3 2 326.27 334.04 26.24 o 7 3 2 74.72 75.02 11.96 o 8 3 2 369.45 342.50 22.27 o 9 3 2 76.27 84.15 31.49 o 10 3 2 11.63 12.61 37.74 o 0 4 2 3229.45 3256.96 62.99 o 1 4 2 32.29 31.71 3.71 o 2 4 2 90.98 74.82 5.57 o 3 4 2 2319.86 2383.62 35.11 o 4 4 2 1181.32 1208.44 25.78 o 5 4 2 109.05 97.86 10.08 o 6 4 2 80.93 71.38 11.96 o 7 4 2 258.45 208.73 19.68 o 8 4 2 23.04 52.11 18.90 o 9 4 2 32.94 -4.37 25.00 o 0 5 2 6.12 7.87 5.25 o 1 5 2 410.44 387.96 10.08 o 2 5 2 399.71 366.21 22.31 o 3 5 2 139.67 148.57 7.42 o 4 5 2 379.67 379.32 14.50 o 5 5 2 741.43 756.17 32.81 o 6 5 2 340.35 363.61 16.70 o 7 5 2 74.56 69.57 12.99 o 8 5 2 90.92 66.75 39.37 o 9 5 2 12.30 3.94 24.13 o 0 6 2 894.03 876.57 21.00 o 1 6 2 451.35 480.28 11.13 o 2 6 2 240.18 230.95 8.20 o 3 6 2 21.84 2.62 7.42 o 4 6 2 63.83 61.35 8.73 o 5 6 2 180.83 157.02 18.37 o 6 6 2 254.07 258.47 25.78 o 7 6 2 1132.06 1160.62 87.92 o 8 6 2 181.16 159.74 24.59 o 9 6 2 13.25 -22.08 31.38 o 0 7 2 36.81 23.62 7.87 o 1 7 2 1128.36 1136.45 24.13 o 2 7 2 28.21 22.82 9.19 o 3 7 2 607.10 573.48 23.62 o 4 7 2 27.20 31.49 9.28 o 5 7 2 79.09 73.86 12.99 o 6 7 2 362.34 436.42 68.24 o 7 7 2 164.05 157.69 24.13 o 8 7 2 65.12 53.94 26.86 o 0 8 2 1025.49 1070.78 34.12 o 1 8 2 523.90 523.97 17.56 o 2 8 2 433.08 430.24 27.56 o 3 8 2 432.70 434.92 21.28 o 4 8 2 578.41 585.55 24.13 o 5 8 2 129.97 123.15 15.69 o 6 8 2 1.54 .24 26.24 o 7 8 2 48.74 37.84 26.63 o 8 8 2 35.54 10.50 24.59 o 0 9 2 .11 21.00 15.75 o 1 9 2 323.57 302.18 14.85 o 2 9 2 118.00 111.97 10.08 o 3 9 2 1183.35 1175.21 39.10 o 4 9 2 306.76 313.44 26.24 o 5 9 2 36.68 21.45 20.80 o 6 9 2 69.61 83.98 26.48 o 7 9 2 9.56 10.11 25.00 o 8 9 2 10.27 46.23 35.87 o 0 10 2 203.94 178.46 26.24 o 1 10 2 211.55 215.55 15.69 o 2 10 2 10.66 8.88 13.12 o 3 10 2 739.32 756.95 36.98 o 4 10 2 237.51 198.18 29.52 o 5 10 2 24.72 -4.59 23.62 o 6 10 2 38.79 21.67 28.72 o 7 10 2 132.78 95.03 39.37 o 0 11 2 145.91 139.10 26.24 o 1 11 2 26.49 13.73 11.96 o 2 11 2 179.80 188.56 17.56 o 3 11 2 7.75 -.75 31.49 o 4 11 2 200.68 221.15 36.74 o 5 11 2 19.67 17.85 26.20 o 6 11 2 133.36 85.82 68.24 o 0 12 2 727.19 750.60 44.62 o 1 12 2 104.82 100.85 28.87 o 2 12 2 23.59 9.57 36.74 o 3 12 2 1.09 -4.62 26.86 o 4 12 2 218.39 224.79 68.24 o 5 12 2 116.04 105.32 40.78 o 