#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2206449.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206449_Fobs loop_ _publ_author_name 'Wang, Ping' 'Xu, Xiao-Nan' 'Zheng, Lan-Fang' 'Bao, Yan-Qing' _publ_section_title ; Bis[3-dimethylamino-1-(2-pyridyl)prop-2-enonato]diperchloratozinc(II) ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1462 _journal_page_last m1463 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 79.358 _cell_angle_beta 78.130 _cell_angle_gamma 70.887 _cell_length_a 7.5449 _cell_length_b 9.1873 _cell_length_c 9.5884 _exptl_crystal_F_000 316.00 _reflns_d_resolution_high 0.8316 _[local]_cod_data_source_file hk6010Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' hu1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 174.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 945.26 882.67 36.95 o 3 0 0 1268.38 1182.43 29.75 o 4 0 0 382.03 374.28 9.70 o 5 0 0 0.52 0.21 0.49 o 6 0 0 1.07 0.76 0.66 o 7 0 0 291.15 297.56 11.62 o 8 0 0 0.73 0.73 0.95 o -8 1 0 10.30 13.84 1.70 o -7 1 0 276.77 267.87 10.70 o -6 1 0 407.92 388.08 14.63 o -5 1 0 243.93 248.28 9.57 o -4 1 0 13.65 15.03 1.06 o -3 1 0 1.85 4.63 0.54 o -2 1 0 2143.09 2066.55 43.16 o -1 1 0 267.66 291.99 8.61 o 0 1 0 1703.01 1810.64 64.12 o 1 1 0 3514.43 3674.96 129.30 o 2 1 0 136.39 166.49 4.35 o 3 1 0 615.37 661.22 16.78 o 4 1 0 1443.61 1446.44 50.80 o 5 1 0 86.47 76.41 3.41 o 6 1 0 93.60 87.52 3.98 o 7 1 0 2.72 2.19 0.82 o 8 1 0 52.47 51.83 3.11 o -7 2 0 7.72 7.69 1.34 o -6 2 0 7.95 5.61 1.11 o -5 2 0 258.34 271.15 12.54 o -4 2 0 301.91 268.73 17.29 o -3 2 0 138.40 165.16 3.71 o -2 2 0 999.14 975.90 20.50 o -1 2 0 1772.26 1772.62 45.45 o 0 2 0 3752.68 4136.17 144.17 o 1 2 0 1516.38 1523.92 53.16 o 2 2 0 3635.30 3585.98 90.22 o 3 2 0 101.88 100.25 2.80 o 4 2 0 129.17 111.11 3.14 o 5 2 0 1382.87 1390.52 35.17 o 6 2 0 287.86 302.44 11.45 o 7 2 0 106.53 103.68 4.71 o 8 2 0 106.68 99.33 4.78 o -7 3 0 15.27 15.12 1.74 o -6 3 0 0.69 0.10 0.76 o -5 3 0 24.98 20.56 1.74 o -4 3 0 353.13 351.52 9.53 o -3 3 0 323.72 337.17 11.46 o -2 3 0 26.80 