#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:13:18 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180984 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/64/2206464.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206464_Fobs loop_ _publ_author_name 'Shi, Yu-Quan' 'Xu, Dan' 'Chen, Bin' 'Cai, Ming-Jian' 'Zhu, Yong' _publ_section_title ; N-Ethyl-5-(pyrrol-1-yl)-1,8-naphthalimide ; _journal_coeditor_code IS6096 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2436 _journal_page_last o2437 _journal_volume 61 _journal_year 2005 _space_group_IT_number 9 _symmetry_space_group_name_Hall 'C -2yc' _symmetry_space_group_name_H-M 'C 1 c 1' _cell_angle_alpha 90.000 _cell_angle_beta 127.771 _cell_angle_gamma 90.000 _cell_length_a 10.2568 _cell_length_b 23.0397 _cell_length_c 7.4235 _exptl_crystal_F_000 608.00 _reflns_d_resolution_high 0.8018 _cod_data_source_file is6096Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 50608D in Cc' _shelx_refln_list_code 4 _shelx_f_calc_maximum 235.47 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 44785.18 40017.27 840.95 o 4 0 0 1100.45 1072.92 14.35 o 6 0 0 613.63 617.54 18.65 o 8 0 0 215.75 228.01 11.27 o 10 0 0 30.07 24.42 5.93 o 1 1 0 1175.17 1096.74 46.33 o 3 1 0 347.03 354.76 5.43 o 5 1 0 446.06 433.43 5.62 o 7 1 0 19.21 22.40 3.40 o 9 1 0 9.01 4.87 2.97 o 2 2 0 1981.31 1940.03 20.71 o 4 2 0 42.63 42.75 1.56 o 6 2 0 16.88 16.93 3.89 o 8 2 0 101.82 98.19 5.48 o 10 2 0 27.01 23.33 6.68 o 1 3 0 596.28 601.02 18.33 o 3 3 0 460.89 493.12 6.38 o 5 3 0 73.46 74.47 3.62 o 7 3 0 32.38 38.18 3.79 o 9 3 0 27.72 26.85 4.23 o 0 4 0 2523.79 2304.84 50.28 o 2 4 0 1274.70 1189.01 19.82 o 4 4 0 274.28 278.56 4.76 o 6 4 0 273.65 268.62 5.85 o 8 4 0 182.42 193.57 7.35 o 1 5 0 172.70 179.49 2.44 o 3 5 0 243.06 240.54 4.44 o 5 5 0 26.25 24.80 1.72 o 7 5 0 49.13 49.06 4.10 o 9 5 0 61.65 55.50 6.41 o 0 6 0 141.07 142.62 3.85 o 2 6 0 1155.91 1165.56 12.60 o 4 6 0 145.46 160.75 3.33 o 6 6 0 74.16 79.79 4.88 o 8 6 0 15.59 16.15 3.23 o 1 7 0 14.87 15.71 0.83 o 3 7 0 346.75 362.25 5.93 o 5 7 0 202.02 214.58 6.10 o 7 7 0 128.79 129.74 5.82 o 9 7 0 11.52 7.17 4.68 o 0 8 0 114.44 99.23 2.41 o 2 8 0 911.84 844.27 9.50 o 4 8 0 534.78 543.27 13.60 o 6 8 0 209.96 215.82 4.66 o 8 8 0 131.27 128.86 5.98 o 1 9 