0 13 2 76.59 70.86 26.24 o 1 13 2 93.83 52.14 27.65 o 2 13 2 13.91 23.62 25.78 o 3 13 2 119.45 116.31 35.65 o 4 13 2 6.22 -15.96 42.51 o 0 14 2 89.44 41.99 47.24 o 1 14 2 86.75 90.03 31.49 o 2 14 2 5.31 24.81 50.40 o 1 0 3 572.49 553.76 13.12 o 2 0 3 2407.24 2351.52 41.99 o 3 0 3 307.09 307.06 10.50 o 4 0 3 2682.41 2837.05 47.24 o 5 0 3 321.61 288.69 15.75 o 6 0 3 362.05 404.17 23.62 o 7 0 3 3540.11 4025.93 110.23 o 8 0 3 316.77 354.30 31.49 o 9 0 3 27.20 21.00 26.24 o 10 0 3 13.07 -18.37 39.37 o 0 1 3 510.25 472.40 10.50 o 1 1 3 633.74 570.04 9.19 o 2 1 3 805.27 808.56 12.60 o 3 1 3 333.24 349.67 10.50 o 4 1 3 1071.56 1139.04 18.56 o 5 1 3 298.25 295.25 18.37 o 6 1 3 608.30 539.85 22.31 o 7 1 3 460.69 460.63 20.41 o 8 1 3 34.84 12.60 13.83 o 9 1 3 3.94 17.13 17.56 o 10 1 3 75.89 122.60 56.43 o 0 2 3 285.49 312.31 7.87 o 1 2 3 556.84 536.92 10.08 o 2 2 3 390.43 368.85 9.28 o 3 2 3 1230.32 1289.88 30.18 o 4 2 3 836.68 971.27 15.69 o 5 2 3 532.21 496.99 23.62 o 6 2 3 162.45 149.24 11.96 o 7 2 3 423.33 401.97 18.56 o 8 2 3 94.38 71.73 15.69 o 9 2 3 1.35 -17.56 17.56 o 10 2 3 45.56 85.19 34.29 o 0 3 3 897.24 858.20 21.00 o 1 3 3 213.32 195.53 5.57 o 2 3 3 133.38 117.14 4.69 o 3 3 3 352.31 368.78 9.28 o 4 3 3 828.24 925.17 18.56 o 5 3 3 301.26 302.39 13.83 o 6 3 3 464.28 545.72 24.93 o 7 3 3 113.42 128.43 15.75 o 8 3 3 32.87 31.49 14.85 o 9 3 3 22.78 43.08 27.56 o 0 4 3 18.76 23.62 5.25 o 1 4 3 156.90 150.92 5.57 o 2 4 3 3.41 7.87 5.57 o 3 4 3 194.48 187.38 8.73 o 4 4 3 189.46 182.12 8.20 o 5 4 3 11.74 15.75 10.50 o 6 4 3 141.50 157.49 14.43 o 7 4 3 74.32 72.36 14.50 o 8 4 3 38.69 13.71 16.39 o 9 4 3 51.57 16.47 25.73 o 0 5 3 1536.28 1661.29 36.74 o 1 5 3 339.47 360.01 11.81 o 2 5 3 310.05 314.29 14.43 o 3 5 3 134.77 126.50 10.08 o 4 5 3 156.34 136.31 15.75 o 5 5 3 89.06 70.31 14.50 o 6 5 3 361.63 356.68 18.28 o 7 5 3 103.08 95.90 18.90 o 8 5 3 28.65 15.47 16.98 o 9 5 3 25.08 -15.68 34.29 o 0 6 3 4323.73 4855.26 91.86 o 1 6 3 371.49 369.83 15.75 o 2 6 3 589.52 582.07 16.39 o 3 6 3 323.94 320.53 12.99 o 4 6 3 1352.14 1440.07 38.84 o 5 6 3 54.15 46.37 22.31 o 6 6 3 10.52 16.27 16.18 o 7 6 3 926.15 1047.94 39.61 o 8 6 3 13.86 4.93 30.18 o 9 6 3 47.49 59.41 31.49 o 0 7 3 139.06 107.60 13.12 o 1 7 3 212.32 208.89 10.08 o 2 7 3 