23.28 1.82 o -1 3 0 584.27 619.06 22.32 o 0 3 0 29.99 28.35 1.35 o 1 3 0 25.52 28.78 1.32 o 2 3 0 29.27 30.95 1.42 o 3 3 0 118.11 59.76 1.82 o 4 3 0 51.39 49.30 1.64 o 5 3 0 338.81 349.30 9.22 o 6 3 0 730.99 818.63 21.04 o 7 3 0 27.78 30.66 2.12 o 8 3 0 18.61 22.90 1.96 o -6 4 0 21.49 23.75 2.15 o -5 4 0 31.87 32.26 2.29 o -4 4 0 3.52 3.00 0.55 o -3 4 0 521.37 506.33 13.45 o -2 4 0 129.43 120.35 3.53 o -1 4 0 89.66 79.65 3.35 o 0 4 0 153.72 128.26 4.94 o 1 4 0 885.45 922.79 21.54 o 2 4 0 10.90 22.62 1.20 o 3 4 0 344.53 324.01 11.74 o 4 4 0 1813.48 2058.68 51.82 o 5 4 0 103.88 111.29 3.32 o 6 4 0 318.37 295.38 8.00 o 7 4 0 442.18 479.73 17.82 o 8 4 0 5.67 5.29 1.09 o -6 5 0 25.97 30.89 2.64 o -5 5 0 4.91 6.02 1.23 o -4 5 0 0.19 -0.68 0.71 o -3 5 0 191.65 181.42 5.27 o -2 5 0 548.77 529.25 29.04 o -1 5 0 37.25 33.17 1.84 o 0 5 0 812.13 908.54 32.15 o 1 5 0 1167.97 1283.24 29.93 o 2 5 0 534.18 535.29 19.08 o 3 5 0 6.64 9.25 0.85 o 4 5 0 350.64 352.35 9.32 o 5 5 0 420.40 439.96 11.58 o 6 5 0 13.71 10.79 1.48 o 7 5 0 164.90 166.22 4.92 o 8 5 0 24.32 28.47 2.20 o -5 6 0 12.44 12.33 1.63 o -4 6 0 89.64 90.64 4.46 o -3 6 0 0.16 0.16 0.73 o -2 6 0 160.51 148.16 4.45 o -1 6 0 48.07 39.21 2.19 o 0 6 0 59.76 69.48 3.16 o 1 6 0 130.99 118.47 5.30 o 2 6 0 600.13 588.48 21.03 o 3 6 0 459.55 498.43 17.94 o 4 6 0 103.45 92.17 2.86 o 5 6 0 465.59 490.57 12.88 o 6 6 0 8.54 9.67 0.78 o 7 6 0 7.04 5.20 0.71 o 8 6 0 62.03 66.34 3.58 o -4 7 0 89.02 90.44 4.67 o -3 7 0 123.40 137.08 6.12 o -2 7 0 15.37 16.25 1.60 o -1 7 0 174.76 179.84 6.68 o 0 7 0 44.23 38.40 2.21 o 1 7 0 0.84 2.40 0.53 o 2 7 0 541.86 545.60 19.66 o 3 7 0 195.34 195.37 7.53 o 4 7 0 15.05 11.11 0.82 o 5 7 0 0.56 0.73 0.43 o 6 7 0 221.27 205.45 5.92 o 7 7 0 31.03 40.38 1.81 o 8 7 0 0.38 -0.03 0.69 o -3 8 0 23.04 19.83 2.03 o -2 8 0 0.47 -0.05 0.78 o -1 8 0 10.78 14.46 1.48 o 1 8 0 66.34 64.41 2.10 o 2 8 0 85.43 82.04 3.70 o 3 8 0 9.96 13.25 1.30 o 4 8 0 3.50 3.58 0.57 o 5 8 0 0.37 0.43 0.63 o 6 8 0 106.14 103.74 5.09 o 7 8 0 79.78 80.43 4.31 o -2 9 0 36.46 41.05 2.74 o -1 9 0 0.12 -0.03 