#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2206505.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206505_Fobs loop_ _publ_author_name 'Zhou, Wei' 'Xia, Chun-Nian' 'Feng, Wen' 'Hu, Wei-Xiao' _publ_section_title ; 2-Methyl-2-nitropropyl methanesulfonate ; _journal_coeditor_code OB6532 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2523 _journal_page_last o2524 _journal_volume 61 _journal_year 2005 _space_group_IT_number 43 _symmetry_space_group_name_Hall 'F -2d 2' _symmetry_space_group_name_H-M 'F 2 d d' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.6520 _cell_length_b 19.8080 _cell_length_c 20.9340 _exptl_crystal_F_000 1664.00 _reflns_d_resolution_high 0.8365 _[local]_cod_data_source_file ob6532Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' F 2dd HU55 12*16*20 2005.3.8 CMQ 26/50' _shelx_refln_list_code 4 _shelx_f_calc_maximum 608.63 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, -z' 'x+1/4, -y+1/4, z+1/4' 'x+1/4, y+1/4, -z+1/4' 'x, y+1/2, z+1/2' 'x, -y+1/2, -z+1/2' 'x+1/4, -y+3/4, z+3/4' 'x+1/4, y+3/4, -z+3/4' 'x+1/2, y, z+1/2' 'x+1/2, -y, -z+1/2' 'x+3/4, -y+1/4, z+3/4' 'x+3/4, y+1/4, -z+3/4' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, -z' 'x+3/4, -y+3/4, z+1/4' 'x+3/4, y+3/4, -z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 170500.39 188490.70 2009.51 o 8 0 0 473.39 702.79 28.74 o 2 2 0 8676.71 9849.23 69.38 o 6 2 0 1254.65 1349.97 37.80 o 10 2 0 1.51 -7.68 35.84 o 0 4 0 370433.97 366779.88 2002.84 o 4 4 0 27897.74 29899.25 174.87 o 8 4 0 750.89 740.44 29.47 o 2 6 0 1822.11 1961.66 41.43 o 6 6 0 3354.74 3278.75 80.38 o 10 6 0 498.73 456.02 33.36 o 0 8 0 338.52 401.98 12.30 o 4 8 0 231.44 176.14 14.35 o 8 8 0 804.24 760.04 32.78 o 2 10 0 3676.34 3844.31 69.02 o 6 10 0 7145.70 7224.03 123.94 o 0 12 0 6939.00 7236.07 98.19 o 4 12 0 2335.74 2204.05 58.11 o 8 12 0 304.84 392.92 29.18 o 2 14 0 11878.65 11297.83 139.77 o 6 14 0 5085.61 5092.66 117.80 o 0 16 0 482.10 480.26 23.15 o 4 16 0 523.69 554.56 28.11 o 2 18 0 4819.21 4748.43 109.13 o 6 18 0 1259.93 1183.39 41.25 o 0 20 0 629.52 680.39 31.03 o 4 20 0 107.49 120.50 24.41 o 2 22 0 295.33 255.69 29.13 o 1 1 1 3780.21 4050.60 32.60 o 3 1 1 2115.32 2784.68 108.19 o 5 1 1 9256.92 9522.94 77.11 o 7 1 1 1960.65 2107.10 39.27 o 9 1 1 316.70 318.33 33.09 o 1 3 1 25894.38 26432.09 669.42 o 3 3 1 22355.39 24150.71 297.53 o 5 3 1 8261.21 9078.12 76.86 o 7 3 1 1488.43 1446.97 30.41 o 9 3 1 152.14 167.76 16.43 o 1 5 1 2225.46 2398.70 60.62 o 3 5 1 3277.39 3435.56 55.45 o 5 5 1 8911.16 9105.51 82.22 o 7 5 1 2160.51 2234.83 68.42 o 9 5 1 475.32 480.23 25.29 o 1 7 1 24208.56 25151.02 136.10 o 3 7 1 1136.14 1188.28 29.02 o 5 7 1 13445.63 13428.49 99.92 o 7 7 1 1074.95 1039.44 23.51 o 9 7 1 596.08 597.39 22.78 o 1 9 1 726.13 650.03 22.86 o 3 9 1 4311.88 4309.67 79.37 o 5 9 1 514.45 566.52 15.73 o 7 9 1 602.51 590.91 20.44 o 9 9 1 345.46 317.49 21.22 o 1 11 1 8757.97 9012.12 73.17 o 3 11 1 804.05 875.31 19.33 o 5 11 1 5140.96 5184.49 214.60 o 7 11 1 1005.96 1029.97 36.38 o 9 11 1 212.66 294.71 38.71 o 1 13 1 398.67 421.43 13.03 o 3 13 1 4316.21 4511.75 77.39 o 5 13 1 626.77 664.50 20.12 o 7 13 1 405.83 430.28 20.32 o 1 15 1 2671.80 2804.63 53.41 o 3 15 1 222.14 247.11 42.89 o 5 15 1 1355.03 1325.91 63.14 o 7 15 1 93.54 125.24 32.12 o 1 17 1 1273.52 1368.23 34.81 o 3 17 1 1389.42 1452.26 32.64 o 5 17 1 908.35 897.24 24.88 o 7 