158.30 155.93 10.08 o 3 7 3 25.31 11.08 8.20 o 4 7 3 70.23 55.24 11.13 o 5 7 3 112.53 107.76 28.87 o 6 7 3 410.80 397.14 34.29 o 7 7 3 12.56 17.72 20.25 o 8 7 3 24.51 12.31 26.86 o 0 8 3 347.30 351.68 21.00 o 1 8 3 42.19 41.48 8.20 o 2 8 3 149.09 141.47 11.96 o 3 8 3 2029.22 2217.77 55.83 o 4 8 3 444.05 458.38 28.87 o 5 8 3 329.51 340.29 27.10 o 6 8 3 199.81 196.44 25.73 o 7 8 3 451.87 441.44 38.05 o 8 8 3 34.07 30.39 28.72 o 0 9 3 8.57 26.24 15.75 o 1 9 3 76.39 70.71 17.06 o 2 9 3 249.27 255.74 15.69 o 3 9 3 250.24 218.56 17.56 o 4 9 3 236.38 168.64 17.47 o 5 9 3 158.27 177.46 24.59 o 6 9 3 44.25 40.68 25.98 o 7 9 3 3.44 -6.00 31.49 o 0 10 3 116.08 99.73 21.00 o 1 10 3 97.98 83.68 17.06 o 2 10 3 83.35 64.79 24.93 o 3 10 3 7.17 7.87 18.37 o 4 10 3 61.10 61.80 26.63 o 5 10 3 121.86 103.12 24.59 o 6 10 3 28.81 -9.57 27.66 o 7 10 3 196.46 229.13 37.74 o 0 11 3 361.29 354.30 34.12 o 1 11 3 241.79 231.62 20.16 o 2 11 3 79.06 95.62 14.50 o 3 11 3 2.72 10.33 23.89 o 4 11 3 106.79 66.46 28.39 o 5 11 3 139.20 156.49 39.37 o 6 11 3 25.70 28.49 35.76 o 0 12 3 13.71 10.50 21.00 o 1 12 3 37.24 26.41 14.50 o 2 12 3 14.49 15.64 23.14 o 3 12 3 52.05 100.19 30.10 o 4 12 3 164.71 185.80 41.99 o 5 12 3 107.00 153.53 42.71 o 0 13 3 4.67 -5.25 23.62 o 1 13 3 3.85 20.49 28.87 o 2 13 3 25.31 .00 25.98 o 3 13 3 24.04 40.96 34.68 o 4 13 3 17.43 -40.50 41.99 o 0 14 3 19.19 2.62 60.36 o 1 14 3 104.23 78.67 36.15 o 2 14 3 14.26 -41.72 41.72 o 0 0 4 41824.22 39012.69 1031.42 o 1 0 4 2630.70 2383.02 49.86 o 2 0 4 430.75 364.80 10.50 o 3 0 4 528.84 509.15 13.12 o 4 0 4 8.63 7.87 5.25 o 5 0 4 519.99 530.14 18.37 o 6 0 4 .06 -7.87 13.12 o 7 0 4 1.17 -15.75 15.75 o 8 0 4 179.26 149.59 23.62 o 9 0 4 53.26 68.24 34.12 o 10 0 4 3.72 13.12 31.49 o 0 1 4 2085.31 2010.34 34.12 o 1 1 4 3337.56 3243.08 40.70 o 2 1 4 221.69 206.40 6.30 o 3 1 4 32.92 44.30 6.56 o 4 1 4 155.16 151.19 7.42 o 5 1 4 172.93 176.65 9.19 o 6 1 4 104.21 100.94 10.08 o 7 1 4 194.04 176.40 13.83 o 8 1 4 382.03 365.55 21.28 o 9 1 4 .00 -17.56 17.56 o 10 1 4 21.44 -2.13 33.99 o 0 2 4 45.65 39.37 5.25 o 1 2 4 1658.59 1598.53 23.14 o 2 2 4 741.41 725.30 34.12 o 3 2 4 769.22 797.93 14.50 o 4 2 4 1150.92 1257.12 20.16 o 5 2 4 85.65 85.60 8.20 o 6 2 4 278.56 280.89 19.68 o 7 2 4 1006.51 1089.32 55.11 