0 708.62 688.13 13.73 o 3 9 0 889.68 857.92 10.02 o 5 9 0 74.58 76.39 2.75 o 7 9 0 127.35 117.90 4.40 o 9 9 0 4.90 0.88 3.42 o 0 10 0 180.62 168.90 3.61 o 2 10 0 1580.73 1692.35 18.05 o 4 10 0 644.61 695.08 8.73 o 6 10 0 268.65 260.47 5.25 o 8 10 0 35.50 38.58 4.27 o 1 11 0 1113.04 1141.71 12.43 o 3 11 0 965.29 944.32 17.22 o 5 11 0 217.67 206.99 4.05 o 7 11 0 56.47 54.61 3.50 o 9 11 0 43.57 36.96 4.67 o 0 12 0 32.98 36.99 1.77 o 2 12 0 1528.16 1536.86 16.65 o 4 12 0 331.37 335.54 5.22 o 6 12 0 49.62 55.21 2.50 o 8 12 0 41.03 47.22 4.86 o 1 13 0 163.00 188.52 2.97 o 3 13 0 189.35 210.89 3.63 o 5 13 0 0.24 0.93 1.20 o 7 13 0 32.00 36.07 4.02 o 0 14 0 95.95 96.01 3.53 o 2 14 0 221.95 223.96 3.57 o 4 14 0 445.98 433.52 6.96 o 6 14 0 34.49 30.27 3.01 o 8 14 0 20.57 21.85 5.56 o 1 15 0 198.89 213.51 3.35 o 3 15 0 234.00 230.66 7.19 o 5 15 0 17.88 18.90 2.02 o 7 15 0 26.12 26.06 3.73 o 0 16 0 347.59 322.96 9.99 o 2 16 0 120.15 119.34 3.24 o 4 16 0 164.07 163.12 4.24 o 6 16 0 11.25 11.78 2.48 o 8 16 0 1.92 -0.75 4.49 o 1 17 0 88.46 97.43 5.08 o 3 17 0 750.35 728.72 15.36 o 5 17 0 397.56 395.14 7.53 o 7 17 0 24.56 24.88 6.81 o 0 18 0 8.23 4.38 2.51 o 2 18 0 1021.39 1003.46 17.04 o 4 18 0 1614.94 1608.98 25.77 o 6 18 0 203.09 199.88 6.25 o 1 19 0 217.79 217.64 11.62 o 3 19 0 595.50 568.63 11.36 o 5 19 0 348.64 334.42 8.42 o 7 19 0 16.39 14.64 5.72 o 0 20 0 34.48 34.68 4.22 o 2 20 0 10.17 6.89 2.20 o 4 20 0 94.43 109.00 4.63 o 6 20 0 9.91 9.19 4.46 o 1 21 0 26.84 26.73 2.97 o 3 21 0 15.88 8.37 2.58 o 5 21 0 130.69 137.39 5.33 o 0 22 0 3.55 0.59 2.73 o 2 22 0 11.91 9.37 2.30 o 4 22 0 60.28 55.88 4.00 o 6 22 0 80.57 87.38 4.83 o 1 23 0 91.95 87.66 4.23 o 3 23 0 25.28 23.65 2.90 o 5 23 0 19.31 22.87 3.33 o 0 24 0 41.59 37.51 4.97 o 2 24 0 8.17 5.47 2.43 o 4 24 0 53.84 58.53 4.36 o 1 25 0 26.91 24.20 3.29 o 3 25 0 3.31 6.83 2.55 o 0 26 0 11.79 5.61 3.47 o 2 26 0 11.23 11.13 3.69 o 4 26 0 11.30 11.29 3.10 o 1 27 0 6.45 11.72 2.89 o 3 27 0 5.89 5.48 2.91 o 0 28 0 206.73 252.75 11.17 o 2 28 0 114.56 123.85 5.71 o -9 1 1 16.40 19.09 3.56 o -7 1 1 22.51 23.52 2.02 o -5 1 1 8661.75 9023.89 114.29 o -3 1 1 55444.73 52535.63 555.17 o -1 1 1 6506.46 5470.16 201.80 o 1 1 1 3035.57 2935.97 53.64 o 3 1 1 137.45 142.94 2.87 o 5 1 1 60.84 64.23 3.05 o 7 1 1 19.66 