17 1 193.13 221.39 19.89 o 1 19 1 1216.27 1148.64 25.76 o 3 19 1 503.48 514.52 21.85 o 5 19 1 186.69 174.41 19.15 o 1 21 1 585.02 643.40 22.71 o 3 21 1 148.06 164.46 17.67 o 1 23 1 478.08 480.29 26.09 o 2 0 2 9295.06 9662.60 68.25 o 6 0 2 176.32 156.49 16.49 o 10 0 2 121.09 175.01 24.80 o 0 2 2 1074.48 1281.31 19.39 o 2 2 2 220150.23 233978.83 1725.59 o 4 2 2 1751.70 1746.47 44.29 o 6 2 2 11542.58 12322.62 138.76 o 8 2 2 281.91 242.37 23.29 o 10 2 2 1443.18 1490.13 46.26 o 0 4 2 72446.70 74726.25 835.20 o 2 4 2 2648.44 2665.58 42.84 o 4 4 2 18338.90 19181.66 141.67 o 6 4 2 46.96 51.25 27.77 o 8 4 2 531.29 438.48 26.75 o 10 4 2 27.35 -23.58 42.30 o 0 6 2 277.00 268.13 10.31 o 2 6 2 20748.65 21370.26 127.21 o 4 6 2 939.86 832.89 24.42 o 6 6 2 9283.13 9371.38 130.56 o 8 6 2 172.88 182.84 22.51 o 0 8 2 404.33 385.31 12.69 o 2 8 2 2142.86 2369.60 50.24 o 4 8 2 2207.61 2001.06 57.14 o 6 8 2 497.98 513.33 23.30 o 8 8 2 2025.80 1845.60 55.51 o 0 10 2 1175.89 1205.53 32.06 o 2 10 2 8130.35 8897.05 101.73 o 4 10 2 329.95 344.56 18.04 o 6 10 2 5236.99 5145.48 107.55 o 8 10 2 97.56 123.76 21.83 o 0 12 2 3401.09 3572.07 70.56 o 2 12 2 1143.89 1142.90 33.13 o 4 12 2 3639.70 3468.87 82.19 o 6 12 2 979.95 884.42 32.10 o 8 12 2 924.95 845.22 35.60 o 0 14 2 1877.38 1741.12 47.25 o 2 14 2 1367.23 1303.42 39.31 o 4 14 2 659.57 651.23 27.04 o 6 14 2 713.09 719.51 32.83 o 8 14 2 125.31 138.44 26.16 o 0 16 2 12297.61 12149.21 153.03 o 2 16 2 128.77 128.47 20.86 o 4 16 2 5856.53 5606.10 117.64 o 6 16 2 128.10 121.32 22.27 o 0 18 2 1150.37 1076.90 34.49 o 2 18 2 1194.09 1245.93 36.48 o 4 18 2 114.09 124.00 22.66 o 6 18 2 15.44 23.63 41.92 o 0 20 2 1918.14 1892.88 54.15 o 2 20 2 11.47 0.00 36.96 o 4 20 2 869.65 805.32 36.87 o 0 22 2 42.12 54.75 39.34 o 2 22 2 211.23 277.42 26.84 o 1 1 3 4238.47 3651.93 36.68 o 3 1 3 23156.76 24936.23 134.84 o 5 1 3 1784.44 1857.04 53.00 o 7 1 3 1075.75 1045.78 31.37 o 9 1 3 242.50 226.42 26.11 o 1 3 3 2304.26 2019.36 31.59 o 3 3 3 5238.99 5284.83 66.94 o 5 3 3 3605.17 3731.54 72.76 o 7 3 3 1052.23 1054.76 31.13 o 9 3 3 782.36 814.75 34.09 o 1 5 3 787.19 690.89 20.10 o 3 5 3 15766.46 15654.26 118.72 o 5 5 3 515.17 529.40 19.31 o 7 5 3 4052.41 3786.39 93.00 o 9 5 3 116.09 154.29 24.07 o 1 7 3 8460.82 8133.18 80.54 o 3 7 3 3731.67 3806.14 65.67 o 5 7 3 2066.62 1973.41 49.49 o 7 7 3 1628.60 1571.64 47.43 o 9 7 3 111.05 107.03 24.90 o 1 9 3 590.28 598.53 17.07 o 3 9 3 9552.17 10141.01 111.45 o 5 9 3 1870.59 1738.48 50.75 o 7 9 3 3512.45 3348.06 93.80 o 9 9 3 651.64 756.25 35.94 o 1 11 3 11813.51 11820.73 122.18 o 3 11 3 907.92 973.50 28.70 o 5 11 3 3262.87 3078.03 82.37 o 7 11 3 637.36 556.81 29.91 o 9 11 3 103.03 123.51 27.09 o 1 13 3 2780.31 2745.96 68.74 o 3 13 3 1692.81 1786.87 50.21 o 5 13 3 4038.26 3850.61 96.35 o 7 13 3 443.19 434.28 29.42 o 1 15 3 2092.82 2139.40 55.86 o 3 15 3 248.84 164.42 22.08 o 5 15 3 274.67 -58.26 58.26 o 7 15 3 497.54 530.52 31.12 o 1 17 3 1033.02 1048.76 33.12 o 3 17 3 745.05 737.81 29.91 o 5 17 3 788.98 815.72 34.05 o 7 17 3 386.49 479.40 31.71 o 1 19 3 763.43 788.64 32.59 o 3 19 3 246.57 265.37 26.41 o 5 19 3 72.48 54.66 24.99 o 1 21 3 493.60 535.97 31.46 o 3 21 3 315.82 334.47 29.47 o 1 23 3 423.86 416.91 32.00 o 0 0 4 310543.47 293697.50 1704.24 o 4 0 4 39356.46 42480.91 206.06 o 8 0 4 1676.13 1597.51 49.67 o 0 2 4 21639.77 20045.22 89.37 o 2 2 4 7731.41 7620.93 68.81 o 4 2 