#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/65/2206542.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206542_Fobs loop_ _publ_author_name 'Shallard-Brown, Howard A.' 'Watkin, David J.' 'Cowley, Andrew R.' _publ_section_title ; Cyclohexanone at 150K ; _journal_coeditor_code SJ6089 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2424 _journal_page_last o2425 _journal_volume 61 _journal_year 2005 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _audit_creation_date 05-05-11 _audit_creation_method CRYSTALS _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 5.3736(2) _cell_length_b 7.0394(3) _cell_length_c 15.1910(7) _[local]_cod_data_source_file sj6089Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 2 0 0 175.50 178.56 3.70 o 4 0 0 1558.50 1626.19 34.10 o 6 0 0 40.20 48.10 4.60 o 2 1 0 769.00 895.44 12.20 o 3 1 0 1114.10 1201.63 15.20 o 4 1 0 230.60 224.01 3.40 o 5 1 0 0.10 1.73 1.14 o 6 1 0 64.90 57.26 3.40 o 0 2 0 4732.80 4702.71 123.20 o 1 2 0 1188.90 1261.90 24.70 o 2 2 0 16.90 13.27 0.60 o 3 2 0 349.10 371.29 6.00 o 4 2 0 13.50 17.71 1.10 o 5 2 0 21.00 18.99 1.60 o 6 2 0 33.00 37.69 3.10 o 1 3 0 2805.30 3011.76 51.70 o 2 3 0 153.70 156.74 3.40 o 3 3 0 71.70 59.91 2.10 o 4 3 0 4.40 6.77 1.70 o 5 3 0 45.20 48.29 1.80 o 6 3 0 -1.10 0.98 3.50 o 0 4 0 1103.10 1049.18 34.00 o 1 4 0 297.40 321.24 5.70 o 2 4 0 51.80 47.04 1.40 o 3 4 0 353.00 394.37 5.90 o 4 4 0 0.40 0.10 1.77 o 5 4 0 9.20 13.19 3.30 o 6 4 0 15.20 10.75 4.70 o 1 5 0 1803.80 1885.10 35.60 o 2 5 0 30.90 39.66 1.40 o 3 5 0 490.10 510.16 10.00 o 4 5 0 1.10 0.64 4.60 o 5 5 0 9.70 5.64 3.30 o 0 6 0 7466.90 6387.46 545.10 o 1 6 0 246.70 263.26 4.70 o 2 6 0 0.10 0.80 0.57 o 3 6 0 20.00 18.19 3.80 o 4 6 0 475.50 447.13 12.90 o 5 6 0 -2.60 0.36 4.10 o 1 7 0 2.70 2.08 1.50 o 2 7 0 20.10 22.97 1.80 o 3 7 0 109.90 114.49 4.60 o 4 7 0 83.00 76.57 6.10 o 0 8 0 518.30 575.31 31.50 o 1 8 0 0.20 4.05 2.95 o 2 8 0 1.50 4.07 5.00 o 3 8 0 3.70 0.02 3.80 o 1 9 0 31.30 36.03 3.90 o 2 0 1 5148.80 6015.18 97.40 o 3 0 1 177.00 179.21 2.50 o 4 0 1 249.50 257.50 4.50 o 5 0 1 7.00 8.60 2.00 o 6 0 1 6.90 6.84 2.80 o 2 1 1 73.30 80.22 1.50 o 3 1 1 827.75 883.40 11.85 o 4 1 1 76.70 79.46 1.95 o 5 1 1 102.05 99.75 2.91 o 6 1 1 45.95 43.39 3.45 o 0 2 1 755.90 644.52 11.00 o 1 2 1 2567.75 2743.70 51.38 o 2 2 1 155.60 169.35 3.10 o 3 2 1 343.45 355.51 5.76 o 4 2 1 69.60 68.18 1.75 o 5 2 1 143.80 152.05 3.40 o 6 2 1 83.40 78.39 4.16 o 0 3 1 219.80 231.40 3.80 o 1 3 1 230.05 211.54 4.07 o 2 3 1 452.00 430.89 8.73 o 3 3 1 471.15 463.67 8.31 o 4 3 1 75.40 71.40 2.35 o 5 3 1 422.45 368.55 9.67 o 6 3 1 11.40 13.99 