0.73 o 0 9 0 11.89 9.02 0.85 o 1 9 0 160.18 178.60 4.83 o 2 9 0 31.95 28.44 1.96 o 3 9 0 18.66 19.38 1.61 o 4 9 0 184.01 179.08 7.96 o 5 9 0 136.60 139.09 6.55 o 6 9 0 14.28 15.90 1.77 o 3 10 0 26.72 28.04 2.60 o 4 10 0 0.19 0.26 0.97 o 5 10 0 29.29 29.53 2.55 o -5 -10 1 4.44 4.95 1.30 o -2 -10 1 132.76 122.42 5.51 o -1 -10 1 56.33 49.98 3.02 o 0 -10 1 0.53 1.00 0.70 o -6 -9 1 53.95 52.34 3.28 o -5 -9 1 102.52 105.77 3.53 o -4 -9 1 19.82 20.73 1.72 o -3 -9 1 1.70 1.68 0.83 o -2 -9 1 232.06 233.67 9.23 o -1 -9 1 2.99 3.54 1.02 o 0 -9 1 5.49 6.63 0.82 o 2 -9 1 3.01 5.64 1.34 o -7 -8 1 36.72 35.52 2.24 o -6 -8 1 17.49 17.64 1.21 o -5 -8 1 44.82 46.13 1.90 o -4 -8 1 26.45 22.95 1.67 o -3 -8 1 94.60 96.17 4.29 o -2 -8 1 32.08 29.90 1.94 o -1 -8 1 242.45 249.76 6.46 o 0 -8 1 17.92 15.27 1.04 o 1 -8 1 17.98 18.40 1.77 o 2 -8 1 95.93 94.95 4.64 o 3 -8 1 61.39 63.96 3.75 o -7 -7 1 104.47 108.27 3.58 o -6 -7 1 62.83 64.62 2.39 o -5 -7 1 47.42 39.75 1.67 o -4 -7 1 266.05 269.62 10.25 o -3 -7 1 503.58 522.19 18.99 o -2 -7 1 9.80 14.65 1.34 o -1 -7 1 91.04 86.58 2.59 o 0 -7 1 70.07 88.09 3.45 o 1 -7 1 14.47 17.34 1.56 o 2 -7 1 44.66 47.94 2.87 o 3 -7 1 188.22 202.99 8.45 o 4 -7 1 44.20 38.06 2.74 o -8 -6 1 2.64 3.77 1.06 o -7 -6 1 4.97 3.42 0.64 o -6 -6 1 97.59 103.24 3.30 o -5 -6 1 245.24 215.96 6.06 o -4 -6 1 6.74 5.40 0.82 o -3 -6 1 725.49 751.26 26.83 o -2 -6 1 143.36 132.76 5.32 o -1 -6 1 134.21 141.78 3.78 o 1 -6 1 169.02 246.41 9.49 o 2 -6 1 7.57 4.46 0.97 o 3 -6 1 11.66 9.55 1.27 o 4 -6 1 52.28 46.35 2.93 o 5 -6 1 5.07 5.54 1.37 o -8 -5 1 110.25 108.07 5.16 o -7 -5 1 3.64 2.38 0.85 o -6 -5 1 50.06 50.26 1.93 o -5 -5 1 948.04 1007.30 30.50 o -4 -5 1 21.97 15.75 1.25 o -3 -5 1 1.22 0.75 0.47 o -2 -5 1 1458.23 1460.51 51.28 o -1 -5 1 699.34 722.51 17.08 o 0 -5 1 676.14 798.79 28.45 o 1 -5 1 439.30 487.58 17.74 o 2 -5 1 105.37 109.36 3.33 o 3 -5 1 0.64 12.05 1.34 o 4 -5 1 4.97 4.32 1.04 o 5 -5 1 97.27 100.58 4.88 o 6 -5 1 8.49 11.13 1.63 o -8 -4 1 129.94 137.51 6.19 o -7 -4 1 184.05 183.54 7.58 o -6 -4 1 118.99 118.65 3.62 o -5 -4 1 