4 1968.28 2185.06 51.50 o 6 2 4 1266.44 1273.48 41.94 o 8 2 4 794.39 812.24 32.10 o 10 2 4 64.59 19.16 46.00 o 0 4 4 140889.06 130775.05 1253.66 o 2 4 4 9085.56 9172.40 79.89 o 4 4 4 16460.14 16141.81 132.90 o 6 4 4 1893.85 1889.05 51.77 o 8 4 4 2079.01 1980.55 63.11 o 10 4 4 151.60 136.89 27.96 o 0 6 4 21263.27 23105.60 124.41 o 2 6 4 6963.31 7184.71 77.90 o 4 6 4 429.43 430.57 16.83 o 6 6 4 3260.60 3096.76 79.98 o 8 6 4 288.03 263.96 23.83 o 0 8 4 38742.92 39728.38 185.48 o 2 8 4 608.94 608.75 18.19 o 4 8 4 5439.76 5343.26 89.29 o 6 8 4 299.95 303.79 22.81 o 8 8 4 1189.55 1111.65 37.45 o 0 10 4 12986.23 13722.44 121.47 o 2 10 4 3425.23 3589.58 69.55 o 4 10 4 846.71 820.63 23.64 o 6 10 4 7553.65 7211.73 128.29 o 8 10 4 165.83 201.17 23.05 o 0 12 4 10360.58 11313.45 123.08 o 2 12 4 6529.92 6614.66 100.24 o 4 12 4 2780.27 2615.14 73.98 o 6 12 4 116.62 64.04 38.37 o 8 12 4 144.42 141.65 24.12 o 0 14 4 23.96 336.78 18.92 o 2 14 4 3482.09 3725.98 82.77 o 4 14 4 1168.22 1086.55 32.98 o 6 14 4 4133.09 3914.84 105.59 o 8 14 4 195.36 174.82 28.74 o 0 16 4 25.90 30.54 18.92 o 2 16 4 3509.62 3621.09 89.96 o 4 16 4 116.40 111.70 21.54 o 6 16 4 75.62 107.85 24.26 o 0 18 4 1271.29 1464.09 45.87 o 2 18 4 728.26 784.16 33.27 o 4 18 4 775.74 773.11 32.73 o 6 18 4 1141.55 1087.92 41.39 o 0 20 4 349.47 307.44 27.82 o 2 20 4 119.89 163.68 22.08 o 4 20 4 230.76 270.08 26.99 o 0 22 4 175.15 154.15 27.91 o 2 22 4 99.80 162.70 26.16 o 1 1 5 25449.97 24109.42 109.32 o 3 1 5 2670.87 2577.44 49.00 o 5 1 5 7527.59 8049.66 105.71 o 7 1 5 4664.07 4672.78 101.54 o 9 1 5 49.52 35.84 37.64 o 1 3 5 48102.99 48053.44 773.93 o 3 3 5 2107.89 2288.52 47.57 o 5 3 5 15185.65 15218.52 144.36 o 7 3 5 1567.94 1564.98 45.78 o 9 3 5 158.24 117.44 24.85 o 1 5 5 12382.90 12367.21 92.19 o 3 5 5 11702.90 12977.49 112.40 o 5 5 5 8772.22 8697.06 115.70 o 7 5 5 1365.50 1552.94 46.80 o 9 5 5 771.71 871.11 33.80 o 1 7 5 5815.68 5912.04 73.10 o 3 7 5 7928.05 8522.11 98.26 o 5 7 5 9804.10 9479.89 123.63 o 7 7 5 802.98 841.52 32.00 o 9 7 5 894.67 939.71 38.03 o 1 9 5 2303.78 2237.16 52.43 o 3 9 5 142.06 115.49 13.66 o 5 9 5 1744.92 1776.22 50.70 o 7 9 5 99.61 76.59 21.15 o 9 9 5 305.46 304.37 28.45 o 1 11 5 1506.26 1307.24 39.32 o 3 11 5 498.17 458.29 19.60 o 5 11 5 2722.05 2958.75 80.40 o 7 11 5 1003.98 1001.77 36.19 o 1 13 5 692.36 786.39 22.86 o 3 13 5 1150.10 1386.29 38.82 o 5 13 5 512.19 499.22 27.43 o 7 13 5 151.83 138.54 24.07 o 1 15 5 7095.99 6921.12 116.69 o 3 15 5 4314.30 4261.53 97.53 o 5 15 5 1365.44 1294.87 38.82 o 7 15 5 351.78 388.31 29.18 o 1 17 5 2271.44 2278.54 63.06 o 3 17 5 148.37 180.17 22.42 o 5 17 5 1231.85 1121.77 39.21 o 1 19 5 1125.35 1128.03 37.36 o 3 19 5 519.62 505.58 29.91 o 5 19 5 203.60 140.78 27.09 o 1 21 5 282.77 230.74 27.09 o 3 21 5 64.68 142.91 24.70 o 1 23 5 65.95 13.66 45.76 o 2 0 6 28409.17 29008.42 141.25 o 6 0 6 895.75 769.75 24.42 o 10 0 6 32.51 -29.32 48.48 o 0 2 6 831.68 773.56 20.29 o 2 2 6 17765.57 17914.81 113.95 o 4 2 6 154.13 128.77 12.01 o 6 2 6 17324.32 17024.23 174.04 o 8 2 6 264.11 293.82 24.41 o 10 2 6 2892.96 3224.78 91.09 o 0 4 6 22526.54 22362.22 121.10 o 2 4 6 2561.17 2438.93 46.51 o 4 4 6 7865.18 8115.82 99.41 o 6 4 6 698.78 702.42 24.66 o 8 4 6 212.62 199.86 25.14 o 0 6 6 10765.48 10806.97 92.83 o 2 6 6 21784.37 21790.88 142.63 o 4 6 6 16.32 32.34 22.66 o 6 6 6 13088.95 12494.73 156.73 o 8 6 6 270.15 259.87 