o 8 2 4 192.70 180.79 17.56 o 9 2 4 4.23 -19.18 23.91 o 0 3 4 757.82 763.72 15.75 o 1 3 4 252.06 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o 1 1 14 90.99 66.71 15.69 o 2 1 14 79.44 56.64 16.98 o 3 1 14 128.82 97.00 22.70 o 4 1 14 4.79 19.57 22.04 o 5 1 14 83.00 81.90 26.86 o 6 1 14 147.37 125.10 33.25 o 0 2 14 36.07 55.11 23.62 o 1 2 14 264.75 258.52 18.56 o 2 2 14 817.15 791.63 33.40 o 3 2 14 183.52 165.56 22.04 o 4 2 14 120.23 124.43 25.78 o 5 2 14 141.39 93.71 31.38 o 6 2 14 65.44 39.37 29.69 o 0 3 14 100.28 55.11 23.62 o 1 3 14 48.63 57.74 16.70 o 2 3 14 84.04 111.39 59.05 o 3 3 14 82.97 85.60 23.91 o 4 3 14 5.85 -30.32 34.12 o 5 3 14 114.35 103.81 32.79 o 6 3 14 6.01 19.83 32.79 o 0 4 14 2.23 -18.37 18.37 o 1 4 14 11.12 28.87 16.39 o 2 4 14 1037.68 1099.71 53.82 o 3 4 14 17.39 -9.78 21.00 o 4 4 14 53.12 -12.47 45.93 o 5 4 14 10.00 32.37 30.58 o 6 4 14 21.34 27.27 37.74 o 0 5 14 .74 18.37 28.87 o 1 5 14 24.72 -.77 15.05 o 2 5 14 47.80 13.12 24.13 o 3 5 14 68.54 89.04 25.78 o 4 5 14 2.14 7.40 31.49 o 5 5 14 32.16 46.19 32.44 o 0 6 14 21.67 36.74 28.87 o 1 6 14 470.83 545.67 43.58 o 2 6 14 92.92 164.35 32.44 o 3 6 14 79.90 26.06 31.49 o 4 6 14 20.24 46.66 32.79 o 5 6 14 127.02 84.25 43.21 o 0 7 14 362.57 322.81 55.11 o 1 7 14 191.97 214.71 46.08 o 2 7 14 122.61 147.40 41.99 o 3 7 14 15.60 12.32 37.05 o 4 7 14 63.24 88.50 38.34 o 0 8 14 59.80 70.86 52.49 o 1 8 14 28.88 41.88 44.62 o 2 8 14 154.09 134.01 39.12 o 3 8 14 36.81 1.73 45.04 o 0 9 14 4.07 21.00 86.61 o 1 9 14 3.37 8.28 48.55 o 2 9 14 29.57 68.24 40.99 o 1 0 15 83.41 86.61 23.62 o 2 0 15 234.64 144.35 41.99 o 3 0 15 73.94 81.36 36.74 o 4 0 15 101.38 144.35 39.37 o 5 0 15 23.60 52.49 47.24 o 0 1 15 64.85 65.61 23.62 o 1 1 15 364.60 393.66 26.24 o 2 1 15 95.41 83.98 24.13 o 3 1 15 247.83 286.69 41.99 o 4 1 15 39.79 46.66 25.00 o 5 1 15 3.93 19.53 29.01 o 0 2 15 12.81 2.62 21.00 o 1 2 15 133.50 106.70 18.56 o 2 2 15 133.83 102.20 21.28 o 3 2 15 112.91 115.18 25.78 o 4 2 15 2.55 -12.16 27.10 o 5 2 15 16.41 33.46 32.03 o 0 3 15 14.86 .00 26.24 o 1 3 15 58.87 18.01 19.68 o 2 3 15 29.09 37.14 43.30 o 3 3 15 208.48 216.40 36.98 o 4 3 15 26.05 18.37 29.69 o 5 3 15 6.28 1.95 32.44 o 0 4 15 122.96 115.48 23.62 o 1 4 15 162.17 172.66 23.28 o 2 4 15 164.50 188.15 