#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/64/2206493.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206493_Fobs loop_ _publ_author_name 'Yang, Shi-Yao' 'Long, La-Sheng' 'Huang, Rong-Bin' 'Zheng, Lan-Sun' 'Ng, Seik Weng' _publ_section_title ; Poly[[bis[(dimethyl sulfoxide)zinc(II)]-di-\m~4~-benzene-1,4-dicarboxylato] dimethyl sulfoxide pentasolvate] ; _journal_coeditor_code LH6473 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1671 _journal_page_last m1673 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 81.311 _cell_angle_beta 80.278 _cell_angle_gamma 73.004 _cell_length_a 10.4449 _cell_length_b 10.9120 _cell_length_c 20.9707 _exptl_crystal_F_000 1044.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file lh6473Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 360.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 7.58 3.73 1.02 o 2 0 0 2039.20 2700.22 40.76 o 3 0 0 900.88 803.60 14.66 o 4 0 0 12835.66 13884.53 191.54 o 5 0 0 619.22 570.66 13.52 o 6 0 0 984.48 1042.60 21.35 o 7 0 0 1642.63 1409.71 44.83 o 8 0 0 488.95 487.09 25.22 o 9 0 0 269.97 339.42 14.63 o 10 0 0 163.75 137.50 10.39 o 11 0 0 839.66 820.73 24.05 o 12 0 0 309.58 342.06 16.36 o -12 1 0 5.30 -6.17 7.01 o -11 1 0 400.24 447.51 18.14 o -10 1 0 270.12 300.32 14.14 o -9 1 0 6.34 -0.30 5.48 o -8 1 0 290.12 299.46 15.30 o -6 1 0 8286.32 8645.52 124.57 o -5 1 0 366.76 335.27 13.58 o -4 1 0 18501.47 18371.88 218.72 o -3 1 0 861.41 674.17 10.95 o -2 1 0 486.62 528.44 8.60 o -1 1 0 100.81 43.13 1.80 o 0 1 0 29753.92 31410.96 374.85 o 1 1 0 1666.41 1400.70 18.10 o 2 1 0 27170.81 32490.58 382.81 o 3 1 0 4.63 45.27 2.20 o 4 1 0 9427.54 9499.81 132.56 o 5 1 0 12.02 7.90 4.66 o 6 1 0 277.32 601.96 14.81 o 7 1 0 191.33 199.82 17.72 o 8 1 0 2296.61 2443.63 47.25 o 9 1 0 194.69 204.79 11.12 o 10 1 0 422.40 392.08 15.39 o 11 1 0 851.90 868.73 24.51 o 12 1 0 866.55 801.46 24.65 o 13 1 0 24.77 17.39 8.49 o -12 2 0 15.86 13.65 14.24 o -11 2 0 985.90 925.71 26.15 o -10 2 0 1185.66 1212.60 37.02 o -9 2 0 408.60 417.13 15.46 o -8 2 0 505.59 466.55 15.35 o -7 2 0 170.85 154.89 16.02 o -6 2 0 4991.73 4844.55 74.17 o -5 2 0 654.08 457.03 9.94 o -4 2 0 6648.54 7627.86 93.86 o -3 2 0 5792.29 6517.80 80.07 o -2 2 0 200.83 177.69 5.73 o -1 2 0 1065.73 1448.23 19.47 o 0 2 0 30113.67 33434.36 465.45 o 1 2 0 312.62 257.84 6.34 o 2 2 0 21169.24 23039.29 271.75 o 3 2 0 3042.71 2738.54 35.14 o 4 2 0 9073.33 9679.92 117.23 o 5 2 0 152.48 136.10 5.64 o 6 2 0 18.95 31.19 4.65 o 7 2 0 373.28 259.79 10.72 o 8 2 0 1578.89 1546.72 30.53 o 9 2 0 15.88 11.09 5.94 o 10 2 0 149.71 89.05 11.19 o 11 2 0 1575.42 1503.76 