24.61 o 0 8 6 30238.42 30253.67 172.31 o 2 8 6 1432.70 1701.49 47.20 o 4 8 6 8631.16 8013.66 111.98 o 6 8 6 3681.79 3633.70 91.67 o 8 8 6 530.78 498.92 29.37 o 0 10 6 12426.71 12371.88 122.80 o 2 10 6 5872.95 5701.93 89.31 o 4 10 6 259.88 222.97 17.75 o 6 10 6 2363.03 2366.77 64.52 o 8 10 6 32.90 44.06 41.09 o 0 12 6 11710.99 11769.84 131.86 o 2 12 6 325.74 352.38 18.67 o 4 12 6 5560.17 5522.26 106.40 o 6 12 6 801.41 781.50 30.59 o 8 12 6 669.97 666.09 33.22 o 0 14 6 2251.89 2057.60 52.85 o 2 14 6 514.99 470.15 21.93 o 4 14 6 569.84 558.47 27.43 o 6 14 6 216.71 193.05 24.75 o 0 16 6 1797.79 2159.98 58.14 o 2 16 6 95.54 82.71 21.15 o 4 16 6 1316.65 1314.94 42.47 o 6 16 6 117.56 152.45 23.10 o 0 18 6 873.46 723.59 31.61 o 2 18 6 14.47 52.03 37.54 o 4 18 6 167.57 216.54 27.23 o 6 18 6 64.88 112.33 26.40 o 0 20 6 820.94 900.94 34.82 o 2 20 6 89.50 149.53 23.19 o 4 20 6 399.03 413.16 30.98 o 0 22 6 375.11 286.63 27.52 o 2 22 6 15.05 -31.17 40.75 o 1 1 7 39943.03 39739.24 753.56 o 3 1 7 19055.86 20018.97 137.73 o 5 1 7 2090.02 1999.52 59.52 o 7 1 7 317.69 254.63 22.37 o 9 1 7 335.00 337.93 28.06 o 1 3 7 3219.87 3524.18 52.73 o 3 3 7 1342.54 1269.49 32.75 o 5 3 7 431.67 412.76 18.77 o 7 3 7 261.85 225.30 22.32 o 9 3 7 308.37 306.80 28.11 o 1 5 7 9564.33 8850.54 86.23 o 3 5 7 11925.61 11658.86 115.14 o 5 5 7 4242.28 3902.48 82.70 o 7 5 7 2860.66 2668.66 67.41 o 9 5 7 876.30 933.04 38.62 o 1 7 7 1695.04 1826.28 45.70 o 3 7 7 3758.15 3771.41 70.87 o 5 7 7 303.47 257.40 18.92 o 7 7 7 406.19 371.40 25.24 o 9 7 7 121.29 150.74 26.60 o 1 9 7 1916.07 2034.61 53.20 o 3 9 7 2110.43 2198.70 59.37 o 5 9 7 5549.77 5452.99 102.65 o 7 9 7 2916.75 2961.81 75.14 o 9 9 7 1040.45 1117.31 42.12 o 1 11 7 7561.36 7218.92 103.50 o 3 11 7 3196.33 3216.06 78.23 o 5 11 7 260.64 301.50 22.95 o 7 11 7 71.68 64.43 22.22 o 1 13 7 4582.19 4398.65 88.89 o 3 13 7 715.29 747.94 25.29 o 5 13 7 5118.66 4846.95 111.23 o 7 13 7 855.78 851.96 35.70 o 1 15 7 184.65 269.99 20.23 o 3 15 7 265.98 330.83 24.36 o 5 15 7 50.67 42.94 20.96 o 7 15 7 88.63 68.86 43.67 o 1 17 7 1057.99 1137.37 34.19 o 3 17 7 227.15 230.50 24.80 o 5 17 7 917.53 912.77 35.99 o 1 19 7 1346.51 1305.93 38.04 o 3 19 7 945.89 853.11 35.07 o 5 19 7 464.68 462.19 33.75 o 1 21 7 109.30 62.00 46.73 o 3 21 7 35.14 47.70 44.01 o 0 0 8 4104.85 4492.08 59.20 o 4 0 8 3096.07 3074.15 65.78 o 8 0 8 4104.44 4736.88 113.04 o 0 2 8 8553.41 8379.06 79.67 o 2 2 8 2199.76 2208.87 46.79 o 4 2 8 816.37 815.40 27.53 o 6 2 8 573.90 549.92 24.27 o 8 2 8 369.54 410.44 25.29 o 0 4 8 14624.26 13394.40 105.39 o 2 4 8 4282.94 4558.48 68.28 o 4 4 8 8482.08 7659.51 103.02 o 6 4 8 4102.15 4166.49 92.18 o 8 4 8 3428.68 3293.42 80.11 o 0 6 8 62.61 84.56 10.41 o 2 6 8 14221.49 14038.66 122.81 o 4 6 8 2027.21 1933.52 57.13 o 6 6 8 3663.73 3410.29 90.75 o 8 6 8 818.37 748.51 33.36 o 0 8 8 36117.37 35695.77 201.48 o 2 8 8 3982.01 4066.21 74.04 o 4 8 8 9673.42 9142.76 124.35 o 6 8 8 107.18 129.35 22.08 o 8 8 8 1399.59 1366.59 39.94 o 0 10 8 970.79 1027.15 31.13 o 2 10 8 6941.91 6804.94 102.11 o 4 10 8 692.40 680.05 24.27 o 6 10 8 3905.27 3685.18 100.19 o 8 10 8 83.21 32.92 40.31 o 0 12 8 6200.39 5938.94 99.28 o 2 12 8 2489.57 2337.16 68.62 o 4 12 8 1893.58 1810.66 55.03 o 6 12 8 143.95 133.14 23.58 o 8 12 8 146.09 56.50 48.63 o 0 14 8 977.59 1075.13 30.69 o 2 14 8 1093.77 1067.37 31.28 o 4 14 8 469.19 467.70 27.96 o 6 14 8 1911.31 