5.08 o 0 4 1 540.50 470.62 10.10 o 1 4 1 450.80 442.25 7.75 o 2 4 1 117.60 106.97 2.46 o 3 4 1 153.00 170.00 3.31 o 4 4 1 75.00 78.94 3.06 o 5 4 1 24.35 20.93 3.35 o 6 4 1 23.65 19.41 6.60 o 0 5 1 362.50 389.01 6.80 o 1 5 1 280.35 298.31 4.95 o 2 5 1 53.90 53.41 1.70 o 3 5 1 472.15 522.46 9.45 o 4 5 1 27.60 20.54 3.73 o 5 5 1 88.40 77.94 5.00 o 0 6 1 133.70 149.93 3.20 o 1 6 1 392.10 402.73 6.50 o 2 6 1 237.85 261.16 3.82 o 3 6 1 136.00 141.69 4.40 o 4 6 1 63.65 64.54 3.73 o 5 6 1 2.35 1.42 4.02 o 0 7 1 27.30 28.29 1.80 o 1 7 1 83.40 85.15 2.45 o 2 7 1 48.15 46.83 2.06 o 3 7 1 -1.00 6.91 1.95 o 4 7 1 28.40 27.49 4.73 o 0 8 1 2.10 4.29 5.30 o 1 8 1 121.70 137.35 5.43 o 2 8 1 9.55 12.41 4.65 o 3 8 1 3.30 13.97 5.87 o 0 9 1 30.30 27.64 4.00 o 1 9 1 12.55 23.06 4.60 o 2 0 2 5984.80 7066.40 90.00 o 3 0 2 5829.80 6356.72 88.60 o 4 0 2 144.20 150.83 2.40 o 5 0 2 169.30 166.71 3.70 o 6 0 2 30.00 16.68 3.30 o 1 1 2 2979.60 3328.00 57.59 o 2 1 2 163.65 200.27 2.61 o 3 1 2 168.45 174.59 2.81 o 4 1 2 801.00 778.31 11.26 o 5 1 2 250.25 226.30 5.51 o 6 1 2 43.00 34.91 3.36 o 0 2 2 299.60 262.16 4.40 o 1 2 2 183.65 205.81 3.40 o 2 2 2 947.75 1032.85 15.46 o 3 2 2 355.40 390.85 5.79 o 4 2 2 120.55 118.03 2.25 o 5 2 2 163.80 151.21 3.61 o 6 2 2 16.15 15.29 2.85 o 0 3 2 1720.90 1572.26 25.50 o 1 3 2 1499.00 1454.73 29.26 o 2 3 2 29.35 34.61 1.75 o 3 3 2 195.70 186.54 3.65 o 4 3 2 1383.35 1331.10 24.45 o 5 3 2 25.65 25.02 3.13 o 6 3 2 7.50 6.83 5.22 o 0 4 2 3.60 4.01 0.80 o 1 4 2 4.05 2.92 0.95 o 2 4 2 743.05 783.55 12.45 o 3 4 2 88.30 94.98 2.25 o 4 4 2 73.55 71.67 2.25 o 5 4 2 35.20 32.06 3.61 o 6 4 2 10.60 3.54 5.09 o 0 5 2 1737.60 1799.19 29.00 o 1 5 2 241.95 251.45 4.10 o 2 5 2 17.10 16.94 1.61 o 3 5 2 45.00 50.96 2.10 o 4 5 2 856.95 826.40 17.06 o 5 5 2 126.70 116.75 5.86 o 0 6 2 46.80 48.29 1.60 o 1 6 2 247.60 252.92 4.70 o 2 6 2 543.80 602.74 9.88 o 3 6 2 708.75 752.79 14.91 o 4 6 2 35.00 30.49 3.22 o 5 6 2 36.95 33.23 4.96 o 0 7 2 176.10 186.93 3.70 o 1 7 2 117.45 119.66 2.90 o 2 7 2 0.20 4.55 1.64 o 3 7 2 5.00 5.74 3.42 o 4 7 2 11.45 4.47 4.48 o 0 8 2 12.10 20.89 4.60 o 1 8 2 13.25 13.19 3.60 o 2 8 2 11.50 5.73 4.38 o 3 8 2 87.90 95.50 8.92 o 0 9 2 86.70 111.55 7.60 o 2 0 3 20.70 23.11 0.90 o 3 0 3 453.00 426.33 6.20 o 4 0 3 27.00 23.92 1.20 o 5 0 3 80.10 96.75 2.30 o 6 0 3 -1.50 3.11 3.30 o 1 1 3 1045.50 1088.74 17.00 o 2 1 3 9.85 10.71 0.75 o 3 1 3 68.95 64.94 1.60 o 4 1 3 172.55 172.31 2.85 o 5 1 3 225.45 219.53 4.50 o 6 1 3 20.35 17.90 3.15 o 0 2 3 994.50 854.15 13.70 o 1 2 3 1043.30 1124.78 16.45 o 2 2 3 8.70 9.58 0.95 o 3 2 3 16.10 15.49 1.08 o 4 2 3 476.95 480.78 8.11 o 