16.01 3.31 o 9 1 1 2.23 -0.21 3.71 o -10 2 1 39.14 43.53 5.13 o -8 2 1 180.05 183.07 6.89 o -6 2 1 223.45 233.20 3.83 o -4 2 1 26.91 26.18 1.20 o -2 2 1 10431.97 9775.65 119.74 o 0 2 1 3967.26 3526.03 57.31 o 2 2 1 353.74 355.75 7.33 o 4 2 1 213.20 213.73 3.98 o 6 2 1 298.08 294.56 7.21 o 8 2 1 128.28 130.05 6.34 o -9 3 1 65.48 57.29 5.93 o -7 3 1 53.60 54.06 3.06 o -5 3 1 317.69 337.22 4.63 o -3 3 1 2323.12 2385.85 36.37 o -1 3 1 1533.35 1479.82 18.68 o 1 3 1 618.81 571.46 8.03 o 3 3 1 20.61 19.47 1.65 o 5 3 1 389.23 413.20 7.84 o 7 3 1 203.50 189.97 7.16 o 9 3 1 4.03 1.44 7.29 o -10 4 1 4.60 8.66 4.65 o -8 4 1 62.56 66.09 4.33 o -6 4 1 93.53 95.60 2.78 o -4 4 1 100.73 97.96 2.26 o -2 4 1 2858.12 2746.69 25.41 o 0 4 1 4477.50 4407.88 52.28 o 2 4 1 933.21 992.32 13.38 o 4 4 1 49.90 57.31 2.13 o 6 4 1 165.28 160.54 5.52 o 8 4 1 52.91 57.19 5.21 o -9 5 1 20.47 19.80 3.74 o -7 5 1 249.46 232.04 5.75 o -5 5 1 2074.89 2138.96 23.74 o -3 5 1 4543.07 4524.84 41.58 o -1 5 1 4480.80 4218.92 48.60 o 1 5 1 1570.53 1535.11 23.40 o 3 5 1 938.61 969.53 18.73 o 5 5 1 512.95 507.38 7.69 o 7 5 1 80.83 73.97 4.78 o 9 5 1 0.51 -0.22 3.78 o -10 6 1 18.18 13.37 3.49 o -8 6 1 29.24 26.92 2.84 o -6 6 1 186.22 187.22 3.95 o -4 6 1 117.81 107.25 2.00 o -2 6 1 992.24 964.15 23.26 o 0 6 1 1054.27 1034.80 19.24 o 2 6 1 469.48 488.03 7.56 o 4 6 1 440.61 477.94 8.29 o 6 6 1 38.00 36.75 3.60 o 8 6 1 7.33 6.50 3.22 o -9 7 1 59.17 57.59 4.97 o -7 7 1 64.76 59.03 5.11 o -5 7 1 161.02 167.68 2.85 o -3 7 1 816.43 841.67 9.38 o -1 7 1 4684.87 4739.91 54.67 o 1 7 1 224.95 238.48 5.92 o 3 7 1 1346.48 1357.63 18.28 o 5 7 1 551.01 534.68 8.10 o 7 7 1 71.46 70.44 6.63 o -10 8 1 60.55 53.63 5.68 o -8 8 1 122.36 120.08 4.55 o -6 8 1 257.26 241.58 3.85 o -4 8 1 35.51 42.92 1.43 o -2 8 1 341.33 362.93 4.73 o 0 8 1 471.87 468.82 4.98 o 2 8 1 1703.19 1715.74 21.90 o 4 8 1 532.95 527.25 25.80 o 6 8 1 82.88 72.81 3.66 o 8 8 1 7.83 7.13 3.85 o -9 9 1 62.94 63.76 5.15 o -7 9 1 226.88 228.43 5.92 o -5 9 1 570.48 551.56 6.63 o -3 9 1 17.64 22.59 1.14 o -1 9 1 1226.50 1286.27 15.83 o 1 9 1 737.66 809.35 9.32 o 3 9 1 658.03 730.81 11.00 o 5 9 1 49.81 50.50 3.08 o 7 9 1 34.58 31.94 3.85 o -10 10 1 1.40 -1.00 3.27 o -8 10 1 35.25 33.79 3.12 o -6 10 1 553.46 534.42 6.79 o -4 10 1 847.82 891.71 10.38 