180.48 193.20 6.54 o -4 -4 1 686.50 637.40 22.80 o -3 -4 1 550.01 580.93 20.74 o -2 -4 1 935.14 975.83 34.37 o -1 -4 1 965.68 965.50 22.57 o 0 -4 1 27.43 29.37 1.56 o 1 -4 1 233.28 288.48 10.67 o 2 -4 1 9.68 7.24 0.58 o 3 -4 1 83.73 78.08 2.51 o 4 -4 1 79.69 90.34 4.26 o 5 -4 1 24.73 27.17 2.17 o 6 -4 1 22.00 25.40 2.26 o -8 -3 1 7.00 7.26 1.25 o -7 -3 1 186.47 194.90 8.00 o -6 -3 1 477.36 474.46 17.46 o -5 -3 1 13.40 17.04 0.92 o -4 -3 1 231.77 218.63 5.89 o -3 -3 1 10.26 5.26 0.61 o -2 -3 1 261.14 269.14 9.80 o -1 -3 1 597.41 634.12 22.41 o 0 -3 1 1682.92 1910.99 66.78 o 1 -3 1 17.80 17.95 1.11 o 2 -3 1 37.20 38.96 1.09 o 3 -3 1 1044.37 1034.12 21.85 o 4 -3 1 376.96 382.13 10.27 o 5 -3 1 0.80 0.62 0.69 o 6 -3 1 22.32 21.70 1.91 o 7 -3 1 24.07 22.33 2.20 o -8 -2 1 30.69 31.93 2.40 o -7 -2 1 72.17 70.69 3.60 o -6 -2 1 58.01 60.61 3.09 o -5 -2 1 146.08 133.84 5.51 o -4 -2 1 626.21 673.14 17.21 o -3 -2 1 2666.68 2773.40 96.74 o -2 -2 1 265.36 234.40 8.52 o -1 -2 1 548.91 577.32 20.34 o 0 -2 1 1172.62 1308.23 45.75 o 1 -2 1 150.96 205.71 8.18 o 2 -2 1 218.97 245.79 5.35 o 4 -2 1 1731.53 1613.64 56.83 o 5 -2 1 14.69 8.58 1.08 o 6 -2 1 0.16 -0.66 0.75 o 7 -2 1 153.80 159.00 6.93 o -8 -1 1 105.17 109.92 5.26 o -7 -1 1 7.24 3.98 0.95 o -6 -1 1 281.04 270.79 10.42 o -5 -1 1 262.98 259.30 9.85 o -4 -1 1 1003.30 953.25 24.15 o -3 -1 1 557.91 610.62 21.70 o -2 -1 1 1222.10 1268.54 44.40 o -1 -1 1 3529.04 3626.96 127.51 o 0 -1 1 180.46 199.78 7.99 o 1 -1 1 1302.30 1482.85 31.11 o 2 -1 1 1308.67 1275.40 26.68 o 3 -1 1 198.17 181.49 7.14 o 4 -1 1 747.76 707.24 25.30 o 5 -1 1 609.86 592.57 21.51 o 6 -1 1 111.65 102.30 4.66 o 7 -1 1 31.83 36.11 2.52 o 8 -1 1 60.15 61.99 3.66 o -8 0 1 62.25 69.39 3.89 o -7 0 1 146.55 139.82 6.17 o -6 0 1 14.02 13.42 1.41 o -5 0 1 295.57 287.95 10.88 o -4 0 1 810.15 761.87 19.36 o -3 0 1 987.66 979.51 20.62 o -2 0 1 51.65 61.59 2.75 o 0 0 1 2355.02 2076.71 52.70 o 1 0 1 175.08 191.94 4.92 o 2 0 1 3744.45 3557.50 89.38 o 3 0 1 76.62 49.81 1.53 o 4 0 1 1.22 0.52 0.25 o 5 0 1 411.39 395.97 14.59 o 6 0 1 101.62 95.47 