5 2 3 16.10 17.42 1.60 o 6 2 3 13.05 7.00 3.81 o 0 3 3 162.50 165.27 2.40 o 1 3 3 1635.80 1598.46 32.95 o 2 3 3 781.25 785.48 12.08 o 3 3 3 27.90 26.00 1.35 o 4 3 3 47.50 51.58 2.01 o 5 3 3 107.20 106.22 3.55 o 6 3 3 17.25 12.36 4.68 o 0 4 3 440.20 411.24 6.10 o 1 4 3 45.70 43.25 1.40 o 2 4 3 20.80 25.18 1.45 o 3 4 3 59.45 54.37 1.91 o 4 4 3 273.25 266.67 6.05 o 5 4 3 17.45 17.14 2.95 o 6 4 3 12.80 0.83 6.35 o 0 5 3 31.20 30.77 1.30 o 1 5 3 1.55 3.53 0.71 o 2 5 3 130.70 108.70 2.95 o 3 5 3 17.15 21.82 1.75 o 4 5 3 124.60 135.28 3.77 o 5 5 3 22.10 19.79 4.20 o 0 6 3 344.70 335.46 5.50 o 1 6 3 1216.10 1213.12 18.96 o 2 6 3 4.05 4.98 1.61 o 3 6 3 102.85 112.80 3.55 o 4 6 3 22.75 23.62 4.02 o 5 6 3 28.30 26.18 7.78 o 0 7 3 2.90 0.03 2.10 o 1 7 3 53.80 54.57 2.10 o 2 7 3 36.85 35.64 2.38 o 3 7 3 -0.55 3.90 3.76 o 4 7 3 12.10 4.16 5.46 o 0 8 3 5.70 2.03 4.00 o 1 8 3 157.90 179.59 7.49 o 2 8 3 7.55 2.77 4.51 o 3 8 3 6.05 16.75 6.80 o 0 9 3 21.20 31.48 5.80 o 2 0 4 23.70 24.61 1.00 o 3 0 4 16.40 14.57 0.80 o 4 0 4 338.10 349.74 5.10 o 5 0 4 308.30 291.83 5.30 o 6 0 4 -4.20 2.13 3.00 o 0 1 4 217.30 198.49 4.50 o 1 1 4 1745.85 1793.60 27.99 o 2 1 4 3097.65 3284.96 50.75 o 3 1 4 188.15 210.27 3.75 o 4 1 4 105.40 104.68 2.10 o 5 1 4 13.30 15.21 1.46 o 6 1 4 36.35 32.59 3.35 o 1 2 4 320.45 309.35 5.15 o 2 2 4 517.10 579.27 8.05 o 3 2 4 90.45 105.82 1.80 o 4 2 4 270.65 301.55 5.32 o 5 2 4 95.55 90.40 2.65 o 6 2 4 8.55 9.28 3.26 o 0 3 4 553.90 500.67 7.80 o 1 3 4 3178.80 3042.92 50.87 o 2 3 4 73.05 65.22 1.60 o 3 3 4 470.75 537.33 7.11 o 4 3 4 258.65 255.59 4.60 o 5 3 4 9.50 9.34 1.83 o 6 3 4 97.95 77.72 6.96 o 0 4 4 1358.00 1053.41 17.60 o 1 4 4 912.75 835.69 12.26 o 2 4 4 281.70 300.57 5.08 o 3 4 4 46.45 47.17 1.87 o 4 4 4 78.45 77.84 2.65 o 5 4 4 44.55 51.59 3.59 o 6 4 4 16.70 10.24 8.32 o 0 5 4 200.40 193.72 3.40 o 1 5 4 671.45 634.62 9.97 o 2 5 4 954.95 1057.21 16.72 o 3 5 4 33.15 42.45 1.66 o 4 5 4 34.80 30.65 2.60 o 5 5 4 7.85 3.65 3.99 o 0 6 4 988.40 979.48 15.90 o 1 6 4 683.45 693.51 11.05 o 2 6 4 125.75 124.91 3.18 o 3 6 4 10.50 12.28 2.11 o 4 6 4 147.85 130.16 7.26 o 5 6 4 82.40 81.28 9.14 o 0 7 4 22.80 18.81 2.20 o 1 7 4 51.50 48.67 2.57 o 2 7 4 104.30 116.44 3.71 o 3 7 4 17.70 24.13 4.96 o 4 7 4 31.05 31.60 5.81 o 0 8 4 909.60 880.13 47.40 o 1 8 4 17.40 17.22 3.85 o 2 8 4 10.55 6.46 4.44 o 3 8 4 17.25 1.79 7.59 o 1 0 5 1547.40 1631.51 32.00 o 2 0 5 1301.00 1422.53 19.80 o 3 0 5 54.40 43.32 1.50 o 4 0 5 98.30 100.01 2.10 o 5 0 5 38.00 51.34 1.90 o 6 0 5 21.20 30.53 3.60 o 0 1 5 3442.30 2843.15 70.30 o 1 1 5 367.10 345.80 5.70 o 2 1 5 107.40 88.88 2.00 o 3 1 5 145.15 130.03 