o -2 10 1 2057.68 2023.51 30.93 o 0 10 1 4921.87 5219.04 52.99 o 2 10 1 141.61 156.33 5.16 o 4 10 1 243.56 253.54 6.32 o 6 10 1 151.31 149.33 4.89 o 8 10 1 15.64 6.14 6.52 o -9 11 1 49.88 53.72 7.27 o -7 11 1 201.20 211.24 5.83 o -5 11 1 200.86 195.31 3.48 o -3 11 1 254.45 240.68 3.63 o -1 11 1 3128.04 3519.54 41.32 o 1 11 1 1752.13 1871.49 31.39 o 3 11 1 321.89 326.28 6.10 o 5 11 1 0.99 1.22 1.83 o 7 11 1 45.60 53.62 7.94 o -8 12 1 53.07 45.69 4.42 o -6 12 1 105.15 105.27 2.70 o -4 12 1 2.17 0.65 0.85 o -2 12 1 725.77 751.64 13.48 o 0 12 1 151.59 177.11 3.15 o 2 12 1 84.10 76.51 2.16 o 4 12 1 6.37 3.83 1.55 o 6 12 1 15.95 19.12 3.65 o 8 12 1 65.08 68.36 5.67 o -9 13 1 71.49 77.69 7.43 o -7 13 1 48.53 48.29 4.28 o -5 13 1 40.31 43.04 2.66 o -3 13 1 59.98 65.29 1.81 o -1 13 1 198.37 186.02 3.68 o 1 13 1 439.00 414.32 5.56 o 3 13 1 242.39 238.69 4.25 o 5 13 1 20.68 19.61 1.76 o 7 13 1 67.52 69.45 6.25 o -8 14 1 8.65 8.19 3.18 o -6 14 1 34.60 31.97 2.76 o -4 14 1 270.24 239.15 4.78 o -2 14 1 155.08 142.06 3.24 o 0 14 1 13.51 18.57 1.02 o 2 14 1 111.20 112.47 2.68 o 4 14 1 20.40 19.28 1.77 o 6 14 1 43.55 44.80 2.31 o -9 15 1 0.45 4.97 4.65 o -7 15 1 72.39 78.69 4.94 o -5 15 1 113.19 116.70 3.75 o -3 15 1 38.94 41.74 2.20 o -1 15 1 16.90 12.12 1.39 o 1 15 1 170.35 183.90 4.36 o 3 15 1 44.70 50.68 2.12 o 5 15 1 37.67 37.50 2.18 o 7 15 1 31.76 27.09 5.93 o -8 16 1 111.47 111.60 6.29 o -6 16 1 354.33 360.31 6.30 o -4 16 1 270.57 260.17 5.26 o -2 16 1 317.72 309.86 5.51 o 0 16 1 313.56 293.88 5.23 o 2 16 1 23.82 28.03 2.04 o 4 16 1 100.46 96.44 3.50 o 6 16 1 13.63 13.35 3.41 o -7 17 1 278.21 289.72 9.27 o -5 17 1 161.12 150.48 4.19 o -3 17 1 55.07 51.11 3.58 o -1 17 1 729.39 714.53 15.09 o 1 17 1 815.94 801.91 14.23 o 3 17 1 82.82 75.83 4.09 o 5 17 1 15.54 13.40 2.47 o -8 18 1 237.29 272.77 9.70 o -6 18 1 242.84 248.30 5.27 o -4 18 1 10.27 8.37 1.75 o -2 18 1 143.15 132.47 5.64 o 0 18 1 1709.11 1642.78 54.05 o 2 18 1 562.83 572.69 11.43 o 4 18 1 8.22 9.88 2.34 o 6 18 1 16.45 14.75 5.13 o -7 19 1 168.42 197.65 12.24 o -5 19 1 52.07 54.91 3.45 o -3 19 1 19.61 20.47 2.64 o -1 19 1 514.62 477.93 9.88 o 1 19 1 1188.12 1185.95 19.92 o 3 19 1 62.04 63.11 3.77 o 5 19 1 95.00 104.79 5.53 o -8 20 1 138.46 143.42 11.38 o -6 20 1 159.38 166.20 5.09 o -4 20 