29.69 o 3 4 15 141.28 98.60 31.49 o 4 4 15 157.12 172.84 35.11 o 5 4 15 48.57 31.49 35.26 o 0 5 15 .02 -31.49 31.49 o 1 5 15 3.31 21.00 20.41 o 2 5 15 207.64 238.94 45.93 o 3 5 15 200.24 148.94 41.99 o 4 5 15 86.70 118.03 33.25 o 0 6 15 107.57 10.50 39.37 o 1 6 15 115.51 113.02 29.00 o 2 6 15 117.74 116.00 32.44 o 3 6 15 135.03 111.54 33.40 o 4 6 15 10.90 6.85 42.56 o 0 7 15 64.27 -47.24 73.49 o 1 7 15 65.23 78.46 50.00 o 2 7 15 19.60 11.01 40.78 o 3 7 15 156.01 153.42 38.05 o 0 8 15 1.76 -112.85 112.85 o 1 8 15 12.91 -21.36 41.99 o 0 0 16 514.99 561.64 57.74 o 1 0 16 .05 5.25 31.49 o 2 0 16 3.36 13.12 39.37 o 3 0 16 18.24 13.12 36.74 o 4 0 16 1.60 -39.37 39.37 o 5 0 16 3.91 -21.00 55.11 o 0 1 16 35.39 5.25 23.62 o 1 1 16 156.67 107.80 25.00 o 2 1 16 52.42 32.70 22.04 o 3 1 16 101.98 120.69 28.36 o 4 1 16 7.34 21.74 34.47 o 5 1 16 60.09 108.41 35.87 o 0 2 16 41.86 26.24 23.62 o 1 2 16 25.02 28.24 23.14 o 2 2 16 48.80 63.39 28.87 o 3 2 16 123.68 119.02 35.88 o 4 2 16 38.86 73.03 36.98 o 0 3 16 4.93 -26.24 26.24 o 1 3 16 104.73 63.24 19.42 o 2 3 16 117.87 116.64 31.00 o 3 3 16 4.78 -30.58 30.58 o 4 3 16 108.00 75.58 34.94 o 0 4 16 30.16 10.50 39.37 o 1 4 16 26.77 48.50 23.14 o 2 4 16 119.44 150.63 53.80 o 3 4 16 11.45 -1.24 31.38 o 4 4 16 36.55 18.37 41.99 o 0 5 16 .07 39.37 62.99 o 1 5 16 74.40 1.31 25.98 o 2 5 16 6.76 -32.44 36.15 o 3 5 16 26.47 10.50 68.24 o 0 6 16 2.08 91.86 97.11 o 1 6 16 9.02 26.35 36.48 o 2 6 16 25.18 -24.32 27.65 o 0 7 16 13.57 -18.37 81.36 o 1 7 16 98.88 62.00 76.11 o 1 0 17 12.90 10.50 36.74 o 2 0 17 137.75 136.47 44.62 o 3 0 17 2.08 34.12 49.86 o 0 1 17 138.55 167.97 34.12 o 1 1 17 12.50 16.15 23.91 o 2 1 17 34.43 10.33 29.00 o 3 1 17 61.16 48.55 35.26 o 0 2 17 38.31 -28.87 39.37 o 1 2 17 105.73 107.05 27.10 o 2 2 17 166.07 158.03 40.70 o 3 2 17 113.86 39.95 32.79 o 0 3 17 3.40 -21.00 36.74 o 1 3 17 8.83 24.86 33.25 o 2 3 17 33.28 66.80 31.49 o 3 3 17 19.86 -25.21 28.61 o 0 4 17 18.48 2.62 60.36 o 1 4 17 138.27 115.32 42.13 o 2 4 17 2.13 25.72 32.12 o 0 5 17 283.36 259.82 68.24 o 1 5 17 37.02 17.09 38.82 o 0 0 18 23.25 2.62 86.61 o 1 0 18 187.68 225.70 47.24 o 2 0 18 8.86 5.25 41.99 o 0 1 18 365.24 317.56 70.86 o 1 1 18 36.89 -7.35 30.57 o 0 2 18 6.65 -49.86 62.99 o 1 2 18 26.08 26.37 50.29 o