2.85 o 4 1 5 145.90 134.27 2.45 o 5 1 5 144.10 145.05 3.56 o 6 1 5 28.00 35.17 6.76 o 0 2 5 -1.40 1.27 0.80 o 1 2 5 1166.50 1095.96 17.65 o 2 2 5 1158.00 1230.32 16.80 o 3 2 5 183.55 203.47 2.86 o 4 2 5 51.05 43.13 1.66 o 5 2 5 23.10 26.70 2.25 o 6 2 5 35.75 25.71 3.71 o 0 3 5 53.20 52.19 1.40 o 1 3 5 226.05 207.54 3.61 o 2 3 5 373.80 425.73 5.76 o 3 3 5 1605.65 1697.27 24.56 o 4 3 5 287.85 280.14 5.53 o 5 3 5 89.10 89.12 3.31 o 6 3 5 -0.50 3.22 7.22 o 0 4 5 67.00 63.18 1.40 o 1 4 5 802.45 717.07 12.01 o 2 4 5 107.70 105.33 2.60 o 3 4 5 140.55 148.65 2.85 o 4 4 5 55.05 60.02 2.63 o 5 4 5 12.90 14.72 3.57 o 0 5 5 162.30 142.98 3.60 o 1 5 5 89.05 87.81 1.90 o 2 5 5 7.60 5.15 1.40 o 3 5 5 251.00 276.65 5.87 o 4 5 5 1.90 5.21 2.90 o 5 5 5 151.85 150.62 8.35 o 0 6 5 9.60 11.07 1.30 o 1 6 5 153.75 164.87 3.30 o 2 6 5 46.20 57.31 1.90 o 3 6 5 23.20 29.37 2.60 o 4 6 5 27.75 33.93 4.69 o 0 7 5 160.70 146.08 4.70 o 1 7 5 10.60 12.58 2.31 o 2 7 5 13.30 13.44 2.45 o 3 7 5 27.20 23.33 4.30 o 4 7 5 38.10 36.88 5.67 o 0 8 5 11.20 8.95 5.10 o 1 8 5 20.70 20.85 4.00 o 2 8 5 90.20 90.88 6.69 o 0 0 6 2529.70 2394.19 49.60 o 1 0 6 201.30 171.41 3.30 o 2 0 6 5236.60 5495.26 102.50 o 3 0 6 3.60 3.51 1.00 o 4 0 6 227.30 211.30 4.00 o 5 0 6 68.40 78.15 2.80 o 6 0 6 150.30 113.48 7.50 o 0 1 6 984.10 892.85 16.40 o 1 1 6 87.00 80.43 1.80 o 2 1 6 357.70 388.30 5.18 o 3 1 6 181.65 176.30 3.26 o 4 1 6 4.30 5.62 1.20 o 5 1 6 82.75 72.40 2.90 o 6 1 6 129.35 98.95 6.83 o 0 2 6 952.30 917.02 15.90 o 1 2 6 688.65 637.05 11.03 o 2 2 6 744.70 826.21 10.40 o 3 2 6 1155.20 1212.67 17.50 o 4 2 6 42.35 48.36 1.90 o 5 2 6 92.65 90.80 2.76 o 6 2 6 75.20 55.14 5.05 o 0 3 6 9681.70 8313.58 146.90 x 1 3 6 45.25 39.95 1.30 o 2 3 6 103.90 103.19 2.30 o 3 3 6 642.35 656.02 10.57 o 4 3 6 715.15 740.08 13.94 o 5 3 6 118.40 96.97 4.38 o 6 3 6 60.60 51.27 7.62 o 0 4 6 8.70 10.35 1.10 o 1 4 6 207.10 198.51 3.40 o 2 4 6 112.50 89.26 2.50 o 3 4 6 504.30 530.27 9.42 o 4 4 6 59.30 70.72 3.39 o 5 4 6 88.10 80.92 5.38 o 0 5 6 10.40 5.24 1.40 o 1 5 6 55.80 52.08 1.65 o 2 5 6 20.60 20.22 2.00 o 3 5 6 176.15 175.41 4.25 o 4 5 6 59.40 46.68 4.50 o 5 5 6 101.25 93.13 6.75 o 0 6 6 142.40 130.88 2.70 o 1 6 6 60.75 48.37 2.21 o 2 6 6 668.20 693.62 14.85 o 3 6 6 5.25 7.52 2.71 o 4 6 6 13.45 13.76 6.05 o 0 7 6 243.20 206.88 6.90 o 1 7 6 15.80 25.04 2.57 o 2 7 6 11.85 12.78 2.80 o 3 7 6 6.20 1.36 5.04 o 0 8 6 76.30 73.80 6.70 o 1 8 6 82.05 75.42 6.05 o 2 8 6 168.80 152.98 6.70 o 1 0 7 1316.80 1156.08 21.20 o 2 0 7 1411.40 1433.18 19.60 o 3 0 7 57.10 57.99 1.50 o 4 0 7 3.40 5.82 1.40 o 5 0 7 83.80 96.82 2.70 o 6 0 7 5.90 12.95 4.70 o 0 