1 83.09 76.38 3.97 o -2 20 1 64.21 65.72 6.76 o 0 20 1 392.42 357.01 9.56 o 2 20 1 795.92 702.09 13.65 o 4 20 1 145.77 134.01 9.91 o 6 20 1 4.78 6.35 3.93 o -7 21 1 19.80 18.33 6.04 o -5 21 1 30.13 34.11 3.12 o -3 21 1 28.55 31.12 3.18 o -1 21 1 157.90 170.07 5.54 o 1 21 1 6.78 7.52 2.14 o 3 21 1 150.68 142.83 5.39 o 5 21 1 39.95 39.25 3.79 o -6 22 1 57.60 69.82 4.44 o -4 22 1 21.01 17.76 4.06 o -2 22 1 183.14 182.10 5.74 o 0 22 1 100.30 85.48 4.15 o 2 22 1 24.90 28.67 7.61 o 4 22 1 27.37 34.50 3.52 o -5 23 1 5.80 -0.62 2.52 o -3 23 1 47.44 56.78 3.74 o -1 23 1 191.50 197.01 6.21 o 1 23 1 228.67 207.92 6.52 o 3 23 1 75.20 76.36 4.36 o 5 23 1 4.33 5.73 3.39 o -6 24 1 0.78 1.57 2.71 o -4 24 1 59.41 65.70 4.24 o -2 24 1 129.53 135.57 5.19 o 0 24 1 46.81 49.10 3.97 o 2 24 1 7.06 4.48 2.34 o 4 24 1 18.70 21.76 7.21 o -5 25 1 5.10 6.43 2.78 o -3 25 1 19.09 15.02 4.06 o -1 25 1 50.31 57.06 4.65 o 1 25 1 39.24 48.17 3.86 o 3 25 1 14.87 21.91 4.22 o -4 26 1 40.13 46.03 5.90 o -2 26 1 37.85 49.91 3.93 o 0 26 1 7.24 10.36 2.81 o 2 26 1 2.86 0.91 2.64 o -3 27 1 32.51 44.91 4.41 o -1 27 1 20.94 17.10 3.18 o 1 27 1 2.06 -1.96 4.92 o -2 28 1 90.51 106.69 5.43 o 0 28 1 27.67 25.00 3.45 o -10 0 2 296.23 251.52 12.24 o -8 0 2 4455.22 4394.46 112.59 o -6 0 2 14333.40 15185.39 324.51 o -4 0 2 1199.74 1212.34 20.00 o -2 0 2 8109.05 7370.39 87.58 o 0 0 2 884.41 814.04 13.33 o 2 0 2 631.87 653.39 13.73 o 4 0 2 11.33 15.87 3.90 o 6 0 2 107.52 113.71 7.96 o 8 0 2 21.14 18.11 5.50 o -11 1 2 38.71 40.58 4.98 o -9 1 2 69.81 66.33 5.16 o -7 1 2 44.93 44.51 2.73 o -5 1 2 284.45 289.00 4.75 o -3 1 2 4460.76 4345.31 53.48 o -1 1 2 3188.27 3054.99 32.03 o 1 1 2 459.15 432.05 7.00 o 3 1 2 270.99 289.69 6.00 o 5 1 2 101.02 109.62 5.50 o 7 1 2 8.43 11.87 3.42 o -10 2 2 28.84 36.14 4.25 o -8 2 2 1023.30 991.60 13.51 o -6 2 2 3057.90 3114.32 34.87 o -4 2 2 78.27 73.40 2.04 o -2 2 2 3311.55 3178.18 33.31 o 0 2 2 1402.31 1364.91 17.43 o 2 2 2 1885.88 1943.23 25.18 o 4 2 2 278.12 289.98 6.34 o 6 2 2 13.55 9.55 3.10 o 8 2 2 8.63 15.48 5.90 o -11 3 2 21.26 26.46 4.02 o -9 3 2 20.13 14.02 3.29 o -7 3 2 60.98 63.45 2.66 o -5 3 2 1065.73 1083.16 13.21 o -3 3 2 2306.54 2224.99 28.04 o -1 3 2 1849.41 1800.55 19.34 o 1 3 2 524.13 567.02 8.58 o 3 3 2 1568.30 1644.27 43.88 o 5 3 2 337.26 