4.34 o 7 0 1 166.06 172.08 7.21 o 8 0 1 1.93 3.09 1.13 o -8 1 1 3.10 2.64 1.11 o -7 1 1 135.95 128.80 5.86 o -6 1 1 298.28 298.60 11.55 o -5 1 1 14.60 16.26 0.98 o -4 1 1 84.81 81.89 2.60 o -3 1 1 3393.82 3277.54 140.09 o -2 1 1 212.10 216.10 5.82 o -1 1 1 589.77 609.62 15.77 o 0 1 1 584.50 698.46 25.56 o 1 1 1 1515.84 1549.24 39.19 o 2 1 1 577.87 577.40 14.60 o 3 1 1 1177.78 1087.92 27.44 o 4 1 1 995.40 1018.51 27.02 o 5 1 1 4.77 3.24 0.42 o 6 1 1 24.36 23.82 1.68 o 7 1 1 19.03 17.00 1.58 o 8 1 1 35.74 35.96 2.55 o -7 2 1 4.71 3.85 1.18 o -6 2 1 205.78 197.85 8.14 o -5 2 1 74.22 67.94 2.38 o -4 2 1 4.42 3.50 0.49 o -3 2 1 1255.18 1355.33 35.00 o -2 2 1 1446.91 1380.42 35.54 o -1 2 1 384.56 382.35 10.03 o 2 2 1 821.04 785.00 19.80 o 3 2 1 168.96 174.62 4.64 o 4 2 1 345.68 311.14 8.14 o 5 2 1 112.48 90.40 2.72 o 6 2 1 85.86 86.60 4.64 o 7 2 1 183.42 193.77 7.84 o 8 2 1 88.66 90.81 4.41 o -7 3 1 7.37 6.70 1.39 o -6 3 1 2.07 0.45 0.83 o -5 3 1 281.87 293.65 8.21 o -4 3 1 113.00 105.66 3.30 o -3 3 1 223.74 244.00 6.73 o -2 3 1 377.55 359.64 9.57 o -1 3 1 36.97 46.31 1.52 o 0 3 1 58.08 52.62 2.15 o 1 3 1 88.11 74.47 1.92 o 2 3 1 4058.67 4163.57 104.42 o 3 3 1 1246.65 1371.57 34.54 o 4 3 1 386.88 435.16 11.26 o 5 3 1 1156.58 1159.87 29.43 o 6 3 1 140.39 136.98 4.00 o 7 3 1 17.24 14.98 1.42 o 8 3 1 64.05 60.05 3.30 o 9 3 1 63.44 67.62 3.75 o -6 4 1 3.62 3.28 1.06 o -5 4 1 7.06 8.09 1.20 o -4 4 1 706.31 691.92 24.05 o -3 4 1 7.63 6.19 0.59 o -2 4 1 10.12 12.05 0.79 o -1 4 1 402.64 377.71 10.06 o 0 4 1 1059.77 1150.53 40.36 o 1 4 1 825.44 983.00 22.91 o 2 4 1 439.51 465.83 11.93 o 3 4 1 2969.50 3062.90 76.75 o 4 4 1 19.16 13.42 0.73 o 5 4 1 104.50 98.32 2.97 o 6 4 1 1188.81 1278.96 32.54 o 7 4 1 63.26 65.89 2.55 o 8 4 1 0.27 2.03 0.82 o -6 5 1 83.18 91.20 4.76 o -5 5 1 3.41 3.61 1.02 o -4 5 1 38.01 37.47 1.67 o -3 5 1 404.34 407.92 12.68 o -2 5 1 4.32 5.02 0.56 o -1 5 1 187.69 189.09 5.34 o 0 5 1 708.82 728.10 25.82 o 1 5 1 715.57 775.62 18.17 o 2 5 1 81.98 95.78 3.94 o 3 5 1 33.57 27.31 1.08 o 4 5 1 1018.32 1126.24 28.60 o 5 5 1 5.97 5.52 