2003.33 56.97 o 0 16 8 173.51 216.40 23.34 o 2 16 8 305.38 301.94 24.02 o 4 16 8 119.26 116.75 21.74 o 6 16 8 11.54 2.58 42.06 o 0 18 8 580.20 578.06 30.15 o 2 18 8 496.03 529.65 28.89 o 4 18 8 857.27 902.01 35.55 o 0 20 8 8.55 -2.33 36.27 o 2 20 8 54.75 87.92 22.66 o 4 20 8 2.73 37.64 41.77 o 0 22 8 6.89 0.00 39.44 o 1 1 9 14474.22 13893.05 109.27 o 3 1 9 5996.33 6077.75 84.51 o 5 1 9 4086.85 3851.14 81.96 o 7 1 9 1568.18 1695.16 49.43 o 9 1 9 550.60 531.79 31.81 o 1 3 9 21702.30 20979.71 138.76 o 3 3 9 4624.96 4190.40 72.41 o 5 3 9 3817.50 3680.47 82.63 o 7 3 9 2133.43 2112.33 62.33 o 9 3 9 250.56 266.53 27.91 o 1 5 9 5979.67 6007.02 79.56 o 3 5 9 6474.68 6552.90 90.75 o 5 5 9 3557.34 3599.03 82.96 o 7 5 9 1630.06 1676.39 50.25 o 9 5 9 236.76 262.50 28.59 o 1 7 9 1605.54 1515.54 38.25 o 3 7 9 675.38 660.47 20.53 o 5 7 9 1755.15 1768.55 52.06 o 7 7 9 2489.25 2640.40 70.51 o 9 7 9 405.70 411.80 31.71 o 1 9 9 5049.67 5078.00 85.33 o 3 9 9 450.61 453.66 20.13 o 5 9 9 925.31 768.08 28.41 o 7 9 9 347.91 416.66 28.06 o 1 11 9 2841.55 2898.94 71.65 o 3 11 9 2383.73 2155.23 55.82 o 5 11 9 1753.81 1951.17 57.51 o 7 11 9 1185.21 1185.28 39.69 o 1 13 9 795.84 707.70 24.32 o 3 13 9 297.93 262.89 21.59 o 5 13 9 191.28 222.47 24.17 o 7 13 9 109.08 95.84 24.99 o 1 15 9 4216.47 4217.79 98.65 o 3 15 9 2936.24 2772.47 70.37 o 5 15 9 839.16 852.11 34.19 o 7 15 9 286.94 210.47 29.42 o 1 17 9 1505.11 1418.64 42.86 o 3 17 9 375.49 344.30 26.21 o 5 17 9 584.08 537.05 33.70 o 1 19 9 286.07 260.51 28.40 o 3 19 9 378.17 403.68 28.93 o 1 21 9 166.91 111.50 27.23 o 3 21 9 27.00 8.22 45.81 o 2 0 10 3173.42 3292.99 60.93 o 6 0 10 593.58 612.61 27.53 o 0 2 10 5487.23 5159.99 72.62 o 2 2 10 13979.99 15791.63 129.85 o 4 2 10 1668.03 1785.71 44.67 o 6 2 10 20179.08 20448.02 203.02 o 8 2 10 161.99 160.76 23.78 o 0 4 10 877.54 825.35 24.91 o 2 4 10 51.31 90.01 11.62 o 4 4 10 243.58 244.66 16.53 o 6 4 10 2119.33 2118.49 58.05 o 8 4 10 33.74 74.11 22.81 o 0 6 10 7480.32 7277.11 93.69 o 2 6 10 1790.43 1585.72 41.17 o 4 6 10 584.13 560.53 20.77 o 6 6 10 7582.30 7473.50 128.92 o 8 6 10 92.40 79.60 22.03 o 0 8 10 13863.48 13059.32 132.12 o 2 8 10 1793.46 1780.65 46.71 o 4 8 10 3722.28 3778.00 84.87 o 6 8 10 1550.35 1571.19 47.87 o 8 8 10 339.06 354.27 28.50 o 0 10 10 73.76 74.89 14.34 o 2 10 10 164.95 125.90 16.58 o 4 10 10 753.80 727.81 28.06 o 6 10 10 1429.32 1346.80 38.28 o 8 10 10 16.73 -30.68 41.96 o 0 12 10 10479.87 10936.48 139.34 o 2 12 10 3605.78 3582.37 85.54 o 4 12 10 3273.50 3500.69 90.83 o 6 12 10 435.45 459.37 28.01 o 0 14 10 0.32 37.68 31.02 o 2 14 10 443.90 518.76 26.07 o 4 14 10 172.09 176.37 23.63 o 6 14 10 385.81 424.49 30.30 o 0 16 10 3163.21 3518.94 94.67 o 2 16 10 568.58 501.36 28.94 o 4 16 10 1278.11 1238.14 39.21 o 6 16 10 97.96 71.97 44.06 o 0 18 10 202.18 133.68 23.93 o 2 18 10 1012.40 1034.55 35.85 o 4 18 10 75.57 45.37 42.74 o 0 20 10 1190.99 1285.52 42.90 o 2 20 10 231.56 272.03 27.72 o 1 1 11 18033.10 18253.10 139.33 o 3 1 11 1143.18 1282.93 37.85 o 5 1 11 5617.87 5246.01 100.76 o 7 1 11 280.26 332.38 23.78 o 9 1 11 377.19 387.73 31.51 o 1 3 11 5574.62 5375.68 80.59 o 3 3 11 101.56 127.50 13.57 o 5 3 11 152.56 156.29 18.28 o 7 3 11 175.66 206.81 21.15 o 9 3 11 36.17 64.96 42.45 o 1 5 11 17898.77 17754.86 146.86 o 3 5 11 1105.82 1103.02 32.69 o 5 5 11 9418.90 9085.65 133.51 o 7 5 11 521.19 452.67 27.53 o 9 5 11 732.53 808.83 37.16 