43.57 o 12 2 0 1412.35 1477.44 35.90 o 13 2 0 32.49 77.50 11.55 o -11 3 0 796.65 787.72 30.52 o -10 3 0 476.00 503.52 18.55 o -9 3 0 431.03 444.76 16.20 o -8 3 0 71.89 55.33 7.56 o -7 3 0 1778.78 1665.06 76.55 o -6 3 0 1765.11 1531.21 78.57 o -5 3 0 14501.53 15087.91 188.14 o -4 3 0 3.37 5.64 2.64 o -3 3 0 34.02 18.55 2.89 o -2 3 0 745.47 777.27 14.56 o -1 3 0 227.45 214.90 7.86 o 0 3 0 1799.05 2016.99 26.60 o 1 3 0 1988.43 1801.20 23.79 o 2 3 0 1745.28 1953.43 25.69 o 3 3 0 2387.74 3102.06 39.73 o 4 3 0 6583.57 6654.46 82.06 o 5 3 0 30.09 97.14 4.59 o 6 3 0 226.88 124.05 4.95 o 7 3 0 146.05 106.36 7.49 o 8 3 0 4044.78 4175.29 67.35 o 9 3 0 619.21 657.48 19.31 o 10 3 0 1856.68 1853.81 38.39 o 11 3 0 45.00 35.21 8.22 o 12 3 0 1123.07 1006.77 29.59 o 13 3 0 195.69 222.33 15.35 o -11 4 0 47.14 42.13 17.21 o -10 4 0 52.85 49.87 11.22 o -9 4 0 484.34 468.66 17.40 o -8 4 0 13.17 25.21 6.74 o -7 4 0 158.54 147.59 13.80 o -6 4 0 960.12 994.57 27.90 o -5 4 0 21.65 33.05 4.34 o -4 4 0 25.33 19.52 3.49 o -3 4 0 12561.06 13048.40 157.91 o -2 4 0 650.60 539.58 10.74 o -1 4 0 1577.05 1928.63 26.76 o 0 4 0 5254.27 5491.40 68.14 o 1 4 0 1202.83 1289.10 22.18 o 2 4 0 6558.50 6912.02 84.52 o 3 4 0 171.18 227.13 5.78 o 4 4 0 194.82 122.41 10.75 o 5 4 0 543.50 364.89 8.74 o 6 4 0 2492.28 2806.04 38.95 o 7 4 0 7.24 6.98 4.24 o 8 4 0 6582.03 6149.23 94.19 o 9 4 0 1512.67 1490.42 48.18 o 10 4 0 1972.91 1953.11 51.87 o 11 4 0 113.70 103.62 10.43 o 12 4 0 982.35 1083.91 29.77 o 13 4 0 10.44 11.00 22.55 o -10 5 0 2.26 -17.80 11.87 o -9 5 0 482.51 489.88 22.66 o -8 5 0 75.72 44.29 7.93 o -7 5 0 3494.92 3341.14 67.27 o -6 5 0 270.91 271.22 11.99 o -5 5 0 2803.60 2789.02 40.48 o -4 5 0 380.54 330.69 10.41 o -3 5 0 9.33 29.72 4.01 o -2 5 0 1260.77 1512.90 23.38 o -1 5 0 863.85 630.55 12.04 o 0 5 0 6152.57 6224.21 77.63 o 1 5 0 14119.55 15766.20 188.67 o 2 5 0 6343.74 7111.13 87.72 o 3 5 0 2419.37 2325.13 31.65 o 4 5 0 2425.35 2432.27 33.41 o 5 5 0 1562.24 1659.01 25.01 o 6 5 0 6937.25 6921.05 97.94 o 7 5 0 101.96 66.51 6.50 o 8 5 0 2841.28 2832.19 61.06 o 9 5 0 656.52 624.49 18.60 o 10 5 0 2780.77 2638.49 75.52 o 11 5 0 147.71 178.32 17.21 o 12 5 0 5.83 25.72 10.37 o 13 5 0 166.41 263.35 33.53 o -9 6 0 69.93 82.27 13.31 o -8 6 0 42.57 48.03 12.31 o -7 6 0 411.07 427.79 20.14 o -6 6 0 12.85 6.70 5.62 o -5 6 0 130.26 100.14 7.62 o -4 6 0 171.77 178.90 13.36 o -2 6 0 1070.92 1039.34 18.50 o -1 6 0 16252.30 17104.20 205.92 o 0 6 0 154.51 371.76 9.11 o 1 6 0 3762.29 3681.40 65.66 o 2 6 0 877.97 804.96 13.95 o 3 6 0 2043.43 2026.87 30.84 o 4 6 0 1591.75 1496.30 22.67 o 5 6 0 1578.07 1592.31 47.68 o 6 6 0 18.99 31.11 