1 7 1647.50 1636.90 25.40 o 1 1 7 21.25 26.15 1.10 o 2 1 7 562.20 547.23 8.41 o 3 1 7 274.85 247.74 4.95 o 4 1 7 30.10 38.65 1.66 o 5 1 7 112.90 105.98 4.03 o 6 1 7 38.60 37.63 4.31 o 0 2 7 13.30 16.79 1.10 o 1 2 7 1929.25 1800.84 28.53 o 2 2 7 34.20 41.58 1.20 o 3 2 7 470.75 521.26 6.96 o 4 2 7 81.60 86.57 2.45 o 5 2 7 11.65 7.97 2.36 o 6 2 7 26.95 25.91 4.66 o 0 3 7 119.70 115.92 2.20 o 1 3 7 130.05 112.84 2.40 o 2 3 7 42.65 50.85 1.85 o 3 3 7 130.50 126.77 2.35 o 4 3 7 30.60 32.57 2.16 o 5 3 7 108.20 87.92 4.58 o 6 3 7 145.65 111.79 12.37 o 0 4 7 160.90 154.94 2.70 o 1 4 7 319.10 303.78 4.96 o 2 4 7 150.65 146.30 2.90 o 3 4 7 170.30 160.35 4.45 o 4 4 7 37.70 44.75 2.86 o 5 4 7 26.95 25.62 4.75 o 0 5 7 117.60 113.90 2.70 o 1 5 7 41.50 28.97 1.55 o 2 5 7 236.45 218.77 5.35 o 3 5 7 238.80 234.05 5.30 o 4 5 7 2.40 1.23 4.78 o 5 5 7 26.75 38.60 7.56 o 0 6 7 4.20 4.42 1.40 o 1 6 7 245.95 208.87 5.35 o 2 6 7 101.30 88.80 3.51 o 3 6 7 30.40 31.74 4.07 o 4 6 7 12.25 7.73 6.39 o 0 7 7 129.90 111.99 4.30 o 1 7 7 24.10 35.51 2.90 o 2 7 7 44.15 39.38 4.10 o 3 7 7 8.70 7.57 6.77 o 0 8 7 28.30 19.95 6.70 o 1 8 7 256.20 239.13 12.26 o 2 8 7 14.05 13.76 5.50 o 0 0 8 93.50 98.81 2.80 o 1 0 8 997.20 871.06 14.00 o 2 0 8 2.80 1.09 1.40 o 3 0 8 68.90 72.83 1.70 o 4 0 8 46.20 69.62 2.30 o 5 0 8 -0.30 2.46 2.19 o 6 0 8 9.70 0.97 4.60 o 0 1 8 132.70 139.85 2.20 o 1 1 8 772.15 738.56 10.77 o 2 1 8 165.95 149.55 2.95 o 3 1 8 189.40 173.67 3.50 o 4 1 8 53.75 57.81 2.00 o 5 1 8 22.90 23.33 2.25 o 6 1 8 27.60 26.93 4.86 o 0 2 8 878.10 809.48 14.50 o 1 2 8 2393.35 2223.40 37.90 o 2 2 8 299.35 297.80 4.51 o 3 2 8 71.80 74.35 1.75 o 4 2 8 168.80 175.35 3.65 o 5 2 8 158.10 147.99 4.85 o 6 2 8 24.00 21.41 4.35 o 0 3 8 301.40 291.54 4.60 o 1 3 8 256.80 220.36 4.45 o 2 3 8 2917.50 2883.82 50.16 o 3 3 8 888.45 935.34 13.00 o 4 3 8 27.45 29.06 2.22 o 5 3 8 -1.00 0.84 3.87 o 0 4 8 429.20 420.10 6.10 o 1 4 8 322.55 282.47 5.58 o 2 4 8 402.75 410.29 6.70 o 3 4 8 79.05 80.46 2.40 o 4 4 8 25.95 30.75 2.90 o 5 4 8 97.30 92.88 6.38 o 0 5 8 158.20 148.57 2.80 o 1 5 8 44.95 40.35 1.95 o 2 5 8 201.20 219.80 5.00 o 3 5 8 2.55 0.19 2.26 o 4 5 8 84.35 81.94 5.10 o 5 5 8 16.40 16.35 7.08 o 0 6 8 -1.80 3.08 1.50 o 1 6 8 84.70 94.93 3.10 o 2 6 8 44.70 41.49 2.72 o 3 6 8 33.65 30.02 4.30 o 4 6 8 24.00 23.05 6.87 o 0 7 8 13.20 11.55 2.60 o 1 7 8 126.65 109.65 5.57 o 2 7 8 42.70 40.28 4.00 o 3 7 8 36.00 40.79 5.81 o 0 8 8 164.70 154.53 10.60 o 1 8 8 296.95 250.60 13.46 o 1 0 9 578.10 528.81 7.90 o 2 0 9 6.00 7.70 1.30 o 3 0 9 102.70 90.32 2.10 o 4 0 9 83.30 83.96 2.50 o 5 0 9 10.40 13.20 2.90 o 6 0 9 9.10 0.93 4.50 o 0 