o 1 7 11 2348.34 2252.27 60.65 o 3 7 11 931.82 875.81 27.43 o 5 7 11 1410.95 1471.64 48.89 o 7 7 11 59.21 55.77 39.10 o 1 9 11 7971.86 8022.12 111.21 o 3 9 11 1374.24 1370.59 40.09 o 5 9 11 4817.83 4725.08 105.28 o 7 9 11 1091.29 1091.62 37.70 o 1 11 11 204.88 211.83 17.85 o 3 11 11 508.20 479.62 25.39 o 5 11 11 120.78 98.96 21.54 o 7 11 11 69.08 63.99 23.83 o 1 13 11 2174.70 2148.97 59.02 o 3 13 11 965.94 859.37 31.66 o 5 13 11 1718.43 1717.01 52.59 o 7 13 11 577.61 512.93 33.61 o 1 15 11 517.53 538.12 26.75 o 3 15 11 797.01 793.51 32.10 o 5 15 11 233.35 237.89 25.77 o 1 17 11 62.65 68.90 38.12 o 3 17 11 0.38 -29.52 35.98 o 5 17 11 647.49 639.43 34.82 o 1 19 11 449.55 458.11 29.81 o 3 19 11 554.18 511.32 31.42 o 1 21 11 27.11 51.35 44.01 o 0 0 12 476.58 389.09 15.56 o 4 0 12 2187.43 2116.05 52.66 o 8 0 12 1588.36 1684.36 48.06 o 0 2 12 1080.78 1033.13 33.42 o 2 2 12 2319.43 2452.45 59.43 o 4 2 12 2312.62 2368.03 66.43 o 6 2 12 1467.60 1497.76 46.31 o 8 2 12 208.86 209.88 23.34 o 0 4 12 5580.36 5339.88 84.43 o 2 4 12 4140.49 4131.77 77.74 o 4 4 12 5348.59 4757.97 94.22 o 6 4 12 95.05 100.41 21.10 o 8 4 12 1419.57 1333.61 41.59 o 0 6 12 123.88 158.92 14.64 o 2 6 12 4283.18 4212.49 82.36 o 4 6 12 1202.55 1209.23 34.10 o 6 6 12 2691.78 2669.96 68.91 o 8 6 12 409.63 433.88 29.52 o 0 8 12 5017.81 4764.25 88.04 o 2 8 12 863.09 839.50 26.70 o 4 8 12 4002.35 3627.76 88.81 o 6 8 12 129.01 149.14 23.10 o 8 8 12 917.66 904.79 38.13 o 0 10 12 5540.78 5043.71 96.13 o 2 10 12 2616.12 2595.73 74.61 o 4 10 12 2111.90 2090.57 59.75 o 6 10 12 1418.60 1475.53 44.80 o 0 12 12 495.04 547.42 26.36 o 2 12 12 1784.17 1793.60 55.08 o 4 12 12 1037.62 961.96 34.44 o 6 12 12 103.87 129.30 24.12 o 0 14 12 4983.00 4628.32 103.93 o 2 14 12 672.43 767.37 30.30 o 4 14 12 1337.56 1281.61 38.33 o 6 14 12 481.12 478.87 32.68 o 0 16 12 485.05 556.30 29.52 o 2 16 12 159.84 159.69 21.59 o 4 16 12 72.68 87.53 22.37 o 0 18 12 81.08 63.07 40.26 o 2 18 12 672.88 787.29 33.70 o 4 18 12 13.09 -7.78 42.40 o 0 20 12 258.25 307.96 29.76 o 2 20 12 261.22 243.82 30.98 o 1 1 13 3314.26 3321.20 69.39 o 3 1 13 3462.37 3465.99 76.49 o 5 1 13 946.45 944.89 30.69 o 7 1 13 878.04 820.46 34.78 o 1 3 13 5262.55 5568.33 89.76 o 3 3 13 3391.24 3155.04 74.10 o 5 3 13 1868.79 1812.10 55.90 o 7 3 13 664.72 685.99 31.27 o 1 5 13 1938.72 1818.25 45.60 o 3 5 13 2459.36 2528.88 69.45 o 5 5 13 422.71 403.74 24.80 o 7 5 13 754.80 789.11 33.46 o 1 7 13 8317.34 8053.22 115.75 o 3 7 13 4551.58 4372.67 91.32 o 5 7 13 1659.79 1547.56 46.61 o 7 7 13 880.72 869.53 34.82 o 1 9 13 101.01 50.43 32.09 o 3 9 13 987.67 866.64 29.23 o 5 9 13 46.52 61.32 19.69 o 7 9 13 101.68 82.37 24.95 o 1 11 13 4812.68 4803.71 100.08 o 3 11 13 3979.69 4048.37 96.59 o 5 11 13 631.59 620.96 29.08 o 7 11 13 955.53 861.27 37.89 o 1 13 13 756.64 751.73 28.99 o 3 13 13 662.11 663.57 29.86 o 5 13 13 151.48 190.96 22.81 o 1 15 13 672.95 728.01 31.08 o 3 15 13 590.27 639.58 31.56 o 5 15 13 387.52 416.81 32.19 o 1 17 13 320.36 346.10 27.28 o 3 17 13 161.66 178.41 25.38 o 1 19 13 65.58 107.17 24.36 o 3 19 13 68.96 87.24 25.58 o 2 0 14 12940.93 12442.60 139.27 o 6 0 14 2402.76 2443.34 66.66 o 0 2 14 832.34 885.52 26.70 o 2 2 14 1692.93 1741.87 47.05 o 4 2 14 102.62 134.07 16.24 o 6 2 14 5306.74 5242.15 118.39 o 8 2 14 15.91 62.14 38.56 o 0 4 14 1031.07 888.50 27.97 o 2 4 14 1562.97 1482.48 44.62 o 4 4 14 714.28 644.15 