0.54 o 6 5 1 260.58 251.38 8.25 o 7 5 1 135.09 165.83 5.91 o 8 5 1 0.67 0.14 0.73 o -5 6 1 88.80 94.49 4.79 o -4 6 1 61.94 54.84 3.16 o -3 6 1 161.78 162.11 4.90 o -2 6 1 819.24 870.02 22.88 o -1 6 1 232.57 247.91 6.94 o 0 6 1 12.31 18.82 1.32 o 1 6 1 265.25 263.29 6.45 o 2 6 1 518.89 527.54 18.82 o 3 6 1 42.20 44.30 1.59 o 4 6 1 527.80 544.51 14.13 o 5 6 1 309.22 318.43 8.57 o 6 6 1 48.86 45.90 1.81 o 7 6 1 74.26 81.62 2.81 o 8 6 1 110.50 132.75 6.08 o -4 7 1 0.74 0.31 0.94 o -3 7 1 14.67 16.37 1.68 o -2 7 1 230.38 235.27 6.82 o -1 7 1 356.57 355.70 9.78 o 0 7 1 4.56 4.43 0.78 o 1 7 1 161.77 153.07 4.00 o 2 7 1 760.23 782.18 27.76 o 3 7 1 60.04 58.48 2.04 o 4 7 1 124.53 138.31 4.06 o 5 7 1 40.97 37.68 1.56 o 6 7 1 59.10 65.05 3.54 o 7 7 1 20.89 22.47 2.00 o 8 7 1 34.46 36.34 2.60 o -3 8 1 5.43 6.15 1.20 o -2 8 1 49.57 53.50 3.06 o -1 8 1 17.69 22.36 1.37 o 0 8 1 186.57 188.90 7.51 o 1 8 1 3.49 3.84 0.52 o 2 8 1 73.45 79.41 2.66 o 3 8 1 555.35 573.86 21.94 o 4 8 1 0.46 0.85 0.80 o 5 8 1 79.83 76.86 4.05 o 6 8 1 132.58 136.71 6.32 o 7 8 1 48.78 44.83 3.00 o -2 9 1 16.59 14.43 1.63 o -1 9 1 5.89 6.61 1.13 o 2 9 1 68.33 67.09 3.82 o 3 9 1 572.51 605.82 23.36 o 4 9 1 209.68 219.89 9.46 o 5 9 1 8.22 8.02 1.32 o 6 9 1 36.46 39.50 2.86 o 7 9 1 106.24 108.48 5.52 o 1 10 1 29.46 43.44 3.28 o 2 10 1 28.28 34.52 2.92 o 3 10 1 5.30 5.78 1.44 o 4 10 1 104.93 108.13 5.68 o 5 10 1 34.20 40.23 2.99 o 6 10 1 5.72 5.26 1.30 o -4 -10 2 67.01 68.98 3.70 o -3 -10 2 52.75 50.58 3.07 o -2 -10 2 2.22 2.19 0.99 o -1 -10 2 11.17 13.14 1.67 o -6 -9 2 58.87 64.43 2.58 o -5 -9 2 22.52 19.62 1.79 o -4 -9 2 14.04 11.21 1.35 o -3 -9 2 1.35 1.23 0.83 o -2 -9 2 0.47 2.10 0.94 o -1 -9 2 21.98 23.49 2.03 o 0 -9 2 31.45 33.91 1.66 o 1 -9 2 21.56 30.18 1.75 o 2 -9 2 7.47 11.41 1.61 o -6 -8 2 40.40 45.77 2.01 o -5 -8 2 142.12 131.22 5.70 o -4 -8 2 25.59 26.42 1.89 o -3 -8 2 41.83 39.07 2.41 o -2 -8 2 44.55 39.97 2.41 o -1 -8 2 132.90 134.68 5.86 o 0 -8 2 19.61 23.96 1.33 o 2 -8 2 73.41 76.10 4.13 o 3 -8 2 4.59 4.77 1.30 o -7 -7 2 52.17 55.45 2.25 o -6 -7 2 4.57 3.23 