1 9 39.50 41.21 1.40 o 1 1 9 514.30 496.48 7.71 o 2 1 9 111.05 122.55 2.25 o 3 1 9 32.30 37.99 1.50 o 4 1 9 104.25 117.66 2.65 o 5 1 9 11.70 13.65 2.70 o 6 1 9 2.70 4.34 4.50 o 0 2 9 33.50 31.14 1.40 o 1 2 9 966.15 909.75 14.37 o 2 2 9 384.95 383.66 6.20 o 3 2 9 1.85 2.11 1.00 o 4 2 9 137.45 145.72 3.35 o 5 2 9 18.65 24.75 3.85 o 0 3 9 1.50 1.87 1.20 o 1 3 9 667.70 627.50 11.10 o 2 3 9 203.45 212.64 3.80 o 3 3 9 413.90 419.18 7.15 o 4 3 9 26.45 23.56 2.33 o 5 3 9 11.45 16.98 3.35 o 0 4 9 81.40 86.70 2.00 o 1 4 9 266.20 249.36 5.11 o 2 4 9 125.75 133.50 3.55 o 3 4 9 16.65 18.83 1.82 o 4 4 9 128.70 138.45 4.80 o 5 4 9 51.95 65.00 6.33 o 0 5 9 -1.50 0.30 1.20 o 1 5 9 27.15 25.98 1.85 o 2 5 9 79.25 80.27 2.85 o 3 5 9 102.95 94.39 4.15 o 4 5 9 54.25 58.44 5.00 o 0 6 9 4.10 6.55 1.60 o 1 6 9 63.25 75.84 3.10 o 2 6 9 5.50 4.44 2.84 o 3 6 9 38.35 39.22 4.62 o 4 6 9 36.30 33.43 7.92 o 0 7 9 20.20 17.92 3.10 o 1 7 9 65.15 61.23 4.13 o 2 7 9 9.95 10.99 3.35 o 3 7 9 5.05 13.82 6.07 o 0 8 9 20.50 11.29 9.60 o 0 0 10 373.20 347.57 9.70 o 1 0 10 213.80 209.54 3.20 o 2 0 10 545.60 467.01 8.00 o 3 0 10 0.40 1.77 1.64 o 4 0 10 5.00 0.72 2.00 o 5 0 10 11.40 7.24 3.60 o 0 1 10 247.70 272.30 3.70 o 1 1 10 679.40 633.45 9.42 o 2 1 10 36.20 43.10 1.55 o 3 1 10 124.75 127.69 2.71 o 4 1 10 4.65 5.87 1.59 o 5 1 10 15.55 18.82 3.78 o 0 2 10 140.20 139.39 2.50 o 1 2 10 95.35 92.95 2.20 o 2 2 10 1790.75 1760.10 27.04 o 3 2 10 26.75 30.34 1.56 o 4 2 10 73.55 62.66 2.80 o 5 2 10 26.65 27.72 3.95 o 0 3 10 184.60 170.24 3.40 o 1 3 10 816.10 772.90 14.24 o 2 3 10 26.95 26.73 1.70 o 3 3 10 250.55 265.02 5.05 o 4 3 10 28.25 21.77 2.82 o 5 3 10 418.95 363.71 14.62 o 0 4 10 0.20 0.00 1.34 o 1 4 10 24.85 29.91 1.75 o 2 4 10 525.70 539.65 11.30 o 3 4 10 4.20 4.12 2.11 o 4 4 10 12.75 18.16 3.37 o 5 4 10 24.20 30.72 5.58 o 0 5 10 318.30 247.94 6.20 o 1 5 10 86.05 82.50 2.75 o 2 5 10 6.85 6.04 2.10 o 3 5 10 119.10 121.59 5.14 o 4 5 10 5.60 8.62 4.20 o 0 6 10 29.60 26.21 2.40 o 1 6 10 27.85 22.78 2.55 o 2 6 10 138.05 132.26 5.60 o 3 6 10 13.45 12.15 3.78 o 0 7 10 -3.20 6.91 4.70 o 1 7 10 162.45 127.95 6.50 o 2 7 10 9.30 8.75 3.83 o 1 0 11 2.60 0.03 1.50 o 2 0 11 96.90 82.30 2.90 o 3 0 11 279.80 310.89 5.10 o 4 0 11 118.10 134.37 3.10 o 5 0 11 0.70 1.11 4.85 o 0 1 11 551.60 503.50 8.00 o 1 1 11 132.55 140.66 2.82 o 2 1 11 219.15 221.70 4.23 o 3 1 11 52.20 53.68 2.11 o 4 1 11 33.05 31.52 2.32 o 5 1 11 22.70 26.55 3.90 o 0 2 11 0.10 0.07 0.89 o 1 2 11 58.25 40.93 2.00 o 2 2 11 346.35 356.49 5.77 o 3 2 11 104.05 111.05 2.75 o 4 2 11 74.95 71.73 3.20 o 5 2 11 17.80 22.14 4.02 o 0 3 11 14.60 12.10 1.30 o 1 3 11 211.20 