25.73 o 6 4 14 1164.12 1087.14 36.19 o 8 4 14 6.54 -40.85 40.85 o 0 6 14 817.71 752.08 23.74 o 2 6 14 806.81 793.80 23.83 o 4 6 14 256.80 284.82 21.25 o 6 6 14 3098.21 2815.23 75.87 o 8 6 14 80.64 104.64 24.75 o 0 8 14 2947.49 2974.48 77.83 o 2 8 14 8.49 48.58 28.06 o 4 8 14 500.02 531.27 25.19 o 6 8 14 309.11 343.37 27.04 o 0 10 14 3558.52 3594.57 87.68 o 2 10 14 461.51 472.71 26.12 o 4 10 14 958.58 961.40 33.22 o 6 10 14 1110.65 1033.93 37.94 o 0 12 14 6675.32 6767.15 122.64 o 2 12 14 2182.73 2018.89 59.85 o 4 12 14 925.66 940.85 35.07 o 6 12 14 291.37 307.63 29.18 o 0 14 14 241.25 219.71 22.95 o 2 14 14 186.04 149.77 23.34 o 4 14 14 581.79 575.62 31.95 o 6 14 14 338.40 345.71 30.30 o 0 16 14 2946.24 2936.79 77.72 o 2 16 14 1000.70 949.86 36.24 o 4 16 14 405.07 436.22 31.17 o 0 18 14 823.56 859.20 35.41 o 2 18 14 710.27 722.02 36.48 o 1 1 15 8130.39 7519.73 111.50 o 3 1 15 73.13 34.62 30.98 o 5 1 15 4153.44 4189.68 98.64 o 7 1 15 352.44 398.04 27.57 o 1 3 15 10433.62 9693.00 127.79 o 3 3 15 832.60 729.44 24.85 o 5 3 15 2799.71 2819.04 84.48 o 7 3 15 112.18 9.63 41.53 o 1 5 15 7550.31 7303.75 114.87 o 3 5 15 1725.95 1548.63 50.31 o 5 5 15 2083.70 1963.92 61.55 o 7 5 15 346.94 326.26 27.18 o 1 7 15 3668.06 3414.22 83.40 o 3 7 15 2322.67 2323.05 60.83 o 5 7 15 27.42 36.08 19.55 o 7 7 15 227.84 238.33 25.09 o 1 9 15 5055.74 5108.95 104.62 o 3 9 15 1401.78 1342.05 39.21 o 5 9 15 1858.47 1851.54 54.00 o 7 9 15 258.41 284.77 28.93 o 1 11 15 311.54 321.59 25.19 o 3 11 15 214.13 238.18 23.39 o 5 11 15 512.29 601.63 31.17 o 1 13 15 985.48 1086.50 34.97 o 3 13 15 280.29 286.23 26.45 o 5 13 15 1389.19 1431.26 44.07 o 1 15 15 364.92 373.72 27.14 o 3 15 15 285.45 239.26 27.82 o 5 15 15 290.03 277.96 28.64 o 1 17 15 94.99 117.19 24.36 o 3 17 15 341.73 406.98 32.14 o 0 0 16 6198.36 6178.92 104.87 o 4 0 16 4715.10 4867.44 106.50 o 0 2 16 7277.53 6996.10 111.25 o 2 2 16 366.57 370.52 20.28 o 4 2 16 2455.55 2515.80 65.40 o 6 2 16 6.71 -15.37 33.45 o 0 4 16 7303.05 7334.06 116.56 o 2 4 16 568.50 516.40 24.90 o 4 4 16 3563.12 3651.50 91.86 o 6 4 16 754.26 712.90 32.05 o 0 6 16 1145.67 1103.40 31.47 o 2 6 16 495.31 477.53 23.98 o 4 6 16 958.10 1029.06 32.69 o 6 6 16 152.28 165.92 24.36 o 0 8 16 2706.15 2677.31 77.72 o 2 8 16 2156.12 1903.80 58.34 o 4 8 16 1152.13 1017.48 35.17 o 6 8 16 620.07 639.04 31.66 o 0 10 16 2366.50 2157.17 61.70 o 2 10 16 957.00 992.82 32.98 o 4 10 16 1404.79 1338.40 42.81 o 6 10 16 331.62 313.42 30.00 o 0 12 16 130.20 159.74 22.37 o 2 12 16 316.05 315.90 25.68 o 4 12 16 163.17 173.70 26.06 o 0 14 16 1396.85 1247.86 37.94 o 2 14 16 401.96 422.31 26.94 o 4 14 16 407.92 384.62 29.52 o 0 16 16 159.79 171.41 24.56 o 2 16 16 312.27 352.17 29.27 o 0 18 16 70.85 99.64 25.14 o 1 1 17 942.68 921.79 28.84 o 3 1 17 2089.28 2023.17 57.46 o 5 1 17 632.88 642.80 31.22 o 7 1 17 576.56 600.90 33.51 o 1 3 17 2966.29 3008.64 80.80 o 3 3 17 1422.25 1329.91 35.71 o 5 3 17 2223.04 2370.27 68.51 o 7 3 17 910.48 860.92 38.08 o 1 5 17 872.60 862.52 28.89 o 3 5 17 1119.33 1090.89 33.37 o 5 5 17 504.19 524.50 27.67 o 7 5 17 500.92 531.79 33.46 o 1 7 17 5671.59 5877.80 112.86 o 3 7 17 2020.36 2039.25 61.55 o 5 7 17 2147.19 2182.16 67.97 o 1 9 17 180.36 191.69 22.81 o 3 9 17 158.81 160.23 22.17 o 5 9 17 18.89 45.71 38.32 o 1 11 17 2077.98 2144.44 64.52 o 3 11 17 1418.65 1445.80 43.93 o 5 11 17 587.99 564.43 33.02 o 1 13 17 99.77 131.20 22.37 