0.64 o -5 -7 2 44.36 48.39 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0.55 o 5 -2 9 20.69 20.00 2.19 o -4 -1 9 17.53 17.55 1.89 o -3 -1 9 0.18 2.29 0.97 o -2 -1 9 24.87 25.88 1.45 o -1 -1 9 60.35 61.31 2.35 o 0 -1 9 4.77 9.09 3.64 o 1 -1 9 0.52 -0.17 0.61 o 2 -1 9 30.76 32.01 2.90 o 3 -1 9 0.09 -0.71 0.80 o 4 -1 9 1.75 0.80 0.94 o 5 -1 9 2.05 1.22 1.01 o -4 0 9 18.63 19.98 1.61 o -3 0 9 86.57 89.12 3.25 o -2 0 9 32.56 33.71 2.36 o -1 0 9 3.56 3.39 0.52 o 0 0 9 189.52 209.91 8.71 o 1 0 9 15.49 13.02 1.46 o 2 0 9 11.22 9.24 1.37 o 3 0 9 67.35 67.35 3.77 o 4 0 9 29.82 28.70 2.36 o 5 0 9 1.69 1.20 0.97 o 6 0 9 24.61 24.29 2.41 o -3 1 9 154.56 155.82 7.26 o -2 1 9 54.90 61.32 3.58 o -1 1 9 0.23 -0.16 0.66 o 0 1 9 132.36 138.07 4.37 o 1 1 9 50.39 53.56 3.13 o 2 1 9 0.37 0.02 0.73 o 3 1 9 79.24 77.87 4.12 o 4 1 9 174.88 175.58 7.73 o 5 1 9 1.84 2.62 1.08 o 6 1 9 0.13 -0.07 0.90 o -3 2 9 57.25 58.94 3.63 o -2 2 9 286.02 287.04 12.23 o -1 2 9 68.70 77.09 4.17 o 0 2 9 51.56 55.07 3.05 o 1 2 9 228.23 236.11 9.20 o 2 2 9 106.62 106.62 5.04 o 3 2 9 13.07 16.28 1.70 o 4 2 9 0.14 0.30 0.85 o 5 2 9 70.47 77.39 4.22 o 6 2 9 4.93 3.04 1.16 o -3 3 9 34.84 48.32 3.30 o -2 3 9 36.09 40.47 2.93 o -1 3 9 157.79 174.01 7.94 o 0 3 9 7.25 7.33 1.16 o 1 3 9 180.87 206.24 6.20 o 2 3 9 183.27 197.11 5.98 o 3 3 9 16.62 16.01 1.68 o 4 3 9 10.22 10.52 1.42 o 5 3 9 55.05 52.37 3.28 o 6 3 9 29.39 29.62 2.47 o -2 4 9 30.32 32.59 2.62 o -1 4 9 14.66 16.80 1.84 o 0 4 9 19.13 20.19 2.07 o 1 4 9 0.97 1.14 0.60 o 2 4 9 3.32 2.10 0.64 o 3 4 9 87.57 88.34 4.06 o 4 4 9 51.08 53.02 3.21 o 5 4 9 3.72 3.73 1.18 o 6 4 9 3.77 4.41 1.23 o -2 5 9 167.94 181.18 8.57 o -1 5 9 4.42 4.32 1.16 o 0 5 9 37.51 39.45 2.90 o 1 5 9 33.99 35.35 2.73 o 2 5 9 105.76 109.68 5.08 o 3 5 9 12.67 12.57 1.05 o 4 5 9 20.07 24.57 1.48 o 5 5 9 1.54 2.00 1.04 o 6 5 9 0.69 1.23 1.06 o -1 6 9 23.09 22.81 2.31 o 0 6 9 74.74 72.65 4.34 o 1 6 9 62.70 66.44 4.03 o 2 6 9 262.69 249.01 7.48 o 3 6 9 38.00 38.18 1.91 o 4 6 9 5.52 5.47 0.82 o 5 6 9 49.67 55.93 3.46 o 6 6 9 4.17 5.45 1.35 o 0 7 9 60.93 