209.70 3.91 o 2 3 11 26.65 30.64 2.10 o 3 3 11 313.60 334.54 6.60 o 4 3 11 35.60 32.60 3.35 o 5 3 11 71.60 64.73 5.12 o 0 4 11 -0.60 0.39 2.17 o 1 4 11 40.70 40.23 2.05 o 2 4 11 105.40 112.90 3.55 o 3 4 11 143.15 150.10 4.86 o 4 4 11 79.70 79.77 4.54 o 0 5 11 12.90 11.47 1.10 o 1 5 11 39.90 37.44 2.75 o 2 5 11 108.35 109.39 4.30 o 3 5 11 109.65 104.57 5.21 o 4 5 11 14.30 10.06 4.56 o 0 6 11 4.30 6.99 2.40 o 1 6 11 11.45 12.85 3.35 o 2 6 11 18.20 16.19 3.85 o 3 6 11 57.25 52.22 4.72 o 0 7 11 131.70 115.06 7.60 o 1 7 11 31.10 20.77 4.50 o 2 7 11 77.75 75.22 5.89 o 0 0 12 34.00 27.36 2.80 o 1 0 12 214.00 196.12 3.90 o 2 0 12 45.60 49.63 2.10 o 3 0 12 114.00 116.32 2.90 o 4 0 12 45.00 64.65 2.80 o 5 0 12 37.50 31.84 5.40 o 0 1 12 4.90 3.08 1.60 o 1 1 12 5.55 5.69 1.45 o 2 1 12 174.85 187.01 3.57 o 3 1 12 292.10 314.63 5.50 o 4 1 12 1.15 1.76 2.35 o 5 1 12 7.80 6.40 4.63 o 0 2 12 1093.00 1100.55 15.30 o 1 2 12 356.75 320.77 6.10 o 2 2 12 23.60 25.58 1.95 o 3 2 12 183.45 196.18 4.45 o 4 2 12 13.00 12.08 2.86 o 5 2 12 86.90 76.79 5.59 o 0 3 12 27.10 32.08 1.60 o 1 3 12 138.45 155.84 3.40 o 2 3 12 1149.50 1151.58 22.11 o 3 3 12 22.25 21.67 2.55 o 4 3 12 8.60 11.24 3.20 o 5 3 12 -0.90 4.51 5.21 o 0 4 12 305.80 278.98 6.30 o 1 4 12 65.85 72.22 2.87 o 2 4 12 43.05 46.85 2.96 o 3 4 12 155.95 156.64 7.65 o 4 4 12 35.90 39.73 3.90 o 0 5 12 0.00 1.67 0.01 o 1 5 12 6.35 8.42 2.55 o 2 5 12 162.45 163.18 6.20 o 3 5 12 177.65 165.16 7.45 o 0 6 12 -2.40 0.67 3.50 o 1 6 12 70.30 52.73 4.75 o 2 6 12 19.10 22.47 5.06 o 3 6 12 62.40 63.44 6.21 o 1 7 12 21.95 16.31 5.77 o 1 0 13 252.90 229.14 5.00 o 2 0 13 25.20 21.78 2.50 o 3 0 13 9.50 6.52 2.50 o 4 0 13 5.40 2.44 2.90 o 5 0 13 68.30 52.77 5.50 o 0 1 13 284.60 259.53 5.00 o 1 1 13 174.60 173.15 3.51 o 2 1 13 204.60 192.45 5.34 o 3 1 13 53.40 55.88 2.45 o 4 1 13 7.40 6.22 2.80 o 5 1 13 27.50 25.77 4.58 o 0 2 13 24.90 26.04 1.60 o 1 2 13 282.10 270.42 5.36 o 2 2 13 181.55 193.92 4.48 o 3 2 13 45.25 55.02 2.85 o 4 2 13 15.05 12.12 2.95 o 0 3 13 2.50 4.44 2.10 o 1 3 13 3.85 6.43 2.01 o 2 3 13 -2.90 1.09 2.87 o 3 3 13 21.10 16.28 3.41 o 4 3 13 14.60 8.42 3.71 o 0 4 13 60.60 65.94 2.20 o 1 4 13 51.90 56.14 2.92 o 2 4 13 96.05 93.72 3.95 o 3 4 13 32.20 33.15 4.16 o 4 4 13 11.90 9.76 4.05 o 0 5 13 30.00 29.36 2.90 o 1 5 13 91.55 93.27 4.16 o 2 5 13 62.00 60.86 5.21 o 3 5 13 41.05 50.09 4.60 o 0 6 13 3.10 2.35 3.80 o 1 6 13 61.15 60.51 5.38 o 2 6 13 22.70 21.50 4.86 o 0 0 14 18.00 20.66 3.10 o 1 0 14 64.00 67.23 3.50 o 2 0 14 656.50 665.53 11.20 o 3 0 14 29.60 32.34 2.50 o 4 0 14 16.00 13.59 3.20 o 0 1 14 186.60 166.07 4.10 o 1 1 14 408.30 402.99 7.75 