o 3 13 17 197.93 283.40 25.82 o 5 13 17 128.85 140.97 27.23 o 1 15 17 375.10 434.12 30.05 o 3 15 17 72.74 -28.35 44.69 o 1 17 17 85.19 40.46 45.51 o 2 0 18 6341.65 6304.25 118.30 o 6 0 18 1044.54 1013.05 37.94 o 0 2 18 768.63 741.82 28.31 o 2 2 18 894.28 890.39 30.84 o 4 2 18 43.02 57.67 36.32 o 6 2 18 806.34 865.81 34.77 o 0 4 18 668.54 635.72 27.48 o 2 4 18 2166.61 2231.93 59.70 o 4 4 18 102.18 141.26 22.51 o 6 4 18 564.02 620.16 32.92 o 0 6 18 2495.14 2515.17 65.06 o 2 6 18 1109.31 1120.75 34.05 o 4 6 18 221.92 270.81 24.12 o 6 6 18 553.34 548.13 32.73 o 0 8 18 1707.65 1853.61 58.96 o 2 8 18 385.03 356.56 25.87 o 4 8 18 55.96 59.52 36.91 o 6 8 18 282.64 298.00 28.89 o 0 10 18 18.30 21.01 35.89 o 2 10 18 674.31 622.38 31.03 o 4 10 18 259.91 334.66 27.57 o 0 12 18 684.31 659.05 31.71 o 2 12 18 224.74 188.43 24.41 o 4 12 18 89.08 74.79 24.51 o 0 14 18 1036.29 1052.88 38.28 o 2 14 18 139.12 139.41 26.06 o 0 16 18 251.14 241.73 28.01 o 1 1 19 2823.92 2903.15 84.00 o 3 1 19 782.53 814.22 30.79 o 5 1 19 1231.59 1338.76 39.89 o 1 3 19 4312.78 4174.76 101.37 o 3 3 19 1694.42 1679.03 49.67 o 5 3 19 1043.49 1046.80 35.80 o 1 5 19 1274.67 1292.76 37.07 o 3 5 19 725.98 775.44 31.90 o 5 5 19 755.23 799.95 35.31 o 1 7 19 689.89 632.26 28.89 o 3 7 19 544.61 583.93 30.15 o 5 7 19 381.02 365.99 30.35 o 1 9 19 967.19 1033.18 34.78 o 3 9 19 375.34 399.01 28.55 o 5 9 19 893.65 961.25 38.71 o 1 11 19 93.87 149.19 22.42 o 3 11 19 287.35 336.42 29.37 o 1 13 19 539.96 566.22 32.19 o 3 13 19 374.52 380.29 31.61 o 1 15 19 100.72 156.38 25.09 o 0 0 20 5274.86 5357.47 113.33 o 4 0 20 1602.72 1595.36 46.31 o 0 2 20 2063.70 1958.01 62.03 o 2 2 20 59.44 62.19 36.66 o 4 2 20 657.83 669.40 31.61 o 6 2 20 32.27 -26.45 41.67 o 0 4 20 2855.71 2725.36 71.59 o 2 4 20 50.45 46.63 35.06 o 4 4 20 834.41 780.22 33.22 o 0 6 20 2685.05 2716.42 73.63 o 2 6 20 36.01 68.03 37.30 o 4 6 20 844.88 868.30 36.53 o 0 8 20 949.58 955.64 34.73 o 2 8 20 43.00 91.08 22.32 o 4 8 20 614.14 667.78 33.95 o 0 10 20 1083.10 1094.19 37.60 o 2 10 20 17.09 7.29 39.73 o 4 10 20 516.03 519.24 34.43 o 0 12 20 649.89 676.74 33.41 o 2 12 20 305.34 321.10 30.05 o 0 14 20 98.88 82.57 25.97 o 1 1 21 266.61 236.05 23.97 o 3 1 21 204.96 196.36 24.36 o 5 1 21 651.46 688.50 35.99 o 1 3 21 1163.93 1259.32 37.41 o 3 3 21 340.35 345.42 27.38 o 5 3 21 1174.07 1364.29 44.80 o 1 5 21 332.83 325.58 26.36 o 3 5 21 57.23 -39.34 39.34 o 5 5 21 450.40 425.37 32.68 o 1 7 21 2142.06 2292.64 71.23 o 3 7 21 803.47 839.98 35.11 o 1 9 21 20.79 65.64 35.98 o 3 9 21 13.88 -8.51 23.83 o 1 11 21 685.37 812.48 36.82 o 2 0 22 559.62 533.89 29.62 o 0 2 22 8.21 -33.70 38.32 o 2 2 22 69.92 30.49 39.00 o 4 2 22 11.69 46.39 38.41 o 0 4 22 1452.95 1537.70 45.39 o 2 4 22 792.00 829.97 34.77 o 4 4 22 217.27 206.33 27.43 o 0 6 22 419.30 468.70 30.88 o 2 6 22 129.38 124.05 25.82 o 4 6 22 224.34 270.66 29.42 o 0 8 22 231.11 198.50 26.70 o 2 8 22 905.94 956.83 38.37 o 0 10 22 804.24 925.77 39.83 o 2 10 22 566.42 501.01 34.97 o 1 1 23 485.24 529.60 30.69 o 3 1 23 420.19 439.47 30.59 o 1 3 23 351.25 383.98 28.40 o 3 3 23 363.31 356.94 29.62 o 1 5 23 482.36 634.79 32.10 o 3 5 23 438.04 525.02 32.73 o 1 7 23 96.11 67.40 41.87 o 1 9 23 520.80 566.51 33.99 o 0 0 24 923.20 963.01 37.40 o 0 2 24 866.78 834.98 35.60 o 2 2 24 4.96 -5.20 38.71 o 0 4 24 357.00 336.13 29.86 o 2 4 24 185.68 219.94 27.57 o 0 6 24 1034.28 1093.33 41.54 o