60.43 3.98 o 1 7 9 4.95 5.23 1.28 o 2 7 9 57.17 63.57 3.98 o 3 7 9 207.22 207.23 6.50 o 4 7 9 35.03 34.57 2.59 o 5 7 9 18.04 15.68 1.75 o 2 8 9 14.01 14.90 1.89 o 3 8 9 52.12 54.48 2.74 o 4 8 9 69.57 61.63 3.70 o -1 -3 10 1.42 1.56 1.01 o 0 -3 10 16.65 16.23 1.28 o 1 -3 10 4.21 4.32 0.83 o 2 -3 10 0.74 1.55 0.73 o -2 -2 10 0.42 1.56 0.97 o -1 -2 10 0.08 -0.42 0.48 o 0 -2 10 9.24 7.52 0.92 o 1 -2 10 3.97 3.50 0.75 o 2 -2 10 1.61 1.91 1.01 o 3 -2 10 0.01 0.14 0.87 o -2 -1 10 7.89 8.32 1.41 o -1 -1 10 20.21 28.84 2.22 o 0 -1 10 6.08 6.65 1.23 o 1 -1 10 5.21 3.94 1.11 o 2 -1 10 14.91 17.24 1.93 o 3 -1 10 3.09 2.50 1.16 o 4 -1 10 2.08 3.52 1.25 o -2 0 10 4.97 4.34 1.08 o 0 0 10 5.05 5.69 1.15 o 1 0 10 9.88 7.73 1.32 o 2 0 10 59.01 59.06 3.53 o 3 0 10 14.32 17.05 1.94 o 4 0 10 0.47 1.25 1.08 o 5 0 10 19.85 16.75 2.00 o -2 1 10 47.07 50.74 3.21 o -1 1 10 1.37 0.87 0.89 o 0 1 10 53.64 54.34 3.20 o 1 1 10 100.18 124.97 5.85 o 2 1 10 0.27 -0.45 0.82 o 3 1 10 42.61 43.90 3.02 o 4 1 10 0.09 -0.38 0.95 o 5 1 10 0.02 -0.92 0.82 o -2 2 10 51.48 52.16 3.39 o -1 2 10 2.27 1.87 0.94 o 0 2 10 39.60 41.60 2.83 o 1 2 10 346.90 380.89 15.00 o 2 2 10 11.27 14.24 1.60 o 3 2 10 2.59 2.15 1.02 o 4 2 10 12.49 14.79 1.75 o 5 2 10 0.04 -0.68 0.92 o -2 3 10 61.06 73.26 4.36 o -1 3 10 51.93 52.49 3.46 o 0 3 10 0.50 0.38 0.76 o 1 3 10 6.53 5.83 0.80 o 2 3 10 118.93 114.18 5.46 o 3 3 10 0.10 1.13 0.92 o 4 3 10 5.32 4.11 1.25 o 5 3 10 43.78 44.31 3.09 o 6 3 10 0.91 0.62 1.09 o -1 4 10 124.87 150.95 7.35 o 0 4 10 5.06 4.98 1.18 o 1 4 10 177.78 180.14 8.27 o 2 4 10 26.96 25.96 1.53 o 3 4 10 36.29 37.78 2.67 o 4 4 10 6.93 5.54 1.30 o 5 4 10 6.47 6.06 1.35 o 6 4 10 66.31 69.79 4.20 o 0 5 10 136.64 147.33 7.23 o 1 5 10 21.99 20.05 2.14 o 2 5 10 9.17 13.88 1.16 o 3 5 10 71.36 74.78 2.94 o 4 5 10 14.87 12.59 1.63 o 5 5 10 19.70 22.52 2.22 o 1 6 10 115.06 124.21 6.46 o 2 6 10 9.25 10.42 1.61 o 3 6 10 8.08 8.73 1.01 o 4 6 10 120.56 127.99 4.44 o 5 6 10 11.13 10.76 1.60 o 2 7 10 86.26 92.56 5.25 o 3 7 10 18.12 17.27 2.04 o 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