o 2 1 14 29.35 33.53 2.45 o 3 1 14 26.85 31.55 2.70 o 4 1 14 9.30 8.91 3.40 o 0 2 14 22.30 20.27 2.20 o 1 2 14 18.10 15.06 2.71 o 2 2 14 46.60 54.88 3.05 o 3 2 14 179.90 175.49 6.21 o 4 2 14 1.05 0.95 4.17 o 0 3 14 294.70 298.45 5.70 o 1 3 14 81.90 79.82 3.28 o 2 3 14 11.50 8.69 3.31 o 3 3 14 38.30 41.59 3.95 o 4 3 14 135.50 154.29 6.76 o 0 4 14 5.20 7.47 2.30 o 1 4 14 21.85 24.86 2.66 o 2 4 14 38.85 39.36 3.50 o 3 4 14 78.55 75.97 5.00 o 0 5 14 95.20 74.64 4.60 o 1 5 14 179.65 171.08 6.51 o 2 5 14 7.50 7.85 4.53 o 3 5 14 10.85 21.95 4.82 o 0 6 14 12.00 3.63 6.00 o 1 6 14 4.60 7.17 4.86 o 1 0 15 3.20 1.67 4.20 o 2 0 15 5.30 2.38 2.50 o 3 0 15 62.70 56.80 3.50 o 4 0 15 33.20 28.45 3.70 o 0 1 15 1.00 0.44 5.40 o 1 1 15 89.85 93.41 3.30 o 2 1 15 113.65 122.18 3.65 o 3 1 15 19.30 22.79 3.30 o 4 1 15 32.65 30.08 3.86 o 0 2 15 16.00 20.22 2.60 o 1 2 15 156.85 143.14 4.70 o 2 2 15 68.65 83.26 3.51 o 3 2 15 39.10 42.21 4.71 o 4 2 15 71.95 72.29 4.95 o 0 3 15 3.60 0.26 2.20 o 1 3 15 30.85 36.56 2.89 o 2 3 15 14.55 14.22 3.37 o 3 3 15 69.15 76.97 4.60 o 0 4 15 -0.20 0.09 2.77 o 1 4 15 49.75 54.00 3.90 o 2 4 15 41.00 49.24 3.70 o 3 4 15 45.25 56.22 4.25 o 0 5 15 0.30 0.01 3.83 o 1 5 15 55.20 57.59 4.56 o 2 5 15 106.35 107.57 6.95 o 0 0 16 314.70 345.58 10.70 o 1 0 16 250.50 232.47 10.20 o 2 0 16 10.70 12.32 3.20 o 3 0 16 40.30 47.46 3.60 o 4 0 16 38.20 31.18 4.20 o 0 1 16 -2.30 0.00 3.00 o 1 1 16 104.95 98.71 3.75 o 2 1 16 277.00 260.47 7.85 o 3 1 16 8.40 9.05 3.46 o 0 2 16 174.20 174.66 4.80 o 1 2 16 38.50 36.81 3.39 o 2 2 16 3.35 0.57 4.16 o 3 2 16 65.00 80.45 4.40 o 0 3 16 22.40 1.70 3.60 o 1 3 16 79.55 83.00 4.29 o 2 3 16 5.15 3.73 3.71 o 3 3 16 2.50 1.77 4.56 o 0 4 16 17.20 19.49 3.30 o 1 4 16 21.15 28.01 3.80 o 2 4 16 6.35 6.08 4.35 o 0 5 16 0.80 3.75 7.87 o 1 5 16 18.60 29.01 5.85 o 1 0 17 160.50 154.87 5.80 o 2 0 17 10.50 6.73 4.00 o 3 0 17 13.30 19.37 3.70 o 0 1 17 252.80 232.35 7.60 o 1 1 17 15.25 13.10 3.31 o 2 1 17 54.60 62.50 3.86 o 3 1 17 48.70 47.66 3.95 o 0 2 17 29.30 30.30 3.10 o 1 2 17 18.20 18.31 3.25 o 2 2 17 12.30 11.07 4.10 o 3 2 17 3.05 4.18 3.91 o 0 3 17 3.70 4.10 3.60 o 1 3 17 10.05 9.98 4.14 o 2 3 17 -0.30 2.53 4.40 o 0 4 17 4.20 6.69 4.10 o 1 4 17 24.05 28.87 4.85 o 0 0 18 125.60 114.57 7.10 o 1 0 18 43.60 38.66 3.50 o 2 0 18 94.30 99.37 5.80 o 0 1 18 189.80 170.36 6.70 o 1 1 18 105.60 91.59 5.10 o 2 1 18 12.95 20.81 4.06 o 0 2 18 26.60 27.96 4.10 o 1 2 18 20.35 21.38 4.30 o 2 2 18 7.90 5.08 4.72 o 0 3 18 10.40 5.10 4.90 o 1 3 18 22.20 16.22 5.71 o 1 0 19 59.80 82.55 5.70 o 0 1 19 75.30 87.56 6.50 o 1 1 19 27.50 29.86 5.06 o 0 2 19 24.50 30.01 5.40 o