329.39 7.34 o 7 3 2 22.16 14.00 3.63 o -10 4 2 26.16 23.04 3.96 o -8 4 2 53.58 51.76 3.35 o -6 4 2 165.45 150.10 3.16 o -4 4 2 54.99 58.61 1.54 o -2 4 2 299.45 315.33 4.80 o 0 4 2 826.25 801.08 10.87 o 2 4 2 1035.80 1129.31 21.29 o 4 4 2 240.10 237.98 5.78 o 6 4 2 55.43 57.41 3.70 o 8 4 2 50.91 53.84 5.52 o -11 5 2 8.73 5.16 3.28 o -9 5 2 20.85 18.75 2.67 o -7 5 2 45.10 43.20 2.84 o -5 5 2 324.17 320.19 4.52 o -3 5 2 2611.04 2644.50 24.64 o -1 5 2 136.72 125.65 2.27 o 1 5 2 78.42 64.82 2.45 o 3 5 2 4.83 2.89 1.62 o 5 5 2 92.80 91.49 4.02 o 7 5 2 20.44 26.72 4.08 o -10 6 2 48.66 45.71 4.72 o -8 6 2 97.86 89.94 3.95 o -6 6 2 136.87 135.31 2.44 o -4 6 2 168.18 163.07 2.42 o -2 6 2 3398.48 3256.01 34.26 o 0 6 2 890.98 830.09 9.80 o 2 6 2 211.62 211.99 5.74 o 4 6 2 74.76 59.75 3.22 o 6 6 2 60.39 57.56 4.97 o -11 7 2 7.47 16.02 5.58 o -9 7 2 1.85 -2.06 2.06 o -7 7 2 88.78 85.80 3.59 o -5 7 2 70.30 67.47 1.83 o -3 7 2 250.65 278.86 3.43 o -1 7 2 2314.37 2302.17 24.61 o 1 7 2 949.65 982.68 11.63 o 3 7 2 33.79 32.42 2.44 o 5 7 2 25.90 27.43 2.79 o 7 7 2 70.04 75.11 5.63 o -10 8 2 19.63 23.83 3.79 o -8 8 2 25.37 26.37 2.66 o -6 8 2 6.83 4.18 0.92 o -4 8 2 686.21 698.11 7.47 o -2 8 2 935.88 960.72 9.64 o 0 8 2 1733.23 1890.19 23.71 o 2 8 2 485.86 548.11 8.92 o 4 8 2 22.70 19.19 2.03 o 6 8 2 22.46 18.70 2.99 o -11 9 2 23.58 23.08 6.04 o -9 9 2 98.76 94.04 4.37 o -7 9 2 48.84 50.80 3.02 o -5 9 2 656.33 664.67 7.43 o -3 9 2 1660.87 1665.59 39.88 o -1 9 2 1114.72 1183.46 12.92 o 1 9 2 1542.69 1686.76 21.85 o 3 9 2 71.39 74.77 3.11 o 5 9 2 16.39 12.13 2.09 o 7 9 2 5.82 6.68 3.58 o -10 10 2 103.14 123.49 9.24 o -8 10 2 171.73 167.10 5.94 o -6 10 2 79.14 94.23 2.33 o -4 10 2 1230.83 1279.09 14.04 o -2 10 2 1018.62 1135.43 14.44 o 0 10 2 725.67 847.67 11.62 o 2 10 2 75.07 75.18 3.72 o 4 10 2 90.79 78.65 3.41 o 6 10 2 21.68 24.53 2.84 o -9 11 2 67.82 61.35 4.95 o -7 11 2 25.15 22.84 2.47 o -5 11 2 1226.18 1276.43 13.16 o -3 11 2 740.47 797.69 10.72 o -1 11 2 216.51 228.46 3.36 o 1 11 2 276.02 275.18 5.25 o 3 11 2 0.83 1.20 1.79 o 5 11 2 96.92 95.11 4.01 o 7 11 2 90.28 102.10 9.54 o -10 12 2 15.99 15.40 3.68 o -8 12 2 15.27 14.29 6.60 o -6 12 2 241.31 242.47 4.41 o -4 12 2 209.32 208.15 3.68 o -2 12 2 18.66 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