5.27 o 7 6 0 279.23 322.32 11.60 o 8 6 0 621.53 531.09 47.03 o 9 6 0 38.58 49.85 10.06 o 10 6 0 1887.20 1858.33 49.27 o 11 6 0 54.32 64.76 12.00 o 12 6 0 112.43 99.23 23.14 o 13 6 0 346.32 356.66 35.01 o -9 7 0 705.36 688.99 40.65 o -8 7 0 22.07 49.31 11.33 o -7 7 0 111.62 107.87 12.90 o -6 7 0 337.82 352.67 17.71 o -5 7 0 3467.01 3585.51 59.72 o -4 7 0 86.34 82.44 7.51 o -3 7 0 1340.90 1418.63 24.42 o -2 7 0 377.98 436.20 19.57 o -1 7 0 2147.08 2302.73 63.67 o 0 7 0 145.17 117.15 8.87 o 1 7 0 5508.31 6043.87 96.78 o 2 7 0 395.32 390.31 12.61 o 4 7 0 444.97 388.67 22.25 o 5 7 0 819.26 923.40 39.76 o 6 7 0 10.65 20.83 5.49 o 7 7 0 266.26 278.26 11.64 o 8 7 0 351.62 361.45 30.12 o 9 7 0 12.54 16.60 8.57 o 10 7 0 1420.28 1373.56 41.08 o 11 7 0 11.61 19.45 9.79 o 12 7 0 297.19 328.43 24.63 o -8 8 0 12.27 6.53 14.24 o -7 8 0 172.45 163.63 22.85 o -6 8 0 99.92 130.19 13.22 o -5 8 0 2579.50 2431.57 93.76 o -4 8 0 750.10 797.93 26.17 o -3 8 0 10.44 25.09 5.94 o -2 8 0 259.53 248.63 13.06 o -1 8 0 1526.69 1543.49 30.75 o 0 8 0 12.72 29.70 6.02 o 1 8 0 40.24 58.80 7.54 o 2 8 0 986.20 829.94 24.92 o 3 8 0 592.31 583.58 16.17 o 4 8 0 185.95 110.05 16.58 o 5 8 0 253.23 248.69 10.82 o 6 8 0 193.25 182.33 9.72 o 7 8 0 280.19 244.98 11.50 o 8 8 0 474.64 480.38 31.90 o 9 8 0 758.77 782.52 28.69 o 10 8 0 2299.22 2335.21 59.10 o 11 8 0 154.96 179.92 16.84 o 12 8 0 44.54 25.78 11.22 o -7 9 0 344.42 379.80 31.45 o -6 9 0 47.85 87.24 18.99 o -5 9 0 599.88 524.31 33.53 o -4 9 0 313.23 308.26 17.30 o -3 9 0 54.25 73.42 10.26 o -2 9 0 32.77 26.31 8.05 o -1 9 0 2045.49 2127.35 50.23 o 0 9 0 20.87 42.88 6.57 o 1 9 0 1117.21 973.70 33.75 o 2 9 0 434.87 445.66 19.22 o 3 9 0 5702.81 5453.46 116.02 o 4 9 0 2429.51 2157.80 61.07 o 5 9 0 36.19 42.75 6.68 o 6 9 0 121.90 115.73 9.30 o 7 9 0 2012.92 1977.06 40.42 o 8 9 0 9.42 3.69 10.68 o 9 9 0 2.46 -2.25 7.75 o 10 9 0 551.09 563.12 26.05 o 11 9 0 498.89 462.49 32.05 o 12 9 0 161.50 213.64 28.49 o -6 10 0 84.46 94.65 20.77 o -5 10 0 56.60 74.18 18.40 o -4 10 0 751.14 743.02 27.37 o -3 10 0 390.28 393.48 24.18 o -2 10 0 10.47 11.12 7.82 o -1 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o 3 12 0 1111.44 1161.98 37.77 o 4 12 0 142.26 166.22 15.79 o 5 12 0 5.92 12.48 8.39 o 6 12 0 156.14 196.88 16.86 o 7 12 0 1395.64 1368.01 41.15 o 8 12 0 260.24 295.23 20.40 o 9 12 0 670.47 720.26 35.31 o -1 13 0 9.13 -0.91 19.44 o 0 13 0 386.15 333.09 21.26 o 1 13 0 181.25 221.52 18.41 o 2 13 0 10.40 0.98 8.48 o 3 13 0 66.10 80.60 13.38 o 4 13 0 65.90 69.19 13.22 o 5 13 0 259.87 298.91 20.28 o 6 13 0 5.11 10.68 9.46 o 7 13 0 8.92 17.99 9.83 o -7 -13 1 33.09 42.46 11.05 o -6 -13 1 74.72 90.27 14.04 o -5 -13 1 268.63 296.08 20.57 o -4 -13 1 1430.43 1410.87 78.04 o -3 -13 1 148.26 131.82 15.87 o -2 -13 1 240.04 257.76 29.23 o -1 -13 1 6.57 19.21 9.12 o 0 -13 1 228.10 238.16 19.04 o 1 -13 1 146.04 127.89 23.44 o -9 -12 1 43.92 49.26 16.91 o -8 -12 1 954.69 922.77 34.22 o -7 -12 1 44.15 70.81 9.74 o -6 -12 1 0.15 0.91 6.32 o -5 -12 1 216.97 217.73 17.41 o -4 -12 1 2359.51 2394.15 60.55 o -3 -12 1 82.84 141.79 15.00 o -2 -12 1 1950.34 1985.92 53.04 o -1 -12 1 42.54 46.55 11.05 o 0 -12 1 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10.53 o 4 -10 1 1166.66 1168.07 35.66 o 5 -10 1 6.36 15.43 13.65 o -11 -9 1 439.45 534.50 26.56 o -10 -9 1 1178.56 1255.91 40.53 o -9 -9 1 0.98 -0.10 7.54 o -8 -9 1 416.04 410.98 21.81 o -7 -9 1 3227.34 3121.58 55.27 o -6 -9 1 2099.54 1857.36 36.89 o -5 -9 1 65.07 73.66 7.49 o -4 -9 1 100.01 113.49 8.65 o -3 -9 1 4.73 62.30 7.63 o -2 -9 1 361.27 417.99 14.92 o -1 -9 1 35.66 37.39 6.63 o 0 -9 1 2150.87 1909.67 110.51 o 1 -9 1 0.05 22.65 6.28 o 2 -9 1 12.33 12.62 9.94 o 3 -9 1 684.14 670.95 31.60 o 4 -9 1 2651.81 2562.51 60.53 o 5 -9 1 124.99 105.34 19.29 o 6 -9 1 52.84 62.61 17.21 o -12 -8 1 17.67 11.82 9.59 o -11 -8 1 53.49 54.07 12.06 o -10 -8 1 1941.13 1920.71 52.20 o -9 -8 1 340.79 301.70 37.09 o -8 -8 1 3.43 7.05 7.60 o -7 -8 1 53.86 48.23 6.62 o -6 -8 1 61.64 61.31 7.74 o -5 -8 1 68.01 55.07 8.21 o -4 -8 1 400.98 375.79 16.35 o -3 -8 1 20.42 28.06 6.40 o -2 -8 1 1533.03 1357.36 27.53 o -1 -8 1 9.86 7.90 4.87 o 0 -8 1 217.23 237.34 10.66 o 1 -8 1 448.32 360.42 20.23 o 2 -8 1 292.04 173.95 12.82 o 3 -8 1 22.03 25.58 5.06 o 4 -8 1 4350.82 4279.35 69.31 o 5 -8 1 45.78 70.42 8.19 o 6 -8 1 5.46 6.40 8.06 o 7 -8 1 79.78 134.86 14.54 o 8 -8 1 758.21 690.77 40.65 o -12 -7 1 15.53 24.14 11.00 o -11 -7 1 411.86 427.73 22.94 o -10 -7 1 1349.43 1379.76 41.20 o -9 -7 1 688.73 639.17 27.89 o -8 -7 1 0.13 10.44 8.90 o -7 -7 1 1752.30 1664.61 32.69 o -6 -7 1 2956.47 2760.39 47.54 o -5 -7 1 7692.03 7358.86 109.52 o -4 -7 1 607.06 486.40 16.68 o -2 -7 1 613.16 605.79 15.73 o -1 -7 1 32.94 23.35 6.39 o 0 -7 1 2129.15 1831.25 27.86 o 1 -7 1 89.17 142.01 9.29 o 2 -7 1 6105.08 6218.43 132.00 o 3 -7 1 45.34 46.93 5.29 o 4 -7 1 3262.41 3140.93 45.73 o 5 -7 1 216.97 291.23 10.84 o 6 -7 1 465.84 452.43 19.82 o 7 -7 1 260.37 264.20 16.99 o 8 -7 1 661.06 701.45 39.17 o 9 -7 1 6.08 -2.37 12.76 o -13 -6 1 555.47 617.48 43.32 o -12 -6 1 49.80 51.77 18.25 o -11 -6 1 194.13 194.38 16.96 o -10 -6 1 504.33 448.45 21.96 o -9 -6 1 630.58 613.79 49.11 o -8 -6 1 12.38 17.95 7.13 o -7 -6 1 1852.26 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